CN107245257A - A kind of toughness reinforcing heatproof water-impervious coating rubber cement and preparation method thereof - Google Patents
A kind of toughness reinforcing heatproof water-impervious coating rubber cement and preparation method thereof Download PDFInfo
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- CN107245257A CN107245257A CN201710499223.0A CN201710499223A CN107245257A CN 107245257 A CN107245257 A CN 107245257A CN 201710499223 A CN201710499223 A CN 201710499223A CN 107245257 A CN107245257 A CN 107245257A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D1/00—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
- C09D1/06—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances cement
- C09D1/08—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances cement with organic additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F220/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
- C08F220/02—Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
- C08F220/52—Amides or imides
- C08F220/54—Amides, e.g. N,N-dimethylacrylamide or N-isopropylacrylamide
- C08F220/56—Acrylamide; Methacrylamide
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/28—Nitrogen-containing compounds
Abstract
The invention discloses a kind of toughness reinforcing heatproof water-impervious coating rubber cement, cement, reusable scattered rubber powder, calcium sulphate retarder, defoamer, plaster of paris, lime, fine sand slurry are included.The invention also discloses the preparation method of toughness reinforcing heatproof water-impervious coating rubber cement.Prepared by the toughness reinforcing heatproof water-impervious coating rubber cement of the present invention convenient, and cost is low, can effective water-impervious effect, the addition of titanium nitride acrylamide copolymer, it will be apparent that the toughness reinforcing heat resistance of raising coating.The coating either indoors or outdoor, tunnel, cistern, drinks the moist place such as water storage tank and can reach good effect, is particularly suitable for use in using the insoluble wall leakage problem of tradition grouting process.
Description
Technical field
The invention belongs to paint field, and in particular to toughness reinforcing heatproof water-impervious coating rubber cement and preparation method thereof.
Background technology
Coatings in body surface can form film under certain conditions and protection, decoration or other functions (absolutely
Edge, antirust, antimildew and antibacterial, heat-resisting etc.) a class I liquid I or solid material.Because the coating of early stage substantially using vegetable oil is main
Raw material, therefore also known as paint.Present synthetic resin largely or entirely instead of vegetable oil, therefore referred to as coating.
Many buildings have the requirement of water proof anti-seepage, but the cement impervious water resistance of normal concrete is bad, water energy
Pass through the micropore permeation of concrete cement.Therefore, many upstream faces or back side waterproof using in normal concrete in construction
The materials such as coiled material, coating isolate water source, and this construction technology is more numerous and diverse, waterproof effect also cannot be guaranteed.Also there is use
Rigid inner waterproofing structure, but its anti-crack ability is poor, can not effect a radical cure whole holes and the healing in crack of loose structure, waterproof effect
Really poor and waterproof cost is high.Cement based penetration crystallization type water proofing paint is also used, this coating both can guarantee that water resistance, again
Waterproof cost is reduced, but it is brushed on the surface of concrete after being mixed mostly with water in use, and concrete surface is deposited
It is extremely difficult in filling up for slight crack.
The content of the invention
The present invention solves the technical problem of providing, a kind of water resistant ability is strong, cohesive force is good, good permeability, heatproof,
Nontoxicity, heavy metal free, formaldehydeless, antimildew and antibacterial toughness reinforcing heatproof water-impervious coating rubber cement.
The technical problems to be solved by the invention are realized using following technical scheme：
A kind of toughness reinforcing heatproof water-impervious coating rubber cement, is made up of the following raw material：
A kind of toughness reinforcing heatproof water-impervious coating rubber cement is by cement, reusable scattered rubber powder, calcium sulphate retarder, defoamer, hot stone
Cream, lime, fine sand slurry composition, each component and its parts by weight are：The reusable dispersion agent of cement, 15-25 comprising 100 parts part
Powder, 0.5-2 parts of calcium sulphate retarder, 0.2-0.8 parts of defoamer, 5-17 parts of plaster of paris, 6-15 parts of lime, 15-27 parts
Fine sand slurry.
Preferably, described toughness reinforcing heatproof water-impervious coating rubber cement comprising 100 parts cement, reusable point of 18-22 parts
Dissipate rubber powder, 0.8-1.2 parts of calcium sulphate retarder, 0.4-0.6 parts of defoamer, 9-13 parts of plaster of paris, 8-12 parts of lime,
18-23 parts of fine sand slurry.
It is highly preferred that described toughness reinforcing heatproof water-impervious coating rubber cement includes 100 parts of cement, 20 parts reusable scattered
Rubber powder, 1 part of calcium sulphate retarder, 0.5 part of defoamer, 10 parts of plaster of paris, 10 parts of lime, 20 parts of fine sand slurry.
In preferably scheme, described toughness reinforcing heatproof water-impervious coating rubber cement also includes toughness reinforcing refractory agent.
In preferably scheme, the toughness reinforcing refractory agent that described toughness reinforcing heatproof water-impervious coating rubber cement is included be titanium nitride-
Acrylamide copolymer.
In preferably scheme, the toughness reinforcing refractory agent that described toughness reinforcing heatproof water-impervious coating rubber cement is included be titanium nitride-
The parts by weight of acrylamide copolymer are 0.4-1.
Another aspect of the present invention provides a kind of method for preparing toughness reinforcing heatproof water-impervious coating rubber cement, comprises the following steps：
1）The cement of formula ratio, reusable scattered rubber powder, plaster of paris, lime are well mixed, are ground on beveller；
2）The mixture of grinding is put into beaker, calcium sulphate retarder, the fine sand slurry of corresponding formula ratio are added, at 40-70 DEG C
At a temperature of stir 30-60min, add defoamer after stirring wherein, 5-15min is stirred in continuation at a temperature of 40-70 DEG C；
3）PH adjusting agent is added, 10-30min is stirred at room temperature, stops stirring, is stood, filtering obtains waterproof, seepage control water paint.
Preferably, the method that toughness reinforcing heatproof water-impervious coating rubber cement is prepared describedly, comprises the following steps：
1）The cement of formula ratio, reusable scattered rubber powder, plaster of paris, lime are well mixed, are ground on beveller；
2）The mixture of grinding is put into beaker, calcium sulphate retarder, the fine sand slurry of corresponding formula ratio are added, at 50-60 DEG C
At a temperature of stir 40-50min, add defoamer after stirring wherein, 10min is stirred in continuation at a temperature of 50-60 DEG C；
3）PH adjusting agent is added, 20min is stirred at room temperature, stops stirring, is stood, filtering obtains waterproof, seepage control water paint.
It is highly preferred that preparing the method for toughness reinforcing heatproof water-impervious coating rubber cement describedly, mixing speed is 500-1000r/
min。
The preparation method of titanium nitride-acrylamide copolymer
By 0.1mmol 2- acrylamide-2-methylpro panesulfonic acids, 0.3mmol dimethyl diallyl ammonium chlorides, 0.1mmol third
Olefin(e) acid, 50mL deionized waters are added in three-necked flask, in the cooling condition, and pH value is reconciled with sodium hydroxide solution（4-6）, heating
To 50 DEG C, the acrylamide of a small amount of deionized water dissolving is added thereto, titanium nitride is added, and the logical nitrogen of sealing adds over cure
Sour hydrogen ammonium, continues to react 2h, stops reaction, obtain viscous gum, that is, obtains synthesized titanium nitride-acrylic amide polymerization
Thing.
The beneficial effects of the invention are as follows：Coating preparation of the present invention is convenient, and raw material is easy, titanium nitride-acrylic amide polymerization
The addition of thing, it will be apparent that improve the toughness reinforcing heat resistance of coating rubber cement, at the same can effective water-impervious effect, the coating is either
Indoors or outdoor, tunnel, cistern, drink water storage tank etc. humidity place can reach good effect, it is particularly suitable
In using the insoluble wall leakage problem of traditional grouting process.
Embodiment
Embodiment 1
The preparation method applied to toughness reinforcing heatproof water-impervious coating rubber cement of the present embodiment, including following preparation process：
Following raw material is all parts by weight,
A, 100 parts of cement, 15 parts of reusable scattered rubber powders, 5 parts of plaster of paris, 6 lime are well mixed, are ground on beveller
Mill；
B, the mixture of grinding is put into beaker, 0.5 part of calcium sulphate retarder, 15 parts of fine sands slurries added, at a temperature of 40 DEG C
30min is stirred, mixing speed is 800r/min, add 0.2 part of defoamer after stirring wherein, continuation is stirred at a temperature of 40 DEG C
10min is mixed, mixing speed is 800r/min；
C, addition pH adjusting agent, stir 20min, mixing speed is 800r/min, stop stirring, stand at room temperature, and filtering is obtained
Waterproof, seepage control water paint rubber cement.
Embodiment 2
The preparation method applied to toughness reinforcing heatproof water-impervious coating rubber cement of the present embodiment, including following preparation process：
Following raw material is all parts by weight,
A, 100 parts of cement, 20 parts of reusable scattered rubber powders, 12 parts of plaster of paris, 10 lime are well mixed, are carried out on beveller
Grinding；
B, the mixture of grinding is put into beaker, 0.5 part of calcium sulphate retarder, 15 parts of fine sands slurries added, at a temperature of 40 DEG C
30min is stirred, mixing speed is 800r/min, add 0.2 part of defoamer after stirring wherein, continuation is stirred at a temperature of 40 DEG C
10min is mixed, mixing speed is 800r/min；
C, addition pH adjusting agent, stir 20min, mixing speed is 800r/min, stop stirring, stand at room temperature, and filtering is obtained
Waterproof, seepage control water paint rubber cement.
Embodiment 3
The preparation method applied to toughness reinforcing heatproof water-impervious coating rubber cement of the present embodiment, including following preparation process：
Following raw material is all parts by weight,
A, 100 parts of cement, 15 parts of reusable scattered rubber powders, 5 parts of plaster of paris, 6 lime are well mixed, are ground on beveller
Mill；
B, the mixture of grinding is put into beaker, adds 1 part of calcium sulphate retarder, 22 parts of fine sands slurries, stirred at a temperature of 40 DEG C
30min is mixed, mixing speed is 800r/min, add 0.4 part of defoamer after stirring wherein, continuation is stirred at a temperature of 40 DEG C
10min, mixing speed is 800r/min；
C, addition pH adjusting agent, stir 20min, mixing speed is 800r/min, stop stirring, stand at room temperature, and filtering is obtained
Waterproof, seepage control water paint rubber cement.
Embodiment 4
The preparation method applied to toughness reinforcing heatproof water-impervious coating rubber cement of the present embodiment, including following preparation process：
Following raw material is all parts by weight,
A, 100 parts of cement, 25 parts of reusable scattered rubber powders, 17 parts of plaster of paris, 15 lime are well mixed, are carried out on beveller
Grinding；
B, the mixture of grinding is put into beaker, adds 2 parts of calcium sulphate retarders, 27 parts of fine sands slurries, stirred at a temperature of 40 DEG C
30min is mixed, mixing speed is 800r/min, add 0.8 part of defoamer after stirring wherein, continuation is stirred at a temperature of 40 DEG C
10min, mixing speed is 800r/min；
C, addition pH adjusting agent, stir 20min, mixing speed is 800r/min, stop stirring, stand at room temperature, and filtering is obtained
Waterproof, seepage control water paint rubber cement.
Embodiment 5
The preparation method applied to toughness reinforcing heatproof water-impervious coating rubber cement of the present embodiment, including following preparation process：
Following raw material is all parts by weight,
A, 100 parts of cement, 15 parts of reusable scattered rubber powders, 5 parts of plaster of paris, 6 lime are well mixed, are ground on beveller
Mill；
B, the mixture of grinding is put into beaker, 0.5 part of calcium sulphate retarder, 15 parts of fine sands slurries added, at a temperature of 70 DEG C
30min is stirred, mixing speed is 800r/min, add 0.2 part of defoamer after stirring wherein, continuation is stirred at a temperature of 70 DEG C
10min is mixed, mixing speed is 800r/min；
C, addition pH adjusting agent, stir 20min, mixing speed is 800r/min, stop stirring, stand at room temperature, and filtering is obtained
Waterproof, seepage control water paint rubber cement.
Embodiment 6
The preparation method applied to toughness reinforcing heatproof water-impervious coating rubber cement of the present embodiment, including following preparation process：
Following raw material is all parts by weight,
A, 100 parts of cement, 15 parts of reusable scattered rubber powders, 5 parts of plaster of paris, 6 lime are well mixed, are ground on beveller
Mill；
B, the mixture of grinding is put into beaker, 0.5 part of calcium sulphate retarder, 15 parts of fine sands slurries added, at a temperature of 40 DEG C
60min is stirred, mixing speed is 800r/min, add 0.2 part of defoamer after stirring wherein, continuation is stirred at a temperature of 40 DEG C
10min is mixed, mixing speed is 800r/min；
C, addition pH adjusting agent, stir 20min, mixing speed is 800r/min, stop stirring, stand at room temperature, and filtering is obtained
Waterproof, seepage control water paint rubber cement.
Embodiment 7
The preparation method applied to toughness reinforcing heatproof water-impervious coating rubber cement of the present embodiment, including following preparation process：
Following raw material is all parts by weight,
A, 100 parts of cement, 25 parts of reusable scattered rubber powders, 17 parts of plaster of paris, 15 lime are well mixed, are carried out on beveller
Grinding；
B, the mixture of grinding is put into beaker, adds 2 parts of calcium sulphate retarders, 27 parts of fine sands slurries, stirred at a temperature of 70 DEG C
30min is mixed, mixing speed is 800r/min, add 0.8 part of defoamer after stirring wherein, continuation is stirred at a temperature of 70 DEG C
10min, mixing speed is 800r/min；
C, addition pH adjusting agent, stir 20min, mixing speed is 800r/min, stop stirring, stand at room temperature, and filtering is obtained
Waterproof, seepage control water paint rubber cement.
Embodiment 8
The preparation method applied to toughness reinforcing heatproof water-impervious coating rubber cement of the present embodiment, including following preparation process：
Following raw material is all parts by weight,
A, 100 parts of cement, 25 parts of reusable scattered rubber powders, 17 parts of plaster of paris, 15 lime are well mixed, are carried out on beveller
Grinding；
B, the mixture of grinding is put into beaker, adds 2 parts of calcium sulphate retarders, 27 parts of fine sands slurries, stirred at a temperature of 40 DEG C
60min is mixed, mixing speed is 800r/min, add 0.8 part of defoamer after stirring wherein, continuation is stirred at a temperature of 40 DEG C
10min, mixing speed is 800r/min；
C, addition pH adjusting agent, stir 20min, mixing speed is 800r/min, stop stirring, stand at room temperature, and filtering is obtained
Waterproof, seepage control water paint rubber cement.
Embodiment 9
The preparation method applied to toughness reinforcing heatproof water-impervious coating rubber cement of the present embodiment, including following preparation process：
Following raw material is all parts by weight,
A, 100 parts of cement, 15 parts of reusable scattered rubber powders, 5 parts of plaster of paris, 6 lime are well mixed, are ground on beveller
Mill；
B, the mixture of grinding is put into beaker, 0.5 part of calcium sulphate retarder, 15 parts of fine sands slurries added, at a temperature of 70 DEG C
60min is stirred, mixing speed is 800r/min, add 0.2 part of defoamer after stirring wherein, continuation is stirred at a temperature of 70 DEG C
10min is mixed, mixing speed is 800r/min；
C, addition pH adjusting agent, stir 20min, mixing speed is 800r/min, stop stirring, stand at room temperature, and filtering is obtained
Waterproof, seepage control water paint rubber cement.
Embodiment 10
The preparation method applied to toughness reinforcing heatproof water-impervious coating rubber cement of the present embodiment, including following preparation process：
Following raw material is all parts by weight,
A, 100 parts of cement, 25 parts of reusable scattered rubber powders, 17 parts of plaster of paris, 15 lime are well mixed, are carried out on beveller
Grinding；
B, the mixture of grinding is put into beaker, adds 2 parts of calcium sulphate retarders, 27 parts of fine sands slurries, stirred at a temperature of 70 DEG C
60min is mixed, mixing speed is 800r/min, add 0.8 part of defoamer after stirring wherein, continuation is stirred at a temperature of 70 DEG C
10min, mixing speed is 800r/min；
C, addition pH adjusting agent, stir 20min, mixing speed is 800r/min, stop stirring, stand at room temperature, and filtering is obtained
Waterproof, seepage control water paint rubber cement.
Embodiment 11
The preparation method applied to toughness reinforcing heatproof water-impervious coating rubber cement of the present embodiment, including following preparation process：
Following raw material is all parts by weight,
A, 100 parts of cement, 20 parts of reusable scattered rubber powders, 10 parts of plaster of paris, 10 lime are well mixed, are carried out on beveller
Grinding；
B, the mixture of grinding is put into beaker, adds 1 part of calcium sulphate retarder, 20 parts of fine sands slurries, stirred at a temperature of 40 DEG C
30min is mixed, mixing speed is 800r/min, add 0.5 part of defoamer after stirring wherein, continuation is stirred at a temperature of 40 DEG C
10min, mixing speed is 800r/min；
C, addition pH adjusting agent, stir 20min, mixing speed is 800r/min, stop stirring, stand at room temperature, and filtering is obtained
Waterproof, seepage control water paint rubber cement.
Embodiment 12
The preparation method applied to toughness reinforcing heatproof water-impervious coating rubber cement of the present embodiment, including following preparation process：
Following raw material is all parts by weight,
A, 100 parts of cement, 20 parts of reusable scattered rubber powders, 10 parts of plaster of paris, 10 lime are well mixed, are carried out on beveller
Grinding；
B, the mixture of grinding is put into beaker, adds 1 part of calcium sulphate retarder, 20 parts of fine sands slurries, stirred at a temperature of 70 DEG C
30min is mixed, mixing speed is 800r/min, add 0.5 part of defoamer after stirring wherein, continuation is stirred at a temperature of 70 DEG C
10min, mixing speed is 800r/min；
C, addition pH adjusting agent, stir 20min, mixing speed is 800r/min, stop stirring, stand at room temperature, and filtering is obtained
Waterproof, seepage control water paint rubber cement.
Embodiment 13
The preparation method applied to toughness reinforcing heatproof water-impervious coating rubber cement of the present embodiment, including following preparation process：
Following raw material is all parts by weight,
A, 100 parts of cement, 20 parts of reusable scattered rubber powders, 10 parts of plaster of paris, 10 lime are well mixed, are carried out on beveller
Grinding；
B, the mixture of grinding is put into beaker, adds 1 part of calcium sulphate retarder, 20 parts of fine sands slurries, stirred at a temperature of 50 DEG C
45min is mixed, mixing speed is 800r/min, add 0.5 part of defoamer after stirring wherein, continuation is stirred at a temperature of 50 DEG C
10min, mixing speed is 800r/min；
C, addition pH adjusting agent, stir 20min, mixing speed is 800r/min, stop stirring, stand at room temperature, and filtering is obtained
Waterproof, seepage control water paint rubber cement.
Embodiment 14
The preparation method applied to toughness reinforcing heatproof water-impervious coating rubber cement of the present embodiment, including following preparation process：
Following raw material is all parts by weight,
A, 100 parts of cement, 20 parts of reusable scattered rubber powders, 10 parts of plaster of paris, 10 lime are well mixed, are carried out on beveller
Grinding；
B, the mixture of grinding is put into beaker, adds 1 part of calcium sulphate retarder, 0.4 part of titanium nitride（TiN）, 20 parts of fine sand slurries,
45min is stirred at a temperature of 50 DEG C, mixing speed is 800r/min, add 0.5 part of defoamer after stirring wherein, continued
10min is stirred at a temperature of 50 DEG C, mixing speed is 800r/min；
C, addition pH adjusting agent, stir 20min, mixing speed is 800r/min, stop stirring, stand at room temperature, and filtering is obtained
Waterproof, seepage control water paint rubber cement.
Embodiment 15
The preparation method applied to toughness reinforcing heatproof water-impervious coating rubber cement of the present embodiment, including following preparation process：
Following raw material is all parts by weight,
A, 100 parts of cement, 20 parts of reusable scattered rubber powders, 10 parts of plaster of paris, 10 lime are well mixed, are carried out on beveller
Grinding；
B, the mixture of grinding is put into beaker, adds 1 part of calcium sulphate retarder, 0.4 part of acrylamide copolymer（Write a Chinese character in simplified form
AP）, 20 parts of fine sand slurries, 45min is stirred at a temperature of 50 DEG C, mixing speed is 800r/min, adds 0.5 after stirring wherein
10min is stirred in part defoamer, continuation at a temperature of 50 DEG C, and mixing speed is 800r/min；
C, addition pH adjusting agent, stir 20min, mixing speed is 800r/min, stop stirring, stand at room temperature, and filtering is obtained
Waterproof, seepage control water paint rubber cement.
Embodiment 16
The preparation method applied to toughness reinforcing heatproof water-impervious coating rubber cement of the present embodiment, including following preparation process：
Following raw material is all parts by weight,
A, 100 parts of cement, 20 parts of reusable scattered rubber powders, 10 parts of plaster of paris, 10 lime are well mixed, are carried out on beveller
Grinding；
B, the mixture of grinding is put into beaker, adds 1 part of calcium sulphate retarder, 0.4 part of titanium nitride-acrylic amide polymerization
Thing, 20 parts of fine sand slurries, stir 45min, mixing speed is 800r/min, adds 0.5 after stirring wherein at a temperature of 50 DEG C
10min is stirred in part defoamer, continuation at a temperature of 50 DEG C, and mixing speed is 800r/min；
C, addition pH adjusting agent, stir 20min, mixing speed is 800r/min, stop stirring, stand at room temperature, and filtering is obtained
Waterproof, seepage control water paint rubber cement.
Embodiment 17
The preparation method applied to toughness reinforcing heatproof water-impervious coating rubber cement of the present embodiment, including following preparation process：
Following raw material is all parts by weight,
A, 100 parts of cement, 20 parts of reusable scattered rubber powders, 10 parts of plaster of paris, 10 lime are well mixed, are carried out on beveller
Grinding；
B, the mixture of grinding is put into beaker, adds 1 part of calcium sulphate retarder, 0.6 part of titanium nitride-acrylic amide polymerization
Thing, 20 parts of fine sand slurries, stir 45min, mixing speed is 800r/min, adds 0.5 after stirring wherein at a temperature of 50 DEG C
10min is stirred in part defoamer, continuation at a temperature of 50 DEG C, and mixing speed is 800r/min；
C, addition pH adjusting agent, stir 20min, mixing speed is 800r/min, stop stirring, stand at room temperature, and filtering is obtained
Waterproof, seepage control water paint rubber cement.
Embodiment 18
The preparation method applied to toughness reinforcing heatproof water-impervious coating rubber cement of the present embodiment, including following preparation process：
Following raw material is all parts by weight,
A, 100 parts of cement, 20 parts of reusable scattered rubber powders, 10 parts of plaster of paris, 10 lime are well mixed, are carried out on beveller
Grinding；
B, the mixture of grinding is put into beaker, add 1 part of calcium sulphate retarder, 1 part of titanium nitride-acrylamide copolymer,
20 parts of fine sand slurries, stir 45min, mixing speed is 800r/min at a temperature of 50 DEG C, add 0.5 part after stirring wherein and disappear
10min is stirred in infusion, continuation at a temperature of 50 DEG C, and mixing speed is 800r/min；
C, addition pH adjusting agent, stir 20min, mixing speed is 800r/min, stop stirring, stand at room temperature, and filtering is obtained
Waterproof, seepage control water paint rubber cement.
Defoamer used in above example is the wax powder 3910 of the triumphant mattress in Shanghai, and pH adjusting agent is sodium hydroxide.
The above-mentioned description to embodiment is understood that for ease of the those skilled in the art and using invention.It is familiar with this
The personnel of art obviously can easily carry out various modifications to these embodiments, and should by General Principle described herein
Use in other embodiment without passing through performing creative labour.Therefore, the invention is not restricted to above-described embodiment, art technology
Personnel according to the announcement of the present invention, do not depart from improvement and modification that scope made all should the present invention protection model
Within enclosing.
Method of testing：
Coating infiltration is tested
The water proofing property of water-repellent paint passes through《Test methods for building waterproof coatings GB/T16777---2008》In " 15. impermeability "
Defined method is tested.Water proof apparatus is《GB/T328.10---2007》In the requirement of 5.2.Embodiment is obtained
Coating pours into the framed middle coating of film, and for convenience of being stripped, film surface can be handled with releasing agent, when prepared by sample in two times
Or three coatings, coating should again be carried out afterwards after preceding coating is done solid work, and interval time is 12-24h twice, and sample thickness reaches 1.5
± 0.5mm, after the surface that last time is coated into sample strikes off, in standing 96h under standard conditions, is then stripped, after the demoulding
Sample reverse side handle to be placed in drying box after 48h, taking-up in 40 ± 2 DEG C of drying boxes and be cooled to room temperature upwards.
By the sample prepared, 150x150mm 3 pieces of sample is cut, according to waterproof test specified in test method
Test apparatus and method are tested, and test pressure is 0.3MPa, keep pressure 90min.
1st, impermeable 2 are represented, infiltration is represented
Coating impact resistance is tested
Assay method determines for GB/T1732-1993 paint films impact resistance.
Coating heat resistance is tested
Assay method is the measure of GB/T1735-2009 paint and varnish heat resistances.
Table 1
| Can be again With point Dissipate glue Powder | Heat Stone Cream | Stone Ash | Gypsum Slow setting Agent | Carefully It is husky Slurry | Disappear Bubble Agent | Titanium nitride-acryloyl Amine polymer | Temperature Degree ℃ | Time min | Water-impervious is surveyed Examination | |
| Embodiment 1 | 15 | 5 | 6 | 0.5 | 15 | 0.2 | 0 | 40 | 30 | 1 |
| Embodiment 2 | 20 | 12 | 10 | 0.5 | 15 | 0.2 | 0 | 40 | 30 | 1 |
| Embodiment 3 | 15 | 5 | 6 | 1 | 22 | 0.4 | 0 | 40 | 30 | 1 |
| Embodiment 4 | 25 | 17 | 15 | 2 | 27 | 0.8 | 0 | 40 | 30 | 1 |
| Embodiment 5 | 15 | 5 | 6 | 0.5 | 15 | 0.2 | 0 | 70 | 30 | 1 |
| Embodiment 6 | 15 | 5 | 6 | 0.5 | 15 | 0.2 | 0 | 40 | 60 | 1 |
| Embodiment 7 | 25 | 17 | 15 | 2 | 27 | 0.8 | 0 | 70 | 30 | 1 |
| Embodiment 8 | 25 | 17 | 15 | 2 | 27 | 0.8 | 0 | 40 | 60 | 1 |
| Embodiment 9 | 15 | 5 | 6 | 0.5 | 15 | 0.2 | 0 | 70 | 60 | 1 |
| Embodiment 10 | 25 | 17 | 15 | 2 | 27 | 0.8 | 0 | 70 | 60 | 1 |
| Embodiment 11 | 20 | 10 | 10 | 1 | 20 | 0.5 | 0 | 40 | 30 | 1 |
| Embodiment 12 | 20 | 10 | 10 | 1 | 20 | 0.5 | 0 | 70 | 30 | 1 |
| Embodiment 13 | 20 | 10 | 10 | 1 | 20 | 0.5 | 0 | 50 | 45 | 1 |
| Embodiment 14 | 20 | 10 | 10 | 1 | 20 | 0.5 | 0.4（TiN） | 50 | 45 | 1 |
| Embodiment 15 | 20 | 10 | 10 | 1 | 20 | 0.5 | 0.4（AP） | 50 | 45 | 1 |
| Embodiment 16 | 20 | 10 | 10 | 1 | 20 | 0.5 | 0.4 | 50 | 45 | 1 |
| Embodiment 17 | 20 | 10 | 10 | 1 | 20 | 0.5 | 0.6 | 50 | 45 | 1 |
| Embodiment 18 | 20 | 10 | 10 | 1 | 20 | 0.5 | 1 | 50 | 45 | 1 |
Table 2
| Can be again With point Dissipate glue Powder | Heat Stone Cream | Stone Ash | Gypsum Slow setting Agent | Carefully It is husky Slurry | Disappear Bubble Agent | Titanium nitride-acryloyl Amine polymer | Temperature Degree ℃ | Time min | Impact strength Kg.cm | |
| Embodiment 1 | 15 | 5 | 6 | 0.5 | 15 | 0.2 | 0 | 40 | 30 | 51 |
| Embodiment 2 | 20 | 12 | 10 | 0.5 | 15 | 0.2 | 0 | 40 | 30 | 54 |
| Embodiment 3 | 15 | 5 | 6 | 1 | 22 | 0.4 | 0 | 40 | 30 | 56 |
| Embodiment 4 | 25 | 17 | 15 | 2 | 27 | 0.8 | 0 | 40 | 30 | 59 |
| Embodiment 5 | 15 | 5 | 6 | 0.5 | 15 | 0.2 | 0 | 70 | 30 | 55 |
| Embodiment 6 | 15 | 5 | 6 | 0.5 | 15 | 0.2 | 0 | 40 | 60 | 53 |
| Embodiment 7 | 25 | 17 | 15 | 2 | 27 | 0.8 | 0 | 70 | 30 | 61 |
| Embodiment 8 | 25 | 17 | 15 | 2 | 27 | 0.8 | 0 | 40 | 60 | 58 |
| Embodiment 9 | 15 | 5 | 6 | 0.5 | 15 | 0.2 | 0 | 70 | 60 | 54 |
| Embodiment 10 | 25 | 17 | 15 | 2 | 27 | 0.8 | 0 | 70 | 60 | 62 |
| Embodiment 11 | 20 | 10 | 10 | 1 | 20 | 0.5 | 0 | 40 | 30 | 56 |
| Embodiment 12 | 20 | 10 | 10 | 1 | 20 | 0.5 | 0 | 70 | 30 | 60 |
| Embodiment 13 | 20 | 10 | 10 | 1 | 20 | 0.5 | 0 | 50 | 45 | 58 |
| Embodiment 14 | 20 | 10 | 10 | 1 | 20 | 0.5 | 0.4（TiN） | 50 | 45 | 63 |
| Embodiment 15 | 20 | 10 | 10 | 1 | 20 | 0.5 | 0.4（AP） | 50 | 45 | 67 |
| Embodiment 16 | 20 | 10 | 10 | 1 | 20 | 0.5 | 0.4 | 50 | 45 | 84 |
| Embodiment 17 | 20 | 10 | 10 | 1 | 20 | 0.5 | 0.6 | 50 | 45 | 88 |
| Embodiment 18 | 20 | 10 | 10 | 1 | 20 | 0.5 | 1 | 50 | 45 | 86 |
Table 3
| Can be again With point Dissipate glue Powder | Heat Stone Cream | Stone Ash | Gypsum Slow setting Agent | Carefully It is husky Slurry | Disappear Bubble Agent | Titanium nitride-acryloyl Amine polymer | Temperature Degree ℃ | Time min | Test temperature DEG C/time h | |
| Embodiment 1 | 15 | 5 | 6 | 0.5 | 15 | 0.2 | 0 | 40 | 30 | 350/12 |
| Embodiment 2 | 20 | 12 | 10 | 0.5 | 15 | 0.2 | 0 | 40 | 30 | 350/12 |
| Embodiment 3 | 15 | 5 | 6 | 1 | 22 | 0.4 | 0 | 40 | 30 | 350/12 |
| Embodiment 4 | 25 | 17 | 15 | 2 | 27 | 0.8 | 0 | 40 | 30 | 350/12 |
| Embodiment 5 | 15 | 5 | 6 | 0.5 | 15 | 0.2 | 0 | 70 | 30 | 350/12 |
| Embodiment 6 | 15 | 5 | 6 | 0.5 | 15 | 0.2 | 0 | 40 | 60 | 350/12 |
| Embodiment 7 | 25 | 17 | 15 | 2 | 27 | 0.8 | 0 | 70 | 30 | 350/12 |
| Embodiment 8 | 25 | 17 | 15 | 2 | 27 | 0.8 | 0 | 40 | 60 | 350/12 |
| Embodiment 9 | 15 | 5 | 6 | 0.5 | 15 | 0.2 | 0 | 70 | 60 | 350/12 |
| Embodiment 10 | 25 | 17 | 15 | 2 | 27 | 0.8 | 0 | 70 | 60 | 350/12 |
| Embodiment 11 | 20 | 10 | 10 | 1 | 20 | 0.5 | 0 | 40 | 30 | 350/12 |
| Embodiment 12 | 20 | 10 | 10 | 1 | 20 | 0.5 | 0 | 70 | 30 | 350/12 |
| Embodiment 13 | 20 | 10 | 10 | 1 | 20 | 0.5 | 0 | 50 | 45 | 350/12 |
| Embodiment 14 | 20 | 10 | 10 | 1 | 20 | 0.5 | 0.4（TiN） | 50 | 45 | 370/12 |
| Embodiment 15 | 20 | 10 | 10 | 1 | 20 | 0.5 | 0.4（AP） | 50 | 45 | 380/12 |
| Embodiment 16 | 20 | 10 | 10 | 1 | 20 | 0.5 | 0.4 | 50 | 45 | 450/20 |
| Embodiment 17 | 20 | 10 | 10 | 1 | 20 | 0.5 | 0.6 | 50 | 45 | 450/20 |
| Embodiment 18 | 20 | 10 | 10 | 1 | 20 | 0.5 | 1 | 50 | 45 | 450/20 |
Claims (10)
1. a kind of toughness reinforcing heatproof water-impervious coating rubber cement, it is characterised in that the toughness reinforcing heatproof antiseepage water paint comprising cement, can
Starched again with scattered rubber powder, calcium sulphate retarder, defoamer, plaster of paris, lime, fine sand.
2. toughness reinforcing heatproof water-impervious coating rubber cement as claimed in claim 1, it is characterised in that by weight, include 100 parts
Cement, 15-25 parts of reusable scattered rubber powder, 0.5-2 parts of calcium sulphate retarder, 0.2-0.8 parts of defoamer, 5-17 parts
Plaster of paris, 6-15 parts of lime, 15-27 parts of fine sand slurry.
3. toughness reinforcing heatproof water-impervious coating rubber cement as claimed in claim 2, it is characterised in that by weight, include 100 parts
Cement, 18-22 parts of reusable scattered rubber powder, 0.8-1.2 parts of calcium sulphate retarder, 0.4-0.6 parts of defoamer, 9-13 parts
Plaster of paris, 8-12 parts of lime, 18-23 parts fine sand slurry.
4. toughness reinforcing heatproof water-impervious coating rubber cement as claimed in claim 3, it is characterised in that by weight, include 100 parts
Cement, 20 parts of reusable scattered rubber powder, 1 part of calcium sulphate retarder, 0.5 part of defoamer, 10 parts of plaster of paris, 10 parts
Lime, 20 parts of fine sand slurry.
5. the toughness reinforcing heatproof water-impervious coating rubber cement as described in claim any one of 1-4, it is characterised in that include toughness reinforcing heatproof
Agent.
6. toughness reinforcing heatproof water-impervious coating rubber cement as claimed in claim 5, it is characterised in that described toughness reinforcing refractory agent is nitrogen
Change titanium-acrylamide copolymer.
7. toughness reinforcing heatproof water-impervious coating rubber cement as claimed in claim 6, it is characterised in that described titanium nitride-acryloyl
Amine polymer parts by weight are 0.4-1.
8. the preparation method of the toughness reinforcing heatproof water-impervious coating rubber cement described in one of claim 1-4, it is characterised in that including with
Lower step：
1）The cement of formula ratio, reusable scattered rubber powder, plaster of paris, lime are well mixed, are ground on beveller；
2）The mixture of grinding is put into beaker, calcium sulphate retarder, the fine sand slurry of corresponding formula ratio are added, at 40-70 DEG C
At a temperature of stir 30-60min, add defoamer after stirring wherein, 5-15min is stirred in continuation at a temperature of 40-70 DEG C；
3）PH adjusting agent is added, 10-30min is stirred at room temperature, stops stirring, is stood, filtering obtains waterproof, seepage control water paint.
9. the preparation method of the toughness reinforcing heatproof water-impervious coating rubber cement described in claim 8, it is characterised in that including following step
Suddenly：
1）The cement of formula ratio, reusable scattered rubber powder, plaster of paris, lime are well mixed, are ground on beveller；
2）The mixture of grinding is put into beaker, calcium sulphate retarder, the fine sand slurry of corresponding formula ratio are added, at 50-60 DEG C
At a temperature of stir 40-50min, add defoamer after stirring wherein, 10min is stirred in continuation at a temperature of 50-60 DEG C；
3）PH adjusting agent is added, 20min is stirred at room temperature, stops stirring, is stood, filtering obtains waterproof, seepage control water paint.
10. the preparation method of the toughness reinforcing heatproof water-impervious coating rubber cement described in claim 9, it is characterised in that described stirring
Speed is 500-1000r/min.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109337203A (en) * | 2018-10-08 | 2019-02-15 | 湖南铭弘体育产业股份有限公司 | A kind of movement of environmental protection floor based on high fire-retardance clay composite material |
| CN109370045A (en) * | 2018-10-08 | 2019-02-22 | 湖南铭弘体育产业股份有限公司 | Wear-resisting track material and preparation method thereof based on modified Nano clay |
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| CN104962149A (en) * | 2015-07-03 | 2015-10-07 | 周文鹏 | Negative ion dry powder interior wall coating material and preparation method for same |
| CN105060816A (en) * | 2015-08-07 | 2015-11-18 | 马鞍山十七冶工程科技有限责任公司 | Cement base permeating crystallizing waterproof paint formed by reinforcing straw fibers |
| CN105801063A (en) * | 2016-03-16 | 2016-07-27 | 韩旭霞 | Light-weight, heat-insulating and environment-friendly composite wall building material |
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| CN103332903A (en) * | 2013-05-31 | 2013-10-02 | 成都新柯力化工科技有限公司 | Self-crystallized polymer cement-based waterproof coating, and preparation method thereof |
| CN104962149A (en) * | 2015-07-03 | 2015-10-07 | 周文鹏 | Negative ion dry powder interior wall coating material and preparation method for same |
| CN105060816A (en) * | 2015-08-07 | 2015-11-18 | 马鞍山十七冶工程科技有限责任公司 | Cement base permeating crystallizing waterproof paint formed by reinforcing straw fibers |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109337203A (en) * | 2018-10-08 | 2019-02-15 | 湖南铭弘体育产业股份有限公司 | A kind of movement of environmental protection floor based on high fire-retardance clay composite material |
| CN109370045A (en) * | 2018-10-08 | 2019-02-22 | 湖南铭弘体育产业股份有限公司 | Wear-resisting track material and preparation method thereof based on modified Nano clay |
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