CN106769984A - Cuttage formula near-infrared probe and its method of work - Google Patents

Cuttage formula near-infrared probe and its method of work Download PDF

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Publication number
CN106769984A
CN106769984A CN201611255173.3A CN201611255173A CN106769984A CN 106769984 A CN106769984 A CN 106769984A CN 201611255173 A CN201611255173 A CN 201611255173A CN 106769984 A CN106769984 A CN 106769984A
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CN
China
Prior art keywords
infrared probe
infrared
testing sample
optical fiber
handheld division
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Withdrawn
Application number
CN201611255173.3A
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Chinese (zh)
Inventor
吴键波
慎石磊
胡建坤
沈超
郭中原
杨伟伟
李小明
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Focused Photonics Hangzhou Inc
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Focused Photonics Hangzhou Inc
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Priority to CN201611255173.3A priority Critical patent/CN106769984A/en
Publication of CN106769984A publication Critical patent/CN106769984A/en
Withdrawn legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G01N21/35Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
    • G01N21/3563Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light for analysing solids; Preparation of samples therefor
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/01Arrangements or apparatus for facilitating the optical investigation

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  • Physics & Mathematics (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)

Abstract

The present invention relates to a kind of cuttage formula near-infrared probe, the near-infrared probe includes:Sharp portion, the sharp portion is located at the head of the near-infrared probe, for inserting testing sample;Calibration system, the calibration system includes standard sources and Temperature Humidity Sensor, positioned at the rear end of the sharp portion;Inserted link, the inserted link connects the calibration system and Handheld Division;Handheld Division, the Handheld Division is connected with optical fiber component, and near-infrared probe can carry out signal transmission by the optical fiber component with near-infrared analyzer;Handover module, the handover module controls the near-infrared probe to be changed between calibration mode and detection pattern.The present invention also provides a kind of method of work of near-infrared probe.The present invention has the advantages that simple to operate, efficiency high, measurement result are accurate.

Description

Cuttage formula near-infrared probe and its method of work
Technical field
The present invention relates to near-infrared analysis field, near-infrared analyzer and its work that more particularly to a kind of cuttage formula is popped one's head in Method.
Background technology
In the storage of grain or transportation, in order to be able to grasping and monitoring the quality of grain, it is necessary to being stacked into bag Grain be analyzed detection.Existing solution is that testing sample is sampled with manual sampling sharp-pointed tube, collects a fixed number After the sample of amount detection is analyzed using near-infrared analyzer.However, there is following defect in this kind of detection mode:
1st, need to carry out manual sampling to each sampling object successively, and sampling sharp-pointed tube sampling operation is poor, intricate operation;
2nd, after sample takes out to before detecting, sample is placed in sample disc, and environment temperature, air humidity etc. can be right The testing result of sample is impacted so that detection accuracy is low, poor repeatability;
3rd, sampling is carried out from detection using different instrument substeps, wastes time and energy and uncertain factor increases, and reduces inspection Survey the accuracy of result.
The content of the invention
In order to solve the deficiency in above-mentioned prior art, the invention provides a kind of simple to operate, efficiency high, detection Result accurately and reliably, the cuttage formula near-infrared probe of sample detection can be completed without manual sampling.
The purpose of the present invention is achieved through the following technical solutions:
A kind of cuttage formula near-infrared probe, the near-infrared probe includes:
Sharp portion, the sharp portion is located at the head of the near-infrared probe, for inserting testing sample;
Calibration system, the calibration system includes standard sources and Temperature Humidity Sensor, positioned at the rear end of the sharp portion;
Inserted link, the inserted link connects the calibration system and Handheld Division;
Handheld Division, the Handheld Division is connected with optical fiber component, and near-infrared probe can be with near-infrared by the optical fiber component Analyzer carries out signal transmission;
Handover module, the handover module controls the near-infrared probe to be changed between calibration mode and detection pattern.
According to above-mentioned near-infrared probe, it is preferable that the handover module is arranged on the Handheld Division.
According to above-mentioned near-infrared probe, alternatively, the handover module includes at least one button.
According to above-mentioned near-infrared probe, it is preferable that the sharp portion is cuttage pipe.
According to above-mentioned near-infrared probe, alternatively, the Handheld Division is pistol shape handle.
According to above-mentioned near-infrared probe, it is preferable that the optical fiber component includes optical fiber and fibre-optical splice.
The present invention also provides a kind of method of work of near-infrared probe, and the method for work is comprised the following steps:
(A1) any of the above-described described near-infrared probe is provided, optical fiber component and near-infrared analyzer is connected;
(A2) near-infrared probe is switched to calibration mode, and the standard sources in calibration system carries out standard light school to system Standard, while being modified to ambient temperature and humidity by Temperature Humidity Sensor;
(A3) sharp portion insertion testing sample, system to be calibrated is submerged after the testing sample and is stopped;
(A4) near-infrared probe is switched to detection pattern, and near-infrared analyzer output light source is got on testing sample and connect Receive and carry diffusing for testing sample information;
(A5) near-infrared analyzer carries out data processing, obtains the content of test substance in testing sample.
According to above-mentioned method of work, it is preferable that the method for work is further included:
(B1) Temperature Humidity Sensor in calibration system reads the humiture of testing sample, and is sent to near-infrared analysis Instrument;
(B1) step is located between (A4) step and (A5) step;
When data processing is carried out, the humiture information to testing sample is compensated/corrected near-infrared analyzer.
According to above-mentioned method of work, alternatively, the test substance is moisture and/or protein.
Compared with prior art, the device have the advantages that being:
First, direct insertion measurement, without manual sampling
The present invention is detected by near-infrared probe is inserted directly into testing sample, without manual sampling, operation side Just quick, efficiency high, and reduce sample waste;Meanwhile, the length of inserted link can be designed according to demand, extend detection empty Between.
2nd, calibration system is carried, detection accuracy is improved
Near-infrared probe of the invention carries calibration system, and the humiture of ambient temperature and humidity and sample interior can be surveyed Amount, and then influence in data processing to above-mentioned humiture is modified, and improves detection accuracy;Simultaneously, it is no longer necessary to Near-infrared analyzer provides calibration function, reduces the requirement to near-infrared analyzer.
3rd, multimetering is realized to same sample, the reliability of detection is improved
The direct insertion measurement of near-infrared probe of the present invention, quickness and high efficiency therefore, it can insert the different portions of same sample Position, realizes the multimetering to same sample, improves sample detection result accuracy and reliability.
Brief description of the drawings
Referring to the drawings, the disclosure will be easier to understand.Skilled addressee readily understands that be:This A little accompanying drawings are used only for illustrating technical scheme, and are not intended to be construed as limiting protection scope of the present invention. In figure:
Fig. 1 be the embodiment of the present invention 1 cuttage formula near-infrared probe be connected with near-infrared analyzer after structural representation.
Implementation method
Fig. 1 and following description describe optional embodiment of the invention with instruct those skilled in the art how to implement and Reproduce the present invention.In order to instruct technical solution of the present invention, some conventional aspects are simplified or have eliminated.Those skilled in the art should The understanding is derived from the modification of these implementation methods or replacement will within the scope of the invention.Those skilled in the art should understand that under Stating feature can combine to form multiple modifications of the invention in a variety of ways.Thus, the invention is not limited in it is following can be real Mode is applied, and is only limited by claim and their equivalent.
Embodiment 1
Fig. 1 schematically illustrate the present embodiment cuttage formula near-infrared probe be connected with near-infrared analyzer after structure Sketch, as shown in figure 1, the near-infrared probe includes:
Sharp portion 1, the sharp portion is located at the head of the near-infrared probe, for inserting testing sample;
Calibration system 2, the calibration system includes standard sources and Temperature Humidity Sensor, after the sharp portion End;
Inserted link 3, the inserted link connects the calibration system and Handheld Division;
Handheld Division 4, the Handheld Division is connected with optical fiber component, and near-infrared probe can be with near-infrared by the optical fiber component Analyzer 7 carries out signal transmission;The optical fiber component includes optical fiber 61 and fibre-optical splice 62;
Handover module 5, the handover module controls the near-infrared probe to be changed between calibration mode and detection pattern; The handover module is arranged on the Handheld Division.
Further, the sharp portion be cuttage pipe, can easily by near-infrared probe insert testing sample in, while skewer Sample can be retained in intubation, is easy to the detection of testing sample.
The near-infrared analyzer includes light source, spectrometer and data handling system, is prior art, no longer goes to live in the household of one's in-laws on getting married herein State.
The present embodiment also provides a kind of method of work of cuttage formula near-infrared probe, and the method for work includes following step Suddenly:
(A1) near-infrared probe of this implementation is provided, optical fiber component and near-infrared analyzer is connected;
(A2) near-infrared probe is switched to calibration mode, and the standard sources in calibration system carries out standard light school to system Standard, while being modified to ambient temperature and humidity by Temperature Humidity Sensor;
(A3) sharp portion insertion testing sample, system to be calibrated is submerged after the testing sample and is stopped;
(A4) near-infrared probe is switched to detection pattern, and near-infrared analyzer output light source is got on testing sample and connect Receive and carry diffusing for testing sample information;
(A5) near-infrared analyzer carries out data processing, obtains and containing for test substance in testing sample is obtained in testing sample Amount.
Further, the test substance is moisture and/or protein.
Above-mentioned near-infrared probe only near-infrared probe and near-infrared analyzer assembling finish after carried out standard sources and The calibration of ambient temperature and humidity, but when bag or sample in heaps is detected into, temperature, humidity and extraneous ring inside testing sample Border differs greatly, and only the influence to ambient temperature and humidity is compensated is inadequate, therefore:
Further, the method for work also includes:
(B1) Temperature Humidity Sensor in calibration system reads the humiture of testing sample, and is sent to near-infrared analysis Instrument;
(B1) step is located between (A4) step and (A5) step;
When data processing is carried out, the humiture information to testing sample is compensated/corrected near-infrared analyzer.
Advantage of this embodiment is that:1st, the direct insertion measurement of near-infrared probe, without manual sampling, simple to operate, efficiency It is high;Multimetering is carried out to same sample, the reliability of testing result is improved;2nd, calibration system is set in near-infrared probe to environment The humiture of humiture and testing sample is measured, and improves the accuracy of testing sample testing result.
Embodiment 2
The cuttage formula near-infrared probe and its method of work of the embodiment of the present invention 1 monitor the application in field in grain quality Example.
In the application examples, testing sample is packed grain (such as corn, wheat), and sharp portion is the point of head opening Thorn-like steel pipe, can be pierced into grain bag easily;Inserted link be sanitation-grade stainless-steel pipe, can be inserted into grain in, and inserted link length Degree can be designed according to demand, expand the scope of grain test point;Handheld Division is pistol shape handle, improves hand-held comfort level, when Handheld Division of different shapes can also so be selected;Handover module is the button being arranged on Handheld Division, is easy to control, the button Can be one or two, button is one in the application example, cutting for calibration mode and detection pattern is carried out by pressing button Change;If two buttons, then one is calibration mode button, and one is detection pattern button, and directly pressing the corresponding button is carried out Pattern switching.
The workflow of above-mentioned cuttage formula near-infrared probe is as follows:
S1. above-mentioned near-infrared probe is connected by optical fiber component with near-infrared analyzer;
S2. button is pressed, near-infrared probe switches to calibration mode, and the standard sources in calibration system enters rower to system Quasi-optical calibration, while being modified to ambient temperature and humidity by Temperature Humidity Sensor;
S3. in sharp portion insertion grain bag, insertion is stopped in grain until calibration system is submerged;
S4. button is pressed again, and near-infrared probe is switched to detection pattern, and near-infrared analyzer output light source gets to grain On food and receive and carry grain information and diffuse;The Temperature Humidity Sensor in calibration system reads the warm and humid of grain simultaneously Degree, and it is sent to near-infrared analyzer;
S5. near-infrared analyzer carries out data processing in the case where grain humiture calibration is carried out, and obtains testing sample In moisture.

Claims (9)

1. a kind of cuttage formula near-infrared probe, it is characterised in that:The near-infrared probe includes:
Sharp portion, the sharp portion is located at the head of the near-infrared probe, for inserting testing sample;
Calibration system, the calibration system includes standard sources and Temperature Humidity Sensor, positioned at the rear end of the sharp portion;
Inserted link, the inserted link connects the calibration system and Handheld Division;
Handheld Division, the Handheld Division is connected with optical fiber component, and near-infrared probe can be with near-infrared analysis by the optical fiber component Instrument carries out signal transmission;
Handover module, the handover module controls the near-infrared probe to be changed between calibration mode and detection pattern.
2. near-infrared probe according to claim 1, it is characterised in that:The handover module is arranged on the Handheld Division On.
3. near-infrared probe according to claim 2, it is characterised in that:The handover module includes at least one button.
4. near-infrared probe according to claim 1, it is characterised in that:The sharp portion is cuttage pipe.
5. near-infrared probe according to claim 1, it is characterised in that:The Handheld Division is pistol shape handle.
6. near-infrared probe according to claim 1, it is characterised in that:The optical fiber component includes that optical fiber and optical fiber connect Head.
7. a kind of method of work of near-infrared probe, it is characterised in that:The method of work is comprised the following steps:
(A1) any described near-infrared probes of claim 1-6 are provided, optical fiber component and near-infrared analyzer is connected;
(A2) near-infrared probe is switched to calibration mode, and the standard sources in calibration system carries out standard optical alignment to system, Ambient temperature and humidity is modified by Temperature Humidity Sensor simultaneously;
(A3) sharp portion insertion testing sample, system to be calibrated is submerged after the testing sample and is stopped;
(A4) near-infrared probe is switched to detection pattern, and near-infrared analyzer output light source is got on testing sample and reception is taken With diffusing for testing sample information;
(A5) near-infrared analyzer carries out data processing, obtains the content of test substance in testing sample.
8. method of work according to claim 7, it is characterised in that:The method of work is further included:
(B1) Temperature Humidity Sensor in calibration system reads the humiture of testing sample, and is sent to near-infrared analyzer;
(B1) step is located between (A4) step and (A5) step;
When data processing is carried out, the humiture information to testing sample is compensated/corrected near-infrared analyzer.
9. method of work according to claim 7, it is characterised in that:The test substance is moisture and/or protein.
CN201611255173.3A 2016-12-30 2016-12-30 Cuttage formula near-infrared probe and its method of work Withdrawn CN106769984A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113959635A (en) * 2021-09-02 2022-01-21 中国科学院合肥物质科学研究院 Hydraulic type calibration device and method for flexible force-sensitive sensor array
CN116818711A (en) * 2023-08-28 2023-09-29 四川威斯派克科技有限公司 Near infrared spectrum detector

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102313700A (en) * 2011-08-09 2012-01-11 聚光科技(杭州)股份有限公司 Analyzer for cereal and oil plants and working method thereof
CN204807345U (en) * 2015-07-13 2015-11-25 河南工业大学 Near -infrared detects uses grain sampling device
CN105466881A (en) * 2016-01-14 2016-04-06 昆明睿意铂科技股份有限公司 Portable near-infrared spectrum detection system
CN106037668A (en) * 2016-07-06 2016-10-26 北京交通大学 Raman probe for in-vivo and in-situ puncture diagnosis
CN206440611U (en) * 2016-12-30 2017-08-25 聚光科技(杭州)股份有限公司 Cuttage formula near-infrared probe

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102313700A (en) * 2011-08-09 2012-01-11 聚光科技(杭州)股份有限公司 Analyzer for cereal and oil plants and working method thereof
CN204807345U (en) * 2015-07-13 2015-11-25 河南工业大学 Near -infrared detects uses grain sampling device
CN105466881A (en) * 2016-01-14 2016-04-06 昆明睿意铂科技股份有限公司 Portable near-infrared spectrum detection system
CN106037668A (en) * 2016-07-06 2016-10-26 北京交通大学 Raman probe for in-vivo and in-situ puncture diagnosis
CN206440611U (en) * 2016-12-30 2017-08-25 聚光科技(杭州)股份有限公司 Cuttage formula near-infrared probe

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113959635A (en) * 2021-09-02 2022-01-21 中国科学院合肥物质科学研究院 Hydraulic type calibration device and method for flexible force-sensitive sensor array
CN116818711A (en) * 2023-08-28 2023-09-29 四川威斯派克科技有限公司 Near infrared spectrum detector
CN116818711B (en) * 2023-08-28 2023-11-10 四川威斯派克科技有限公司 Near infrared spectrum detector

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