CN106879749A - 包含dha和epa的有机乳液 - Google Patents
包含dha和epa的有机乳液 Download PDFInfo
- Publication number
- CN106879749A CN106879749A CN201710085116.3A CN201710085116A CN106879749A CN 106879749 A CN106879749 A CN 106879749A CN 201710085116 A CN201710085116 A CN 201710085116A CN 106879749 A CN106879749 A CN 106879749A
- Authority
- CN
- China
- Prior art keywords
- emulsion
- dha
- tocopherol
- acid
- gross weight
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000839 emulsion Substances 0.000 title claims abstract description 57
- JAZBEHYOTPTENJ-JLNKQSITSA-N all-cis-5,8,11,14,17-icosapentaenoic acid Chemical compound CC\C=C/C\C=C/C\C=C/C\C=C/C\C=C/CCCC(O)=O JAZBEHYOTPTENJ-JLNKQSITSA-N 0.000 claims abstract description 16
- 235000020673 eicosapentaenoic acid Nutrition 0.000 claims abstract description 16
- 229960005135 eicosapentaenoic acid Drugs 0.000 claims abstract description 16
- JAZBEHYOTPTENJ-UHFFFAOYSA-N eicosapentaenoic acid Natural products CCC=CCC=CCC=CCC=CCC=CCCCC(O)=O JAZBEHYOTPTENJ-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000000203 mixture Substances 0.000 claims abstract description 12
- QAQJMLQRFWZOBN-LAUBAEHRSA-N L-ascorbyl-6-palmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](O)[C@H]1OC(=O)C(O)=C1O QAQJMLQRFWZOBN-LAUBAEHRSA-N 0.000 claims abstract description 6
- 239000011786 L-ascorbyl-6-palmitate Substances 0.000 claims abstract description 6
- 235000010385 ascorbyl palmitate Nutrition 0.000 claims abstract description 6
- 235000020748 rosemary extract Nutrition 0.000 claims description 13
- 239000011732 tocopherol Substances 0.000 claims description 13
- 229930003799 tocopherol Natural products 0.000 claims description 12
- 229960001295 tocopherol Drugs 0.000 claims description 11
- GVJHHUAWPYXKBD-UHFFFAOYSA-N d-alpha-tocopherol Natural products OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims description 10
- 235000010384 tocopherol Nutrition 0.000 claims description 10
- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 claims description 10
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 9
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 9
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 239000003995 emulsifying agent Substances 0.000 claims description 7
- 239000003513 alkali Substances 0.000 claims description 6
- 241000206672 Gelidium Species 0.000 claims description 5
- 108010059642 isinglass Proteins 0.000 claims description 5
- 229910052627 muscovite Inorganic materials 0.000 claims description 5
- 235000010323 ascorbic acid Nutrition 0.000 claims description 4
- 239000011668 ascorbic acid Substances 0.000 claims description 4
- 229960005070 ascorbic acid Drugs 0.000 claims description 4
- 235000013305 food Nutrition 0.000 claims description 4
- WGVKWNUPNGFDFJ-DQCZWYHMSA-N β-tocopherol Chemical compound OC1=CC(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C WGVKWNUPNGFDFJ-DQCZWYHMSA-N 0.000 claims description 4
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 claims description 2
- 244000215068 Acacia senegal Species 0.000 claims description 2
- 235000001815 DL-alpha-tocopherol Nutrition 0.000 claims description 2
- 229920000084 Gum arabic Polymers 0.000 claims description 2
- 102000004407 Lactalbumin Human genes 0.000 claims description 2
- 108090000942 Lactalbumin Proteins 0.000 claims description 2
- 239000000205 acacia gum Substances 0.000 claims description 2
- 235000010489 acacia gum Nutrition 0.000 claims description 2
- 229940066595 beta tocopherol Drugs 0.000 claims description 2
- 230000007062 hydrolysis Effects 0.000 claims description 2
- 238000006460 hydrolysis reaction Methods 0.000 claims description 2
- 239000000787 lecithin Substances 0.000 claims description 2
- 235000010445 lecithin Nutrition 0.000 claims description 2
- 229940067606 lecithin Drugs 0.000 claims description 2
- 239000001814 pectin Substances 0.000 claims description 2
- 235000010987 pectin Nutrition 0.000 claims description 2
- 229920001277 pectin Polymers 0.000 claims description 2
- 235000019149 tocopherols Nutrition 0.000 claims description 2
- 235000007680 β-tocopherol Nutrition 0.000 claims description 2
- 239000011590 β-tocopherol Substances 0.000 claims description 2
- QUEDXNHFTDJVIY-UHFFFAOYSA-N γ-tocopherol Chemical class OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1 QUEDXNHFTDJVIY-UHFFFAOYSA-N 0.000 claims description 2
- GZIFEOYASATJEH-VHFRWLAGSA-N δ-tocopherol Chemical compound OC1=CC(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1 GZIFEOYASATJEH-VHFRWLAGSA-N 0.000 claims 2
- GZIFEOYASATJEH-UHFFFAOYSA-N D-delta tocopherol Natural products OC1=CC(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1 GZIFEOYASATJEH-UHFFFAOYSA-N 0.000 claims 1
- 235000010389 delta-tocopherol Nutrition 0.000 claims 1
- 235000010382 gamma-tocopherol Nutrition 0.000 claims 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 claims 1
- 239000002478 γ-tocopherol Substances 0.000 claims 1
- QUEDXNHFTDJVIY-DQCZWYHMSA-N γ-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1 QUEDXNHFTDJVIY-DQCZWYHMSA-N 0.000 claims 1
- 239000002446 δ-tocopherol Substances 0.000 claims 1
- 239000012530 fluid Substances 0.000 abstract description 2
- 241001465754 Metazoa Species 0.000 description 7
- 239000002253 acid Substances 0.000 description 7
- QRYRORQUOLYVBU-VBKZILBWSA-N Carnosic acid Natural products CC([C@@H]1CC2)(C)CCC[C@]1(C(O)=O)C1=C2C=C(C(C)C)C(O)=C1O QRYRORQUOLYVBU-VBKZILBWSA-N 0.000 description 5
- 125000001931 aliphatic group Chemical group 0.000 description 5
- 241001529742 Rosmarinus Species 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 235000020777 polyunsaturated fatty acids Nutrition 0.000 description 4
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- DOUMFZQKYFQNTF-WUTVXBCWSA-N (R)-rosmarinic acid Chemical compound C([C@H](C(=O)O)OC(=O)\C=C\C=1C=C(O)C(O)=CC=1)C1=CC=C(O)C(O)=C1 DOUMFZQKYFQNTF-WUTVXBCWSA-N 0.000 description 2
- 241000251468 Actinopterygii Species 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 241000239366 Euphausiacea Species 0.000 description 2
- OYHQOLUKZRVURQ-HZJYTTRNSA-N Linoleic acid Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(O)=O OYHQOLUKZRVURQ-HZJYTTRNSA-N 0.000 description 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 2
- GHVNFZFCNZKVNT-UHFFFAOYSA-N decanoic acid Chemical compound CCCCCCCCCC(O)=O GHVNFZFCNZKVNT-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000000284 extract Substances 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 2
- 229960004232 linoleic acid Drugs 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- SECPZKHBENQXJG-FPLPWBNLSA-N palmitoleic acid Chemical compound CCCCCC\C=C/CCCCCCCC(O)=O SECPZKHBENQXJG-FPLPWBNLSA-N 0.000 description 2
- QAIPRVGONGVQAS-DUXPYHPUSA-N trans-caffeic acid Chemical compound OC(=O)\C=C\C1=CC=C(O)C(O)=C1 QAIPRVGONGVQAS-DUXPYHPUSA-N 0.000 description 2
- ACEAELOMUCBPJP-UHFFFAOYSA-N (E)-3,4,5-trihydroxycinnamic acid Natural products OC(=O)C=CC1=CC(O)=C(O)C(O)=C1 ACEAELOMUCBPJP-UHFFFAOYSA-N 0.000 description 1
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 1
- TWJNQYPJQDRXPH-UHFFFAOYSA-N 2-cyanobenzohydrazide Chemical compound NNC(=O)C1=CC=CC=C1C#N TWJNQYPJQDRXPH-UHFFFAOYSA-N 0.000 description 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 1
- PIFPCDRPHCQLSJ-WYIJOVFWSA-N 4,8,12,15,19-Docosapentaenoic acid Chemical compound CC\C=C\CC\C=C\C\C=C\CC\C=C\CC\C=C\CCC(O)=O PIFPCDRPHCQLSJ-WYIJOVFWSA-N 0.000 description 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 1
- 239000005632 Capric acid (CAS 334-48-5) Substances 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- XUSYGBPHQBWGAD-PJSUUKDQSA-N Carnosol Chemical compound CC([C@@H]1C2)(C)CCC[C@@]11C(=O)O[C@@H]2C2=C1C(O)=C(O)C(C(C)C)=C2 XUSYGBPHQBWGAD-PJSUUKDQSA-N 0.000 description 1
- MMFRMKXYTWBMOM-UHFFFAOYSA-N Carnosol Natural products CCc1cc2C3CC4C(C)(C)CCCC4(C(=O)O3)c2c(O)c1O MMFRMKXYTWBMOM-UHFFFAOYSA-N 0.000 description 1
- 241000283153 Cetacea Species 0.000 description 1
- PIFPCDRPHCQLSJ-UHFFFAOYSA-N Clupanodonic acid Natural products CCC=CCCC=CCC=CCCC=CCCC=CCCC(O)=O PIFPCDRPHCQLSJ-UHFFFAOYSA-N 0.000 description 1
- 239000001828 Gelatine Substances 0.000 description 1
- 241000207923 Lamiaceae Species 0.000 description 1
- 235000021360 Myristic acid Nutrition 0.000 description 1
- TUNFSRHWOTWDNC-UHFFFAOYSA-N Myristic acid Natural products CCCCCCCCCCCCCC(O)=O TUNFSRHWOTWDNC-UHFFFAOYSA-N 0.000 description 1
- 239000005642 Oleic acid Substances 0.000 description 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 1
- 235000021314 Palmitic acid Nutrition 0.000 description 1
- 235000021319 Palmitoleic acid Nutrition 0.000 description 1
- 235000004347 Perilla Nutrition 0.000 description 1
- 244000124853 Perilla frutescens Species 0.000 description 1
- CEEMRWKKNNEQDT-UHFFFAOYSA-N Rosmanol Natural products CC(C)c1cc2C(OC(=O)C)C3OC(=O)C4(CCCC(C)(C)C34)c2c(OC(=O)C)c1OC(=O)C CEEMRWKKNNEQDT-UHFFFAOYSA-N 0.000 description 1
- ZZAFFYPNLYCDEP-HNNXBMFYSA-N Rosmarinsaeure Natural products OC(=O)[C@H](Cc1cccc(O)c1O)OC(=O)C=Cc2ccc(O)c(O)c2 ZZAFFYPNLYCDEP-HNNXBMFYSA-N 0.000 description 1
- 244000178231 Rosmarinus officinalis Species 0.000 description 1
- 235000021355 Stearic acid Nutrition 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
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- 235000013361 beverage Nutrition 0.000 description 1
- 210000004556 brain Anatomy 0.000 description 1
- 210000000481 breast Anatomy 0.000 description 1
- 229940074360 caffeic acid Drugs 0.000 description 1
- 235000004883 caffeic acid Nutrition 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 235000004654 carnosol Nutrition 0.000 description 1
- QAIPRVGONGVQAS-UHFFFAOYSA-N cis-caffeic acid Natural products OC(=O)C=CC1=CC=C(O)C(O)=C1 QAIPRVGONGVQAS-UHFFFAOYSA-N 0.000 description 1
- SECPZKHBENQXJG-UHFFFAOYSA-N cis-palmitoleic acid Natural products CCCCCCC=CCCCCCCCC(O)=O SECPZKHBENQXJG-UHFFFAOYSA-N 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 229930004069 diterpene Natural products 0.000 description 1
- 150000004141 diterpene derivatives Chemical class 0.000 description 1
- POULHZVOKOAJMA-UHFFFAOYSA-M dodecanoate Chemical compound CCCCCCCCCCCC([O-])=O POULHZVOKOAJMA-UHFFFAOYSA-M 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 210000001508 eye Anatomy 0.000 description 1
- 235000019197 fats Nutrition 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 239000000499 gel Substances 0.000 description 1
- 229920000159 gelatin Polymers 0.000 description 1
- 235000019322 gelatine Nutrition 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
- 229940070765 laurate Drugs 0.000 description 1
- 235000020778 linoleic acid Nutrition 0.000 description 1
- OYHQOLUKZRVURQ-IXWMQOLASA-N linoleic acid Natural products CCCCC\C=C/C\C=C\CCCCCCCC(O)=O OYHQOLUKZRVURQ-IXWMQOLASA-N 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- GRVDJDISBSALJP-UHFFFAOYSA-N methyloxidanyl Chemical group [O]C GRVDJDISBSALJP-UHFFFAOYSA-N 0.000 description 1
- 235000021290 n-3 DPA Nutrition 0.000 description 1
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 description 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 1
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 1
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000000144 pharmacologic effect Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- DOUMFZQKYFQNTF-MRXNPFEDSA-N rosemarinic acid Natural products C([C@H](C(=O)O)OC(=O)C=CC=1C=C(O)C(O)=CC=1)C1=CC=C(O)C(O)=C1 DOUMFZQKYFQNTF-MRXNPFEDSA-N 0.000 description 1
- LCAZOMIGFDQMNC-FORWCCJISA-N rosmanol Chemical compound C1CCC(C)(C)[C@@H]2[C@H]3[C@@H](O)C(C=C(C(=C4O)O)C(C)C)=C4[C@]21C(=O)O3 LCAZOMIGFDQMNC-FORWCCJISA-N 0.000 description 1
- TVHVQJFBWRLYOD-UHFFFAOYSA-N rosmarinic acid Natural products OC(=O)C(Cc1ccc(O)c(O)c1)OC(=Cc2ccc(O)c(O)c2)C=O TVHVQJFBWRLYOD-UHFFFAOYSA-N 0.000 description 1
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- 210000000697 sensory organ Anatomy 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D7/00—Edible oil or fat compositions containing an aqueous phase, e.g. margarines
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/185—Acids; Anhydrides, halides or salts thereof, e.g. sulfur acids, imidic, hydrazonic or hydroximic acids
- A61K31/19—Carboxylic acids, e.g. valproic acid
- A61K31/20—Carboxylic acids, e.g. valproic acid having a carboxyl group bound to a chain of seven or more carbon atoms, e.g. stearic, palmitic, arachidic acids
- A61K31/202—Carboxylic acids, e.g. valproic acid having a carboxyl group bound to a chain of seven or more carbon atoms, e.g. stearic, palmitic, arachidic acids having three or more double bonds, e.g. linolenic
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D7/00—Edible oil or fat compositions containing an aqueous phase, e.g. margarines
- A23D7/005—Edible oil or fat compositions containing an aqueous phase, e.g. margarines characterised by ingredients other than fatty acid triglycerides
- A23D7/0053—Compositions other than spreads
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D7/00—Edible oil or fat compositions containing an aqueous phase, e.g. margarines
- A23D7/01—Other fatty acid esters, e.g. phosphatides
- A23D7/011—Compositions other than spreads
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D7/00—Edible oil or fat compositions containing an aqueous phase, e.g. margarines
- A23D7/06—Preservation of finished products
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/158—Fatty acids; Fats; Products containing oils or fats
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/115—Fatty acids or derivatives thereof; Fats or oils
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L35/00—Food or foodstuffs not provided for in groups A23L5/00 – A23L33/00; Preparation or treatment thereof
- A23L35/10—Emulsified foodstuffs
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
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Abstract
本发明涉及包含DHA和EPA的有机乳液,具体地,包含二十二碳六烯酸(DHA)和二十碳五烯酸(EPA)的油组合物的乳液,其特征在于,该乳液基本上不含抗坏血酸棕榈酸酯。
Description
本申请是申请日为2013年1月11日的中国专利申请201380005351.5(PCT/EP2013/050447)的分案申请。
本发明涉及包含二十二碳六烯酸(DHA)和二十碳五烯酸(EPA)的油组合物的乳液,其特征在于,该乳液基本上不含抗坏血酸棕榈酸酯。
PUFA油的乳液是已知的。它们可用于多个应用领域,并且它们以液体或干燥形式使用。
PUFA油,即多不饱和脂肪酸,非常易于氧化。由于这一事实,乳液常常包含防止油被氧化的成分。
另一方面,强烈需要提供天然和/或有机的乳液。
在本发明的上下文中,“天然的”和“有机的”与其销售国所设定的法律定义有关。
例如,在欧盟为欧盟生态管理(EU-Eco-regulation),在美国为国家有机计划标准(National Organic Program(NOP)Standards),在日本为JAS标准。
本发明的目标是提供包含二十二碳六烯酸(DHA)和二十碳五烯酸(EPA)油的乳液,根据国家规定(特别是欧洲(EU)、美国、日本和中国)其为天然的和/或有机的。
因此,本发明涉及一种乳液,其包含:
基于乳液的总重,5-40重量-%(wt-%)的二十二碳六烯酸(DHA)和二十碳五烯酸(EPA)油;和
基于乳液的总重,3-15wt-%的至少一种乳化剂;和
基于乳液的总重,1-5wt-%的抗坏血酸和/或柠檬酸;
基于乳液的总重,0.5-5wt-%的至少一种碱;和
基于乳液的总重,35-90.5wt-%的水;和
150ppm-1000ppm的至少一种生育酚;和
1000ppm-5000ppm的迷迭香提取物,
其中,
该乳液的pH介于5和7之间;并且
该乳液基本上不含抗坏血酸棕榈酸酯;并且
该乳液是天然的和/或有机的。
在本发明的上下文中,“基本上不含抗坏血酸棕榈酸酯(AP)”指的是,根据“有机”和“天然”的法律定义,根据本发明的乳液仍可视为“有机的”和/或“天然的”。
根据本发明的所有成分都是天然和/或有机的。这表示,该乳液的所有成分都是通过使用天然和/或有机的方法来生产(或提取)的。
DHA和EPA油可以来自任意天然和/或有机源,例如植物和/或动物。ω-3脂肪酸(例如DHA)的一种来源包括动物源。动物源的实例包括水生动物(例如鱼、海洋哺乳动物和甲壳类动物,如磷虾和其它磷虾目动物)和动物组织(例如脑、肝、眼等)、和动物产品(例如蛋或乳)。
DHA和EPA可以纯化至不同程度。所述纯化可以通过本领域技术人员已知的任何方式来实现。在本发明的上下文中,纯化必须使得经纯化的油是天然和/或有机的。
油中可以存在额外的脂肪酸。这些脂肪酸可以包括在纯化过程中未被除去的脂肪酸,也就是,从原料中与DHA和EPA一起共分离的脂肪酸。这些脂肪酸可以以各种浓度存在。在一些实施方式中,所述油包含0.1%至60%的的一种或多种下列脂肪酸或其酯:(a)癸酸;(b)月桂酸;(c)肉豆蔻酸;(d)棕榈酸;e)棕榈油酸;(f)硬脂酸;(g)油酸;(h)亚油酸;(i)α-亚油酸;(j)二十二碳五烯酸22:5n-3,22:5w3(DPAn3);和(k)4,7,10,13,16,19,22,25-二十八碳八烯酸(C28:8)。所有这些油也符合天然和/或有机的标准。
根据本发明的乳液中使用的乳化剂也是天然和/或有机的。这样的乳化剂可以是任何来源的。用于根据本发明的乳液的合适乳化剂是卵磷脂、乳清蛋白、阿拉伯树胶(水提取的)、水解的骨胶原、果胶和鱼明胶(fish gelatine)。特别优选的是鱼明胶。
抗坏血酸以及柠檬酸是天然和/或有机的。通常它们来自植物。
根据本发明的乳液中使用的碱可以是(在化学上)有机或无机的。但该碱必须始终符合如上所述的法律术语“有机”的标准。特别优选的碱是NaOH。
术语“生育酚”指的是dl-α-生育酚、d-□-生育酚、β-生育酚、□.生育酚和□-生育酚及其混合物,而根据本发明的乳液中使用的生育酚是天然和/或有机的。
在一些实施方式中,生育酚以150ppm到1000ppm的量存在于乳液中,在一个优选的实施方式中,生育酚以200到800ppm的量存在。
生育酚(或生育酚的混合物)可以混入乳液中,或者其可以先混入PUFA油中,然后作为混合物添加到乳液中。
根据本发明的乳液包含迷迭香提取物。
短语“迷迭香提取物”指的是能从迷迭香得到的、具有抗氧化活性的任意提取物。提取以能得到天然和/或有机迷迭香提取物的方式进行。
迷迭香(Rosmarinus officinalis,唇形科)是一种在地中海地区无处不在的织物,其特征是抗氧化和抗菌的药理性质。
迷迭香提取物是从迷迭香植物中提取的天然和已知的材料。
迷迭香提取物可以通过如下获得:干燥迷迭香(属于紫苏科)的叶子、粉碎经干燥的叶子、以及使所产生的粉碎物经历(用水、热水、己烷、乙醇、丙酮、乙酸乙酯、或这些溶剂的混合物)萃取。在本文中使用时,术语“迷迭香提取物”是一个通用术语,描述了一些可能包含多种不同活性成分的不同化学组合物。其中在迷迭香提取物中发现的常见的组分有:咖啡酸;鼠尾草酚;鼠尾草酸;甲氧基鼠尾草酸;迷迭香酸;迷迭香酚;和迷迭香二酚;所有这些组分可以以不同的比例存在,这取决于单个提取物。众多的迷迭香提取物也可以商购,并且任何一种或多种可以在本发明中使用。
合适的迷迭香提取物是商购自例如Kalsec(Kalamazoo,M1,USA)或Naturex(Avignon,France)公司的那些。
根据本发明的乳液包含1000ppm-5000ppm的迷迭香提取物,优选500ppm到4000ppm,更优选500到3500ppm。
此外,本发明涉及一种用于生产根据本发明的乳液的方法,其中所有成分以及工艺步骤都是天然和/或有机的。
根据本发明的乳液可用于其中需要该乳液的任何应用。
该乳液可用于例如食物、饲料或个人护理产品。
这些产品可以为任何形式,例如液体、凝胶状或固体。这些产品可以是随时可使用(随时可消费)的产品、以及需要进一步加工(例如通过稀释、溶解,加热等)的产品。
特别重要的是这些乳液是在食品(如饮料)中的用途。
下列实施例说明本发明。如上所述感官值和rancimat值是确定了的。
实施例
成分 | 量[wt-%] |
EPA | 4.8 |
DHA | 3 |
鱼明胶 | 8.0 |
抗坏血酸 | 2.2 |
NaOH(50%的水溶液) | 1.0 |
水含量(总计) | 62.8 |
其它油 | 18.2 |
通过下列方法制备乳液:分别制备油相和水相,随后通过适当的预均化装置(例如转子-定子、micer圆盘等)将油相在水相中均质化,并且随后施加高压均质。
该乳液的pH值为6。
该天然和有机的乳液储存稳定并且易于掺入任意制剂。
Claims (10)
1.一种乳液,其包含:
基于所述乳液的总重,5-40wt-%的二十二碳六烯酸(DHA)和二十碳五烯酸(EPA)油;和
基于所述乳液的总重,3-15wt-%的至少一种乳化剂;和
基于所述乳液的总重,1-5wt-%的抗坏血酸和/或柠檬酸;
基于所述乳液的总重,0.5-5wt-%的至少一种碱;和
基于所述乳液的总重,35-90.5wt-%的水;和
150ppm-1000ppm的至少一种生育酚;和
1000ppm-5000ppm的迷迭香提取物,
其中,
所述乳液的pH介于5和7之间;并且
所述乳液基本上不含抗坏血酸棕榈酸酯。
2.如权利要求1所述的乳液,其中,所述乳液是天然和/或有机的。
3.如前面任何一个权利要求所述的乳液,其中,所述乳化剂选自由卵磷脂、乳清蛋白、阿拉伯树胶(水提取的)、水解的骨胶原、果胶和鱼明胶组成的组。
4.如前面任何一个权利要求所述的乳液,其中,所述乳化剂是鱼明胶。
5.如前面任何一个权利要求所述的乳液,其中,所用的碱是NaOH。
6.如前面任何一个权利要求所述的乳液,其中,所述生育酚选自由dl-α-生育酚、d-α-生育酚、β-生育酚、γ-生育酚和δ-生育酚组成的组。
7.如前面任何一个权利要求所述的乳液,其中,使用200到800ppm的生育酚。
8.如前面任何一个权利要求所述的乳液,其中,使用500到4000ppm的迷迭香提取物。
9.权利要求1-8中任意一项所述的乳液在食物、饲料或个人护理产品中的用途。
10.包含权利要求1-8中任意一项所述乳液的食物、饲料或个人护理产品。
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CN105231333A (zh) * | 2015-11-12 | 2016-01-13 | 东北农业大学 | 一种dha营养乳液的制备方法 |
KR101854018B1 (ko) | 2015-12-23 | 2018-05-02 | 주식회사 다인소재 | 항산화 활성을 갖는 초음파분산 나노 에멀젼 형태의 조성물 |
BR112020024464A2 (pt) * | 2018-06-14 | 2021-03-02 | Mars, Incorporated | composição de suporte para animal com câncer |
KR102151022B1 (ko) * | 2019-08-29 | 2020-09-02 | 유씨엘 주식회사 | 로즈마리로부터 카페인산과 로즈마린산을 추출하는 방법 |
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WO2007120500A2 (en) * | 2006-04-07 | 2007-10-25 | Ocean Nutrition Canada Ltd. | Emulsions and microcapsules with substances having low interfacial tension, methods of making and using thereof |
DE102009023482A1 (de) * | 2009-06-02 | 2010-12-09 | Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. | Emulsion oder Gel zur Herstellung von Omega-3-Fettsäure-haltigen Nahrungsmitteln |
CN102939079B (zh) * | 2010-04-09 | 2016-01-06 | 帝斯曼知识产权资产管理有限公司 | 包含含有多不饱和脂肪酸的油的热稳定的水包油乳液 |
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CN101472485A (zh) * | 2006-04-07 | 2009-07-01 | 加拿大海洋营养食品有限公司 | 含有具有低界面张力的物质的乳状液和微胶囊、其制备及使用的方法 |
CN102041169A (zh) * | 2010-12-23 | 2011-05-04 | 厦门金达威集团股份有限公司 | 一种适用于不饱和脂肪酸及其酯的抗氧化剂组合物 |
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NZ627354A (en) | 2016-07-29 |
MX2014008494A (es) | 2014-10-14 |
BR112014017048A8 (pt) | 2017-07-04 |
IN2014DN05811A (zh) | 2015-05-15 |
KR20140116482A (ko) | 2014-10-02 |
AU2013208915B2 (en) | 2016-03-17 |
CN104039159A (zh) | 2014-09-10 |
US20140356464A1 (en) | 2014-12-04 |
US9579301B2 (en) | 2017-02-28 |
AU2013208915A1 (en) | 2014-07-31 |
MX349987B (es) | 2017-08-22 |
JP2015506175A (ja) | 2015-03-02 |
BR112014017048A2 (pt) | 2017-06-13 |
WO2013104740A1 (en) | 2013-07-18 |
EP2802217A1 (en) | 2014-11-19 |
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