CN107098417A - A kind of processing unit and technique of oil plant oil-polluted water - Google Patents

A kind of processing unit and technique of oil plant oil-polluted water Download PDF

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Publication number
CN107098417A
CN107098417A CN201710305201.6A CN201710305201A CN107098417A CN 107098417 A CN107098417 A CN 107098417A CN 201710305201 A CN201710305201 A CN 201710305201A CN 107098417 A CN107098417 A CN 107098417A
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CN
China
Prior art keywords
oil
vapour
falling film
polluted water
film evaporator
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710305201.6A
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Chinese (zh)
Inventor
龚卫星
黄炜
毛炜
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanghai Light Energy Ltd By Share Ltd
Original Assignee
Shanghai Light Energy Ltd By Share Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shanghai Light Energy Ltd By Share Ltd filed Critical Shanghai Light Energy Ltd By Share Ltd
Priority to CN201710305201.6A priority Critical patent/CN107098417A/en
Publication of CN107098417A publication Critical patent/CN107098417A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/02Treatment of water, waste water, or sewage by heating
    • C02F1/04Treatment of water, waste water, or sewage by heating by distillation or evaporation
    • C02F1/048Purification of waste water by evaporation
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/02Treatment of water, waste water, or sewage by heating
    • C02F1/04Treatment of water, waste water, or sewage by heating by distillation or evaporation
    • C02F1/043Details
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/02Treatment of water, waste water, or sewage by heating
    • C02F1/04Treatment of water, waste water, or sewage by heating by distillation or evaporation
    • C02F1/08Thin film evaporation
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F11/00Treatment of sludge; Devices therefor
    • C02F11/12Treatment of sludge; Devices therefor by de-watering, drying or thickening
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2101/00Nature of the contaminant
    • C02F2101/30Organic compounds
    • C02F2101/32Hydrocarbons, e.g. oil
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2103/00Nature of the water, waste water, sewage or sludge to be treated
    • C02F2103/34Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32
    • C02F2103/36Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32 from the manufacture of organic compounds
    • C02F2103/365Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32 from the manufacture of organic compounds from petrochemical industry (e.g. refineries)

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  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Heat Treatment Of Water, Waste Water Or Sewage (AREA)

Abstract

The present invention relates to a kind of processing unit and technique of oil plant oil-polluted water, processing unit includes falling film evaporator, vapour liquid separator, vapour compression machine, film drier, condenser and condensate drum;Handling process comprises the following steps:Oil-polluted water is delivered in falling film evaporator and is evaporated concentration;Concentrate obtained by being concentrated by evaporation is partly recycled in falling film evaporator to be concentrated again, is partly delivered in film drier;Evaporation obtained by evaporation mutually enters vapour liquid separator and carries out vapour, liquid separation, and liquid phase delivers to concentrate pipeline, and vapour phase is delivered to vapour compression machine and recompressed as the utilization of falling film evaporator thermal source, and excess steam delivers to condenser;Concentrate is dried in film drier, dewatered sludge discharge, and the steam of generation is delivered to condenser condensation;The condensed water that condenser is produced is delivered to condensate drum.Apparatus of the present invention are simple, and technique is easy to operate, effectively carry out decrement to the water in oil-polluted water, reduce solid phase intractability, reduce energy resource consumption.

Description

A kind of processing unit and technique of oil plant oil-polluted water
Technical field
The invention belongs to the technical field of oily waste water treatment, the processing of more particularly to a kind of oil plant oil-polluted water is filled Put and technique.
Background technology
Oily waste water is a kind of industrial wastewater having a large capacity and a wide range, from steel, machinery and petrochemical industry etc..With China's work The fast development of industry, the discharge capacity of oily waste water increases year by year, and composition is also increasingly sophisticated.If directly discharging, because of the oil on its top layer Film hinders oxygen to dissolve in water, so as to cause anoxic in water, biological death gives out a foul smell, severe contamination environment.
The waste water particularly produced in the exploitation of oil, refining, storage and transport process, the condensation separation water of such as oil gas and oil product, Washings, reaction generation water, tank car washings, refining equipment washing draining etc..Due to complicated component, current most of refinings Oily factory uses flotation, adds flocculant and is separated.Solid fraction after separation is still burnt containing the moisture for having more than 85% Burn, consume the substantial amounts of energy.
The content of the invention
The technical problems to be solved by the invention are to provide a kind of processing unit and technique of oil plant oil-polluted water, device Simply, technique is easy to operate, effectively carries out decrement to the water in oil-polluted water, reduces solid phase intractability, reduces energy resource consumption.
The technical solution adopted for the present invention to solve the technical problems is to provide a kind of processing dress of oil plant oil-polluted water Put, including falling film evaporator, vapour liquid separator, vapour compression machine, film drier, condenser and condensate drum, the falling liquid film The charging aperture of evaporator is connected with oil-polluted water delivery pipe, the concentrate discharging opening of falling film evaporator respectively with falling film evaporator The charging aperture connection of charging aperture and film drier, evaporation phase discharging opening are connected with vapour liquid separator, the vapour liquid separator Liquid-phase outlet is connected with the concentrate delivery pipe of falling film evaporator, vapor phase exit is connected with vapour compression machine and condenser, described The steam (vapor) outlet of vapour compression machine is connected with the thermal source inlet of falling film evaporator, the thermal source inlet and steam of the falling film evaporator Delivery pipe connection, thermal source outlet are connected with condensate drum, and the film drier dries the siccative produced and passes through siccative discharging opening Discharge, the steam produced deliver to condenser, and the heating agent entrance of the film drier connect with steam pipeline, heating agent is exported and arranged Go out condensed water, the condensate outlet of the condenser is connected with condensate drum.
As one kind of the invention preferred embodiment, the oil-polluted water delivery pipe passes through wastewater feed pump pumping oil-containing Sewage.
As another preferred embodiment of the present invention, the concentrate discharging opening of the falling film evaporator passes through concentrate Pump pumps evaporation concentrated solution.
As another preferred embodiment of the present invention, the liquid outlet of the condensate drum is discharged cold by condensate pump Lime set.
As another preferred embodiment of the present invention, the condenser is connected to vavuum pump and by vavuum pump whole Negative pressure is produced inside individual device.
Another technical scheme that its technical problem of present invention solution is used is to provide a kind of above-mentioned oil plant of utilization and contained The processing unit of oily water handles the technique of oil-polluted water, comprises the following steps:
(1) oil-polluted water is delivered in falling film evaporator and is evaporated concentration;
(2) step (1) is concentrated by evaporation gained concentrate and is partly recycled in falling film evaporator, is partly delivered to film drying In device;
(3) evaporation of step (1) evaporation gained mutually enters vapour liquid separator progress vapour, liquid separation, and liquid phase conveying is steamed with falling liquid film The concentrate for sending out device merges, and vapour phase is delivered to vapour compression machine progress vapor recompression and entered as the evaporation thermal source of falling film evaporator Row is utilized, and unnecessary steam is delivered to condenser condensation;
(4) concentrate is dried in film drier, and gained dewatered sludge is discharged by siccative discharging opening, and gained steams Vapour is delivered to condenser condensation;
(5) condensed water that condenser is produced is delivered to condensate drum.
Beneficial effect
In the present invention, first pass through falling film evaporator to concentrate oil-polluted water (96%~99% is aqueous), remove useless Most water in water, effectively carries out decrement to the water in oil-polluted water, and concentrate is dried by film drier, obtained again To the water content of dewatered sludge be reduced to 30% or so, reduce solid phase treating capacity, meanwhile, compressed and utilized by evaporated vapor, The demand of exogenous steam is reduced, overall energy resource consumption is reduced, device is simple, and technique is easy to operate.
Brief description of the drawings
Fig. 1 is process chart of the invention.
Embodiment
With reference to specific embodiment, the present invention is expanded on further.It should be understood that these embodiments are merely to illustrate the present invention Rather than limitation the scope of the present invention.In addition, it is to be understood that after the content of the invention lectured has been read, people in the art Member can make various changes or modifications to the present invention, and these equivalent form of values equally fall within the application appended claims and limited Scope.
A kind of processing unit of oil plant oil-polluted water as shown in Figure 1, including falling film evaporator 1, vapour liquid separator 2, Vapour compression machine 3, film drier 4, condenser 5 and condensate drum 6.
The charging aperture of falling film evaporator 1 is connected with oil-polluted water delivery pipe, and oil-polluted water is pumped by wastewater feed pump P1. The concentrate discharging opening of falling film evaporator 1 connects with the charging aperture of falling film evaporator 1 and the charging aperture of film drier 4 respectively, Evaporation phase discharging opening is connected with vapour liquid separator 2, and the concentrate discharging opening of falling film evaporator 1 is pumped by concentrate pump P2 to be evaporated Concentrate.The thermal source inlet of falling film evaporator 1 is connected with steam pipeline, thermal source outlet is connected with condensate drum 6.
The liquid-phase outlet of vapour liquid separator 2 is connected with the concentrate delivery pipe of falling film evaporator 1, vapor phase exit and vapour pressure Contracting machine 3 is connected with condenser 5, and the steam (vapor) outlet of vapour compression machine 3 is connected with the thermal source inlet of falling film evaporator 1.By steaming Vapour compressor 3 is compressed utilization to evaporated vapor, can reduce the demand to exogenous steam, advantageously reduces the energy and disappears Consumption.
Film drier 4 dries the dewatered sludge produced and is delivered to condensation by the discharge of siccative discharging opening, the steam produced Device 5.The chuck heating agent entrance of film drier 4 is connected with steam pipeline, heating agent outlet discharge condensed water.Condenser 5 it is cold Condensate outlet is connected with condensate drum 6, and the liquid outlet of condensate drum 6 discharges condensate liquid by condensate pump P3.Condenser 5 is connected To vavuum pump P4, negative pressure is produced inside whole device by vavuum pump P4, to reduce evaporating temperature, it is to avoid high-temperature coking.
The technique that a kind of processing unit using the oil plant oil-polluted water carries out oily waste water treatment is provided below, including Following steps:
(1) oil-polluted water is delivered in falling film evaporator 1 and is evaporated concentration;
(2) step (1) is concentrated by evaporation gained concentrate and is partly recycled in falling film evaporator 1, is partly delivered to film and does In dry device 4;
(3) evaporation of step (1) evaporation gained mutually enters the progress of vapour liquid separator 2 vapour, liquid separation, and liquid phase conveying is steamed with falling liquid film The concentrate for sending out device 1 merges, and vapour phase is delivered to vapour compression machine 3 and carries out vapor recompression as the heat of evaporation of falling film evaporator 1 Source is utilized, and unnecessary vapour phase is delivered to condenser 5 and condensed,;
(4) concentrate is dried in film drier 4, and gained dewatered sludge is discharged by siccative discharging opening, gained Steam is delivered to condenser 5 and condensed;
(5) condensed water that condenser 5 is produced is delivered to condensate drum 6.

Claims (6)

1. a kind of processing unit of oil plant oil-polluted water, including falling film evaporator (1), vapour liquid separator (2), vapour compression machine (3), film drier (4), condenser (5) and condensate drum (6), it is characterised in that:The charging aperture of the falling film evaporator (1) Connected with oil-polluted water delivery pipe, the concentrate discharging opening of falling film evaporator (1) respectively with the charging aperture of falling film evaporator (1) and The charging aperture connection of film drier (4), evaporation phase discharging opening are connected with vapour liquid separator (2), the vapour liquid separator (2) Liquid-phase outlet is connected with the concentrate delivery pipe of falling film evaporator (1), vapor phase exit and vapour compression machine (3) and condenser (5) Connection, the steam (vapor) outlet of the vapour compression machine (3) is connected with the thermal source inlet of falling film evaporator (1), the falling film evaporator (1) thermal source inlet is connected with steam pipeline, thermal source outlet is connected with condensate drum (6), and the film drier (4) is dried The siccative of generation is discharged by siccative discharging opening, the steam of generation enters condenser (5), the heating agent of the film drier (4) Entrance is connected with steam pipeline, heating agent outlet discharge condensed water, the condensate outlet and condensate drum of the condenser (5) (6) connect.
2. a kind of processing unit of oil plant oil-polluted water according to claim 1, it is characterised in that:The oil-polluted water Delivery pipe pumps oil-polluted water by wastewater feed pump (P1).
3. a kind of processing unit of oil plant oil-polluted water according to claim 1, it is characterised in that:The falling film evaporation The concentrate discharging opening of device (1) pumps evaporation concentrated solution by concentrate pump (P2).
4. a kind of processing unit of oil plant oil-polluted water according to claim 1, it is characterised in that:The condensate drum (6) liquid outlet discharges condensate liquid by condensate pump (P3).
5. a kind of processing unit of oil plant oil-polluted water according to claim 1, it is characterised in that:The condenser (5) it is connected to vavuum pump (P4) and negative pressure is produced inside whole device by vavuum pump (P4).
6. a kind of processing unit of the oil plant oil-polluted water described in utilization claim 1 handles the technique of oil-polluted water, including Following steps:
(1) oil-polluted water is delivered in falling film evaporator (1) and is evaporated concentration;
(2) step (1) is concentrated by evaporation gained concentrate and is partly recycled to falling film evaporator (1), is partly delivered to film drier (4) in;
(3) evaporation of step (1) evaporation gained mutually enters vapour liquid separator (2) progress vapour, liquid separation, liquid phase and falling film evaporator (1) concentrate merges, and vapour phase is delivered to vapour compression machine (3) and carries out vapor recompression as the evaporation of falling film evaporator (1) Thermal source is utilized, and unnecessary steam is delivered to condenser (5) condensation;
(4) concentrate is dried in film drier (4), and gained dewatered sludge is discharged by siccative discharging opening, and gained steams Vapour is delivered to condenser (5) condensation;
(5) condensed water that condenser (5) is produced is delivered to condensate drum (6).
CN201710305201.6A 2017-05-03 2017-05-03 A kind of processing unit and technique of oil plant oil-polluted water Pending CN107098417A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108862437A (en) * 2018-07-24 2018-11-23 中石化石油工程技术服务有限公司 A kind of vertical tube falling evaporation recycling treatment process of oilfield sewage
CN110282803A (en) * 2019-07-11 2019-09-27 苏州希图环保科技有限公司 A kind of oil-containing waste water treating device and its technique
CN111423094A (en) * 2020-05-09 2020-07-17 江苏天牛环保科技有限公司 Energy-saving sludge drying method
CN113371975A (en) * 2021-07-21 2021-09-10 中洁蓝环保科技有限公司 Sludge heat drying system and method
CN113646058A (en) * 2019-02-01 2021-11-12 能量集成公司 Method and system for energy efficient drying of co-products in biorefinery

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WO2012074673A1 (en) * 2010-11-30 2012-06-07 General Electric Compay Method and system for treating oily wastewater
CN104671306A (en) * 2015-02-13 2015-06-03 何文元 Waste treatment equipment for producing palm oil
CN105329959A (en) * 2015-10-19 2016-02-17 河北乐恒化工设备制造有限公司 Organic waste water integrated processing system and method

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WO2012074673A1 (en) * 2010-11-30 2012-06-07 General Electric Compay Method and system for treating oily wastewater
CN104671306A (en) * 2015-02-13 2015-06-03 何文元 Waste treatment equipment for producing palm oil
CN105329959A (en) * 2015-10-19 2016-02-17 河北乐恒化工设备制造有限公司 Organic waste water integrated processing system and method

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108862437A (en) * 2018-07-24 2018-11-23 中石化石油工程技术服务有限公司 A kind of vertical tube falling evaporation recycling treatment process of oilfield sewage
CN113646058A (en) * 2019-02-01 2021-11-12 能量集成公司 Method and system for energy efficient drying of co-products in biorefinery
CN110282803A (en) * 2019-07-11 2019-09-27 苏州希图环保科技有限公司 A kind of oil-containing waste water treating device and its technique
CN111423094A (en) * 2020-05-09 2020-07-17 江苏天牛环保科技有限公司 Energy-saving sludge drying method
CN113371975A (en) * 2021-07-21 2021-09-10 中洁蓝环保科技有限公司 Sludge heat drying system and method

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Application publication date: 20170829

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