CN107028787A - Water lock moisture saver mask and preparation method containing theanine - Google Patents

Water lock moisture saver mask and preparation method containing theanine Download PDF

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Publication number
CN107028787A
CN107028787A CN201710454668.7A CN201710454668A CN107028787A CN 107028787 A CN107028787 A CN 107028787A CN 201710454668 A CN201710454668 A CN 201710454668A CN 107028787 A CN107028787 A CN 107028787A
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Prior art keywords
water
extract
theanine
added
compatibile
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CN201710454668.7A
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Chinese (zh)
Inventor
吴婧
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Hangzhou Grass Biotechnology Co Ltd
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Hangzhou Grass Biotechnology Co Ltd
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Priority to CN201710454668.7A priority Critical patent/CN107028787A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/42Amides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Dermatology (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Cosmetics (AREA)

Abstract

The present invention relates to face skin nursing product, it is desirable to provide a kind of water lock moisture saver mask and preparation method containing theanine.This method includes:Theanine, tremella polysaccharides, compatibile extract and aloe barbadensis Miller leaf extract are added in sterilized water, dissolving is mixed;Glycerine, butanediol, panthenol, Sodium Hyaluronate are added in appropriate amounts of sterilized water in the lump, double imidazolidinyl urea is added after stirring and evenly mixing and is heated;Two kinds of liquid are mixed, are stirring evenly and then adding into the sterilized water of fructose, Fructus Hordei Germinatus oligose glucoside, carbomer, allantoin, EDETATE SODIUM and surplus, are evenly stirred until in gel, as product.Theanine in the present invention can be relaxed one's muscles with calm nerves, and theanine small molecule characteristic can rapid osmotic skin surface, absorbed by deep layer;Realize that nutrient molecule and moisturizing factor in compatibile and Aloe Barbadensis Miller are separately enriched with and are used in combination;Facial mask is by scientific composition, and trophic factors enriches, with efficient water lock moistening effect.

Description

Water lock moisture saver mask and preparation method containing theanine
Technical field
The present invention relates to face skin nursing product, and in particular to a kind of water lock moisture saver mask and preparation side containing theanine Method.
Background technology
Facial mask is as the important class of cosmetic kind, the key player played the part of in face skin nursing.When facial mask is applied When on the face, face skin with external environment condition is of short duration isolates, between facial mask in the environment of relative closure, skin temperature all goes out Now certain rising, promotes facial pores to expand, and accelerates sweat gland secretion and metabolism, promotes skin metabolism product and grease to add Fast discharge, while the moisture and nutrient in facial mask can penetrate into the cuticula of epidermis, makes skin moisture content quickly increase, becomes It is soft and bright.Although with scientific and technological progress, the feature facial mask such as all kinds of whitenings, nti-freckle emerges in an endless stream, however, facial mask is the most It is important that promoting facial moisture absorption.Therefore, water lock moistening effect is most important for facial mask quality.
Existing various mask products containing plant extracts at present, but plant extracts contained by these facial masks is mostly Whole water soluble ingredients are simply simply extracted, the functional component in plant is not finely divided and is enriched with, simultaneously for Concertedness and complementary consideration are not enough between all kinds of active components of plants.
The content of the invention
The technical problem to be solved in the present invention is to overcome that of the prior art not enough there is provided a kind of water lock containing theanine Moisture saver mask and preparation method.
To solve technical problem, solution of the invention is:
A kind of water lock moisture saver mask containing theanine is provided, is made up of the component of following mass percents:
In the present invention, the preparation method of the compatibile extract is:By dry compatibile with 1: 8/g: ml Mass volume ratio example adds concentration in 85% ethanol water, 30min is extracted at 50 DEG C;Obtained after filtering alcohol extract and Filter residue, concentrates and reclaims ethanol, obtain alcohol extracting concentrate;Filter residue is added in 100 DEG C of water with 1: 10/g: ml mass volume ratio example, It is continuous to extract 2 times, merge aqueous extract after 25min, filtering are extracted every time;Aqueous extract carries out segmentation with 100,000 dalton films and oozed Thoroughly, segmentation is retained into partial concentration, obtains water extracting liquid;It is spray-dried after alcohol extracting concentrate is merged with water extracting liquid, Obtain compatibile extract.
In the present invention, the preparation method of the aloe barbadensis Miller leaf extract is:By dry Aloe Barbadensis Miller with 1: It is 85% ethanol water that 10/g: ml mass volume ratio example, which adds concentration, and 30min is extracted at 50 DEG C;Alcohol is obtained after filtering Extract solution and filter residue, concentrate and reclaim ethanol, obtain alcohol extracting concentrate;Filter residue adds 100 with 1: 10/g: ml mass volume ratio example It is continuous to extract 2 times in DEG C water, merge aqueous extract after 25min, filtering are extracted every time;Aqueous extract is carried out with 50,000 dalton films Segmentation infiltration, retains partial concentration by segmentation, obtains water extracting liquid;Sprayed after alcohol extracting concentrate is merged with water extracting liquid Dry, that is, obtain Aloe Barbadensis Miller extract.
In the present invention, the purity of the theanine is more than 98%;The purity of tremella polysaccharides is that molecular weight is more than 80% 200000-200 ten thousand dalton.
Invention further provides the preparation method of the water lock moisture saver mask containing theanine, comprise the following steps:
(1) each raw material components are weighed by the proportion relation;
(2) theanine, tremella polysaccharides, compatibile extract and aloe barbadensis Miller leaf extract are added into appropriate nothing in the lump In bacterium water, fully dissolving is mixed;
(3) glycerine, butanediol, panthenol, Sodium Hyaluronate are added in appropriate amounts of sterilized water in the lump, stirred and evenly mixed;Then plus Enter double imidazolidinyl urea, and be heated to 60 DEG C;
(3) liquid obtained by step (2) and (3) is mixed, stirred;Then fructose, Fructus Hordei Germinatus oligose glucoside, card are added Ripple nurse, allantoin, the sterilized water of EDETATE SODIUM and surplus, are evenly stirred until in gel;
(4) it will be bottled obtained by step (3) in gelatinous product.
The application method of product of the present invention:
Clean face will be uniformly applied in gelatinous product, smearing thickness is between 0.05~0.3mm.At room temperature Taken off after waiting 20-30min, without cleaning again.Using once, skin of face can be seen in continuous use more than 3 times within 2 days Smoothness and elasticity have clear improvement.
Realization principle description of the present invention:
In the present invention:
The action principle of each component is respectively:Theanine is topmost amino acid in tealeaves, makes one excited with caffeine Difference, theanine can be relaxed one's muscles with calm nerves, and the small molecule characteristic of theanine can rapid osmotic skin table Layer, is absorbed by deep layer;Flavones, phenols, anthraquinone in compatibile, Aloe Barbadensis Miller are extracted by (50 DEG C) orientations of ethanol low temperature There is anti-oxidant, suppression tyrosinase activity Deng small-molecule active substance, accelerate cell metabolism isoreactivity, while easily being inhaled by skin Receive;Retaining compatibile, the macromolecule polysaccharide in Aloe Barbadensis Miller and tremella polysaccharides prepared by means using film not only can be with Skin nutrition is provided, moisture loss can also be blocked in skin formation diaphragm.In addition, theanine and compatibile, Curacao Small-molecule substance in Chinese aloe leaf has synergy, can promote loosening all muscles, accelerates facial metabolin and excludes, promotes nutrient Absorb, further enhancing the effect that facial mask keeps moisture and nutrition skin of face.
Compared with prior art, the beneficial effects of the present invention are:
(1) theanine can be relaxed one's muscles with calm nerves, and the small molecule characteristic of theanine can rapid osmotic skin Skin top layer, is absorbed by deep layer;
(2) using orientation abstraction technique, i.e., compatibile and Aloe Barbadensis Miller small molecular activity are extracted using ethanol Material:Polyphenol, flavones, anthraquinone, vitamin etc., and using water extraction UF membrane retention high molecular polysaccharide material, realize great Ye seas Nutrient molecule and moisturizing factor in algae and Aloe Barbadensis Miller are separately enriched with and are used in combination;
(3) facial mask of the present invention is by scientific composition, and trophic factors enriches, with efficient water lock moistening effect.
Embodiment
In the present invention, constituent part directly purchased in market can be obtained, such as theanine, tremella polysaccharides, fructose, Fructus Hordei Germinatus oligose glucose Glycosides, glycerine, butanediol, panthenol, Sodium Hyaluronate, carbomer, double imidazolidinyl urea, allantoin, EDETATE SODIUM;Sterilized water can lead to Cross conventional laboratory methods preparation.Wherein, the purity of theanine is more than 98%;The purity of tremella polysaccharides is, more than 80%, to divide Son amount is 200,000-200 ten thousand dalton.
In the present invention, the preparation method of constituent part is described as follows:
The preparation method of compatibile extract is:Dry compatibile is added with 1: 8/g: ml mass volume ratio example Enter concentration in 85% ethanol water, 30min is extracted at 50 DEG C;Alcohol extract and filter residue are obtained after filtering, concentrates and returns Ethanol is received, alcohol extracting concentrate is obtained;Filter residue is added in 100 DEG C of water with 1: 10/g: ml mass volume ratio example, continuously extraction 2 times, often Secondary extraction 25min, merges aqueous extract after filtering;Aqueous extract carries out segmentation infiltration with 100,000 dalton films, and segmentation is retained Partial concentration, obtains water extracting liquid;It is spray-dried after alcohol extracting concentrate is merged with water extracting liquid, that is, obtains compatibile Extract.
The preparation method of aloe barbadensis Miller leaf extract is:By dry Aloe Barbadensis Miller with 1: 10/g: ml quality It is 85% ethanol water that volume ratio, which adds concentration, and 30min is extracted at 50 DEG C;Alcohol extract and filter residue are obtained after filtering, Concentrate and reclaim ethanol, obtain alcohol extracting concentrate;Filter residue is added in 100 DEG C of water with 1: 10/g: ml mass volume ratio example, is continuously carried Take 2 times, merge aqueous extract after 25min, filtering are extracted every time;Aqueous extract carries out segmentation infiltration with 50,000 dalton films, will divide Section retention partial concentration, obtains water extracting liquid;It is spray-dried after alcohol extracting concentrate is merged with water extracting liquid, that is, obtains storehouse Drag-line Folium Aloe extract.
Embodiment 1
(1) theanine 1kg, tremella polysaccharides 0.5kg, compatibile extract 1.5kg, aloe barbadensis Miller leaf extract are taken 2kg, is added in appropriate amounts of sterilized water in the lump, and fully dissolving is mixed;
(2) glycerine 5kg, butanediol 3kg, panthenol 1kg, Sodium Hyaluronate 0.05kg are taken, is added in the lump in appropriate amounts of sterilized water, Stir and evenly mix;Then double imidazolidinyl urea 0.05kg is added, and is heated to 60 DEG C;
(3) liquid obtained by step (2) and (3) is mixed, stirred;Then fructose 0.5kg, Fructus Hordei Germinatus oligose glucose are added Glycosides 0.05kg, carbomer 0.08kg, allantoin 0.1kg, EDETATE SODIUM 0.01kg, plus sterilized water to gross mass are 100kg, stirring Uniform is extremely in gel;
(4) it will be bottled obtained by step (3) in gelatinous product.
Embodiment 2
(1) theanine 10kg, tremella polysaccharides 3kg, compatibile extract 3kg, aloe barbadensis Miller leaf extract are taken 0.1kg, is added in appropriate amounts of sterilized water in the lump, and fully dissolving is mixed;
(2) glycerine 10kg, butanediol 8kg, panthenol 3kg, Sodium Hyaluronate 0.1kg are taken, is added in the lump in appropriate amounts of sterilized water, Stir and evenly mix;Then double imidazolidinyl urea 0.1kg is added, and is heated to 60 DEG C;
(3) liquid obtained by step (2) and (3) is mixed, stirred;Then fructose 1kg, Fructus Hordei Germinatus oligose glucoside are added 0.2kg, carbomer 0.2kg, allantoin 0.3kg, EDETATE SODIUM 0.05kg, plus sterilized water to gross mass is 100kg, is stirred To in gel;
(4) it will be bottled obtained by step (3) in gelatinous product.
Embodiment 3
(1) theanine 6kg, tremella polysaccharides 1.5kg, compatibile extract 0.5kg, aloe barbadensis Miller leaf extract are taken 1.5kg, is added in appropriate amounts of sterilized water in the lump, and fully dissolving is mixed;
(2) glycerine 7kg, butanediol 5kg, panthenol 2kg, Sodium Hyaluronate 0.08kg are taken, is added in the lump in appropriate amounts of sterilized water, Stir and evenly mix;Then double imidazolidinyl urea 0.08kg is added, and is heated to 60 DEG C;
(3) liquid obtained by step (2) and (3) is mixed, stirred;Then fructose 0.8kg, Fructus Hordei Germinatus oligose glucose are added Glycosides 0.1kg, carbomer 0.12kg, allantoin 0.2kg, EDETATE SODIUM 0.03kg, plus sterilized water to gross mass are 100kg, stirring Uniform is extremely in gel;
(4) it will be bottled obtained by step (3) in gelatinous product.
Moistening effect is tested
Test crowd:There is the people of female volunteers 100 being periodically accustomed to using facial mask.
Application method:Clean after face, clean face will be uniformly applied in gelatinous product, smearing thickness exists Between 0.05~0.3mm.Taken off at room temperature after waiting 20-30min, without cleaning again.Use once within 2 days, continuously using 3 It is secondary.
Therapeutic evaluation:To facial skin smoothness and Appreciation gist of the elastic improvement situation as moistening effect, with full marks 10 points of scoring mechanism, is given a mark by tester to facial mask.Test result is shown in Table 1.
The facial mask moistening effect of table 1 is tested
10 points 9 points 8 points 7 points 6 points 5-0 points
27 people 48 people 19 people 4 people 2 people 0 people
From test result, most users accept very much to the moistening effect of facial mask of the present invention.
Finally, in addition it is also necessary to it is to be noted that, it is clear that the invention is not restricted to above example, can also there are many deformations, ability All deformations that the those of ordinary skill in domain directly can export or associate from present disclosure, are considered as this hair Bright protection domain.

Claims (5)

1. a kind of water lock moisture saver mask containing theanine, it is characterised in that be made up of the component of following mass percents:
2. the water lock moisture saver mask according to claim 1 containing theanine, it is characterised in that the compatibile extract Preparation method be:Dry compatibile is added into concentration as 85% ethanol water using 1: 8/g: ml mass volume ratio example In, extract 30min at 50 DEG C;Alcohol extract and filter residue are obtained after filtering, concentrates and reclaims ethanol, obtain alcohol extracting concentrate;Filter Slag is added in 100 DEG C of water with 1: 10/g: ml mass volume ratio example, continuous to extract 2 times, and 25min is extracted every time, is merged after filtering Aqueous extract;Aqueous extract carries out segmentation infiltration with 100,000 dalton films, and segmentation is retained into partial concentration, obtains water extraction concentration Liquid;It is spray-dried after alcohol extracting concentrate is merged with water extracting liquid, that is, obtains compatibile extract.
3. the water lock moisture saver mask according to claim 1 containing theanine, it is characterised in that the Aloe Barbadensis Miller is carried The preparation method for taking thing is:Dry Aloe Barbadensis Miller is added into concentration as 85% using 1: 10/g: ml mass volume ratio example Ethanol water, 30min is extracted at 50 DEG C;Alcohol extract and filter residue are obtained after filtering, concentrates and reclaims ethanol, obtain alcohol concentrate Contracting liquid;Filter residue is added in 100 DEG C of water with 1: 10/g: ml mass volume ratio example, continuous to extract 2 times, and 25min, mistake are extracted every time Merge aqueous extract after filter;Aqueous extract carries out segmentation infiltration with 50,000 dalton films, and segmentation is retained into partial concentration, water is obtained Carry concentrate;It is spray-dried after alcohol extracting concentrate is merged with water extracting liquid, that is, obtains Aloe Barbadensis Miller extract.
4. the water lock moisture saver mask according to claim 1 containing theanine, it is characterised in that the purity of the theanine is More than 98%;The purity of tremella polysaccharides is that, more than 80%, molecular weight is 200,000-200 ten thousand dalton.
5. the preparation method of the water lock moisture saver mask containing theanine described in Claims 1-4 any one, it is characterised in that Comprise the following steps:
(1) each raw material components are weighed by the proportion relation;
(2) theanine, tremella polysaccharides, compatibile extract and aloe barbadensis Miller leaf extract are added into appropriate amounts of sterilized water in the lump In, fully dissolving is mixed;
(3) glycerine, butanediol, panthenol, Sodium Hyaluronate are added in appropriate amounts of sterilized water in the lump, stirred and evenly mixed;Then add double Imidazolidinyl urea, and it is heated to 60 DEG C;
(3) liquid obtained by step (2) and (3) is mixed, stirred;Then fructose, Fructus Hordei Germinatus oligose glucoside, card ripple are added Nurse, allantoin, the sterilized water of EDETATE SODIUM and surplus, are evenly stirred until in gel;
(4) it will be bottled obtained by step (3) in gelatinous product.
CN201710454668.7A 2017-06-16 2017-06-16 Water lock moisture saver mask and preparation method containing theanine Pending CN107028787A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108272655A (en) * 2018-03-15 2018-07-13 广州普立森生物科技有限公司 The high moisture saver mask Essence of tremella polysaccharides and facial mask and preparation method thereof
CN108542810A (en) * 2018-06-30 2018-09-18 义乌市商立生物科技有限公司 A kind of preparation method suitable for face skin nursing agent
CN108685809A (en) * 2018-06-19 2018-10-23 江苏德和生物科技有限公司 Whitening emulsion and preparation method thereof
CN109157452A (en) * 2018-10-17 2019-01-08 广州市雅彩盛生物科技有限公司 A kind of disposable sleep mask of plant extracts containing theanine

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101732228A (en) * 2010-02-01 2010-06-16 云南龙润茶业集团有限公司 Tea facial mask and preparation method thereof
CN106176551A (en) * 2016-08-30 2016-12-07 徐媛媛 Moisturizing face mask of traditional Chinese medicine and preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101732228A (en) * 2010-02-01 2010-06-16 云南龙润茶业集团有限公司 Tea facial mask and preparation method thereof
CN106176551A (en) * 2016-08-30 2016-12-07 徐媛媛 Moisturizing face mask of traditional Chinese medicine and preparation method thereof

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108272655A (en) * 2018-03-15 2018-07-13 广州普立森生物科技有限公司 The high moisture saver mask Essence of tremella polysaccharides and facial mask and preparation method thereof
CN108685809A (en) * 2018-06-19 2018-10-23 江苏德和生物科技有限公司 Whitening emulsion and preparation method thereof
CN108542810A (en) * 2018-06-30 2018-09-18 义乌市商立生物科技有限公司 A kind of preparation method suitable for face skin nursing agent
CN109157452A (en) * 2018-10-17 2019-01-08 广州市雅彩盛生物科技有限公司 A kind of disposable sleep mask of plant extracts containing theanine

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Application publication date: 20170811