CN107158575A - A kind of quick patch of infrared nose and preparation method thereof - Google Patents
A kind of quick patch of infrared nose and preparation method thereof Download PDFInfo
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- CN107158575A CN107158575A CN201710440118.XA CN201710440118A CN107158575A CN 107158575 A CN107158575 A CN 107158575A CN 201710440118 A CN201710440118 A CN 201710440118A CN 107158575 A CN107158575 A CN 107158575A
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61N—ELECTROTHERAPY; MAGNETOTHERAPY; RADIATION THERAPY; ULTRASOUND THERAPY
- A61N5/00—Radiation therapy
- A61N5/06—Radiation therapy using light
- A61N5/0613—Apparatus adapted for a specific treatment
- A61N5/0625—Warming the body, e.g. hyperthermia treatment
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61H—PHYSICAL THERAPY APPARATUS, e.g. DEVICES FOR LOCATING OR STIMULATING REFLEX POINTS IN THE BODY; ARTIFICIAL RESPIRATION; MASSAGE; BATHING DEVICES FOR SPECIAL THERAPEUTIC OR HYGIENIC PURPOSES OR SPECIFIC PARTS OF THE BODY
- A61H39/00—Devices for locating or stimulating specific reflex points of the body for physical therapy, e.g. acupuncture
- A61H39/06—Devices for heating or cooling such points within cell-life limits
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61N—ELECTROTHERAPY; MAGNETOTHERAPY; RADIATION THERAPY; ULTRASOUND THERAPY
- A61N2/00—Magnetotherapy
- A61N2/002—Magnetotherapy in combination with another treatment
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61H—PHYSICAL THERAPY APPARATUS, e.g. DEVICES FOR LOCATING OR STIMULATING REFLEX POINTS IN THE BODY; ARTIFICIAL RESPIRATION; MASSAGE; BATHING DEVICES FOR SPECIAL THERAPEUTIC OR HYGIENIC PURPOSES OR SPECIFIC PARTS OF THE BODY
- A61H2201/00—Characteristics of apparatus not provided for in the preceding codes
- A61H2201/02—Characteristics of apparatus not provided for in the preceding codes heated or cooled
- A61H2201/0207—Characteristics of apparatus not provided for in the preceding codes heated or cooled heated
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61N—ELECTROTHERAPY; MAGNETOTHERAPY; RADIATION THERAPY; ULTRASOUND THERAPY
- A61N5/00—Radiation therapy
- A61N5/06—Radiation therapy using light
- A61N2005/0635—Radiation therapy using light characterised by the body area to be irradiated
- A61N2005/0643—Applicators, probes irradiating specific body areas in close proximity
- A61N2005/0645—Applicators worn by the patient
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61N—ELECTROTHERAPY; MAGNETOTHERAPY; RADIATION THERAPY; ULTRASOUND THERAPY
- A61N5/00—Radiation therapy
- A61N5/06—Radiation therapy using light
- A61N2005/0658—Radiation therapy using light characterised by the wavelength of light used
- A61N2005/0659—Radiation therapy using light characterised by the wavelength of light used infrared
- A61N2005/066—Radiation therapy using light characterised by the wavelength of light used infrared far infrared
Landscapes
- Health & Medical Sciences (AREA)
- Public Health (AREA)
- Engineering & Computer Science (AREA)
- Biomedical Technology (AREA)
- Veterinary Medicine (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Radiology & Medical Imaging (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Rehabilitation Therapy (AREA)
- Epidemiology (AREA)
- Pain & Pain Management (AREA)
- Physical Education & Sports Medicine (AREA)
- Pathology (AREA)
- Radiation-Therapy Devices (AREA)
- Medicinal Preparation (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
Abstract
The invention belongs to biomedicine technical field, it is related to quick patch of a kind of infrared nose and preparation method thereof.The quick patch of infrared nose that the present invention is provided is made up of lid lining material, far-infrared magnet therapeutic matrix and back lining materials, far-infrared magnet therapeutic matrix is located between lid lining material and back lining materials, wherein, far-infrared magnet therapeutic matrix includes the components such as far-infrared material, medical pressure sensitive adhesive and transdermal enhancer.The quick patch of infrared nose that the present invention is provided is free of drug ingedient, only plays therapeutic action by physical property, available for allergic rhinitis, the auxiliary treatment of acute or chronic rhinitis, effect is notable.The quick patch far-infrared material of infrared nose that the present invention is provided need not be heated with regard to that can produce far infrared, and non-stimulated to skin, it is easy to peel off, and uses comfortable, no lotion Seepage.
Description
Technical field
The invention belongs to biomedicine technical field, more particularly to a kind of quick patch of infrared nose and preparation method thereof.
Background technology
Far infrared refers to the electromagnetic wave that wave-length coverage is 4~400 μm.The far infrared wavelength that human body is launched is at 9.6 μm
Left and right, the infrared ray that wave-length coverage is sent by 8~14 μm of far infrared and human body is in the same band scope, easily by human body
Absorb.Because frequency and the molecule of human body living cells, the intraatomic vibration ratio of far infrared are identical, so far infrared quilt
Aggravate the molecular vibration of intraor extracellular after absorption of human body, produce fuel factor, with the growth change for accelerating human body, promote capillary
Blood vessel dilatation, blood flow is accelerated, and improves blood circulation, mitigates pain, increases of flaccid muscles, acceleration metabolism, improves body and exempt from
The effect of epidemic disease power.
Far-infrared material is the material for referring to produce far infrared, at present, and the material for commonly using generation far infrared is main
Including charcoal, tourmaline, far-infrared ceramic, jade, metal oxide and carborundum.But these materials, it is upper in application
In the presence of certain limitation and drawback, such as charcoal, which needs to be powered or heated, could produce far infrared；Tourmaline, far-infrared ceramic
Because, as raw material, ore constituent differs using natural crystal, the release performance of the far infrared of different product is caused to exist
Fluctuation；Jade source is few, expensive；Metal oxide and carborundum can just send far infrared in temperature higher than 150 DEG C.
Emplastrum refers to material medicine and suitable matrix paste is made, is coated on back lining materials for skin paste
Apply, a kind of systemic or local action laminar preparation can be produced.Far-infrared material is applied in emplastrum, can promote medicine
The quick absorption of thing, improves the utilization rate of medicine, reaches the beneficial effect that drug therapy is combined with physical treatment.The general love in Hubei
Far infrared cough relieving paste (the authentication code of pharmaceutcal corporation, Ltd's production：Hubei Province food medicine prison tool (standard) word 2010 the 2261455th), by day
The compositions such as right Chinese herbal medicine extract, far-infared ceramic powder and medical pressure sensitive adhesive are made, the work relievingd asthma with preventing phlegm from forming and stopping coughing, qi-regulating
With, it is adaptable to the disease such as cough caused by acute/chronic bronchitis, flu.Chinese patent application CN 1709336A disclose one kind
Infrared nasitis plaster and preparation method, the effective component of chinese medicine being made up of Chinese medicine materials such as semen brassicae, the roots of gansui, far-infared ceramic powder,
Skin penetration enhancer and rubber cement etc. are constituted, and have therapeutic action to allergic rhinitis, acute and chronic rhinitis etc..
The emplastrum of existing application far-infrared material, equal drug containing composition, and the main composition for playing therapeutic action is also medicine
Thing composition.In addition, the emplastrum stickiness of existing application far-infrared material is larger, relative difficulty is peeled off, and it is existing to there is lotion seepage
As.
The content of the invention
To solve problems of the prior art, the invention provides a kind of quick patch of infrared nose, by lid lining material, far red
Outer magnetic therapy matrix and back lining materials composition, far-infrared magnet therapeutic matrix are located between lid lining material and back lining materials, its mid and far infrared
Magnetic therapy matrix includes the components such as far-infrared material, medical pressure sensitive adhesive and transdermal enhancer.The quick patch of infrared nose that the present invention is provided is not
Drug containing composition, only plays therapeutic action by physical property, is controlled according to China's medical science inner disease outer treat theory and channels and collaterals conduction acupuncture point
Principle is treated, with reference to the effect of the physical factors such as far infrared, a kind of external use plaster being developed into.The quick patch of infrared nose that the present invention is provided
Far-infrared material need not be heated with regard to that can produce far infrared, non-stimulated to skin, and it is easy to peel off, no lotion Seepage.
Technical scheme will be further described in detail below reflect and description.
A kind of quick patch of infrared nose, is made up of, far-infrared magnet therapeutic matrix lid lining material, far-infrared magnet therapeutic matrix and back lining materials
Between lid lining material and back lining materials, the lid lining material is preferred to use release liners, and the back lining materials are preferred to use nothing
Cloth is spun, the far-infrared magnet therapeutic matrix is counted by weight, including following component：3~10 parts of far-infrared material, medical pressure-sensing
0.1~1 part of 40~60 parts of glue and transdermal enhancer；
Wherein, the preparation method of the far-infrared material comprises the following steps：
S1, take Tourmaline stone, medical stone, modification biological charcoal, aluminum oxide, carborundum, titanium carbide, calcium carbonate, cerium oxide and
Titanium dioxide, is respectively prepared powder, mixes, obtains mixture I；
S2, zirconium silicate, sodium metasilicate, tetraethyl orthosilicate are taken, added water, after stirring and evenly mixing together with mixture I described in step S1
Add in ball grinder, 48~72h of ball milling mixing obtains mixtures II；
S3, by mixtures II pressure be 30~60MPa under conditions of carry out high-pressure molding, then under the protection of nitrogen
It is sintered, sintering temperature is 1100~1300 DEG C, the sintered heat insulating time is 0.5~2h；
After S4, Temperature fall, crush, produce far-infrared material.
Further, the far-infrared material, is counted by weight, is made up of following component：3~8 parts of Tourmaline stone, wheat
5~12 parts of meal stone, 1~3 part of zirconium silicate, 8~15 parts of sodium metasilicate, 5~10 parts of tetraethyl orthosilicate, 20~30 parts of modification biological charcoal,
3~5 parts of aluminum oxide, 1~3 part of carborundum, 0.5~2 part of titanium carbide, 5~15 parts of calcium carbonate, 0.1~0.8 part of cerium oxide, dioxy
Change 50~70 parts of 2~5 parts of titanium and water.
Further, the far-infrared material, is counted by weight, is made up of following component：6 parts of Tourmaline stone, wheat meal
10 parts of stone, 2 parts of zirconium silicate, 10 parts of sodium metasilicate, 7 parts of tetraethyl orthosilicate, 25 parts of modification biological charcoal, 3 parts of aluminum oxide, 2 parts of carborundum,
60 parts of 1 part of titanium carbide, 15 parts of calcium carbonate, 0.5 part of cerium oxide, 3 parts of titanium dioxide and water.
Further, the preparation method of the modification biological charcoal comprises the following steps：
(1) bamboo powder, camphorwood dust, mulberry tree wood chip and wild jujube wood chip are taken, by solid-to-liquid ratio 1：8~12g/mL add pH value be 9~
10 sodium hydroxide solution, soaks 10~15h, and filtering is carbonized after retaining filtrate, filter residue and drying under the protection of nitrogen, with
2 DEG C/min~5 DEG C/min programming rate is warming up to 500~700 DEG C, is incubated after 2~6h, Temperature fall, crushes, obtains biological
Charcoal；
(2) step (1) described charcoal is pressed into solid-to-liquid ratio 1:6~10g/mL adds the mixed solution of iron chloride and zinc chloride
In, 1~2h of ultrasonic immersing under conditions of temperature is 40~60 DEG C, addition step (1) described filtrate, ultrasound mixing 20~
30min, filtering, filter residue and drying is crushed, produces modification biological charcoal.
Further, in the preparation method of the modification biological charcoal, step (1), by weight, bamboo powder：Camphorwood dust：Mulberry
Trees are considered to be worth doing：Wild jujube wood chip is 20~30：5~15：10~20：1；In the mixed solution of step (2) iron chloride and zinc chloride,
Fe3+ concentration is 0.1~0.2mol/L, and Zn2+ concentration is 0.08~0.15mol/L.
Further, in the preparation method of the modification biological charcoal, step (2), ultrasonic power is 120~150W.
Further, the one kind or many of the transdermal enhancer in peppermint oil, caryophyllus oil, eucalyptus oil and propane diols
Kind.
Further, also containing 1~4 part of isopropyl palmitate, 1~5 part of rosin and recessed in the far-infrared magnet therapeutic matrix
Convex 3~8 parts of rod soil.
Correspondingly, the present invention also provides a kind of preparation method of the quick patch of infrared nose, comprises the following steps：
I, take that particle size is ground to form after far-infrared material, rosin and attapulgite, mixing is 2~10 μm of powder, obtain
Mixed material；
II, medical pressure sensitive adhesive is heated to after 80~150 DEG C, complete colloidal sol, adds mixed material and palm described in step I
Isopropyl propionate, keeping temperature is constant, stirs 1~2h, and Temperature fall when temperature is down to 40~60 DEG C, adds transdermal enhancer, after
15~30min of continuous stirring, is coated on back lining materials, covers lid lining material, cuts into slices, and detects, packaging is produced.
The quick patch main performance index of infrared nose that the present invention is provided is as follows：
1) infrared normal direction total emissivity >=0.85 of the emplastrum in 4 μm~16 μ m wavelength ranges；
2) peel strength >=1.0N/cm of back lining materials；
3) initial cohesiveness of far-infrared magnet therapeutic matrix clings No. 3 steel balls and stopped more than 5 seconds；
4) the surface coating of far-infrared magnet therapeutic matrix is uniform, and bright and clean, color and luster is consistent, without de- cream, loses glutinous phenomenon.
The main far infrared effect on human body cave by giving off 4 μm~16 mum wavelengths of the quick patch of infrared nose that the present invention is provided
Position, is transmitted through human body to the stimulation of " RESONANCE ABSORPTION " and magnetic field energy of the far infrared, so that active cell tissue, increase office
Portion's CBF, improves blood circulation, metabolism is improved, to reach the purpose of auxiliary treatment nasal allergy and health care.
The application method for the quick patch of infrared nose that the present invention is provided is：Take off and abandon lid lining material, cleaning skin, stick on Tiantu,
Big vertebra, fei shu, air door, connected valleys, Pishu and bl acupuncture point；Slight person can only paste two acupuncture points of fei shu or big vertebra.Children paste daily
Once, each 2-4 pieces, every time patch 4-6 hours, it is one-year-old within children cut down according to the circumstance the time.Adult pastes once daily, each 2-6 pieces, often
Secondary patch 4-8 hours, skin sensitivity person is cut down according to the circumstance the time.
The quick patch of infrared nose that the present invention is provided can be used for allergic rhinitis, the auxiliary treatment of acute or chronic rhinitis, it can also be used to
" three fit perfectly " for the treatment of winter disease in summer and " three nine-day periods after the winter solstice patch " of winter sick protection in winter：The first fu of the annual lunar calendar " dog days ", second of the three ten-day periods of the hot season, dog days；Every year
The lunar calendar " coldest days of winter " one or nine, two or nine, three nine-day periods after the winter solstice；It is attached to big vertebra, feishu, at Tiantu, often fits perfectly 1-3 time, each 4-8 hours left side
The right side, or follow the doctor's advice.
Compared with prior art, the beneficial effects of the present invention are：
(1) the quick patch of far infrared nose that the present invention is provided is free of drug ingedient, only plays therapeutic action by physical property, can be used for
Auxiliary treatment allergic rhinitis, acute or chronic rhinitis, effect are notable；
(2) the quick patch of far infrared nose that the present invention is provided need not be heated with regard to that can produce far infrared, non-stimulated to skin, stripping
From easy, using comfortable, without lotion Seepage during sticking.
Embodiment
Below by specific embodiment, the present invention is described in further detail.
Material used in the embodiment of the present invention, is the material commercially obtained unless otherwise specified.Such as
Medical pressure sensitive adhesive is purchased from Dongguan into inscription adhesive Co., Ltd.
Wood chip described in modification biological charcoal preparing raw material of the present invention is sawdust, the wood shavings powder left when wood is processed, or
The wood powder that timber polishing is ground into.
The preparation of the modification biological charcoal of embodiment 1
(1) bamboo powder is pressed：Camphorwood dust：Mulberry tree wood chip：Wild jujube wood chip is 20：8：12：1 weight ratio, take bamboo powder, camphorwood dust,
Mulberry tree wood chip and wild jujube wood chip, by solid-to-liquid ratio 1：10g/mL adds the sodium hydroxide solution that pH value is 9, soaks 12h, and filtering retains
Carbonized after filtrate, filter residue and drying under the protection of nitrogen, 550 DEG C be warming up to 3 DEG C/min programming rate, be incubated 6h,
After Temperature fall, crush, obtain charcoal；
(2) step (1) described charcoal is pressed into solid-to-liquid ratio 1:6g/mL adds Fe3+Concentration be 0.2mol/L, Zn2+It is dense
Spend in 0.12mol/L iron chloride and the mixed solution of zinc chloride, the ultrasonic immersing 2h under conditions of temperature is 45 DEG C is added
Step (1) described filtrate, ultrasound mixes 20min, and filtering, filter residue and drying is crushed, produces modification biological charcoal, wherein, ultrasonic power
For 120W.
The preparation of the modification biological charcoal of embodiment 2
(1) bamboo powder is pressed：Camphorwood dust：Mulberry tree wood chip：Wild jujube wood chip is 25：10：15：1 weight ratio, take bamboo powder, camphorwood dust,
Mulberry tree wood chip and wild jujube wood chip, by solid-to-liquid ratio 1：12g/mL adds the sodium hydroxide solution that pH value is 10, soaks 10h, and filtering is protected
Carbonized after reserved filtrate, filter residue and drying under the protection of nitrogen, 650 DEG C, insulation are warming up to 4 DEG C/min programming rate
After 5h, Temperature fall, crush, obtain charcoal；
(2) step (1) described charcoal is pressed into solid-to-liquid ratio 1:8g/mL adds Fe3+Concentration be 0.15mol/L, Zn2+'s
Concentration for 0.10mol/L iron chloride and zinc chloride mixed solution in, temperature be 50 DEG C under conditions of ultrasonic immersing 1.5h,
Step (1) described filtrate is added, ultrasound mixes 25min, and filtering, filter residue and drying is crushed, produces modification biological charcoal, wherein, ultrasound
Power is 150W.
The preparation of the modification biological charcoal of embodiment 3
Embodiment 3 and the difference of the modification biological charcoal of embodiment 2 are that preparing raw material is free of camphorwood dust.
The preparation of the far-infrared material of embodiment 4~10
Formula：Count, be made up of following component by weight：
Preparation method：
S1, take Tourmaline stone, medical stone, modification biological charcoal, aluminum oxide, carborundum, titanium carbide, calcium carbonate, cerium oxide and
Titanium dioxide, is respectively prepared powder, mixes, obtains mixture I；
S2, zirconium silicate, sodium metasilicate, tetraethyl orthosilicate are taken, added water, after stirring and evenly mixing together with mixture I described in step S1
Add in ball grinder, ball milling mixing 60h obtains mixtures II；
S3, by mixtures II pressure be 50MPa under conditions of carry out high-pressure molding, then under the protection of nitrogen carry out
Sintering, sintering temperature is 1200 DEG C, and the sintered heat insulating time is 1.5h；
After S4, Temperature fall, crush, produce far-infrared material.
The preparation of the quick patch of infrared nose of embodiment 11~15
Far-infrared magnet therapeutic matrix formulations：Count, be made up of following component by weight：
Preparation method：
I, take that particle size is ground to form after far-infrared material, rosin and attapulgite, mixing is 2~10 μm of powder, obtain
Mixed material；
II, medical pressure sensitive adhesive is heated to after 120 DEG C, complete colloidal sol, adds mixed material and palmitic acid described in step I different
Propyl ester, keeping temperature is constant, stirs 2h, and Temperature fall when temperature is down to 50 DEG C, adds transdermal enhancer, continues to stir
30min, is coated on back lining materials, covers lid lining material, cuts into slices, and detects, packaging is produced.
The quick patch of the infrared nose of comparative example 1
Compared with embodiment 13, the comparative example 1 quick patch of infrared nose is differed only in：The far-infrared material is embodiment 7
Obtained far-infrared material.
The quick patch of the infrared nose of comparative example 2
Compared with embodiment 13, the quick patch of the infrared nose of comparative example 2 is differed only in：The far-infrared material is that embodiment 8 is made
The far-infrared material obtained.
The quick patch of the infrared nose of comparative example 3
Compared with embodiment 13, the quick patch of the infrared nose of comparative example 3 is differed only in：The far-infrared material is that embodiment 9 is made
The far-infrared material obtained.
The quick patch of the infrared nose of comparative example 4
Compared with embodiment 13, the quick patch of the infrared nose of comparative example 4 is differed only in：The far-infrared material is that embodiment 10 is made
The far-infrared material obtained.
The quick patch of the infrared nose of comparative example 5
Compared with embodiment 13, the quick patch of the infrared nose of comparative example 5 is differed only in：The far-infrared material is commercially available far infrared
Material, is purchased from that Wuhan is auspicious to inspire confidence in because of development in science and technology Co., Ltd.
The quick patch of the infrared nose of comparative example 6
Compared with embodiment 13, the quick patch of the infrared nose of comparative example 6 is differed only in：Without rosin.
The quick patch of the infrared nose of comparative example 7
Compared with embodiment 13, the quick patch of the infrared nose of comparative example 7 is differed only in：Without attapulgite.
The quick patch performance test of test example one, infrared nose
1st, test specimen：The quick patch of infrared nose made from embodiment 11~15, comparative example 1~7.
2nd, method of testing：
Normal direction total emissivity is detected：The quick patch of infrared nose is taken, uncapping lining material is detected with far infrared detector.
Plastic property is tested：According to version in 2015《Chinese Pharmacopoeia》Plastic property method of testing is entered in 4th 0122 emplastrum
OK.
Hold viscous force and peel strength test：According to version in 2015《Chinese Pharmacopoeia》Stick phase in a determination method for 4th 0952
Pass method is carried out.
3rd, result of the test：It is shown in Table 1.
As seen from the experiment, quick a length of 4 μm~16 μm of the far infrared wave of patch of infrared nose that the present invention is provided, normal direction full transmitting
Rate >=0.85, stickiness is moderate, and it is easy to peel off, and cream face is without trickling phenomenon, using being not in that matrix residual is existing on skin when peeling off
As using comfortable.
In the preparation process of the results showed that far-infrared material of comparative example, tetraethyl orthosilicate, modification biological charcoal and
The addition of cerium oxide, is conducive to improving the normal direction total emissivity of finished product；And only add palmitic acid in far-infrared magnet therapeutic matrix
Isopropyl ester and rosin, although can reduce the peel strength of the quick patch of infrared nose, are conducive to improving the plasticity of the quick patch of infrared nose, improve
The affinity of the infrared quick patch of nose, but be easily caused lotion and Seepage occur；Only add isopropyl palmitate and attapulgite then
The quick patch of infrared nose can be caused holds viscous force variation.
Test example two, effete test embodiment
1st, test specimen：Embodiment 11, embodiment 13, embodiment 15, the quick patch of infrared nose made from comparative example 1~5.
2nd, test method：240, which are filtered out, by allergic rhinitis, the diagnostic criteria of acute or chronic rhinitis meets diagnostic criteria
Clinical volunteers patient, wherein Allergic Rhinitis 86, acute rhinitis patient 56, rhinitis chronic patient 98 press
Kinds of Diseases are randomly divided into 8 groups, every group each 30.Each group uses embodiment 11, embodiment 13, embodiment 15, comparative example 1 respectively
The infrared quick exchange premium row treatment of nose made from~5.Curative effect is evaluated after one month.
3rd, curative effect determinate standard：
Cure：Clinical symptoms are wholly absent；
It is effective：Most of symptom disappears, and attack degree substantially mitigates, and duration of seizure and number of times are significantly reduced；
Effectively：Partial symptoms are clearly better earlier above, and attack degree mitigates, and duration of seizure and number of times are reduced earlier above；
It is invalid：Symptom is without significant change.
4th, result of the test：It is shown in Table 2.
| Group | Cure | It is effective | Effectively | It is invalid | Total effective rate |
| Embodiment 11 | 6 | 8 | 12 | 4 | 86.67% |
| Embodiment 13 | 8 | 10 | 10 | 2 | 93.33% |
| Embodiment 15 | 5 | 10 | 12 | 3 | 90% |
| Comparative example 1 | 3 | 7 | 14 | 6 | 80% |
| Comparative example 2 | 4 | 5 | 14 | 7 | 76.67% |
| Comparative example 3 | 2 | 9 | 11 | 8 | 73.337% |
| Comparative example 4 | 2 | 5 | 15 | 8 | 73.337% |
| Comparative example 5 | 1 | 3 | 17 | 9 | 70% |
As seen from the experiment, the quick patch of the infrared nose that provides of the present invention available for allergic rhinitis, acute or chronic rhinitis it is auxiliary
Treatment is helped, effect is notable.Process of the test does not find allergic case, and feedback, the quick patch of infrared nose of the invention are used through volunteer
Plasticity is preferably, more easily peelable without dermal sensation is pullled when movable, is remained in after stripping without lotion on skin, illustrates that the present invention is red
The quick patch of external nose is without skin irritation and anaphylaxis, using comfortable, using process without lotion Seepage.
Above content is to combine specific preferred embodiment further description made for the present invention, it is impossible to assert
The specific implementation of the present invention is confined to these explanations.For general technical staff of the technical field of the invention,
On the premise of not departing from present inventive concept, some simple deduction or replace can also be made, should all be considered as belonging to the present invention's
Protection domain.
Claims (10)
1. a kind of quick patch of infrared nose, is made up of, far-infrared magnet therapeutic matrix is set lid lining material, far-infrared magnet therapeutic matrix and back lining materials
Between lid lining material and back lining materials, it is characterised in that the far-infrared magnet therapeutic matrix, count by weight, including it is as follows
Component：0.1~1 part of 3~10 parts of far-infrared material, 40~60 parts of medical pressure sensitive adhesive and transdermal enhancer；
Wherein, the preparation method of the far-infrared material comprises the following steps：
S1, take Tourmaline stone, medical stone, modification biological charcoal, aluminum oxide, carborundum, titanium carbide, calcium carbonate, cerium oxide and dioxy
Change titanium, powder is respectively prepared, mix, obtain mixture I；
S2, zirconium silicate, sodium metasilicate, tetraethyl orthosilicate are taken, add water, added after stirring and evenly mixing together with mixture I described in step S1
In ball grinder, 48~72h of ball milling mixing obtains mixtures II；
S3, by mixtures II pressure be 30~60MPa under conditions of carry out high-pressure molding, then under the protection of nitrogen carry out
Sintering, sintering temperature is 1100~1300 DEG C, and the sintered heat insulating time is 0.5~2h；
After S4, Temperature fall, crush, produce far-infrared material.
2. the quick patch of infrared nose according to claim 1, it is characterised in that the far-infrared material, is counted by weight, by
Following component composition：3~8 parts of Tourmaline stone, 5~12 parts of medical stone, 1~3 part of zirconium silicate, 8~15 parts of sodium metasilicate, positive silicic acid second
5~10 parts of ester, 20~30 parts of modification biological charcoal, 3~5 parts of aluminum oxide, 1~3 part of carborundum, 0.5~2 part of titanium carbide, calcium carbonate 5
50~70 parts of~15 parts, 0.1~0.8 part of cerium oxide, 2~5 parts of titanium dioxide and water.
3. the quick patch of infrared nose according to claim 2, it is characterised in that the far-infrared material, is counted by weight, by
Following component composition：6 parts of Tourmaline stone, 10 parts of medical stone, 2 parts of zirconium silicate, 10 parts of sodium metasilicate, 7 parts of tetraethyl orthosilicate, modified life
25 parts of thing charcoal, 3 parts of aluminum oxide, 2 parts of carborundum, 1 part of titanium carbide, 15 parts of calcium carbonate, 0.5 part of cerium oxide, 3 parts of titanium dioxide and water
60 parts.
4. the quick patch of infrared nose according to claim 1, it is characterised in that the preparation method of the modification biological charcoal is included such as
Lower step：
(1) bamboo powder, camphorwood dust, mulberry tree wood chip and wild jujube wood chip are taken, by solid-to-liquid ratio 1：It is 9~10 that 8~12g/mL, which adds pH value,
Sodium hydroxide solution, soaks 10~15h, and filtering retains filtrate, is carbonized under the protection of nitrogen after filter residue and drying, with 2 DEG C/
Min~5 DEG C/min programming rate is warming up to 500~700 DEG C, is incubated after 2~6h, Temperature fall, crushes, obtains charcoal；
(2) step (1) described charcoal is pressed into solid-to-liquid ratio 1:6~10g/mL is added in the mixed solution of iron chloride and zinc chloride,
1~2h of ultrasonic immersing under conditions of temperature is 40~60 DEG C, adds step (1) described filtrate, and ultrasound mixes 20~30min,
Filtering, filter residue and drying is crushed, produces modification biological charcoal.
5. the quick patch of infrared nose according to claim 4, it is characterised in that the preparation method of the modification biological charcoal, step
(1) in, by weight, bamboo powder：Camphorwood dust：Mulberry tree wood chip：Wild jujube wood chip is 20~30：5~15：10~20：1；Step (2)
In the mixed solution of the iron chloride and zinc chloride, Fe3+Concentration be 0.1~0.2mol/L, Zn2+Concentration for 0.08~
0.15mol/L。
6. the quick patch of infrared nose according to claim 4, it is characterised in that the preparation method of the modification biological charcoal, step
(2) in, ultrasonic power is 120~150W.
7. the quick patch of infrared nose according to claim 1, it is characterised in that the transdermal enhancer is selected from peppermint oil, cloves
One or more in oil, eucalyptus oil and propane diols.
8. the quick patch of infrared nose according to claim 1, it is characterised in that the lid lining material is release liners；The backing
Material is non-woven fabrics.
9. the quick patch of infrared nose according to claim 1, it is characterised in that also contain palm in the far-infrared magnet therapeutic matrix
3~8 parts of 1~4 part of isopropyl propionate, 1~5 part of rosin and attapulgite.
10. a kind of preparation method of the infrared quick patch of nose according to claim 9, it is characterised in that the preparation method bag
Include following steps：
I, take that particle size is ground to form after far-infrared material, rosin and attapulgite, mixing is 2~10 μm of powder, must mix
Material；
II, medical pressure sensitive adhesive is heated to after 80~150 DEG C, complete colloidal sol, adds mixed material and palmitic acid described in step I different
Propyl ester, keeping temperature is constant, stirs 1~2h, and Temperature fall when temperature is down to 40~60 DEG C, adds transdermal enhancer, continues to stir
15~30min is mixed, back lining materials are coated on, lid lining material is covered, cut into slices, is detected, packaging is produced.
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