CN107163760A - A kind of heat-proof combustion-resistant water-repellent paint and preparation method thereof - Google Patents
A kind of heat-proof combustion-resistant water-repellent paint and preparation method thereof Download PDFInfo
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- CN107163760A CN107163760A CN201710609810.0A CN201710609810A CN107163760A CN 107163760 A CN107163760 A CN 107163760A CN 201710609810 A CN201710609810 A CN 201710609810A CN 107163760 A CN107163760 A CN 107163760A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D143/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and containing boron, silicon, phosphorus, selenium, tellurium, or a metal; Coating compositions based on derivatives of such polymers
- C09D143/04—Homopolymers or copolymers of monomers containing silicon
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2227—Oxides; Hydroxides of metals of aluminium
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/02—Flame or fire retardant/resistant
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
The invention discloses a kind of heat-proof combustion-resistant water-repellent paint, belong to technical field of coatings, include the raw material of following parts by weight：38 44 parts of silicone acrylic emulsion, 17 21 parts of vinyl chloride metachloroethylene copolymer, 15 19 parts of silica flour, poly- 2,68 10 parts of polyethylene naphthalates, 9 11 parts of organosilicon hydrophobic powder, 8 10 parts of portland cement, 68 parts of alundum (Al2O3), 68 parts of epoxidized methyl acetorieinoleate, 12 parts of alcohol ester, 24 parts of calgon, 12 parts of hydroxyethyl cellulose, 13 parts of defoamer, 0.5 1.5 parts of water reducer, 0.5 1 parts of early strength agent, appropriate amount of water；The invention also discloses a kind of preparation method of heat-proof combustion-resistant water-repellent paint；Adhesive ability of the present invention is strong, and environmental pollution is small, and good water-proof effect, service life is long, with excellent heat-proof combustion-resistant ability.
Description
Technical field
The present invention relates to technical field of coatings, specifically, a kind of heat-proof combustion-resistant water-repellent paint and its preparation side relate to
Method.
Background technology
Architectural waterproof material refers to moisture, the steam prevented in rainwater, underground water, plumbing, corrosive liquids and air
Deng the material of intrusion building.Building needs the position for carrying out water-proofing treatment to be mainly roofing, metope, ground and basement,
It is main by coating, sprawl, clog, irrigate, the technique such as be bonded and constructed.Domestic waterproof material is developed so far, and is basically formed
Class is more complete, produce and the fairly perfect industrial system of application technology, and species includes modified bituminous pitch coiled material, macromolecule waterproof
The major class product of coiled material, water-repellent paint, encapsulant, loss circulation material and rigidity water-proofing material etc. five.
Polymer cement waterproof paint be develop in recent years a kind of it is nontoxic, can wet trade, easy construction it is new
Environmental protection waterproof material, it is the bi-component water-repellent paint based on aqueous polymer dispersions and cement, and two components are existing
Field stirs into uniform, fine and smooth slurry, brushes or is sprayed at matrix surface, flexible, high-strength waterproof coating can be formed after solidification.
This existing cementitious materials intensity of coating is high, easily bonded with moisture substrate, has the elastic big, waterproof of polymer coating film concurrently again
Property good advantage, especially using water as carrier, overcome the disadvantage that pitch, tar, organic solvent type waterproof material pollute environment
End.It is applicable not only to various waterproofing works, it may also be used for repairing work, interface processing, concrete protection, decoration, structure are close
Envelope etc..Just because of this, this material since the advent of the world, that is, obtained fast development and extensive use.But its heat-proof combustion-resistant energy
Power is not enough, and service life is shorter.
In Publication No. CN1386809A patent document, a kind of organic-inorganic composite waterproofing paint is disclosed, by liquid
Material and powder composition, its coordination in works is liquid material: powder: water=10: 15: 0-2.The percentage by weight of wherein liquid material is：Methyl
Methyl acrylate 1-10, styrene 1-10, butyl acrylate 1-20, acrylic acid 0.1-1, ammonium persulfate 0.1-1, sodium acid carbonate
0.1-1, crosslinking agent 0.1-0.5, anion emulsifier 0.1-0.5, nonionic emulsifier 0.3-1, softening agent 0.1-1, deionization
Water 20-30, organic siliconresin 0.1-1, acrylate copolymer 20-70；The percentage by weight of powder is：Portland cement 50-
80, powder defoamer 0.05-1, dispersant 0.05-1, waterproofing agent 0.5-2, quartz sand 20-48.The invention uses rear cohesive force
By force, seamless, good integrity, permeable watertight, not hollowing, freeze thawing resistance, high temperature resistant, it is corrosion-resistant, it is cold construction, can wet trade, apply
Work is easy, nontoxic, environmental protection the advantages of；But the heat-proof combustion-resistant scarce capacity of the invention.
The content of the invention
It is an object of the invention to overcoming above-mentioned the deficiencies in the prior art there is provided a kind of heat-proof combustion-resistant water-repellent paint and its
Preparation method, prepares simple, and adhesive ability is strong, and environmental pollution is small, and good water-proof effect, service life is long, with excellent heat-resisting
Fire retardancy.
A kind of heat-proof combustion-resistant water-repellent paint that the present invention is provided, includes the raw material of following parts by weight：
38-44 parts of silicone acrylic emulsion, 17-21 parts of vinyl chloride-vinylidene chloride copolymer, 15-19 parts of silica flour, poly- NDA
8-10 parts of second diester, 9-11 parts of organosilicon hydrophobic powder, 8-10 parts of portland cement, 6-8 parts of alundum (Al2O3), epoxy acetylricinoleate
6-8 parts of methyl oleate, 1-5 parts of alcohol ester 12,2-4 parts of calgon, 1-2 parts of hydroxyethyl cellulose, 1-3 parts of defoamer, subtract
0.5-1.5 parts of aqua, 0.5-1 parts of early strength agent, appropriate amount of water.
Preferably, the solid content of silicone acrylic emulsion is 46%, viscosity 650mPas；Portland cement is No. 42.5 flyash
Portland cement.
Preferably, the mesh number of silica flour is 325 mesh, the mesh number of organosilicon hydrophobic powder is 270 mesh, alundum (Al2O3)
Mesh number is 400 mesh.
Preferably, defoamer is silicone emulsion, the fatty acid ester compounded thing of higher alcohols, polyoxyethylene polyoxypropylene Ji Wusi
Alcohol ether, polyoxyethylene polyoxy propyl alcohol amidogen ether, polypropylene glycerol aether, polyoxyethylene polyoxypropylene glycerin ether, polydimethylsiloxanes
One or two or more kinds of mixtures of alkane.
Preferably, water reducer be lignosulfonates, naphthalene sulfonate water reducer, Amino-sulfonic Acid-based Water-reducer,
Fatty acid series high efficiency water reducing agent, powder polycarboxylate, casein, one or two or more kinds of mixtures of melamine based water reducer.
Preferably, early strength agent is triethanolamine, calcium formate, urea, sodium sulphate, the mixture of calcium chloride, its weight ratio
For 2:3:1:4:2.
Present invention also offers a kind of preparation method of heat-proof combustion-resistant water-repellent paint, comprise the following steps：
（1）, by above-mentioned parts by weight weigh various raw materials；
（2）, by silica flour, poly- NDA second diester, organosilicon hydrophobic powder, portland cement, alundum (Al2O3), six inclined
Sodium phosphate, hydroxyethyl cellulose are added in mixer and stirred；
（3）, by water, silicone acrylic emulsion, vinyl chloride-vinylidene chloride copolymer, epoxidized methyl acetorieinoleate, alcohol ester 12, disappear
Infusion, water reducer, early strength agent are added sequentially in mixer, are stirred while adding, until stirring.
Wherein,
Step（2）、（3）Mixing speed be 400-420r/min.
Step（3）In temperature be 30-40 DEG C.
A kind of heat-proof combustion-resistant water-repellent paint of the present invention and preparation method thereof, is prepared simply, adhesive ability is strong, environmental pollution
Small, good water-proof effect, service life is long, with excellent heat-proof combustion-resistant ability, specifically has the beneficial effect that：
（1）, silicone acrylic emulsion is water-fast, acidproof, alkaline-resisting, dirt-resistant, UV resistant, anti-aging, adhesive ability are strong；Vinyl chloride-inclined chlorine
Ethylene copolymer is also known as chlorine partial emulsion, with preferably fire prevention, moistureproof, mould proof, waterproof, wear-resisting performance；Silicone acrylic emulsion and chlorine
The mixing of ethene-metachloroethylene copolymer is effective to ensure that the various performances of coating；
（2）, silica flour addition both can guarantee that the intensity of coating, the high temperature resistant and abrasive resistance of coating can be improved again；Poly- 2,6-
Polyethylene naphthalate has stronger heat-resisting ability；Organosilicon hydrophobic powder can improve waterproof ability；Portland cement can be carried
The adhesive ability of high coating；
（3）, alundum (Al2O3) can improve fire retardancy, also with moisture absorption ability；Epoxidized methyl acetorieinoleate has plasticising
Ability, improve coating toughness；Alcohol ester 12 is coalescents；Calgon is dispersant；
（4）, hydroxyethyl cellulose has good thickening, suspension, scattered, emulsification, bonding, film forming, protects moisture and offer guarantor
The characteristics such as colloid are protected, the various performances of coating can be effectively improved；Defoamer can prevent bubble, and water reducer can reduce and use water
Amount；Early strength agent can improve the early strength of coating, shorten hardening time；
（5）, various raw materials correspondence ratios of the invention mixing, be effective to ensure that the physical strength of coating, acid and alkali-resistance, attachment,
The performance such as waterproof and heat-resistant fireproof, increases the service life of coating；Preparation method effectively will can be mixed fully between each raw material
Close.
Embodiment
Invention is described in further detail below in conjunction with specific embodiment.
Embodiment 1
A kind of heat-proof combustion-resistant water-repellent paint of the present embodiment, includes the raw material of following parts by weight：
38 parts of silicone acrylic emulsion, 17 parts of vinyl chloride-vinylidene chloride copolymer, 15 parts of silica flour, poly- NDA second diester 8
Part, 9 parts of organosilicon hydrophobic powder, 8 parts of portland cement, 6 parts of alundum (Al2O3), 6 parts of epoxidized methyl acetorieinoleate, alcohol ester ten
21 parts, 2 parts of calgon, 1 part of hydroxyethyl cellulose, 1 part of defoamer, 0.5 part of water reducer, 0.5 part of early strength agent, appropriate amount of water.
In the present embodiment, the solid content of silicone acrylic emulsion is 46%, viscosity 650mPas；Portland cement is No. 42.5 fine coal
Grey portland cement.
In the present embodiment, the mesh number of silica flour is 325 mesh, and the mesh number of organosilicon hydrophobic powder is 270 mesh, alundum (Al2O3)
Mesh number be 400 mesh.
In the present embodiment, defoamer is silicone emulsion, the fatty acid ester compounded thing of higher alcohols, polyoxyethylene polyoxypropylene season penta
Four alcohol ethers, polyoxyethylene polyoxy propyl alcohol amidogen ether, polypropylene glycerol aether, polyoxyethylene polyoxypropylene glycerin ether, poly dimethyl silicon
The mixture of oxygen alkane.
In the present embodiment, water reducer is lignosulfonates, naphthalene sulfonate water reducer, the efficient diminishing of sulfamate system
Agent, fatty acid series high efficiency water reducing agent, powder polycarboxylate, casein, the mixture of melamine based water reducer.
In the present embodiment, early strength agent is triethanolamine, calcium formate, urea, sodium sulphate, the mixture of calcium chloride, its weight
Than for 2:3:1:4:2.
The present embodiment additionally provides a kind of preparation method of heat-proof combustion-resistant water-repellent paint, comprises the following steps：
（1）, by above-mentioned parts by weight weigh various raw materials；
（2）, by silica flour, poly- NDA second diester, organosilicon hydrophobic powder, portland cement, alundum (Al2O3), six inclined
Sodium phosphate, hydroxyethyl cellulose are added in mixer and stirred；
（3）, by water, silicone acrylic emulsion, vinyl chloride-vinylidene chloride copolymer, epoxidized methyl acetorieinoleate, alcohol ester 12, disappear
Infusion, water reducer, early strength agent are added sequentially in mixer, are stirred while adding, until stirring.
Wherein,
Step（2）、（3）Mixing speed be 400r/min.
Step（3）In temperature be 30 DEG C.
Embodiment 2
A kind of heat-proof combustion-resistant water-repellent paint of the present embodiment, includes the raw material of following parts by weight：
41 parts of silicone acrylic emulsion, 19 parts of vinyl chloride-vinylidene chloride copolymer, 17 parts of silica flour, poly- NDA second diester 9
Part, 10 parts of organosilicon hydrophobic powder, 9 parts of portland cement, 7 parts of alundum (Al2O3), 7 parts of epoxidized methyl acetorieinoleate, alcohol ester
12 parts, 3 parts of calgon, 1.5 parts of hydroxyethyl cellulose, 2 parts of defoamer, 1 part of water reducer, 0.8 part of early strength agent, water fit
Amount.
In the present embodiment, the solid content of silicone acrylic emulsion is 46%, viscosity 650mPas；Portland cement is No. 42.5 fine coal
Grey portland cement.
In the present embodiment, the mesh number of silica flour is 325 mesh, and the mesh number of organosilicon hydrophobic powder is 270 mesh, alundum (Al2O3)
Mesh number be 400 mesh.
In the present embodiment, defoamer is silicone emulsion, the fatty acid ester compounded thing of higher alcohols, polyoxyethylene polyoxypropylene season penta
Four alcohol ethers, polyoxyethylene polyoxy propyl alcohol amidogen ether, polypropylene glycerol aether, polyoxyethylene polyoxypropylene glycerin ether, poly dimethyl silicon
The mixture of oxygen alkane.
In the present embodiment, water reducer is lignosulfonates, naphthalene sulfonate water reducer, the efficient diminishing of sulfamate system
Agent, fatty acid series high efficiency water reducing agent, powder polycarboxylate, casein, the mixture of melamine based water reducer.
In the present embodiment, early strength agent is triethanolamine, calcium formate, urea, sodium sulphate, the mixture of calcium chloride, its weight
Than for 2:3:1:4:2.
The present embodiment additionally provides a kind of preparation method of heat-proof combustion-resistant water-repellent paint, comprises the following steps：
（1）, by above-mentioned parts by weight weigh various raw materials；
（2）, by silica flour, poly- NDA second diester, organosilicon hydrophobic powder, portland cement, alundum (Al2O3), six inclined
Sodium phosphate, hydroxyethyl cellulose are added in mixer and stirred；
（3）, by water, silicone acrylic emulsion, vinyl chloride-vinylidene chloride copolymer, epoxidized methyl acetorieinoleate, alcohol ester 12, disappear
Infusion, water reducer, early strength agent are added sequentially in mixer, are stirred while adding, until stirring.
Wherein,
Step（2）、（3）Mixing speed be 410r/min.
Step（3）In temperature be 35 DEG C.
Embodiment 3
A kind of heat-proof combustion-resistant water-repellent paint of the present embodiment, includes the raw material of following parts by weight：
44 parts of silicone acrylic emulsion, 21 parts of vinyl chloride-vinylidene chloride copolymer, 19 parts of silica flour, poly- NDA second diester 10
Part, 11 parts of organosilicon hydrophobic powder, 10 parts of portland cement, 8 parts of alundum (Al2O3), 8 parts of epoxidized methyl acetorieinoleate, alcohol ester
12 parts, 4 parts of calgon, 2 parts of hydroxyethyl cellulose, 3 parts of defoamer, 1.5 parts of water reducer, 1 part of early strength agent, appropriate amount of water.
In the present embodiment, the solid content of silicone acrylic emulsion is 46%, viscosity 650mPas；Portland cement is No. 42.5 fine coal
Grey portland cement.
In the present embodiment, the mesh number of silica flour is 325 mesh, and the mesh number of organosilicon hydrophobic powder is 270 mesh, alundum (Al2O3)
Mesh number be 400 mesh.
In the present embodiment, defoamer is silicone emulsion, the fatty acid ester compounded thing of higher alcohols, polyoxyethylene polyoxypropylene season penta
Four alcohol ethers, polyoxyethylene polyoxy propyl alcohol amidogen ether, polypropylene glycerol aether, polyoxyethylene polyoxypropylene glycerin ether, poly dimethyl silicon
The mixture of oxygen alkane.
In the present embodiment, water reducer is lignosulfonates, naphthalene sulfonate water reducer, the efficient diminishing of sulfamate system
Agent, fatty acid series high efficiency water reducing agent, powder polycarboxylate, casein, the mixture of melamine based water reducer.
In the present embodiment, early strength agent is triethanolamine, calcium formate, urea, sodium sulphate, the mixture of calcium chloride, its weight
Than for 2:3:1:4:2.
The present embodiment additionally provides a kind of preparation method of heat-proof combustion-resistant water-repellent paint, comprises the following steps：
（1）, by above-mentioned parts by weight weigh various raw materials；
（2）, by silica flour, poly- NDA second diester, organosilicon hydrophobic powder, portland cement, alundum (Al2O3), six inclined
Sodium phosphate, hydroxyethyl cellulose are added in mixer and stirred；
（3）, by water, silicone acrylic emulsion, vinyl chloride-vinylidene chloride copolymer, epoxidized methyl acetorieinoleate, alcohol ester 12, disappear
Infusion, water reducer, early strength agent are added sequentially in mixer, are stirred while adding, until stirring.
Wherein,
Step（2）、（3）Mixing speed be 420r/min.
Step（3）In temperature be 40 DEG C.
Described above is only the preferred embodiment of the present invention, and protection scope of the present invention is not limited merely to above-mentioned implementation
Example, all technical schemes belonged under thinking of the present invention belong to protection scope of the present invention.It should be pointed out that for the art
Those of ordinary skill for, some improvements and modifications without departing from the principles of the present invention, these improvements and modifications
It should be regarded as protection scope of the present invention.
Claims (9)
1. a kind of heat-proof combustion-resistant water-repellent paint, it is characterised in that：Include the raw material of following parts by weight：
38-44 parts of silicone acrylic emulsion, 17-21 parts of vinyl chloride-vinylidene chloride copolymer, 15-19 parts of silica flour, poly- NDA
8-10 parts of second diester, 9-11 parts of organosilicon hydrophobic powder, 8-10 parts of portland cement, 6-8 parts of alundum (Al2O3), epoxy acetylricinoleate
6-8 parts of methyl oleate, 1-5 parts of alcohol ester 12,2-4 parts of calgon, 1-2 parts of hydroxyethyl cellulose, 1-3 parts of defoamer, subtract
0.5-1.5 parts of aqua, 0.5-1 parts of early strength agent, appropriate amount of water.
2. heat-proof combustion-resistant water-repellent paint according to claim 1, it is characterised in that：The solid content of silicone acrylic emulsion is 46%, is glued
Spend 650mPas；Portland cement is No. 42.5 Portland fly ash cements.
3. heat-proof combustion-resistant water-repellent paint according to claim 1, it is characterised in that：The mesh number of silica flour is 325 mesh, is had
The mesh number of machine silicon hydrophobic powder is 270 mesh, and the mesh number of alundum (Al2O3) is 400 mesh.
4. heat-proof combustion-resistant water-repellent paint according to claim 1, it is characterised in that：Defoamer is silicone emulsion, higher alcohols
Fatty acid ester compounded thing, polyoxyethylene polyoxypropylene pentaerythrite ether, polyoxyethylene polyoxy propyl alcohol amidogen ether, polyoxypropylene glyceryl
Ether, polyoxyethylene polyoxypropylene glycerin ether, one or two or more kinds of mixtures of dimethyl silicone polymer.
5. heat-proof combustion-resistant water-repellent paint according to claim 1, it is characterised in that：Water reducer is lignosulfonates, naphthalene
It is sulfonate water reducer, Amino-sulfonic Acid-based Water-reducer, fatty acid series high efficiency water reducing agent, powder polycarboxylate, casein, close
One or two or more kinds of mixtures of amine system water reducer.
6. heat-proof combustion-resistant water-repellent paint according to claim 1, it is characterised in that：Early strength agent be triethanolamine, calcium formate,
Urea, sodium sulphate, the mixture of calcium chloride, its weight ratio are 2:3:1:4:2.
7. a kind of preparation method of heat-proof combustion-resistant water-repellent paint according to claim 1-6 any one, it is characterised in that：
Comprise the following steps：
（1）, by above-mentioned parts by weight weigh various raw materials；
（2）, by silica flour, poly- NDA second diester, organosilicon hydrophobic powder, portland cement, alundum (Al2O3), six inclined
Sodium phosphate, hydroxyethyl cellulose are added in mixer and stirred；
（3）, by water, silicone acrylic emulsion, vinyl chloride-vinylidene chloride copolymer, epoxidized methyl acetorieinoleate, alcohol ester 12, disappear
Infusion, water reducer, early strength agent are added sequentially in mixer, are stirred while adding, until stirring.
8. the preparation method of heat-proof combustion-resistant water-repellent paint according to claim 7, it is characterised in that：Step（2）、（3）'s
Mixing speed is 400-420r/min.
9. the preparation method of heat-proof combustion-resistant water-repellent paint according to claim 7, it is characterised in that：Step（3）In temperature
Spend for 30-40 DEG C.
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| CN115572497A (en) * | 2022-10-13 | 2023-01-06 | 远大洪雨（唐山）防水材料有限公司 | High-water-resistance polymer cement waterproof coating and preparation method thereof |
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