CN107056176A - A kind of novel energy saving thermal insulation material and preparation method thereof - Google Patents
A kind of novel energy saving thermal insulation material and preparation method thereof Download PDFInfo
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- CN107056176A CN107056176A CN201710429340.XA CN201710429340A CN107056176A CN 107056176 A CN107056176 A CN 107056176A CN 201710429340 A CN201710429340 A CN 201710429340A CN 107056176 A CN107056176 A CN 107056176A
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- thermal insulation
- insulation material
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- 239000012774 insulation material Substances 0.000 title claims abstract description 72
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 239000002994 raw material Substances 0.000 claims abstract description 50
- 229910052902 vermiculite Inorganic materials 0.000 claims abstract description 39
- 239000010455 vermiculite Substances 0.000 claims abstract description 39
- 235000019354 vermiculite Nutrition 0.000 claims abstract description 39
- 239000011521 glass Substances 0.000 claims abstract description 38
- 229920003023 plastic Polymers 0.000 claims abstract description 29
- 239000004033 plastic Substances 0.000 claims abstract description 29
- 239000011324 bead Substances 0.000 claims abstract description 27
- 239000002699 waste material Substances 0.000 claims abstract description 22
- 229920002635 polyurethane Polymers 0.000 claims abstract description 19
- 239000004814 polyurethane Substances 0.000 claims abstract description 19
- 238000007667 floating Methods 0.000 claims abstract description 18
- 238000003756 stirring Methods 0.000 claims abstract description 18
- 239000011230 binding agent Substances 0.000 claims abstract description 14
- 239000004088 foaming agent Substances 0.000 claims abstract description 14
- 239000012760 heat stabilizer Substances 0.000 claims abstract description 13
- 238000012423 maintenance Methods 0.000 claims abstract description 12
- 239000004372 Polyvinyl alcohol Substances 0.000 claims abstract description 9
- 229960000892 attapulgite Drugs 0.000 claims abstract description 9
- 239000004568 cement Substances 0.000 claims abstract description 9
- RGPUVZXXZFNFBF-UHFFFAOYSA-K diphosphonooxyalumanyl dihydrogen phosphate Chemical compound [Al+3].OP(O)([O-])=O.OP(O)([O-])=O.OP(O)([O-])=O RGPUVZXXZFNFBF-UHFFFAOYSA-K 0.000 claims abstract description 9
- JMGZBMRVDHKMKB-UHFFFAOYSA-L disodium;2-sulfobutanedioate Chemical compound [Na+].[Na+].OS(=O)(=O)C(C([O-])=O)CC([O-])=O JMGZBMRVDHKMKB-UHFFFAOYSA-L 0.000 claims abstract description 9
- 239000010881 fly ash Substances 0.000 claims abstract description 9
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229910052625 palygorskite Inorganic materials 0.000 claims abstract description 9
- 229920002451 polyvinyl alcohol Polymers 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 9
- MPPQGYCZBNURDG-UHFFFAOYSA-N 2-propionyl-6-dimethylaminonaphthalene Chemical compound C1=C(N(C)C)C=CC2=CC(C(=O)CC)=CC=C21 MPPQGYCZBNURDG-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000005995 Aluminium silicate Substances 0.000 claims abstract description 8
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000004113 Sepiolite Substances 0.000 claims abstract description 8
- 235000012211 aluminium silicate Nutrition 0.000 claims abstract description 8
- 239000000843 powder Substances 0.000 claims abstract description 8
- 229910052624 sepiolite Inorganic materials 0.000 claims abstract description 8
- 235000019355 sepiolite Nutrition 0.000 claims abstract description 8
- 239000013590 bulk material Substances 0.000 claims description 12
- 239000011268 mixed slurry Substances 0.000 claims description 12
- 235000019353 potassium silicate Nutrition 0.000 claims description 11
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical group [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 11
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical group [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 6
- AGXUVMPSUKZYDT-UHFFFAOYSA-L barium(2+);octadecanoate Chemical group [Ba+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O AGXUVMPSUKZYDT-UHFFFAOYSA-L 0.000 claims description 6
- 239000011888 foil Substances 0.000 claims description 6
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical group [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 claims description 6
- 229940048086 sodium pyrophosphate Drugs 0.000 claims description 6
- 239000004575 stone Substances 0.000 claims description 6
- 235000019818 tetrasodium diphosphate Nutrition 0.000 claims description 6
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 claims description 6
- 241000545744 Hirudinea Species 0.000 claims description 5
- 238000005245 sintering Methods 0.000 claims description 5
- 235000008331 Pinus X rigitaeda Nutrition 0.000 claims 1
- 235000011613 Pinus brutia Nutrition 0.000 claims 1
- 241000018646 Pinus brutia Species 0.000 claims 1
- 239000003795 chemical substances by application Substances 0.000 claims 1
- 229910052622 kaolinite Inorganic materials 0.000 claims 1
- 239000011435 rock Substances 0.000 claims 1
- 239000002689 soil Substances 0.000 claims 1
- 230000006835 compression Effects 0.000 abstract description 21
- 238000007906 compression Methods 0.000 abstract description 21
- 238000009413 insulation Methods 0.000 abstract description 15
- 230000007613 environmental effect Effects 0.000 abstract description 6
- 239000004566 building material Substances 0.000 abstract description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 10
- 239000000126 substance Substances 0.000 description 10
- 239000004035 construction material Substances 0.000 description 8
- 230000000052 comparative effect Effects 0.000 description 7
- 230000000694 effects Effects 0.000 description 7
- 239000000463 material Substances 0.000 description 6
- 229920006328 Styrofoam Polymers 0.000 description 5
- 239000001569 carbon dioxide Substances 0.000 description 5
- 229910002092 carbon dioxide Inorganic materials 0.000 description 5
- 230000001351 cycling effect Effects 0.000 description 5
- 238000004134 energy conservation Methods 0.000 description 5
- 238000005187 foaming Methods 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 5
- 229910052500 inorganic mineral Inorganic materials 0.000 description 5
- 239000011707 mineral Substances 0.000 description 5
- 231100000252 nontoxic Toxicity 0.000 description 5
- 230000003000 nontoxic effect Effects 0.000 description 5
- 239000011148 porous material Substances 0.000 description 5
- 239000008261 styrofoam Substances 0.000 description 5
- 230000009967 tasteless effect Effects 0.000 description 5
- 229920005830 Polyurethane Foam Polymers 0.000 description 4
- 238000010276 construction Methods 0.000 description 4
- 238000013461 design Methods 0.000 description 4
- 239000006260 foam Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 239000011496 polyurethane foam Substances 0.000 description 4
- -1 0.3 part of retarder Substances 0.000 description 3
- 239000011810 insulating material Substances 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 238000006467 substitution reaction Methods 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000000686 essence Substances 0.000 description 1
- 235000013312 flour Nutrition 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
-
- E—FIXED CONSTRUCTIONS
- E04—BUILDING
- E04B—GENERAL BUILDING CONSTRUCTIONS; WALLS, e.g. PARTITIONS; ROOFS; FLOORS; CEILINGS; INSULATION OR OTHER PROTECTION OF BUILDINGS
- E04B1/00—Constructions in general; Structures which are not restricted either to walls, e.g. partitions, or floors or ceilings or roofs
- E04B1/62—Insulation or other protection; Elements or use of specified material therefor
- E04B1/74—Heat, sound or noise insulation, absorption, or reflection; Other building methods affording favourable thermal or acoustical conditions, e.g. accumulating of heat within walls
- E04B1/76—Heat, sound or noise insulation, absorption, or reflection; Other building methods affording favourable thermal or acoustical conditions, e.g. accumulating of heat within walls specifically with respect to heat only
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00017—Aspects relating to the protection of the environment
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
- C04B2111/28—Fire resistance, i.e. materials resistant to accidental fires or high temperatures
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/52—Sound-insulating materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/30—Mortars, concrete or artificial stone characterised by specific physical values for heat transfer properties such as thermal insulation values, e.g. R-values
- C04B2201/32—Mortars, concrete or artificial stone characterised by specific physical values for heat transfer properties such as thermal insulation values, e.g. R-values for the thermal conductivity, e.g. K-factors
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/50—Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
-
- E—FIXED CONSTRUCTIONS
- E04—BUILDING
- E04B—GENERAL BUILDING CONSTRUCTIONS; WALLS, e.g. PARTITIONS; ROOFS; FLOORS; CEILINGS; INSULATION OR OTHER PROTECTION OF BUILDINGS
- E04B1/00—Constructions in general; Structures which are not restricted either to walls, e.g. partitions, or floors or ceilings or roofs
- E04B1/62—Insulation or other protection; Elements or use of specified material therefor
- E04B1/74—Heat, sound or noise insulation, absorption, or reflection; Other building methods affording favourable thermal or acoustical conditions, e.g. accumulating of heat within walls
- E04B2001/742—Use of special materials; Materials having special structures or shape
- E04B2001/746—Recycled materials, e.g. made of used tires, bumpers or newspapers
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A30/00—Adapting or protecting infrastructure or their operation
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A30/00—Adapting or protecting infrastructure or their operation
- Y02A30/24—Structural elements or technologies for improving thermal insulation
- Y02A30/244—Structural elements or technologies for improving thermal insulation using natural or recycled building materials, e.g. straw, wool, clay or used tires
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02B—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO BUILDINGS, e.g. HOUSING, HOUSE APPLIANCES OR RELATED END-USER APPLICATIONS
- Y02B30/00—Energy efficient heating, ventilation or air conditioning [HVAC]
- Y02B30/90—Passive houses; Double facade technology
Abstract
The present invention provides a kind of novel energy saving thermal insulation material and preparation method thereof, is related to building material technical field, novel energy saving thermal insulation material includes the raw material of following parts by weight：30 40 parts of pitchstone glass bead, 37 parts of light magnesium oxide, 0.7 1.3 parts of prodan, 0.2 0.6 parts of aluminium dihydrogen phosphate, 0.2 0.6 parts of polyvinyl alcohol, 0.5 0.9 parts of kaolin, 24 parts of flyash, 24 parts of attapulgite, 10 12 parts of sepiolite powder, 13 parts of sodium sulfosuccinate, 12 14 parts of cement, 5 11 parts of aeroge, 68 parts of floating bead, 11 25 parts of scrap glass, 9 15 parts of waste polyurethane foamed plastics, discarded 12 20 parts of extruded sheet, 10 22 parts of vermiculite, 0.3 0.7 parts of heat stabilizer, 0.2 0.4 parts of retarder, 0.1 0.3 parts of binding agent, 9 13 parts of 0.2 0.4 parts of foaming agent and water；Preparation method comprises the following steps：（1）Weigh raw material,（2）Roasting vermiculite,（3）Stirring,（4）Enter mold forming and maintenance.Novel energy saving thermal insulation material produced by the present invention is provided simultaneously with compression strength height, the advantage that heat insulation property is good and environmental protection and energy saving is good.
Description
Technical field
The invention belongs to building material technical field, and in particular to a kind of novel energy saving thermal insulation material and preparation method thereof.
Background technology
With the development and the progress of science and technology of society, building trade occurs in dramatic change, especially building trade
Building material field.Current requirement of the people to construction material in terms of energy-conserving and environment-protective is very high, but energy-conservation on the market
The application effect of the construction material of environmental protection is general, and construction material due to its output it is big, cause its consumption to resource
Greatly, and now non-renewable resources are used, the increasingly depleted of renewable resource is caused.
Construction waste material is the chief component of municipal refuse, accounts for the 20%-30% of municipal refuse total amount.Only 2004 I
State just produces about 9,000,000,000 tons of building and industrial refuse, and 2010-2015 data are also far longer than this number certainly.Currently to yet to be built
Building refuse with traditional air storage, deep-cut based on landfill, although this mode treating capacity is big, convenient and simple, processing cost is low,
But substantial amounts of land resource is actually occupied, generate the environmental pollution that can not be retrieved.
Construction material is widely used big with demand due to it, and former material consumption is very big, if by construction waste material
As a part for raw material in construction material, the problem of construction material former material consumption is very big is solved well.
Construction material also requires that to lack on height, but current construction market to the performance of itself simultaneously is provided simultaneously with pressure resistance
Degree is high, the construction material that heat insulation property is good and environmental protection and energy saving is good.
The content of the invention
It is provided simultaneously with that compression strength is high, heat insulation property is good and environmental protection and energy saving to solve to lack in current construction market
It is the problem of insulation material got well, obtained it is an object of the invention to provide a kind of novel energy saving thermal insulation material and preparation method thereof
Novel energy saving thermal insulation material is provided simultaneously with compression strength height, the advantage that heat insulation property is good and environmental protection and energy saving is good.
The invention provides following technical scheme：
A kind of novel energy saving thermal insulation material, includes the raw material of following parts by weight：30-40 parts of pitchstone glass bead, lightweight oxidation
3-7 parts of magnesium, 0.7-1.3 parts of prodan, 0.2-0.6 parts of aluminium dihydrogen phosphate, 0.2-0.6 parts of polyvinyl alcohol, kaolin 0.5-0.9
Part, 2-4 parts of flyash, 2-4 parts of attapulgite, 10-12 parts of sepiolite powder, 1-3 parts of sodium sulfosuccinate, 12-14 parts of cement, gas
5-11 parts of gel, 6-8 parts of floating bead, 11-25 parts of scrap glass, 9-15 parts of waste polyurethane foamed plastics, discarded extruded sheet 12-20
Part, 10-22 parts of vermiculite, 0.3-0.7 parts of heat stabilizer, 0.2-0.4 parts of retarder, 0.1-0.3 parts of binding agent, foaming agent 0.2-
0.4 part and 9-13 parts of water.
Scrap glass, waste polyurethane foamed plastics and discarded extruded sheet, scrap glass, waste polyurethane bubble are with the addition of in raw material
Foam plastics and discarded extruded sheet are shelved on city for a long time, do not only take up urban land, and the local environment of pollution, now will be discarded
Glass and discarded styrofoam cycling and reutilization, have reached the purpose of energy-conserving and environment-protective；Scrap glass have insulation, compression strength high and
The characteristics of chemical stability is good；The flexible good, good toughness of waste polyurethane foamed plastics, compression strength height and chemical stability
It is good；Discarded extruded sheet has continuous uniform top layer and closed pore formula honeycomb, is not in space completely, is conducive to improving energy-conservation
The heat-insulating property and compressive property of insulation material.
It with the addition of aeroge in raw material, aeroge has that thermal conductivity factor is low, density is small, pliability good and fireproof advantage.
It with the addition of floating bead in raw material, floating bead has light weight, surface-closed and smooth, high intensity, wear-resisting, high temperature resistant and insulation
Heat-insulated the characteristics of.
It with the addition of vermiculite in raw material, vermiculite is a kind of natural, tasteless, nontoxic and dilatable mineral matter at high temperature,
It is calcined at a temperature of 800-1000 DEG C, volume can expand rapidly, increases 6-15 times, the vermiculite unit weight after expansion is 100-200kg/
M3, with tiny air buffer, causes it to have excellent heat-insulating property, vermiculite is in adsorptivity, sound-proofing, frost resistance in addition
It is good with being showed in fire resistance.
Preferably, the raw material of following parts by weight is included：35 parts of pitchstone glass bead, 5 parts of light magnesium oxide, prodan
1 part, 0.4 part of aluminium dihydrogen phosphate, 0.4 part of polyvinyl alcohol, 0.7 part of kaolin, 3 parts of flyash, 3 parts of attapulgite, sepiolite powder
11 parts, 2 parts of sodium sulfosuccinate, 13 parts of cement, 8 parts of aeroge, 7 parts of floating bead, 18 parts of scrap glass, waste polyurethane foam plastic
12 parts of material, discarded 16 parts of extruded sheet, 16 parts of vermiculite, 0.5 part of heat stabilizer, 0.3 part of retarder, 0.2 part of binding agent, foaming agent
0.3 part and 11 parts of water.
Preferably, the heat stabilizer is barium stearate, it is possible to increase the thermostability of novel energy saving thermal insulation material.
Preferably, the retarder is sodium pyrophosphate, the time for delaying the raw material of novel energy saving thermal insulation material to harden so that
By extend mixing time by raw material stir it is more uniform so that improve novel energy saving thermal insulation material thermal and insulating performance and
Compression strength.
Preferably, the binding agent is waterglass, and waterglass has the characteristics of caking property is strong, intensity is high and heat-resist,
Improve the intensity of novel energy saving thermal insulation material.
Preferably, the foaming agent is sodium acid carbonate, and carbon dioxide is released in heating, and foaming effect is good, it is possible to increase new
The thermal and insulating performance of energy-saving and heat-insulating material.
A kind of preparation method of novel energy saving thermal insulation material, comprises the following steps：
（1）Parts by weight according to novel energy saving thermal insulation material feedstock weigh raw material；
（2）Vermiculite is put into kiln kiln roasting 20-25min, sintering temperature is controlled at 800-1000 DEG C, produces the leech after roasting
Stone；
（3）By step（2）In roasting after vermiculite and other surplus stocks be put into mixer and stir 25-40min, produce
Mixed slurry after stirring；
（4）By step（3）In mixed slurry pour into bulk material with mould high temperature, temperature control during cast is in 180-
185 DEG C, along with vibration during cast, bulk material and mould are smoothly put into curing field together, cover plastic foil heat and moisture preserving
It is stripped after maintenance, the 3-4d that rests, carries out stacking covering wet curing.
Preferably, the step（3）In mixer be twin-shaft mixer, twin-shaft mixer has structure design conjunction
Reason, good, easy to maintenance and efficiency high the advantage of balance.
The beneficial effects of the invention are as follows：
1st, the present invention develops novel energy saving thermal insulation material, obtained novel energy saving thermal insulation material be provided simultaneously with compression strength it is high,
The advantage that heat insulation property is good and environmental protection and energy saving is good.
2nd, scrap glass, waste polyurethane foamed plastics and discarded extruded sheet are with the addition of in raw material of the invention, discards glass
Glass, waste polyurethane foamed plastics and discarded extruded sheet are shelved on city for a long time, do not only take up urban land, and pollution is local
Environment, now by scrap glass and discarded styrofoam cycling and reutilization, reached the purpose of energy-conserving and environment-protective；Scrap glass, which has, to be protected
The characteristics of temperature, compression strength height and good chemical stability；The flexible good, good toughness of waste polyurethane foamed plastics, pressure resistance
Degree is high and chemical stability is good；Discarded extruded sheet has continuous uniform top layer and closed pore formula honeycomb, is not in sky completely
Gap, is conducive to improving the heat-insulating property and compressive property of energy-saving and heat-insulating material.
3rd, it with the addition of aeroge in raw material of the invention, aeroge has that thermal conductivity factor is low, density is small, pliability good and anti-
The advantage of fire.
4th, it with the addition of floating bead in raw material of the invention, floating bead has light weight, surface-closed and smooth, high intensity, wear-resisting, resistance to
The characteristics of high temperature and insulation.
5th, vermiculite is with the addition of in raw material of the invention, vermiculite is a kind of natural, tasteless, nontoxic and dilatable at high temperature
Mineral matter, is calcined at a temperature of 800-1000 DEG C, and volume can expand rapidly, increases 6-15 times, and the vermiculite unit weight after expansion is
100-200kg/m3, with tiny air buffer, causes it to have excellent heat-insulating property, in addition vermiculite adsorptivity, every
Showed in sound, frost resistance and fire resistance good.
6th, heretofore described heat stabilizer is barium stearate, it is possible to increase the thermostability of novel energy saving thermal insulation material.
7th, heretofore described retarder be sodium pyrophosphate, the time for delaying the raw material of novel energy saving thermal insulation material to harden,
So that by extend mixing time by raw material stir it is more uniform, so as to improve the heat insulation property of novel energy saving thermal insulation material
Energy and compression strength.
8th, heretofore described binding agent is waterglass, and waterglass has the spy that caking property is strong, intensity is high and heat-resist
Point, improves the intensity of novel energy saving thermal insulation material.
9th, heretofore described foaming agent is sodium acid carbonate, and carbon dioxide is released in heating, and foaming effect is good, it is possible to increase new
The thermal and insulating performance of type energy-saving and heat-insulating material.
10th, heretofore described step（3）In mixer be twin-shaft mixer, there is twin-shaft mixer structure to set
Meter is reasonable, good, easy to maintenance and efficiency high the advantage of balance.
Embodiment
Embodiment 1
A kind of novel energy saving thermal insulation material, includes the raw material of following parts by weight：35 parts of pitchstone glass bead, light magnesium oxide 5
Part, 1 part of prodan, 0.4 part of aluminium dihydrogen phosphate, 0.4 part of polyvinyl alcohol, 0.7 part of kaolin, 3 parts of flyash, attapulgite 3
It is part, 11 parts of sepiolite powder, 2 parts of sodium sulfosuccinate, 13 parts of cement, 8 parts of aeroge, 7 parts of floating bead, 18 parts of scrap glass, discarded
12 parts of polyurethane foam plastics, discarded 16 parts of extruded sheet, 16 parts of vermiculite, 0.5 part of heat stabilizer, 0.3 part of retarder, binding agent
11 parts of 0.2 part, 0.3 part of foaming agent and water.
Scrap glass, waste polyurethane foamed plastics and discarded extruded sheet, scrap glass, waste polyurethane bubble are with the addition of in raw material
Foam plastics and discarded extruded sheet are shelved on city for a long time, do not only take up urban land, and the local environment of pollution, now will be discarded
Glass and discarded styrofoam cycling and reutilization, have reached the purpose of energy-conserving and environment-protective；Scrap glass have insulation, compression strength high and
The characteristics of chemical stability is good；The flexible good, good toughness of waste polyurethane foamed plastics, compression strength height and chemical stability
It is good；Discarded extruded sheet has continuous uniform top layer and closed pore formula honeycomb, is not in space completely, is conducive to improving energy-conservation
The heat-insulating property and compressive property of insulation material.
It with the addition of aeroge in raw material, aeroge has that thermal conductivity factor is low, density is small, pliability good and fireproof advantage.
It with the addition of floating bead in raw material, floating bead has light weight, surface-closed and smooth, high intensity, wear-resisting, high temperature resistant and insulation
Heat-insulated the characteristics of.
It with the addition of vermiculite in raw material, vermiculite is a kind of natural, tasteless, nontoxic and dilatable mineral matter at high temperature,
It is calcined at a temperature of 800-1000 DEG C, volume can expand rapidly, increases 6-15 times, the vermiculite unit weight after expansion is 100-200kg/
M3, with tiny air buffer, causes it to have excellent heat-insulating property, vermiculite is in adsorptivity, sound-proofing, frost resistance in addition
It is good with being showed in fire resistance.
Heat stabilizer is barium stearate, it is possible to increase the thermostability of novel energy saving thermal insulation material.
Retarder is sodium pyrophosphate, the time for delaying the raw material of novel energy saving thermal insulation material to harden so that stirred by extension
Mix the time by raw material stir it is more uniform, so as to improve the thermal and insulating performance and compression strength of novel energy saving thermal insulation material.
Binding agent is waterglass, and waterglass has the characteristics of caking property is strong, intensity is high and heat-resist, improves new section
The intensity of energy insulation material.
Foaming agent is sodium acid carbonate, and carbon dioxide is released in heating, and foaming effect is good, it is possible to increase novel energy saving thermal insulation material
Thermal and insulating performance.
A kind of preparation method of novel energy saving thermal insulation material, comprises the following steps：
（1）Parts by weight according to novel energy saving thermal insulation material feedstock weigh raw material；
（2）Vermiculite is put into kiln kiln roasting 20-25min, sintering temperature is controlled at 800-1000 DEG C, produces the leech after roasting
Stone；
（3）By step（2）In roasting after vermiculite and other surplus stocks be put into mixer and stir 25-40min, produce
Mixed slurry after stirring；
（4）By step（3）In mixed slurry pour into bulk material with mould high temperature, temperature control during cast is in 180-
185 DEG C, along with vibration during cast, bulk material and mould are smoothly put into curing field together, cover plastic foil heat and moisture preserving
It is stripped after maintenance, the 3-4d that rests, carries out stacking covering wet curing.
Step（3）In mixer be twin-shaft mixer, twin-shaft mixer has reasonable in design, balance
The good, advantage of easy to maintenance and efficiency high.
Embodiment 2
A kind of novel energy saving thermal insulation material, includes the raw material of following parts by weight：30 parts of pitchstone glass bead, light magnesium oxide 3
Part, 0.7 part of prodan, 0.2 part of aluminium dihydrogen phosphate, 0.2 part of polyvinyl alcohol, 0.5 part of kaolin, 2 parts of flyash, attapulgite
2 parts, it is 10 parts of sepiolite powder, 1 part of sodium sulfosuccinate, 12 parts of cement, 5 parts of aeroge, 6 parts of floating bead, 11 parts of scrap glass, discarded
9 parts of polyurethane foam plastics, discarded 12 parts of extruded sheet, 10 parts of vermiculite, 0.3 part of heat stabilizer, 0.2 part of retarder, binding agent 0.1
9 parts of part, 0.2 part of foaming agent and water.
Scrap glass, waste polyurethane foamed plastics and discarded extruded sheet, scrap glass, waste polyurethane bubble are with the addition of in raw material
Foam plastics and discarded extruded sheet are shelved on city for a long time, do not only take up urban land, and the local environment of pollution, now will be discarded
Glass and discarded styrofoam cycling and reutilization, have reached the purpose of energy-conserving and environment-protective；Scrap glass have insulation, compression strength high and
The characteristics of chemical stability is good；The flexible good, good toughness of waste polyurethane foamed plastics, compression strength height and chemical stability
It is good；Discarded extruded sheet has continuous uniform top layer and closed pore formula honeycomb, is not in space completely, is conducive to improving energy-conservation
The heat-insulating property and compressive property of insulation material.
It with the addition of aeroge in raw material, aeroge has that thermal conductivity factor is low, density is small, pliability good and fireproof advantage.
It with the addition of floating bead in raw material, floating bead has light weight, surface-closed and smooth, high intensity, wear-resisting, high temperature resistant and insulation
Heat-insulated the characteristics of.
It with the addition of vermiculite in raw material, vermiculite is a kind of natural, tasteless, nontoxic and dilatable mineral matter at high temperature,
It is calcined at a temperature of 800-1000 DEG C, volume can expand rapidly, increases 6-15 times, the vermiculite unit weight after expansion is 100-200kg/
M3, with tiny air buffer, causes it to have excellent heat-insulating property, vermiculite is in adsorptivity, sound-proofing, frost resistance in addition
It is good with being showed in fire resistance.
Heat stabilizer is barium stearate, it is possible to increase the thermostability of novel energy saving thermal insulation material.
Retarder is sodium pyrophosphate, the time for delaying the raw material of novel energy saving thermal insulation material to harden so that stirred by extension
Mix the time by raw material stir it is more uniform, so as to improve the thermal and insulating performance and compression strength of novel energy saving thermal insulation material.
Binding agent is waterglass, and waterglass has the characteristics of caking property is strong, intensity is high and heat-resist, improves new section
The intensity of energy insulation material.
Foaming agent is sodium acid carbonate, and carbon dioxide is released in heating, and foaming effect is good, it is possible to increase novel energy saving thermal insulation material
Thermal and insulating performance.
A kind of preparation method of novel energy saving thermal insulation material, comprises the following steps：
（1）Parts by weight according to novel energy saving thermal insulation material feedstock weigh raw material；
（2）Vermiculite is put into kiln kiln roasting 20-25min, sintering temperature is controlled at 800-1000 DEG C, produces the leech after roasting
Stone；
（3）By step（2）In roasting after vermiculite and other surplus stocks be put into mixer and stir 25-40min, produce
Mixed slurry after stirring；
（4）By step（3）In mixed slurry pour into bulk material with mould high temperature, temperature control during cast is in 180-
185 DEG C, along with vibration during cast, bulk material and mould are smoothly put into curing field together, cover plastic foil heat and moisture preserving
It is stripped after maintenance, the 3-4d that rests, carries out stacking covering wet curing.
Step（3）In mixer be twin-shaft mixer, twin-shaft mixer has reasonable in design, balance
The good, advantage of easy to maintenance and efficiency high.
Embodiment 3
A kind of novel energy saving thermal insulation material, includes the raw material of following parts by weight：40 parts of pitchstone glass bead, light magnesium oxide 7
Part, 1.3 parts of prodan, 0.6 part of aluminium dihydrogen phosphate, 0.6 part of polyvinyl alcohol, 0.9 part of kaolin, 4 parts of flyash, attapulgite
4 parts, it is 12 parts of sepiolite powder, 3 parts of sodium sulfosuccinate, 14 parts of cement, 11 parts of aeroge, 8 parts of floating bead, 25 parts of scrap glass, useless
Abandon 15 parts of polyurethane foam plastics, discarded 20 parts of extruded sheet, 22 parts of vermiculite, 0.7 part of heat stabilizer, 0.4 part of retarder, binding agent
13 parts of 0.3 part, 0.4 part of foaming agent and water.
Scrap glass, waste polyurethane foamed plastics and discarded extruded sheet, scrap glass, waste polyurethane bubble are with the addition of in raw material
Foam plastics and discarded extruded sheet are shelved on city for a long time, do not only take up urban land, and the local environment of pollution, now will be discarded
Glass and discarded styrofoam cycling and reutilization, have reached the purpose of energy-conserving and environment-protective；Scrap glass have insulation, compression strength high and
The characteristics of chemical stability is good；The flexible good, good toughness of waste polyurethane foamed plastics, compression strength height and chemical stability
It is good；Discarded extruded sheet has continuous uniform top layer and closed pore formula honeycomb, is not in space completely, is conducive to improving energy-conservation
The heat-insulating property and compressive property of insulation material.
It with the addition of aeroge in raw material, aeroge has that thermal conductivity factor is low, density is small, pliability good and fireproof advantage.
It with the addition of floating bead in raw material, floating bead has light weight, surface-closed and smooth, high intensity, wear-resisting, high temperature resistant and insulation
Heat-insulated the characteristics of.
It with the addition of vermiculite in raw material, vermiculite is a kind of natural, tasteless, nontoxic and dilatable mineral matter at high temperature,
It is calcined at a temperature of 800-1000 DEG C, volume can expand rapidly, increases 6-15 times, the vermiculite unit weight after expansion is 100-200kg/
M3, with tiny air buffer, causes it to have excellent heat-insulating property, vermiculite is in adsorptivity, sound-proofing, frost resistance in addition
It is good with being showed in fire resistance.
Heat stabilizer is barium stearate, it is possible to increase the thermostability of novel energy saving thermal insulation material.
Retarder is sodium pyrophosphate, the time for delaying the raw material of novel energy saving thermal insulation material to harden so that stirred by extension
Mix the time by raw material stir it is more uniform, so as to improve the thermal and insulating performance and compression strength of novel energy saving thermal insulation material.
Binding agent is waterglass, and waterglass has the characteristics of caking property is strong, intensity is high and heat-resist, improves new section
The intensity of energy insulation material.
Foaming agent is sodium acid carbonate, and carbon dioxide is released in heating, and foaming effect is good, it is possible to increase novel energy saving thermal insulation material
Thermal and insulating performance.
A kind of preparation method of novel energy saving thermal insulation material, comprises the following steps：
（1）Parts by weight according to novel energy saving thermal insulation material feedstock weigh raw material；
（2）Vermiculite is put into kiln kiln roasting 20-25min, sintering temperature is controlled at 800-1000 DEG C, produces the leech after roasting
Stone；
（3）By step（2）In roasting after vermiculite and other surplus stocks be put into mixer and stir 25-40min, produce
Mixed slurry after stirring；
（4）By step（3）In mixed slurry pour into bulk material with mould high temperature, temperature control during cast is in 180-
185 DEG C, along with vibration during cast, bulk material and mould are smoothly put into curing field together, cover plastic foil heat and moisture preserving
It is stripped after maintenance, the 3-4d that rests, carries out stacking covering wet curing.
Step（3）In mixer be twin-shaft mixer, twin-shaft mixer has reasonable in design, balance
The good, advantage of easy to maintenance and efficiency high.
Comparative example 1
A kind of insulation material, includes the raw material of following parts by weight：50 parts of pitchstone glass bead, 6 parts of light magnesium oxide, fluosilicic acid
1.1 parts of sodium, 1 part of aluminium dihydrogen phosphate, 0.4 part of polyvinyl alcohol, 0.8 part of kaolin, 2.4 parts of flyash, 3 parts of attapulgite, Hai Pao
9 parts of 16 parts of stone flour, 1.4 parts of sodium sulfosuccinate, 16 parts of cement and water.
A kind of preparation method of insulation material, comprises the following steps：
（1）Parts by weight according to insulation material raw material weigh raw material；
（2）Raw material is put into mixer and stirs 30-40min, the mixed slurry after stirring is produced；
（3）By step（2）In mixed slurry pour into bulk material with mould high temperature, temperature control during cast is in 180-
190 DEG C, along with vibration during cast, bulk material and mould are smoothly put into curing field together, cover plastic foil heat and moisture preserving
It is stripped after maintenance, the 3-4d that rests, carries out stacking covering wet curing.
Embodiment 1, embodiment 2 and embodiment 3 are made in novel energy saving thermal insulation material and comparative example 1 into obtained insulation material to enter
Row performance test, test result is as shown in table 1：
| Index | Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example 1 |
| Compression strength（Mpa） | 35.6 | 30.2 | 26.1 | 20.3 |
| Thermal conductivity factor（W/m ﹒ k） | 0.025 | 0.029 | 0.032 | 0.049 |
| Material loss slip（%） | 26 | 24 | 21 | 0 |
From the data of table 1 compare as can be seen that it is an advantage of the invention that：
1st, a kind of novel energy saving thermal insulation material and preparation method thereof, from the compression strength measured as can be seen that embodiment 1-3's is anti-
Compressive Strength is above comparative example 1, illustrates that the compression strength of novel energy saving thermal insulation material of the present invention is high.
2nd, a kind of novel energy saving thermal insulation material and preparation method thereof, from the thermal conductivity factor measured as can be seen that embodiment 1-3
Thermal conductivity factor be below comparative example 1, illustrate the high insulating effect of novel energy saving thermal insulation material of the present invention.
3rd, a kind of novel energy saving thermal insulation material and preparation method thereof, reality is can be seen that from the material loss slip measured
The material loss slip for applying a 1-3 is above comparative example 1, illustrates the good energy saving property of novel energy saving thermal insulation material of the present invention.
4th, a kind of novel energy saving thermal insulation material and preparation method thereof, reality is can be seen that from the data of each index measured
Apply example 1 and be superior to embodiment 2, embodiment 3 and comparative example 1, illustrate the composition of raw materials and system of novel energy saving thermal insulation material of the present invention
The reasonability of Preparation Method.
The preferred embodiments of the present invention are the foregoing is only, are not intended to limit the invention, although with reference to foregoing reality
Apply example the present invention is described in detail, for those skilled in the art, it still can be to foregoing each implementation
Technical scheme described in example is modified, or equivalent substitution, all essences in the present invention are carried out to which part technical characteristic
God is with principle, and any modification, equivalent substitution and improvements made etc. should be included in the scope of the protection.
Claims (8)
1. a kind of novel energy saving thermal insulation material, it is characterised in that include the raw material of following parts by weight：Pitchstone glass bead 30-
40 parts, 3-7 parts of light magnesium oxide, 0.7-1.3 parts of prodan, 0.2-0.6 parts of aluminium dihydrogen phosphate, 0.2-0.6 parts of polyvinyl alcohol,
0.5-0.9 parts of kaolin, 2-4 parts of flyash, 2-4 parts of attapulgite, 10-12 parts of sepiolite powder, 1-3 parts of sodium sulfosuccinate,
12-14 parts of cement, 5-11 parts of aeroge, 6-8 parts of floating bead, 11-25 parts of scrap glass, 9-15 parts of waste polyurethane foamed plastics,
Discarded 12-20 parts of extruded sheet, 10-22 parts of vermiculite, 0.3-0.7 parts of heat stabilizer, 0.2-0.4 parts of retarder, binding agent 0.1-0.3
9-13 parts of part, 0.2-0.4 parts of foaming agent and water.
2. novel energy saving thermal insulation material according to claim 1, it is characterised in that include the raw material of following parts by weight：Pine
35 parts of fat rock glass bead, 5 parts of light magnesium oxide, 1 part of prodan, 0.4 part of aluminium dihydrogen phosphate, 0.4 part of polyvinyl alcohol, kaolinite
0.7 part of soil, 3 parts of flyash, 3 parts of attapulgite, 11 parts of sepiolite powder, 2 parts of sodium sulfosuccinate, 13 parts of cement, aeroge 8
It is part, 7 parts of floating bead, 18 parts of scrap glass, 12 parts of waste polyurethane foamed plastics, discarded 16 parts of extruded sheet, 16 parts of vermiculite, thermally-stabilised
11 parts of 0.5 part of agent, 0.3 part of retarder, 0.2 part of binding agent, 0.3 part of foaming agent and water.
3. novel energy saving thermal insulation material according to claim 1, it is characterised in that：The heat stabilizer is barium stearate.
4. novel energy saving thermal insulation material according to claim 1, it is characterised in that：The retarder is sodium pyrophosphate.
5. novel energy saving thermal insulation material according to claim 1, it is characterised in that：The binding agent is waterglass.
6. novel energy saving thermal insulation material according to claim 1, it is characterised in that：The foaming agent is sodium acid carbonate.
7. a kind of preparation method of novel energy saving thermal insulation material as described in claim 1-6 any one, it is characterised in that
Comprise the following steps：
（1）Parts by weight according to novel energy saving thermal insulation material feedstock weigh raw material；
（2）Vermiculite is put into kiln kiln roasting 20-25min, sintering temperature is controlled at 800-1000 DEG C, produces the leech after roasting
Stone；
（3）By step（2）In roasting after vermiculite and other surplus stocks be put into mixer and stir 25-40min, produce
Mixed slurry after stirring；
（4）By step（3）In mixed slurry pour into bulk material with mould high temperature, temperature control during cast is in 180-
185 DEG C, along with vibration during cast, bulk material and mould are smoothly put into curing field together, cover plastic foil heat and moisture preserving
It is stripped after maintenance, the 3-4d that rests, carries out stacking covering wet curing.
8. novel energy saving thermal insulation material according to claim 7, it is characterised in that：The step（3）In mixer be
Twin-shaft mixer.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108483996A (en) * | 2018-04-09 | 2018-09-04 | 合肥聪亨新型建材科技有限公司 | A kind of corrosion-resistant thermal insulation material of construction wall and preparation method thereof |
| CN108863284A (en) * | 2018-07-19 | 2018-11-23 | 张建 | A kind of heat preservation construction material and preparation method thereof containing waste |
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| CN101921091A (en) * | 2010-06-29 | 2010-12-22 | 上海大学 | Method for preparing thermal-insulation material for dry powder from waste polyurethane foamed plastics |
| CN102617110A (en) * | 2012-03-22 | 2012-08-01 | 天津市庆顺海蓝建材科技发展有限公司 | Inorganic active building heat insulating material |
| CN103449772A (en) * | 2013-08-09 | 2013-12-18 | 广西青龙化学建材有限公司 | Thermal insulating material and preparation method thereof |
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| CN101468906A (en) * | 2007-12-27 | 2009-07-01 | 上海暄洋化工材料科技有限公司 | SiO2 enriched nano composite inorganic flame-retardant heat insulating thermal preserving board and manufacturing process thereof |
| CN101456712A (en) * | 2008-12-29 | 2009-06-17 | 俞锡贤 | Inorganic mineral earth surface insulating mortar |
| CN101921091A (en) * | 2010-06-29 | 2010-12-22 | 上海大学 | Method for preparing thermal-insulation material for dry powder from waste polyurethane foamed plastics |
| CN102617110A (en) * | 2012-03-22 | 2012-08-01 | 天津市庆顺海蓝建材科技发展有限公司 | Inorganic active building heat insulating material |
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| CN108483996A (en) * | 2018-04-09 | 2018-09-04 | 合肥聪亨新型建材科技有限公司 | A kind of corrosion-resistant thermal insulation material of construction wall and preparation method thereof |
| CN108863284A (en) * | 2018-07-19 | 2018-11-23 | 张建 | A kind of heat preservation construction material and preparation method thereof containing waste |
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Application publication date: 20170818 |