CN107188664A - A kind of Chinese toon high yield height sustained release compoiste fertilizer - Google Patents
A kind of Chinese toon high yield height sustained release compoiste fertilizer Download PDFInfo
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- CN107188664A CN107188664A CN201710334120.9A CN201710334120A CN107188664A CN 107188664 A CN107188664 A CN 107188664A CN 201710334120 A CN201710334120 A CN 201710334120A CN 107188664 A CN107188664 A CN 107188664A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B1/00—Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
- C05B1/04—Double-superphosphate; Triple-superphosphate; Other fertilisers based essentially on monocalcium phosphate
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pest Control & Pesticides (AREA)
- Soil Sciences (AREA)
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Abstract
The invention discloses a kind of Chinese toon high yield height sustained release compoiste fertilizer, its raw material includes feces of livestock and poultry, wheat stalk, turf, rice husk, Microcystis aeruginosa, hydroxymethyl starch, chitin, urea, urea phosphate, borax, ammonium chloride, potassium chloride, Diammonium phosphate (DAP), potassium nitrate, calcium humate, humic acid magnesium, boric acid, ammonium nitrate, calcium dihydrogen phosphate, zinc-amino acid chelate, zinc sulfate, manganese sulfate, zinc acetate, molybdenum trisulfate, stalk fermentation microbial inoculum, weathered coal residue, modified sustained release agent and the modifying agent of resistance to Ultraviolet.The compoiste fertilizer of the present invention has excellent sustained release and UV resistant decomposability, can high-effect high-quality nutriment supply is carried out to Chinese toon, disclosure satisfy that the nutritional need in the whole growth course of Chinese toon, improve the yield and quality of Chinese toon.
Description
Technical field
The present invention relates to the technical field of fertilizer, more particularly to a kind of Chinese toon high yield height sustained release compoiste fertilizer.
Background technology
Chinese toon also known as Chinese toon bud, fragrant pile crown, bright red Ailanthus altissima, Chinese toon day etc., also troat seedling in Anhui province.Root has two layers
Skin, also known as the bark of the root or stem of the tree of heaven, originate in China, are distributed in the extensive area in the Changjiang river north and south, are Meliaceae.Deciduous tree, dioecism, leaf
In even number winglike compound leaf, panicle, both sexes floral white, fruit is oval capsule, and aliform seed, seed can be bred.Tree
Body is tall and big, is also the preferred seeds of afforestation in addition to edible for Chinese toon bud.Ancient times Chinese toon is called Chinese toon, and tree-of-heaven is called the tree of heaven.Chinese
Edible Chinese toon Cheng Xi for a long time, Han dynasty just spreads all on both sides of the Changjiang River.Chinese toon bud is nutritious, and with dietary function, cure mainly catch cold,
Arthralgia pain due to rheumatism, stomachache, dysentery etc..
The fertilizer that uses of Chinese toon plantation is mostly organic agriculture fertilizer or inorganic fertilizer in the prior art, its fertilizer efficiency and applied material
Release efficiency, and the demand of Chinese toon growth can not be met to the adjustment effect of soil, so it is a kind of fragrant to need design badly
Chinese toon high yield height is sustained compoiste fertilizer to solve the problems of the prior art.
The content of the invention
To solve technical problem present in background technology, the present invention proposes a kind of Chinese toon high yield height sustained release organic composite
Fertilizer, with excellent sustained release and UV resistant decomposability, can high-effect high-quality to Chinese toon carry out nutriment supply, can
The nutritional need in the whole growth course of Chinese toon is met, the yield and quality of Chinese toon is improved.
A kind of Chinese toon high yield height sustained release compoiste fertilizer proposed by the present invention, its raw material includes by weight：Feces of livestock and poultry
30-50 parts, 15-25 parts of wheat stalk, 20-60 parts of turf, 10-30 parts of rice husk, 3-5 parts of Microcystis aeruginosa, 2-5 parts of hydroxymethyl starch,
2-5 parts of chitin, 20-40 parts of urea, 2-3 parts of urea phosphate, 2-5 parts of borax, 1-4 parts of ammonium chloride, 3-9 parts of potassium chloride, di(2-ethylhexyl)phosphate
2-5 parts of ammonium, 1-3 parts of potassium nitrate, 2-5 parts of calcium humate, 3-6 parts of humic acid magnesium, 1-5 parts of boric acid, 1-4 parts of ammonium nitrate, di(2-ethylhexyl)phosphate
2-6 parts of hydrogen calcium, 3-5 parts of zinc-amino acid chelate, 4-8 parts of zinc sulfate, 6-12 parts of manganese sulfate, 4-9 parts of zinc acetate, 2-5 parts of molybdenum trisulfate,
2-5 parts of stalk fermentation microbial inoculum, 1-5 parts of weathered coal residue, modified 4-9 parts of sustained release agent, 4-9 parts of the modifying agent of resistance to Ultraviolet.
Preferably, modified sustained release agent is prepared by following technique：Chitosan, pyridine and chloroform are well mixed, Yu Bing
Add acyl chlorides in water-bath to be well mixed, then stirring heats up, and is incubated, then with acetone extraction, then dries, be cooled to room temperature,
Then add glacial acetic acid to be well mixed, stirring stands obtain being modified sustained release agent at room temperature.
Preferably, modified sustained release agent is prepared by following technique：Chitosan, pyridine and chloroform are well mixed, Yu Bing
Acyl chlorides is added in water-bath to be well mixed, 20-40min is stirred in 350-550r/min rotating speeds, then heats to 60-80 DEG C, insulation
20-40min, then uses acetone extraction 6-10h, then dries 20-26h, is cooled to room temperature, then adds glacial acetic acid mixing equal
It is even, 1-3h is stirred in 850-1050r/min rotating speeds, 22-26h is stood at room temperature and obtains being modified sustained release agent.
Preferably, in the preparation technology of modified sustained release agent, chitosan, pyridine, chloroform, the weight ratio of acyl chlorides and glacial acetic acid are
1-3：2-5：3-5：2-6：2-4.
Preferably, the raw material for the modifying agent of resistance to Ultraviolet includes by weight：It is 3-9 parts of nano titanium oxide, silane coupled
4-6 parts of agent KH-570,2-5 parts of neopelex, 1-4 parts of acrylamide, 2-5 parts of N,N methylene bis acrylamide,
3-9 parts of ammonium persulfate.
Preferably, the modifying agent of resistance to Ultraviolet is prepared by following technique：By nano titanium oxide and silane coupler
KH-570 is well mixed, and adjusts pH, then the ultrasonic disperse in water-bath, is incubated after heating, is then taken solid after suction filtration, is washed,
Vacuum drying, is cooled to room temperature, then adds deionized water and neopelex is well mixed, adjust pH, ultrasound point
Dissipate, add acrylamide and N, N- methylene-bisacrylamide are well mixed, stirring, pH is adjusted, after being heated up in water-bath crucible
Insulation, is subsequently added into ammonium persulfate and is well mixed, and suction filtration takes solid, and washing is cooled to room temperature and obtained after being dried in vacuo in baking oven
To the modifying agent of resistance to Ultraviolet.
Preferably, the modifying agent of resistance to Ultraviolet is prepared by following technique：By nano titanium oxide and silane coupler
KH-570 is well mixed, and adjusts pH to 4.5-5.5, then the ultrasonic disperse 5-15min in 35-45 DEG C of water-bath, is warming up to 65-75
DEG C, 20-30min is incubated, then solid is taken after suction filtration, washed, 5-7h is dried in vacuo in 55-65 DEG C, is cooled to room temperature, Ran Houjia
Enter deionized water and neopelex is well mixed, adjust pH to 3.5-4.5, ultrasonic disperse 35-45min, add third
Acrylamide and N, N- methylene-bisacrylamide are well mixed, and 20-40min is stirred in 650-850r/min rotating speeds, regulation pH to
6.0-8.0, is warming up to 45-55 DEG C in water-bath crucible, is incubated 10-20min, is subsequently added into ammonium persulfate and is well mixed, suction filtration
Solid is taken, is washed after being dried in vacuo 20-26h in 40-50 DEG C of baking oven, is cooled to room temperature and obtains the modifying agent of resistance to Ultraviolet.
A kind of Chinese toon high yield height sustained release compoiste fertilizer of the present invention, its raw material includes feces of livestock and poultry, wheat stalk, grass
Charcoal, rice husk, Microcystis aeruginosa, hydroxymethyl starch, chitin, urea, urea phosphate, borax, ammonium chloride, potassium chloride, Diammonium phosphate (DAP), nitric acid
Potassium, calcium humate, humic acid magnesium, boric acid, ammonium nitrate, calcium dihydrogen phosphate, zinc-amino acid chelate, zinc sulfate, manganese sulfate, acetic acid
Zinc, molybdenum trisulfate, stalk fermentation microbial inoculum, weathered coal residue, modified sustained release agent and the modifying agent of resistance to Ultraviolet.The present invention's is organic multiple
Hefei has excellent sustained release and UV resistant decomposability, can high-effect high-quality nutriment supply, energy are carried out to Chinese toon
The nutritional need in the whole growth course of Chinese toon is enough met, the yield and quality of Chinese toon is improved.Wherein, modified sustained release agent passes through
Chitosan, pyridine and chloroform are well mixed, acyl chlorides is added in ice-water bath and is well mixed, then stirring heats up, and is incubated, so
Acetone extraction is used afterwards, then dries, is cooled to room temperature, glacial acetic acid is then added and is well mixed, and stirring stands changed at room temperature
Property sustained release agent, apply to the present invention compoiste fertilizer in, the sustained release performance of compoiste fertilizer of the present invention can be effectively improved, transport
In the compoiste fertilizer for using the present invention, the sustained release performance of compoiste fertilizer of the present invention is effectively increased so that nutriment
Release more uniform high-efficiency, disclosure satisfy that the nutrient requirement of the varying level in the whole growth course of Chinese toon.Wherein, resistance to purple
Outer decomposition modifying agent adjusts pH, then in water-bath by the way that nano titanium oxide and Silane coupling reagent KH-570 are well mixed
Ultrasonic disperse, is incubated after heating, then takes solid after suction filtration, washs, and vacuum drying is cooled to room temperature, then adds deionization
Water and neopelex are well mixed, adjust pH, and ultrasonic disperse adds acrylamide and N, N- methylene bisacrylamide acyl
Amine is well mixed, stirring, adjusts pH, is incubated after being heated up in water-bath crucible, is subsequently added into ammonium persulfate and is well mixed, suction filtration takes
Solid, washing is cooled to room temperature and obtains the modifying agent of resistance to Ultraviolet after being dried in vacuo in baking oven, applies to the organic of the present invention
In fertilizer, coordinate with the modification sustained release agent that the present invention is added, impart the excellent UV resistant performance of compoiste fertilizer of the present invention.
Embodiment
The present invention is described in detail with reference to specific embodiment, it should be appreciated that embodiment is served only for illustrating this hair
It is bright, rather than for limiting the invention, any modification made on the basis of the present invention, equivalent substitution etc. are in this hair
In bright protection domain.
Embodiment 1
A kind of Chinese toon high yield height sustained release compoiste fertilizer proposed by the present invention, its raw material includes by weight：Feces of livestock and poultry
40 parts, 20 parts of wheat stalk, 40 parts of turf, 20 parts of rice husk, 4 parts of Microcystis aeruginosa, 3.5 parts of hydroxymethyl starch, 3.5 parts of chitin, urine
30 parts of element, 2.5 parts of urea phosphate, 3.5 parts of borax, 2.5 parts of ammonium chloride, 6 parts of potassium chloride, 3.5 parts of Diammonium phosphate (DAP), 2 parts of potassium nitrate, corruption
3.5 parts of phytic acid calcium, 4.5 parts of humic acid magnesium, 3 parts of boric acid, 2.5 parts of ammonium nitrate, 4 parts of calcium dihydrogen phosphate, 4 parts of zinc-amino acid chelate,
6 parts of zinc sulfate, 9 parts of manganese sulfate, 6.5 parts of zinc acetate, 3.5 parts of molybdenum trisulfate, 3.5 parts of stalk fermentation microbial inoculum, 3 parts of weathered coal residue,
Modified 6.5 parts of sustained release agent, 6.5 parts of the modifying agent of resistance to Ultraviolet.
Modified sustained release agent is prepared by following technique：2 parts of chitosans, 3.5 parts of pyridines and 4 parts of chloroforms are mixed by weight
Close uniform, 4 parts of acyl chlorides added in ice-water bath and are well mixed, 30min is stirred in 450r/min rotating speeds, then heats to 70 DEG C,
30min is incubated, acetone extraction 8h is then used, 23h is then dried, is cooled to room temperature, 3 parts of glacial acetic acid is then added and is well mixed,
2h is stirred in 950r/min rotating speeds, 24h is stood at room temperature and obtains being modified sustained release agent.
The modifying agent of resistance to Ultraviolet is prepared by following technique：By weight by 6 parts of nano titanium oxides and 5 parts of silane
Coupling agent kh-570 is well mixed, and adjusts pH to 5, then the ultrasonic disperse 10min in 40 DEG C of water-baths, is warming up to 70 DEG C, insulation
25min, then takes solid after suction filtration, washing, is dried in vacuo 6h in 60 DEG C, is cooled to room temperature, then adds deionized water and 3.5
Part neopelex is well mixed, and adjusts pH to 4.0, ultrasonic disperse 40min, adds 2.5 parts of acrylamides and 3.5 parts
N, N- methylene-bisacrylamide are well mixed, and 30min is stirred in 750r/min rotating speeds, pH to 7.0 are adjusted, in water-bath crucible
50 DEG C are warming up to, 15min is incubated, 6 parts of ammonium persulfates is subsequently added into and is well mixed, suction filtration takes solid, wash after 45 DEG C of baking ovens
Middle vacuum drying 23h, is cooled to room temperature and obtains the modifying agent of resistance to Ultraviolet.
Embodiment 2
A kind of Chinese toon high yield height sustained release compoiste fertilizer proposed by the present invention, its raw material includes by weight：Feces of livestock and poultry
30 parts, 25 parts of wheat stalk, 20 parts of turf, 30 parts of rice husk, 3 parts of Microcystis aeruginosa, 5 parts of hydroxymethyl starch, 2 parts of chitin, urea 40
Part, 2 parts of urea phosphate, 5 parts of borax, 1 part of ammonium chloride, 9 parts of potassium chloride, 2 parts of Diammonium phosphate (DAP), 3 parts of potassium nitrate, 2 parts of calcium humate, corruption
6 parts of phytic acid magnesium, 1 part of boric acid, 4 parts of ammonium nitrate, 2 parts of calcium dihydrogen phosphate, 5 parts of zinc-amino acid chelate, 4 parts of zinc sulfate, manganese sulfate 12
Part, 4 parts of zinc acetate, 5 parts of molybdenum trisulfate, 2 parts of stalk fermentation microbial inoculum, 5 parts of weathered coal residue, modified 4 parts of sustained release agent, resistance to Ultraviolet
9 parts of modifying agent.
Modified sustained release agent is prepared by following technique：1 part of chitosan, 5 parts of pyridines and 3 parts of chloroforms are mixed by weight
Uniformly, 6 parts of acyl chlorides are added in ice-water bath to be well mixed, 40min is stirred in 350r/min rotating speeds, then heat to 60 DEG C, guarantor
Warm 40min, then uses acetone extraction 6h, then dries 26h, is cooled to room temperature, then adds 2 parts of glacial acetic acid and is well mixed, in
1050r/min rotating speeds stir 1h, and 26h is stood at room temperature and obtains being modified sustained release agent.
The modifying agent of resistance to Ultraviolet is prepared by following technique：By weight by 3 parts of nano titanium oxides and 6 parts of silane
Coupling agent kh-570 is well mixed, and adjusts pH to 4.5, then the ultrasonic disperse 5min in 45 DEG C of water-baths, is warming up to 75 DEG C, insulation
20min, then takes solid after suction filtration, washing, is dried in vacuo 5h in 65 DEG C, is cooled to room temperature, then adds deionized water and 5 parts
Neopelex is well mixed, and adjusts pH to 3.5, ultrasonic disperse 45min, adds 1 part of acrylamide and 5 parts of N, N- are sub-
Bisacrylamide is well mixed, and 40min is stirred in 650r/min rotating speeds, is adjusted pH to 6.0, is warming up in water-bath crucible
55 DEG C, 10min is incubated, 9 parts of ammonium persulfates is subsequently added into and is well mixed, suction filtration takes solid, wash after vacuum in 40 DEG C of baking ovens
26h is dried, room temperature is cooled to and obtains the modifying agent of resistance to Ultraviolet.
Embodiment 3
A kind of Chinese toon high yield height sustained release compoiste fertilizer proposed by the present invention, its raw material includes by weight：Feces of livestock and poultry
50 parts, 15 parts of wheat stalk, 60 parts of turf, 10 parts of rice husk, 5 parts of Microcystis aeruginosa, 2 parts of hydroxymethyl starch, 5 parts of chitin, urea 20
Part, 3 parts of urea phosphate, 2 parts of borax, 4 parts of ammonium chloride, 3 parts of potassium chloride, 5 parts of Diammonium phosphate (DAP), 1 part of potassium nitrate, 5 parts of calcium humate, corruption
3 parts of phytic acid magnesium, 5 parts of boric acid, 1 part of ammonium nitrate, 6 parts of calcium dihydrogen phosphate, 3 parts of zinc-amino acid chelate, 8 parts of zinc sulfate, manganese sulfate 6
Part, 9 parts of zinc acetate, 2 parts of molybdenum trisulfate, 5 parts of stalk fermentation microbial inoculum, 1 part of weathered coal residue, modified 9 parts of sustained release agent, resistance to Ultraviolet
4 parts of modifying agent.
Modified sustained release agent is prepared by following technique：3 parts of chitosans, 2 parts of pyridines and 5 parts of chloroforms are mixed by weight
Uniformly, 2 parts of acyl chlorides are added in ice-water bath to be well mixed, 20min is stirred in 550r/min rotating speeds, then heat to 80 DEG C, guarantor
Warm 20min, then uses acetone extraction 10h, then dries 20h, is cooled to room temperature, then adds 4 parts of glacial acetic acid and is well mixed, in
850r/min rotating speeds stir 3h, and 22h is stood at room temperature and obtains being modified sustained release agent.
The modifying agent of resistance to Ultraviolet is prepared by following technique：By weight by 9 parts of nano titanium oxides and 4 parts of silane
Coupling agent kh-570 is well mixed, and adjusts pH to 5.5, then the ultrasonic disperse 15min in 35 DEG C of water-baths, is warming up to 65 DEG C, guarantor
Warm 30min, then takes solid after suction filtration, washing, is dried in vacuo 7h in 55 DEG C, is cooled to room temperature, then adds deionized water and 2
Part neopelex is well mixed, and adjusts pH to 4.5, ultrasonic disperse 35min, adds 4 parts of acrylamides and 2 parts of N, N-
Methylene-bisacrylamide is well mixed, and 20min is stirred in 850r/min rotating speeds, adjusts pH to 8.0, is heated up in water-bath crucible
To 45 DEG C, 20min is incubated, 3 parts of ammonium persulfates is subsequently added into and is well mixed, suction filtration takes solid, and washing is after true in 50 DEG C of baking ovens
Sky dries 20h, is cooled to room temperature and obtains the modifying agent of resistance to Ultraviolet.
Embodiment 4
A kind of Chinese toon high yield height sustained release compoiste fertilizer proposed by the present invention, its raw material includes by weight：Feces of livestock and poultry
35 parts, 22 parts of wheat stalk, 25 parts of turf, 25 parts of rice husk, 3.5 parts of Microcystis aeruginosa, 4 parts of hydroxymethyl starch, 3 parts of chitin, urea
35 parts, 2.2 parts of urea phosphate, 4 parts of borax, 2 parts of ammonium chloride, 8 parts of potassium chloride, 3 parts of Diammonium phosphate (DAP), 2.5 parts of potassium nitrate, calcium humate
3 parts, 5 parts of humic acid magnesium, 2 parts of boric acid, 3 parts of ammonium nitrate, 3 parts of calcium dihydrogen phosphate, 4.5 parts of zinc-amino acid chelate, 5 parts of zinc sulfate,
It is 11 parts of manganese sulfate, 5 parts of zinc acetate, 4 parts of molybdenum trisulfate, 3 parts of stalk fermentation microbial inoculum, 4 parts of weathered coal residue, modified 5 parts of sustained release agent, resistance to
8 parts of Ultraviolet modifying agent.
Modified sustained release agent is prepared by following technique：By weight by 1.5 parts of chitosans, 4 parts of pyridines and 3.5 parts of chloroforms
Well mixed, 5 parts of acyl chlorides of addition are well mixed in ice-water bath, are stirred 35min in 380r/min rotating speeds, are then heated to 65
DEG C, 35min is incubated, acetone extraction 7h is then used, 24h is then dried, is cooled to room temperature, 2.5 parts of glacial acetic acid mixing are then added
Uniformly, 1.5h is stirred in 1020r/min rotating speeds, 25h is stood at room temperature and obtains being modified sustained release agent.
The modifying agent of resistance to Ultraviolet is prepared by following technique：By weight by 4 parts of nano titanium oxides and 5.5 parts of silicon
Alkane coupling agent kh-570 is well mixed, and adjusts pH to 4.8, then the ultrasonic disperse 8min in 42 DEG C of water-baths, is warming up to 72 DEG C, guarantor
Warm 22min, then takes solid after suction filtration, washing, is dried in vacuo 5.5h in 62 DEG C, is cooled to room temperature, then adds deionized water
It is well mixed with 4 parts of neopelexes, pH to 3.8, ultrasonic disperse 42min are adjusted, 2 parts of acrylamides and 4 parts are added
N, N- methylene-bisacrylamide are well mixed, and 35min is stirred in 680r/min rotating speeds, pH to 6.5 are adjusted, in water-bath crucible
52 DEG C are warming up to, 12min is incubated, 8 parts of ammonium persulfates is subsequently added into and is well mixed, suction filtration takes solid, wash after 42 DEG C of baking ovens
Middle vacuum drying 24h, is cooled to room temperature and obtains the modifying agent of resistance to Ultraviolet.
Embodiment 5
A kind of Chinese toon high yield height sustained release compoiste fertilizer proposed by the present invention, its raw material includes by weight：Feces of livestock and poultry
45 parts, 18 parts of wheat stalk, 55 parts of turf, 15 parts of rice husk, 4.5 parts of Microcystis aeruginosa, 3 parts of hydroxymethyl starch, 4 parts of chitin, urea
25 parts, 2.8 parts of urea phosphate, 3 parts of borax, 3 parts of ammonium chloride, 4 parts of potassium chloride, 4 parts of Diammonium phosphate (DAP), 1.5 parts of potassium nitrate, calcium humate
4 parts, 4 parts of humic acid magnesium, 4 parts of boric acid, 2 parts of ammonium nitrate, 5 parts of calcium dihydrogen phosphate, 3.5 parts of zinc-amino acid chelate, 7 parts of zinc sulfate,
It is 7 parts of manganese sulfate, 8 parts of zinc acetate, 3 parts of molybdenum trisulfate, 4 parts of stalk fermentation microbial inoculum, 2 parts of weathered coal residue, modified 8 parts of sustained release agent, resistance to
5 parts of Ultraviolet modifying agent.
Modified sustained release agent is prepared by following technique：By weight by 2.5 parts of chitosans, 3 parts of pyridines and 4.5 parts of chloroforms
Well mixed, 3 parts of acyl chlorides of addition are well mixed in ice-water bath, are stirred 25min in 520r/min rotating speeds, are then heated to 75
DEG C, 25min is incubated, acetone extraction 9h is then used, 22h is then dried, is cooled to room temperature, 3.5 parts of glacial acetic acid mixing are then added
Uniformly, 2.5h is stirred in 880r/min rotating speeds, 23h is stood at room temperature and obtains being modified sustained release agent.
The modifying agent of resistance to Ultraviolet is prepared by following technique：By weight by 8 parts of nano titanium oxides and 4.5 parts of silicon
Alkane coupling agent kh-570 is well mixed, and adjusts pH to 5.2, then the ultrasonic disperse 12min in 38 DEG C of water-baths, is warming up to 68 DEG C,
28min is incubated, then solid is taken after suction filtration, washed, 6.5h is dried in vacuo in 58 DEG C, is cooled to room temperature, then adds deionization
Water and 3 parts of neopelexes are well mixed, and are adjusted pH to 4.2, ultrasonic disperse 38min, are added 3 parts of acrylamides and 3
Part N, N- methylene-bisacrylamides are well mixed, and 25min is stirred in 820r/min rotating speeds, pH to 7.5 are adjusted, in water-bath crucible
In be warming up to 48 DEG C, be incubated 18min, be subsequently added into 4 parts of ammonium persulfates and be well mixed, suction filtration takes solid, and washing is after 48 DEG C of bakings
22h is dried in vacuo in case, room temperature is cooled to and obtains the modifying agent of resistance to Ultraviolet.
Chinese toon high yield height sustained release compoiste fertilizer in 1- of embodiment of the present invention embodiments 5 is applied to the actual plantation of Chinese toon
In, and blank control group is set, blank control group is the Chinese toon planted using common fertilizer, the obtained data such as institute of table 1
Show.
Table 1：
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto,
Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its
Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.
Claims (7)
1. a kind of Chinese toon high yield height sustained release compoiste fertilizer, it is characterised in that its raw material includes by weight：Feces of livestock and poultry 30-
50 parts, 15-25 parts of wheat stalk, 20-60 parts of turf, 10-30 parts of rice husk, 3-5 parts of Microcystis aeruginosa, 2-5 parts of hydroxymethyl starch, crust
Plain 2-5 parts, 20-40 parts of urea, 2-3 parts of urea phosphate, 2-5 parts of borax, 1-4 parts of ammonium chloride, 3-9 parts of potassium chloride, Diammonium phosphate (DAP) 2-5
Part, 1-3 parts of potassium nitrate, 2-5 parts of calcium humate, 3-6 parts of humic acid magnesium, 1-5 parts of boric acid, 1-4 parts of ammonium nitrate, calcium dihydrogen phosphate 2-
6 parts, 3-5 parts of zinc-amino acid chelate, 4-8 parts of zinc sulfate, 6-12 parts of manganese sulfate, 4-9 parts of zinc acetate, 2-5 parts of molybdenum trisulfate, stalk hair
2-5 parts of yeast-like fungi agent, 1-5 parts of weathered coal residue, modified 4-9 parts of sustained release agent, 4-9 parts of the modifying agent of resistance to Ultraviolet.
2. Chinese toon high yield height sustained release compoiste fertilizer according to claim 1, it is characterised in that modified sustained release agent is by as follows
It is prepared by technique：Chitosan, pyridine and chloroform are well mixed, acyl chlorides is added in ice-water bath and is well mixed, stirring, then
Heating, insulation, then with acetone extraction, then dries, is cooled to room temperature, then adds glacial acetic acid and is well mixed, stirring, room temperature
Lower standing obtains being modified sustained release agent.
3. Chinese toon high yield height sustained release compoiste fertilizer according to claim 1 or 2, it is characterised in that modified sustained release agent is pressed
It is prepared by following technique：Chitosan, pyridine and chloroform are well mixed, acyl chlorides is added in ice-water bath and is well mixed, in
350-550r/min rotating speeds stir 20-40min, then heat to 60-80 DEG C, are incubated 20-40min, then use acetone extraction 6-
10h, then dries 20-26h, is cooled to room temperature, then adds glacial acetic acid and is well mixed, in the stirring of 850-1050r/min rotating speeds
1-3h, stands 22-26h and obtains being modified sustained release agent at room temperature.
4. the Chinese toon high yield height sustained release compoiste fertilizer according to claim any one of 1-3, it is characterised in that modified sustained release
In the preparation technology of agent, chitosan, pyridine, chloroform, the weight ratio of acyl chlorides and glacial acetic acid are 1-3：2-5：3-5：2-6：2-4.
5. the Chinese toon high yield height sustained release compoiste fertilizer according to claim any one of 1-4, it is characterised in that resistance to ultraviolet point
The raw material of solution modifying agent includes by weight：3-9 parts of nano titanium oxide, 4-6 parts of Silane coupling reagent KH-570, dodecyl
2-5 parts of benzene sulfonic acid sodium salt, 1-4 parts of acrylamide, 2-5 parts of N,N methylene bis acrylamide, 3-9 parts of ammonium persulfate.
6. the Chinese toon high yield height sustained release compoiste fertilizer according to claim any one of 1-5, it is characterised in that resistance to ultraviolet point
Solution modifying agent is prepared by following technique：Nano titanium oxide and Silane coupling reagent KH-570 are well mixed, pH is adjusted, so
After ultrasonic disperse in water-bath, it is incubated after heating, then takes solid after suction filtration, washed, vacuum drying is cooled to room temperature, then
Add deionized water and neopelex is well mixed, adjust pH, ultrasonic disperse adds acrylamide and N, N- methylene
Base bisacrylamide is well mixed, stirring, adjusts pH, is incubated after being heated up in water-bath crucible, is subsequently added into ammonium persulfate mixing
Uniformly, suction filtration takes solid, and washing is cooled to room temperature and obtains the modifying agent of resistance to Ultraviolet after being dried in vacuo in baking oven.
7. the Chinese toon high yield height sustained release compoiste fertilizer according to claim any one of 1-6, it is characterised in that resistance to ultraviolet point
Solution modifying agent is prepared by following technique：Nano titanium oxide and Silane coupling reagent KH-570 are well mixed, regulation pH to
4.5-5.5, then the ultrasonic disperse 5-15min in 35-45 DEG C of water-bath, is warming up to 65-75 DEG C, is incubated 20-30min, then takes out
Solid is taken after filter, is washed, 5-7h is dried in vacuo in 55-65 DEG C, is cooled to room temperature, deionized water and detergent alkylate is then added
Sodium sulfonate is well mixed, and adjusts pH to 3.5-4.5, ultrasonic disperse 35-45min, adds acrylamide and N, N- di-2-ethylhexylphosphine oxide third
Acrylamide is well mixed, and 20-40min is stirred in 650-850r/min rotating speeds, adjusts pH to 6.0-8.0, is risen in water-bath crucible
Temperature is incubated 10-20min to 45-55 DEG C, is subsequently added into ammonium persulfate and is well mixed, suction filtration takes solid, washs after 40-50 DEG C
20-26h is dried in vacuo in baking oven, room temperature is cooled to and obtains the modifying agent of resistance to Ultraviolet.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111903274A (en) * | 2020-07-28 | 2020-11-10 | 安徽东方金桥农林科技股份有限公司 | High-yield greenhouse planting method for cedrela sinensis |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1793182A (en) * | 2005-12-21 | 2006-06-28 | 华侨大学 | Process for preparing dual-philic N,N-di-acylating shellglycan |
| CN106280616A (en) * | 2016-08-27 | 2017-01-04 | 安徽天瞳智能科技有限公司 | A kind of high tenacity uvioresistant composite |
| CN106588412A (en) * | 2016-12-03 | 2017-04-26 | 安徽爱能洁生物科技有限公司 | Zinc-rich high-yield slow release compound fertilizer for rice planting and preparation method of compound fertilizer |
-
2017
- 2017-05-12 CN CN201710334120.9A patent/CN107188664A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1793182A (en) * | 2005-12-21 | 2006-06-28 | 华侨大学 | Process for preparing dual-philic N,N-di-acylating shellglycan |
| CN106280616A (en) * | 2016-08-27 | 2017-01-04 | 安徽天瞳智能科技有限公司 | A kind of high tenacity uvioresistant composite |
| CN106588412A (en) * | 2016-12-03 | 2017-04-26 | 安徽爱能洁生物科技有限公司 | Zinc-rich high-yield slow release compound fertilizer for rice planting and preparation method of compound fertilizer |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111903274A (en) * | 2020-07-28 | 2020-11-10 | 安徽东方金桥农林科技股份有限公司 | High-yield greenhouse planting method for cedrela sinensis |
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