CN107058046A - A kind of preparation method of cortex acanthopanacis stem of noble dendrobium health-care vinegar - Google Patents

A kind of preparation method of cortex acanthopanacis stem of noble dendrobium health-care vinegar Download PDF

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CN107058046A
CN107058046A CN201710365532.9A CN201710365532A CN107058046A CN 107058046 A CN107058046 A CN 107058046A CN 201710365532 A CN201710365532 A CN 201710365532A CN 107058046 A CN107058046 A CN 107058046A
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stem
cortex acanthopanacis
noble dendrobium
health
care vinegar
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徐鑫
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Wuhu City Sanshan District Green Food Industry Association
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Wuhu City Sanshan District Green Food Industry Association
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    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12JVINEGAR; PREPARATION OR PURIFICATION THEREOF
    • C12J1/00Vinegar; Preparation or purification thereof
    • C12J1/04Vinegar; Preparation or purification thereof from alcohol
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/25Araliaceae (Ginseng family), e.g. ivy, aralia, schefflera or tetrapanax
    • A61K36/254Acanthopanax or Eleutherococcus
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/46Eucommiaceae (Eucommia family), e.g. hardy rubber tree
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/70Polygonaceae (Buckwheat family), e.g. spineflower or dock
    • A61K36/704Polygonum, e.g. knotweed
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/73Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/88Liliopsida (monocotyledons)
    • A61K36/896Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
    • A61K36/8969Polygonatum (Solomon's seal)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/88Liliopsida (monocotyledons)
    • A61K36/898Orchidaceae (Orchid family)
    • A61K36/8984Dendrobium

Abstract

The invention discloses a kind of preparation method of cortex acanthopanacis stem of noble dendrobium health-care vinegar, belong to health-care vinegar manufacture field.It is characterized in that:Described cortex acanthopanacis stem of noble dendrobium health-care vinegar, use the high stem of noble dendrobium of health value, cortex acanthopanacis for raw material, add after the nutritional ingredient of health-care vinegar, respective pretreatment, process is brewageed by extraction, making fermenting grain, filtering, fermentation, ageing, flavouring after-ripening and packaging, the active material of raw material can be sufficiently reserved, the nutritive value of health-care vinegar is improved, makes the mouthfeel of health-care vinegar soft pure, A sweety scent assails the nostrils, also there is replenishing the vital essence and removing heat, liver-kidney tonifying, the health-care efficacy of reinforcing stomach reg fluid.

Description

A kind of preparation method of cortex acanthopanacis stem of noble dendrobium health-care vinegar
Technical field
The present invention relates to a kind of preparation method of health-care vinegar, more particularly, to a kind of making side of cortex acanthopanacis stem of noble dendrobium health-care vinegar Method.
Background technology
The stem of noble dendrobium, alias:Dendrobium, Shi Lan, bracketplant, HERBA DENDROBII, maple beans, in cylinder or oblate cylindricality, meat is more Juice, frangibility.Gas is micro-, mildly bitter flavor and Hui Tian, and that chews has stickiness.The stem of noble dendrobium be the orchid recorded earliest in China's ancient documents it Before one, 2000《Sheng Nong's herbal classic》In it is just on the books, its slightly sweet flavor is micro- salty, and property belongs to clear and rich, it is clear in have benefit, bowl spares has clearly, Can replenishing the vital essence and removing heat, reinforcing stomach reg fluid.There is certain antipyretic effect, gastric secretion can be promoted, it is aid digestion;Also strengthen new old generation Thank, anti-aging, the effect such as promote longevity.The stem of noble dendrobium is the traditional rare Chinese medicine of China, and current clinical medicine confirms that the stem of noble dendrobium can suppress Kidney micro-some Na/K-ATP enzymatic activitys, can nourishing Yin and clearing heat.Current diabetes, which are increasingly becoming, influences the first of human health to kill greatly Hand.Modern medicine study shows, the stem of noble dendrobium can significantly reduce glycosuria germ rat model blood glucose, hyperglycemic factor, increase insulin, The secretion of C peptides.Suppress insulin degraded, improve insulin sensitivity index, suppress the secretion of free fatty, significantly reduce obesity The TNF of diabetic model rats, since thousand it always and ganoderma lucidum, ginseng, cordyceps sinensis etc. is equally listed in Product Chinese medicine.
Cortex acanthopanacis, is the dry root skin of Araliaceae acanthopanax gracilistylus.Summer, season in autumn two excavation root, clean, strip root Skin, is dried, its pungent, hardship, warm-natured.There is wind-damp dispelling, tonify the liver and kidney, strengthen muscles and bones, the effect of inducing diuresis for removing edema, for rheumatism numbness Disease, muscles and bones impotence, children's retardation of walking is physically weak weak, oedema, tinea pedis.
At present, the stem of noble dendrobium, cortex acanthopanacis are used for raw material, cortex acanthopanacis stem of noble dendrobium health-care vinegar is processed into, there are no relevant report And launch, provide a new way for the deep processing of the stem of noble dendrobium and cortex acanthopanacis.
The content of the invention
It is an object of the invention to provide a kind of preparation method of cortex acanthopanacis stem of noble dendrobium health-care vinegar, using the stem of noble dendrobium of nutrition and health care, Cortex acanthopanacis is raw material, is processed into cortex acanthopanacis stem of noble dendrobium health-care vinegar, and a new way is provided for the deep processing of the stem of noble dendrobium and cortex acanthopanacis.
The technical scheme adopted by the invention to solve the technical problem is that:
A kind of preparation method of cortex acanthopanacis stem of noble dendrobium health-care vinegar, it is characterised in that described processing method uses following steps:
A, cortex acanthopanacis pretreatment:The cortex acanthopanacis of dry and high quality is selected, appropriate Bark of Eucommia Ulmoides, polygoni cuspidati,radix is added, after cleaning, low temperature is done Dry, broken wall is crushed, and cortex acanthopanacis fine powder is made;
B, stem of noble dendrobium pretreatment:The HERBA DENDROBII of high-quality is selected, a little radix polygonati officinalis, Rui cores is added, after cleaning, is put into baking oven and softens, It is 55 DEG C to set temperature, and low temperature is baked after 30min, and break process is freeze-dried, and broken wall is crushed, and stem of noble dendrobium fine powder is made;
C, extraction:Cortex acanthopanacis fine powder, stem of noble dendrobium fine powder are pressed 2:After 3 ratio is well mixed, mixed material is made, using many cascades Continuous countercurrent extraction machine, one end adds 35 DEG C of softened waters, and the other end adds mixed material, realizes that multiple stage continuous adverse current is extracted, just carries The stage is taken to set temperature to be 45 DEG C, the time is 10min;Deep stage setting temperature of extracting is 50 DEG C, and the time is 8min;Ooze and wash rank Section Extracting temperature is 55 DEG C, and the time is 3min, and extract solution is made in filtering;
D, making fermenting grain:The glutinous rice for selecting high-quality is matrix, adds appropriate blood wheat and coix seed, cleans impurity elimination, enters pot and cook Afterwards, distiller's yeast is added when being cooled to 38 DEG C, the weight ratio of ripe mixed material and distiller's yeast is 50:1, remix infiltration, heat-preservation fermentation 8 My god, every stirring in 10 hours once, fermenting grain is made;
E, filtering:Using plate and frame filter press, fermenting grain is filtered, zymocyte liquid and filter residue is obtained;
F, fermentation:Take extract solution, the zymocyte liquid of 55 parts by weight, the material residue of 10 parts by weight, the grape of 5 parts by weight of 30 parts by weight Liquid glucose, is well mixed, and accesses 12% acetic acid bacteria, and carrying out eddy current type acetic acid deep drainpipe using Fring types acidifier ferments, 32 Fermented 10 days under conditions of DEG C, until acidity no longer rises, the acidity of adjustment acetic fermentation unstrained spirits is 12g/100ml, fermentation ends;
G, ageing:By acetic fermentation unstrained spirits through filter plant refined filtration, filtrate is made;Filtrate is pumped into wooden barrel, using microwave radiation technology Cold treatment accelerate filtrate ageing, microwave frequency 220MHz, 2 days cold treatment time, 6 DEG C of temperature, add a little chitosan with Alum is clarified, and extracts to obtain clarified solution;
H, flavouring after-ripening:Clarified solution is placed under air-proof condition and carries out flavouring after-ripening in 55 DEG C, is terminated after 1 day, cortex acanthopanacis is made Stem of noble dendrobium health-care vinegar;
I, packaging:Cortex acanthopanacis stem of noble dendrobium health-care vinegar is subjected to sterile filling with vial, after packing, as finished product.
Beneficial effect:The cortex acanthopanacis stem of noble dendrobium health-care vinegar that this method makes, uses the high stem of noble dendrobium of health value, cortex acanthopanacis for original Material, is added after the nutritional ingredient of health-care vinegar, respective pretreatment, by extracting, making fermenting grain, filtering, fermentation, ageing, increasing Fragrant after-ripening and packaging brewage process, can be sufficiently reserved the active material of raw material, improve the nutritive value of health-care vinegar, make guarantor The mouthfeel of strong vinegar is soft pure, and A sweety scent assails the nostrils, also with replenishing the vital essence and removing heat, liver-kidney tonifying, the health-care efficacy of reinforcing stomach reg fluid.
Embodiment
Embodiment 1:
A kind of preparation method of cortex acanthopanacis stem of noble dendrobium health-care vinegar, it is characterised in that use following steps:
A, cortex acanthopanacis pretreatment:The cortex acanthopanacis of dry and high quality is selected, the appropriate bighead atractylodes rhizome, the fruit-rind of Chinese trichosanthes is added, after cleaning, low temperature drying, Broken wall is crushed, and cortex acanthopanacis fine powder is made;
B, stem of noble dendrobium pretreatment:The HERBA DENDROBII of high-quality is selected, a little Radix Rhapontici seu Radix Echinopsis root, radix polygonati officinalis is added, after cleaning, is put into soft in baking oven Change, it is 55 DEG C to set temperature, and low temperature is baked after 30min, and break process is freeze-dried, and broken wall is crushed, and stem of noble dendrobium fine powder is made;
C, extraction:Cortex acanthopanacis fine powder, stem of noble dendrobium fine powder are pressed 1:After 1 ratio is well mixed, mixed material is made, using many cascades Continuous countercurrent extraction machine, one end adds 35 DEG C of softened waters, and the other end adds mixed material, realizes that multiple stage continuous adverse current is extracted, just carries The stage is taken to set temperature to be 45 DEG C, the time is 10min;Deep stage setting temperature of extracting is 50 DEG C, and the time is 8min;Ooze and wash rank Section Extracting temperature is 55 DEG C, and the time is 3min, and extract solution is made in filtering;
D, making fermenting grain:The glutinous rice for selecting high-quality is matrix, adds appropriate bitter buckwheat and coix seed, cleans impurity elimination, enters pot and cook Afterwards, distiller's yeast is added when being cooled to 38 DEG C, the weight ratio of ripe mixed material and distiller's yeast is 50:1, remix infiltration, heat-preservation fermentation 8 My god, every stirring in 10 hours once, fermenting grain is made;
E, filtering:Using plate and frame filter press, fermenting grain is filtered, zymocyte liquid and filter residue is obtained;
F, fermentation:Take extract solution, the zymocyte liquid of 55 parts by weight, the material residue of 10 parts by weight, the grape of 5 parts by weight of 30 parts by weight Liquid glucose, is well mixed, and accesses 12% acetic acid bacteria, and carrying out eddy current type acetic acid deep drainpipe using Fring types acidifier ferments, 32 Fermented 10 days under conditions of DEG C, until acidity no longer rises, the acidity of adjustment acetic fermentation unstrained spirits is 12g/100ml, fermentation ends;
G, ageing:By acetic fermentation unstrained spirits through filter plant refined filtration, filtrate is made;Filtrate is pumped into wooden barrel, using microwave radiation technology Cold treatment accelerate filtrate ageing, microwave frequency 220MHz, 2 days cold treatment time, 6 DEG C of temperature, add a little chitosan with Alum is clarified, and extracts to obtain clarified solution;
H, flavouring after-ripening:Clarified solution is placed under air-proof condition and carries out flavouring after-ripening in 55 DEG C, is terminated after 1 day, cortex acanthopanacis is made Stem of noble dendrobium health-care vinegar;
I, packaging:Cortex acanthopanacis stem of noble dendrobium health-care vinegar is subjected to sterile filling with vial, after packing, as finished product.
Embodiment 2:
A kind of preparation method of cortex acanthopanacis stem of noble dendrobium health-care vinegar, it is characterised in that use following steps:
A, cortex acanthopanacis pretreatment:The cortex acanthopanacis of dry and high quality is selected, appropriate radix bardanae, adenophora tetraphylla is added, after cleaning, low temperature is done Dry, broken wall is crushed, and cortex acanthopanacis fine powder is made;
B, stem of noble dendrobium pretreatment:The HERBA DENDROBII of high-quality is selected, a little fruit of Cherokee rose, the root bark of white mulberry is added, after cleaning, is put into soft in baking oven Change, it is 55 DEG C to set temperature, and low temperature is baked after 30min, and break process is freeze-dried, and broken wall is crushed, and stem of noble dendrobium fine powder is made;
C, extraction:Cortex acanthopanacis fine powder, stem of noble dendrobium fine powder are pressed 3:After 1 ratio is well mixed, mixed material is made, using many cascades Continuous countercurrent extraction machine, one end adds 35 DEG C of softened waters, and the other end adds mixed material, realizes that multiple stage continuous adverse current is extracted, just carries The stage is taken to set temperature to be 45 DEG C, the time is 10min;Deep stage setting temperature of extracting is 50 DEG C, and the time is 8min;Ooze and wash rank Section Extracting temperature is 55 DEG C, and the time is 3min, and extract solution is made in filtering;
D, making fermenting grain:The glutinous rice for selecting high-quality is matrix, adds appropriate dregs of beans and blood wheat, cleans impurity elimination, is entered after pot cooks, Add distiller's yeast when being cooled to 38 DEG C, the weight ratio of ripe mixed material and distiller's yeast is 35:1, remix infiltration, heat-preservation fermentation 8 days, often Every stirring in 10 hours once, fermenting grain is made;
E, filtering:Using plate and frame filter press, fermenting grain is filtered, zymocyte liquid and filter residue is obtained;
F, fermentation:Take extract solution, the zymocyte liquid of 55 parts by weight, the material residue of 10 parts by weight, the grape of 5 parts by weight of 30 parts by weight Liquid glucose, is well mixed, and accesses 12% acetic acid bacteria, and carrying out eddy current type acetic acid deep drainpipe using Fring types acidifier ferments, 32 Fermented 10 days under conditions of DEG C, until acidity no longer rises, the acidity of adjustment acetic fermentation unstrained spirits is 12g/100ml, fermentation ends;
G, ageing:By acetic fermentation unstrained spirits through filter plant refined filtration, filtrate is made;Filtrate is pumped into wooden barrel, using microwave radiation technology Cold treatment accelerate filtrate ageing, microwave frequency 220MHz, 2 days cold treatment time, 6 DEG C of temperature, add a little chitosan with Alum is clarified, and extracts to obtain clarified solution;
H, flavouring after-ripening:Clarified solution is placed under air-proof condition and carries out flavouring after-ripening in 55 DEG C, is terminated after 1 day, cortex acanthopanacis is made Stem of noble dendrobium health-care vinegar;
I, packaging:Cortex acanthopanacis stem of noble dendrobium health-care vinegar is subjected to sterile filling with vial, after packing, as finished product.
Embodiment 3:
A kind of preparation method of cortex acanthopanacis stem of noble dendrobium health-care vinegar, it is characterised in that use following steps:
A, cortex acanthopanacis pretreatment:The cortex acanthopanacis of dry and high quality is selected, the appropriate fruit of glossy privet, rhizoma imperatae is added, after cleaning, low temperature is done Dry, broken wall is crushed, and cortex acanthopanacis fine powder is made;
B, stem of noble dendrobium pretreatment:The HERBA DENDROBII of high-quality is selected, a little rhizoma Gastrodiae, the fruit of Chinese magnoliavine is added, after cleaning, is put into soft in baking oven Change, it is 55 DEG C to set temperature, and low temperature is baked after 30min, and break process is freeze-dried, and broken wall is crushed, and stem of noble dendrobium fine powder is made;
C, extraction:Cortex acanthopanacis fine powder, stem of noble dendrobium fine powder are pressed 3:After 2 ratio is well mixed, mixed material is made, using many cascades Continuous countercurrent extraction machine, one end adds 35 DEG C of softened waters, and the other end adds mixed material, realizes that multiple stage continuous adverse current is extracted, just carries The stage is taken to set temperature to be 45 DEG C, the time is 10min;Deep stage setting temperature of extracting is 50 DEG C, and the time is 8min;Ooze and wash rank Section Extracting temperature is 55 DEG C, and the time is 3min, and extract solution is made in filtering;
D, making fermenting grain:The glutinous rice for selecting high-quality is matrix, adds appropriate gingko and coix seed, cleans impurity elimination, enters pot and cook Afterwards, distiller's yeast is added when being cooled to 38 DEG C, the weight ratio of ripe mixed material and distiller's yeast is 50:1, remix infiltration, heat-preservation fermentation 8 My god, every stirring in 10 hours once, fermenting grain is made;
E, filtering:Using plate and frame filter press, fermenting grain is filtered, zymocyte liquid and filter residue is obtained;
F, fermentation:Take extract solution, the zymocyte liquid of 55 parts by weight, the material residue of 10 parts by weight, the grape of 5 parts by weight of 30 parts by weight Liquid glucose, is well mixed, and accesses 12% acetic acid bacteria, and carrying out eddy current type acetic acid deep drainpipe using Fring types acidifier ferments, 32 Fermented 10 days under conditions of DEG C, until acidity no longer rises, the acidity of adjustment acetic fermentation unstrained spirits is 12g/100ml, fermentation ends;
G, ageing:By acetic fermentation unstrained spirits through filter plant refined filtration, filtrate is made;Filtrate is pumped into wooden barrel, using microwave radiation technology Cold treatment accelerate filtrate ageing, microwave frequency 220MHz, 2 days cold treatment time, 6 DEG C of temperature, add a little chitosan with Alum is clarified, and extracts to obtain clarified solution;
H, flavouring after-ripening:Clarified solution is placed under air-proof condition and carries out flavouring after-ripening in 55 DEG C, is terminated after 1 day, cortex acanthopanacis is made Stem of noble dendrobium health-care vinegar;
I, packaging:Cortex acanthopanacis stem of noble dendrobium health-care vinegar is subjected to sterile filling with vial, after packing, as finished product.
Embodiment 4:
A kind of preparation method of cortex acanthopanacis stem of noble dendrobium health-care vinegar, it is characterised in that use following steps:
A, cortex acanthopanacis pretreatment:The cortex acanthopanacis of dry and high quality is selected, appropriate Bark of Eucommia Ulmoides, wild pseudo-ginseng is added, after cleaning, low temperature is done Dry, broken wall is crushed, and cortex acanthopanacis fine powder is made;
B, stem of noble dendrobium pretreatment:The HERBA DENDROBII of high-quality is selected, a little asparagus, Amomum cardamomum is added, after cleaning, is put into soft in baking oven Change, it is 45 DEG C to set temperature, and low temperature is baked after 30min, and break process is freeze-dried, and broken wall is crushed, and stem of noble dendrobium fine powder is made;
C, extraction:Cortex acanthopanacis fine powder, stem of noble dendrobium fine powder are pressed 3:After 1 ratio is well mixed, mixed material is made, using many cascades Continuous countercurrent extraction machine, one end adds 35 DEG C of softened waters, and the other end adds mixed material, realizes that multiple stage continuous adverse current is extracted, just carries The stage is taken to set temperature to be 45 DEG C, the time is 10min;Deep stage setting temperature of extracting is 50 DEG C, and the time is 8min;Ooze and wash rank Section Extracting temperature is 55 DEG C, and the time is 3min, and extract solution is made in filtering;
D, making fermenting grain:The glutinous rice for selecting high-quality is matrix, adds appropriate long-grained nonglutinous rice and embryo nelumbinis, cleans impurity elimination, enters pot and cook Afterwards, distiller's yeast is added when being cooled to 38 DEG C, the weight ratio of ripe mixed material and distiller's yeast is 55:1, remix infiltration, heat-preservation fermentation 8 My god, every stirring in 10 hours once, fermenting grain is made;
E, filtering:Using plate and frame filter press, fermenting grain is filtered, zymocyte liquid and filter residue is obtained;
F, fermentation:Take extract solution, the zymocyte liquid of 55 parts by weight, the material residue of 10 parts by weight, the grape of 5 parts by weight of 30 parts by weight Liquid glucose, is well mixed, and accesses 8% acetic acid bacteria, and carrying out eddy current type acetic acid deep drainpipe using Fring types acidifier ferments, at 32 DEG C Under conditions of ferment 10 days, until acidity no longer rises, the acidity of adjustment acetic fermentation unstrained spirits is 12g/100ml, fermentation ends;
G, ageing:By acetic fermentation unstrained spirits through filter plant refined filtration, filtrate is made;Filtrate is pumped into wooden barrel, using microwave radiation technology Cold treatment accelerate filtrate ageing, microwave frequency 220MHz, 2 days cold treatment time, 6 DEG C of temperature, add a little chitosan with Alum is clarified, and extracts to obtain clarified solution;
H, flavouring after-ripening:Clarified solution is placed under air-proof condition and carries out flavouring after-ripening in 55 DEG C, is terminated after 1 day, cortex acanthopanacis is made Stem of noble dendrobium health-care vinegar;
I, packaging:Cortex acanthopanacis stem of noble dendrobium health-care vinegar is subjected to sterile filling with vial, after packing, as finished product.
Embodiment 5:
A kind of preparation method of cortex acanthopanacis stem of noble dendrobium health-care vinegar, it is characterised in that use following steps:
A, cortex acanthopanacis pretreatment:The cortex acanthopanacis of dry and high quality is selected, appropriate cortex albiziae, caulis bambusae in taenian is added, after cleaning, low temperature drying, Broken wall is crushed, and cortex acanthopanacis fine powder is made;
B, stem of noble dendrobium pretreatment:The HERBA DENDROBII of high-quality is selected, a little tuber of dwarf lilyturf, the root bark of Chinese wolf-berry is added, after cleaning, is put into soft in baking oven Change, it is 55 DEG C to set temperature, and low temperature is baked after 30min, and break process is freeze-dried, and broken wall is crushed, and stem of noble dendrobium fine powder is made;
C, extraction:Cortex acanthopanacis fine powder, stem of noble dendrobium fine powder are pressed 2:After 3 ratio is well mixed, mixed material is made, using many cascades Continuous countercurrent extraction machine, one end adds 35 DEG C of softened waters, and the other end adds mixed material, realizes that multiple stage continuous adverse current is extracted, just carries The stage is taken to set temperature to be 45 DEG C, the time is 10min;Deep stage setting temperature of extracting is 50 DEG C, and the time is 8min;Ooze and wash rank Section Extracting temperature is 55 DEG C, and the time is 3min, and extract solution is made in filtering;
D, making fermenting grain:The glutinous rice for selecting high-quality is matrix, adds appropriate cymose buckwheat rhizome and walnut kernel, cleans impurity elimination, enters pot steaming After ripe, distiller's yeast is added when being cooled to 38 DEG C, the weight ratio of ripe mixed material and distiller's yeast is 50:1, remix infiltration, heat-preservation fermentation 8 My god, every stirring in 10 hours once, fermenting grain is made;
E, filtering:Using plate and frame filter press, fermenting grain is filtered, zymocyte liquid and filter residue is obtained;
F, fermentation:Take extract solution, the zymocyte liquid of 50 parts by weight, the material residue of 10 parts by weight, the grape of 5 parts by weight of 35 parts by weight Liquid glucose, is well mixed, and accesses 12% acetic acid bacteria, and carrying out eddy current type acetic acid deep drainpipe using Fring types acidifier ferments, 32 Fermented 10 days under conditions of DEG C, until acidity no longer rises, the acidity of adjustment acetic fermentation unstrained spirits is 12g/100ml, fermentation ends;
G, ageing:By acetic fermentation unstrained spirits through filter plant refined filtration, filtrate is made;Filtrate is pumped into wooden barrel, using microwave radiation technology Cold treatment accelerate filtrate ageing, microwave frequency 220MHz, 2 days cold treatment time, 6 DEG C of temperature, add a little chitosan with Alum is clarified, and extracts to obtain clarified solution;
H, flavouring after-ripening:Clarified solution is placed under air-proof condition and carries out flavouring after-ripening in 55 DEG C, is terminated after 1 day, cortex acanthopanacis is made Stem of noble dendrobium health-care vinegar;
I, packaging:Cortex acanthopanacis stem of noble dendrobium health-care vinegar is subjected to sterile filling with vial, after packing, as finished product.
The preferred embodiment of the present invention described in detail above, still, the present invention are not limited in above-mentioned embodiment Detail, in the range of the technology design of the present invention, a variety of simple variants can be carried out to technical scheme, this A little simple variants belong to protection scope of the present invention.
In addition, various embodiments of the present invention can be combined randomly, as long as it is without prejudice to originally The thought of invention, it should equally be considered as content disclosed in this invention.
Part that the present invention does not relate to is same as the prior art or can be realized using prior art.

Claims (1)

1. a kind of preparation method of cortex acanthopanacis stem of noble dendrobium health-care vinegar, it is characterised in that described processing method uses following steps:
A, cortex acanthopanacis pretreatment:The cortex acanthopanacis of dry and high quality is selected, appropriate Bark of Eucommia Ulmoides, polygoni cuspidati,radix is added, after cleaning, low temperature is done Dry, broken wall is crushed, and cortex acanthopanacis fine powder is made;
B, stem of noble dendrobium pretreatment:The HERBA DENDROBII of high-quality is selected, a little radix polygonati officinalis, Rui cores is added, after cleaning, is put into baking oven and softens, It is 55 DEG C to set temperature, and low temperature is baked after 30min, and break process is freeze-dried, and broken wall is crushed, and stem of noble dendrobium fine powder is made;
C, extraction:Cortex acanthopanacis fine powder, stem of noble dendrobium fine powder are pressed 2:After 3 ratio is well mixed, mixed material is made, using many cascades Continuous countercurrent extraction machine, one end adds 35 DEG C of softened waters, and the other end adds mixed material, realizes that multiple stage continuous adverse current is extracted, just carries The stage is taken to set temperature to be 45 DEG C, the time is 10min;Deep stage setting temperature of extracting is 50 DEG C, and the time is 8min;Ooze and wash rank Section Extracting temperature is 55 DEG C, and the time is 3min, and extract solution is made in filtering;
D, making fermenting grain:The glutinous rice for selecting high-quality is matrix, adds appropriate blood wheat and coix seed, cleans impurity elimination, enters pot and cook Afterwards, distiller's yeast is added when being cooled to 38 DEG C, the weight ratio of ripe mixed material and distiller's yeast is 50:1, remix infiltration, heat-preservation fermentation 8 My god, every stirring in 10 hours once, fermenting grain is made;
E, filtering:Using plate and frame filter press, fermenting grain is filtered, zymocyte liquid and filter residue is obtained;
F, fermentation:Take extract solution, the zymocyte liquid of 55 parts by weight, the material residue of 10 parts by weight, the grape of 5 parts by weight of 30 parts by weight Liquid glucose, is well mixed, and accesses 12% acetic acid bacteria, and carrying out eddy current type acetic acid deep drainpipe using Fring types acidifier ferments, 32 Fermented 10 days under conditions of DEG C, until acidity no longer rises, the acidity of adjustment acetic fermentation unstrained spirits is 12g/100ml, fermentation ends;
G, ageing:By acetic fermentation unstrained spirits through filter plant refined filtration, filtrate is made;Filtrate is pumped into wooden barrel, using microwave radiation technology Cold treatment accelerate filtrate ageing, microwave frequency 220MHz, 2 days cold treatment time, 6 DEG C of temperature, add a little chitosan with Alum is clarified, and extracts to obtain clarified solution;
H, flavouring after-ripening:Clarified solution is placed under air-proof condition and carries out flavouring after-ripening in 55 DEG C, is terminated after 1 day, cortex acanthopanacis is made Stem of noble dendrobium health-care vinegar;
I, packaging:Cortex acanthopanacis stem of noble dendrobium health-care vinegar is subjected to sterile filling with vial, after packing, as finished product.
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CN107384742A (en) * 2017-09-28 2017-11-24 程龙凤 The preparation method of setose thistle purple dendrobium health-care vinegar
CN107674816A (en) * 2017-09-28 2018-02-09 王军 A kind of compound stem of noble dendrobium vinegar and preparation method thereof
CN109370865A (en) * 2018-12-28 2019-02-22 徐州黎明食品有限公司 A kind of Dietotherapy health A black garlic vinegar and a method for preparing the same and preparation method thereof

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CN105795037A (en) * 2016-05-29 2016-07-27 刘永 Preparation method of flowers of Chinese redbud and rosemary compound extract
CN106222060A (en) * 2016-08-22 2016-12-14 彭常安 A kind of processing method of Calyx Seu Fructus Physalis Fructus Crataegi Health-care fruit vinegar
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CN105779248A (en) * 2016-03-21 2016-07-20 张俊辉 Processing method of Melastoma dodecandrum Lour.and Fructus Crataegi healthy vinegar
CN105795037A (en) * 2016-05-29 2016-07-27 刘永 Preparation method of flowers of Chinese redbud and rosemary compound extract
CN106222060A (en) * 2016-08-22 2016-12-14 彭常安 A kind of processing method of Calyx Seu Fructus Physalis Fructus Crataegi Health-care fruit vinegar
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* Cited by examiner, † Cited by third party
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CN107384742A (en) * 2017-09-28 2017-11-24 程龙凤 The preparation method of setose thistle purple dendrobium health-care vinegar
CN107674816A (en) * 2017-09-28 2018-02-09 王军 A kind of compound stem of noble dendrobium vinegar and preparation method thereof
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Application publication date: 20170818