CN106854034A - The processing method and device of sludge in oil field oil water settling tank tank - Google Patents

The processing method and device of sludge in oil field oil water settling tank tank Download PDF

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Publication number
CN106854034A
CN106854034A CN201710025005.3A CN201710025005A CN106854034A CN 106854034 A CN106854034 A CN 106854034A CN 201710025005 A CN201710025005 A CN 201710025005A CN 106854034 A CN106854034 A CN 106854034A
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CN
China
Prior art keywords
sludge
tank
sewage
settling tank
oil
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Pending
Application number
CN201710025005.3A
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Chinese (zh)
Inventor
王红梅
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Heilongjiang Province Rong Ze Petroleum Equipment Co Ltd
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Heilongjiang Province Rong Ze Petroleum Equipment Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Application filed by Heilongjiang Province Rong Ze Petroleum Equipment Co Ltd filed Critical Heilongjiang Province Rong Ze Petroleum Equipment Co Ltd
Priority to CN201710025005.3A priority Critical patent/CN106854034A/en
Publication of CN106854034A publication Critical patent/CN106854034A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F11/00Treatment of sludge; Devices therefor
    • C02F11/12Treatment of sludge; Devices therefor by de-watering, drying or thickening
    • C02F11/121Treatment of sludge; Devices therefor by de-watering, drying or thickening by mechanical de-watering
    • C02F11/127Treatment of sludge; Devices therefor by de-watering, drying or thickening by mechanical de-watering by centrifugation
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F11/00Treatment of sludge; Devices therefor
    • C02F11/12Treatment of sludge; Devices therefor by de-watering, drying or thickening
    • C02F11/14Treatment of sludge; Devices therefor by de-watering, drying or thickening with addition of chemical agents
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2103/00Nature of the water, waste water, sewage or sludge to be treated
    • C02F2103/10Nature of the water, waste water, sewage or sludge to be treated from quarries or from mining activities

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Organic Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Separation Of Suspended Particles By Flocculating Agents (AREA)

Abstract

The processing method of sludge is related to a kind of separation method and device with device in oil field oil water settling tank tank in settling tank of the invention, realizes through the following steps:In moisture content is 80~99.8% oily sludges, flocculant and smart iron powder are separately added into, stirred;To be separated through the material of upper step process, the content < 150mg/L of mud in the sewage separated;Secondary separation will be carried out through the sludge after upper step process, the content < 100mg/L of mud in the sewage separated;To be separated through the sludge after upper step process with super magnetic separating device, isolated sludge and sewage containing iron powder.The method of the present invention and device, can effectively reduce the aqueous amount of sludge in tank, and dehydrating effect is good, the sludge of moisture content 80 99.8% can be processed and arrive moisture content≤60%, and the sewage after treatment returns to sewage recovery pond in station and recycles;Oil, mud, water can also be separated, and it is most of oily in oily sludge in recycling can, and save energy processes non-secondary pollution.

Description

The processing method and device of sludge in oil field oil water settling tank tank
Technical field
The present invention relates to a kind of separation method and device, oil field oil water settling tank tank in a kind of settling tank is especially related to The processing method and device of interior sludge.
Background technology
As the large-scale promotion driven with ternary composite driving is gathered in oil field, oil field mining liquid is taken husky amount and is increased, in gravity and wadding In the presence of solidifying agent, settling tank(Natural subsidence tank, coagulating setting tank)Bottom produces a large amount of sludge.These sludge not only moisture content Height, volume is big, and constituent is also more complicated, containing substantial amounts of ageing oil, wax, asphalitine, colloidal substance outside, also containing big Amount benzene homologues, heavy metal, sex pheromone, and the noxious material such as unstabilized organic matter.If do not dealt carefully with, not only can wave Take resource, direct or indirect pollution can be also caused to environment.
The content of the invention
It is contemplated that in overcoming the deficiencies in the prior art, there is provided the treatment of sludge in a kind of oil field oil water settling tank tank Method and apparatus.
The processing method of sludge, realizes through the following steps in oil field oil water settling tank tank of the invention:
It is a, quenched:In moisture content is 80~99.8% oily sludges, it is 80- to be separately added into the g/L of flocculant 0.5~2 and particle diameter 100 μm of smart 0.3~1g/L of iron powder, stirs at a temperature of 40~80 DEG C;
B, primary separation:To be separated through the material of a step process, isolated sludge and sewage, dehydration rate up to 94% with On, the content < 150mg/L of mud in the sewage separated;
C, secondary separation:Sludge after being processed through b step carries out secondary separation, isolates sludge and sewage, and dehydration rate is reachable More than 94%, the content < 100mg/L of mud in the sewage separated;
D, mud-water separation:Sludge after being processed through step c is separated with super magnetic separating device, isolates the sludge containing iron powder And sewage.
As a further improvement on the present invention, the sludge that above-mentioned Step d mud-water separation goes out carries out separation of solid and liquid, separates Mud moisture content≤60%.
As a further improvement on the present invention, the sewage that above-mentioned steps b, step c, step d are isolated carries out suspension retention, Sludge, sewage is carried out to separate.
As a further improvement on the present invention, agitator is stirred with 20~35rpm in above-mentioned a steps.
The processing unit of sludge in oil field oil water settling tank tank of the invention, including settling tank, suspension device for trapping, dirt Water surge tank and sump oil surge tank, the outlet of settling tank are connected with the entrance pipe of mixing pit, and outlet and the waterpower of mixing pit are revolved The entrance pipe connection of device group is flowed, the solid outlet pipeline of hydrocyclone group is connected to the entrance of super magnetic separating device, overflow Mouthful pipeline is connected to suspension device for trapping, super magnetic separating device be provided with solids outlet port, liquid export line be connected to it is outstanding Float device for trapping, the liquid export line of suspension device for trapping is connected to sewage surge tank;Iron powder is provided with mixing pit Mouth a and flocculant is added to add mouth b.
As a further improvement on the present invention, the outlet of mixing pit is connected to hydrocyclone group by the pipeline of elevator pump I, The solid outlet of hydrocyclone group is connected to the entrance of secondary hydrocyclone group, secondary waterpower rotation by the pipeline of elevator pump II The solid outlet of stream device group is connected to super magnetic separating device, overfall pipeline and is connected to suspension device for trapping, suspension retention Suspension export pipeline in device is connected on the output pipe c of settling tank.
As a further improvement on the present invention, the solids outlet port on super magnetic separating device is connected to Horizontal helical type centrifuge Entrance, Horizontal helical type centrifuge is provided with solids outlet port e, liquid export line and is connected to suspension device for trapping.
As a further improvement on the present invention, sewage surge tank is provided with water out d, and receipts oil dress is provided with sewage surge tank Put, oil-collecting device export pipeline is connected to sump oil surge tank.
As a further improvement on the present invention, the export pipeline of settling tank is connected to mixing pit through sludge pump.
The processing method and device of sludge in oil field oil water settling tank tank of the invention, can effectively reduce sludge in tank and contain The amount of water, dehydrating effect is good, the sludge of moisture content 80-99.8% can be processed and arrive moisture content≤60%, and the sewage after treatment is returned to Sewage recovery pond is recycled in standing;Oil, mud, water can also be separated, and it is most of oily in oily sludge in recycling can, save The energy, processes non-secondary pollution.
Brief description of the drawings
Fig. 1 is the structural representation of the processing method of sludge and device in oil field oil water settling tank tank of the invention.
Specific embodiment
Embodiment 1
The processing method of sludge, realizes through the following steps in oil field oil water settling tank tank of the invention:
It is a, quenched:In moisture content is 80~99.8% oily sludges, it is 80- to be separately added into the g/L of flocculant 0.5~2 and particle diameter 100 μm of smart 0.3~1g/L of iron powder, stirs at a temperature of 40~80 DEG C;Its flocculant is flocculated from polyacrylamide Agent, concentration is 0.3%~0.5%;
B, primary separation:To be separated through the material of a step process, isolated sludge and sewage, dehydration rate up to 94% with On, the content < 150mg/L of mud in the sewage separated;
C, secondary separation:Sludge after being processed through b step carries out secondary separation, isolates mud and sewage, and dehydration rate is up to 94% More than, the content < 100mg/L of mud in the sewage separated;
D, mud-water separation:Sludge after being processed through step c is separated with super magnetic separating device, isolates the sludge containing iron powder And sewage.
Embodiment 2
The processing method of sludge, realizes through the following steps in oil field oil water settling tank tank of the invention:
It is a, quenched:Settling tank(Natural subsidence tank/coagulating setting tank)Interior moisture content is 80-99.8% oily sludges, into mixing Pond, chemicals dosing plant does not dissolve essence iron powder to the height of liquid flocculant 1.3g/L and particle diameter for 80-100 μm is added in modifying device 0.8g/L.Mixing pit is provided with agitator, and agitator is stirred with 20~35rpm, is formed after being sufficiently stirred for smart iron as core The small flocculation group of the heart;At 40-80 DEG C or so, sludge stops ten minutes, sludge to quenched agitator temperature control in modifying device Interior profit carries out initial gross separation;
B, primary separation:Enter hydrocyclone group by quenched sludge, 50 μm of sewage particulate >, carry out sludge tentatively dense Contracting, separates water into out, the sewage clay content < 150mg/L for separating, and is buffered into sewage by suspension device for trapping In tank;Remaining mud is discharged from bottom, and secondary hydrocyclone group is lifted into by elevator pump I;
C, secondary separation:After being processed through hydrocyclone group, the sludge of 50 μm of particle > enters secondary hydrocyclone after concentration Group, carries out secondary concentration, separates, and sewage dehydration rate is up to more than 94%.The sewage clay content < 100mg/L for separating, pass through Suspension device for trapping enters in sewage surge tank;The mud separated enters excess of imports magnetic separating device carries out mud-water separation;
D, mud-water separation:Secondary waterpower cyclone fraction separates out the sludge for coming and enters in excess of imports magnetic separating device, and particle diameter is 80-100 μ The insoluble essence iron powder of the height of m is that the sludge of the small flocculation group of core is drawn by disk, separated, into horizontal screw centrifuge; Point
E, centrifugation:Super magnetic separating device mud out enters rotary drum rotating speed for 3800rpm, separation factor are the sleeping of 3551G Spiral shell formula centrifuge carries out separation of solid and liquid, mud moisture content≤60% separated, and is transported outward by conveyer into solid block;Isolate The water for coming is entered in sewage surge tank by suspension device for trapping;
F, separation buffer:The water for separating out is entered in sewage surge tank by suspension device for trapping;It is provided with outstanding before sewage surge tank Float device for trapping, hydrocyclone group and secondary hydrocyclone group, super magnetic separating device, Horizontal helical type centrifuge are separated Suspension retention in sewage out, sends into mixing pit, circular treatment.
Float apparatus for collecting oil is provided with sewage surge tank, the oil in surge tank is collected into oil skimming tank, surge tank Interior sewage enters sewage recovery pond in inbound and recycles.
The hydrocyclone group and secondary hydrocyclone group used in the present invention are limited by Weihai City sea king's cyclone Company's production, be commercial goods;Horizontal helical type centrifuge is produced selected from Alfa Laval company, is also commercial goods;Super magnetic It, selected from Shanghai Mei Wan water utilities company, is also commercial goods that separator is.
Embodiment 3
The processing unit of sludge in oil field oil water settling tank tank of the invention, including settling tank 1, suspension device for trapping 2, sewage Surge tank 3 and sump oil surge tank 4.The export pipeline of settling tank 1 is connected to the entrance of mixing pit 5 through sludge pump 13, and mixing pit 5 goes out Mouth is connected to the entrance of hydrocyclone group 6 by the pipeline of elevator pump I 9, and the solid outlet of hydrocyclone group 6 passes through elevator pump II 11 pipelines are connected to the entrance of secondary hydrocyclone group 10, and the solid outlet of secondary hydrocyclone group 10 is connected to super magnetic Separator 7, super magnetic separating device 7 is provided with solids outlet port, and solids outlet port is connected to the entrance of Horizontal helical type centrifuge 12, Horizontal helical type centrifuge 12 is provided with solids outlet port e.It is the overfall of hydrocyclone group 6 and secondary hydrocyclone group 10, super The liquid outlet of magnetic separating device 7, the equal pipeline of liquid outlet of Horizontal helical type centrifuge 12 are connected to suspension device for trapping 2, hang Suspension export pipeline in float device for trapping 2 is connected on the output pipe c of settling tank 1, the liquid of suspension device for trapping 2 Body export pipeline is connected to sewage surge tank 3.3 are provided with water out d in sewage surge tank, and receipts are provided with 3 in sewage surge tank Oily device 8, the export pipeline of oil-collecting device 8 are connected to sump oil surge tank 4.The pressure of elevator pump I 9 and elevator pump II 11 be 0.3~ 0.7MPa.Iron powder is provided with mixing pit 5 adds mouth a and flocculant to add mouth b.
Implementation method 4
The present invention is realized by following technical process:To be entered by sludge pump 13 in raw sludge natural subsidence tank 1 first In entering mixing pit 5, iron powder adds mouth a and flocculant to add mouth b to adding the g/L of liquid flocculant 1 in mixing pit 5 and particle diameter is The insoluble essence iron powder 0.5g/L of 80-100 μm of height, agitator is stirred with 23rpm;The temperature control of quenched agitator 14 exists 50 DEG C or so, sludge is stopped ten minutes in mixing pit 5;Sump oil initial gross separation in sludge is out.Mud and sewage after quenched Lifted by the elevator pump I 9 of the MPa of pressure 0. 3~1.0, tangentially entered in primary hydrocyclone group 6 by entrance, sludge, sewage Strong vortex is internally produced, primary sludge concentration is carried out, is separated, the sludge and fraction water of quality weight separate entrance Secondary hydrocyclone group 10, carries out secondary sludge concentration, separates, and the sludge separated enters excess of imports magnetic separating device 7, particle diameter Drawn by disk for sludge that the small flocculation of core is rolled into a ball for the insoluble essence iron powder of 80-100 μm of height, separated, into sleeping Screw centrifuge 12 carries out mud-water separation, and the mud separated is blocking to be transported outward by conveyer.From primary hydrocyclone group, secondary water It is water, oil and lighter than water miscellaneous that power cyclone group, super magnetic separating device, horizontal screw centrifuge 12 separate filtrate main component Matter enters suspension device for trapping 2, and suspension, impurity are trapped in device, are back to mixing pit, and the profit after filter enters sewage In surge tank 3,30min is buffered, float apparatus for collecting oil 8 starts to receive oil in sewage surge tank, receipts are entered into sump oil surge tank 4 is interior Oil system;Sewage enters sewage recovery pond recycling d in inbound in water pot.

Claims (9)

1. in oil field oil water settling tank tank sludge processing method, realize through the following steps:
It is a, quenched:In moisture content is 80~99.8% oily sludges, it is 80- to be separately added into the g/L of flocculant 0.5~2 and particle diameter 100 μm of smart 0.3~1g/L of iron powder, stirs at a temperature of 40~80 DEG C;
B, primary separation:To be separated through the material of a step process, separate sludge and sewage, dehydration rate up to 94% with On, the content < 150mg/L of mud in the sewage separated;
C, secondary separation:Sludge after being processed through b step carries out secondary separation, separates sludge and sewage, and dehydration rate is reachable More than 94%, the content < 100mg/L of mud in the sewage separated;
D, mud-water separation:Sludge after being processed through step c is separated with super magnetic separating device, isolates the sludge containing iron powder And sewage.
2. in oil field oil water settling tank tank as claimed in claim 1 sludge processing method, it is characterised in that through Step d muddy water The sludge isolated carries out separation of solid and liquid, mud moisture content≤60% separated.
3. in oil field oil water settling tank tank as claimed in claim 1 or 2 sludge processing method, it is characterised in that will be through step The sewage that b, step c, step d are isolated carries out suspension retention, carries out sludge, sewage and separates.
4. in oil field oil water settling tank tank as claimed in claim 1 sludge processing method, it is characterised in that in a steps stir Device is stirred with 20~35rpm.
5. in oil field oil water settling tank tank sludge processing unit, including settling tank(1), suspension device for trapping(2), sewage delay Rush tank(3)Sump oil surge tank(4), it is characterised in that settling tank(1)Outlet and mixing pit(5)Entrance pipe connection, mixing Pond(5)Outlet and hydrocyclone group(6)Entrance pipe connection, hydrocyclone group(6)Solid outlet pipeline connection To super magnetic separating device(7)Entrance, overfall pipeline be connected to suspension device for trapping(2), super magnetic separating device(7)On set There are solids outlet port, liquid export line to be connected to suspension device for trapping(2), suspension device for trapping(2)Liquid outlet Pipeline is connected to sewage surge tank(3);In mixing pit(5)Being provided with iron powder adds mouth a and flocculant to add mouth b.
6. in oil field oil water settling tank tank as claimed in claim 5 sludge processing unit, it is characterised in that mixing pit(5)'s Outlet passes through elevator pump I(9)Pipeline is connected to hydrocyclone group(6), hydrocyclone group(6)Solid outlet by lifting Pump II(11)Pipeline is connected to secondary hydrocyclone group(10)Entrance, secondary hydrocyclone group(10)Solid outlet connect It is connected to super magnetic separating device(7), overfall pipeline be connected to suspension device for trapping(2), suspension device for trapping(2)In it is outstanding Float export pipeline is connected to settling tank(1)Output pipe c on.
7. in the oil field oil water settling tank tank as described in claim 5 or 6 sludge processing unit, it is characterised in that super Magneto separate Device(7)On solids outlet port be connected to Horizontal helical type centrifuge(12)Entrance, Horizontal helical type centrifuge(12)It is provided with solid Outlet e, liquid export line are connected to suspension device for trapping(2).
8. in oil field oil water settling tank tank as claimed in claim 5 sludge processing unit, it is characterised in that sewage surge tank It is interior(3)Water out d is provided with, in sewage surge tank(3)Inside it is provided with oil-collecting device(8), oil-collecting device(8)Export pipeline is connected to Sump oil surge tank(4).
9. in oil field oil water settling tank tank as claimed in claim 5 sludge processing unit, it is characterised in that settling tank(1)'s Export pipeline is through sludge pump(13)It is connected to mixing pit(5).
CN201710025005.3A 2017-01-13 2017-01-13 The processing method and device of sludge in oil field oil water settling tank tank Pending CN106854034A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108674838A (en) * 2018-03-16 2018-10-19 济南瑞东实业有限公司 Storage tank comprehensive management of environmental protection device and administering method
CN111689676A (en) * 2020-06-30 2020-09-22 西安长庆科技工程有限责任公司 Oil-containing sludge reduction device and method
CN112279486A (en) * 2020-10-16 2021-01-29 大庆油田有限责任公司 A kind of container non-stop dredging and sludge reduction treatment device
CN115784560A (en) * 2022-11-17 2023-03-14 北京和荣工程技术有限公司 Method for treating oil sludge
CN116332398A (en) * 2023-02-24 2023-06-27 中钢集团武汉安全环保研究院有限公司 A method for pretreatment of wastewater from hot-dip galvanizing skin pass machine

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04180898A (en) * 1990-11-14 1992-06-29 Sanitarii:Kk Treatment of mixture of oils and fats and sludge
CN101963358A (en) * 2010-09-30 2011-02-02 昆明理工大学 Combined treatment method for oilfield solid waste
CN201962164U (en) * 2010-11-15 2011-09-07 袁光汉 System for treating drilling sludge slurry

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04180898A (en) * 1990-11-14 1992-06-29 Sanitarii:Kk Treatment of mixture of oils and fats and sludge
CN101963358A (en) * 2010-09-30 2011-02-02 昆明理工大学 Combined treatment method for oilfield solid waste
CN201962164U (en) * 2010-11-15 2011-09-07 袁光汉 System for treating drilling sludge slurry

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108674838A (en) * 2018-03-16 2018-10-19 济南瑞东实业有限公司 Storage tank comprehensive management of environmental protection device and administering method
CN111689676A (en) * 2020-06-30 2020-09-22 西安长庆科技工程有限责任公司 Oil-containing sludge reduction device and method
CN112279486A (en) * 2020-10-16 2021-01-29 大庆油田有限责任公司 A kind of container non-stop dredging and sludge reduction treatment device
CN112279486B (en) * 2020-10-16 2022-12-27 大庆油田有限责任公司 Container is not stopped production desilting and mud minimizing device
CN115784560A (en) * 2022-11-17 2023-03-14 北京和荣工程技术有限公司 Method for treating oil sludge
CN115784560B (en) * 2022-11-17 2025-07-15 北京和荣工程技术有限公司 A method for treating oily sludge
CN116332398A (en) * 2023-02-24 2023-06-27 中钢集团武汉安全环保研究院有限公司 A method for pretreatment of wastewater from hot-dip galvanizing skin pass machine

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