CN106665570B - A kind of agent of foam cleaning and sterilizing and its application containing Peracetic acid - Google Patents
A kind of agent of foam cleaning and sterilizing and its application containing Peracetic acid Download PDFInfo
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- CN106665570B CN106665570B CN201611185724.3A CN201611185724A CN106665570B CN 106665570 B CN106665570 B CN 106665570B CN 201611185724 A CN201611185724 A CN 201611185724A CN 106665570 B CN106665570 B CN 106665570B
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- sterilizing agent
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/16—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group; Thio analogues thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/22—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing ingredients stabilising the active ingredients
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/30—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests characterised by the surfactants
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
Landscapes
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Dentistry (AREA)
- Zoology (AREA)
- Plant Pathology (AREA)
- Environmental Sciences (AREA)
- Engineering & Computer Science (AREA)
- Agronomy & Crop Science (AREA)
- Wood Science & Technology (AREA)
- Pest Control & Pesticides (AREA)
- Toxicology (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Detergent Compositions (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Apparatus For Disinfection Or Sterilisation (AREA)
Abstract
The foam cleaning and sterilizing agent containing Peracetic acid that the present invention relates to a kind of, a kind of foam cleaning and sterilizing agent containing Peracetic acid, which is characterized in that the foam cleaning and sterilizing agent includes acetic acid, hydrogen peroxide, surfactant and water.The present invention also provides the method and its application for the foam cleaning and sterilizing agent for using this to contain Peracetic acid.The foam cleaning and sterilizing agent for containing Peracetic acid utilizes the high-effective disinfecting effect of Peracetic acid, being obtained by addition cleaning and foaming with surfactant can widely applied foam cleaning and sterilizing agent, foam disinfectant more saves disinfectant consumption than immersion or fountain disinfection, can be used for the foam disinfectant of equipment surface, inclined surface, irrigation canals and ditches, rough earth etc.；Cleaning action more can be played while disinfection, does not have to cumbersome ground multistep and carries out.
Description
Technical field
The present invention relates to disinfectant field more particularly to a kind of foam cleaning and sterilizing agent containing Peracetic acid and its answer
With.
Background technique
There are miscellaneous foam cleaning agent and disinfectant in food and drink, the fields such as health care.Wherein sodium hypochlorite disappears
Toxic agent is very popular, not only has Disinfection Effect and can decompose organic dirt, has cleaning effect.But the cleaning containing sodium hypochlorite
Stability is poor all the time for sterile products, and 30 days contents decrease beyond 10% under suitable condition of storage；Sodium hypochlorite corrosion
Property is strong, easily causes spot corrosion to equipment.Unitary Peracetic acid is widely used on various occasions as high effect disinfectants in recent years, makes
Peroxyacetic acid disinfectant is impregnated, is rinsed, spraying article to be sterilized by the used time, to high operation requirements and thimerosal utilization rate it is low, mistake
The cleaning ability of fluoroacetic acid is limited, before disinfection or needs to further use cleaning agent after disinfection and be cleaned.
Therefore, it is necessary to provide a kind of foam cleaning and sterilizing agent, stable foam can be generated, so as to there is inclination
It is small that the body surface of angle or vertical object surface carry out the cleaning and sterilizing of foam coverage, disinfectant consumption, and while disinfection
Cleaning action can be played.
Summary of the invention
The foam cleaning and sterilizing agent containing Peracetic acid that one of the objects of the present invention is to provide a kind of, foam cleaning disappear
Toxic agent can save disinfectant consumption, and foam wall built-up effect is good, can play cleaning action while disinfection.
To realize that the purpose, the present invention provide a kind of foam cleaning and sterilizing agent containing Peracetic acid, the foam cleaning
Disinfectant includes acetic acid, hydrogen peroxide, surfactant and water.
Preferably, calculating according to mass percent, the foam cleaning and sterilizing agent includes following components:
Preferably, the surfactant includes oxidation amine surfactants and alkyl benzene sulphonate or its salt.
Preferably, the oxidation amine surfactants are N- dimethyl-alkyl amine oxide, according to mass percentage
It calculates, the content of the oxidation amine surfactants is 1%~9%.
Preferably, the alkylbenzene sulfonate is alkyl benzene sulphonate sodium salt or benzene sulfonamide acid potassium salt, according to quality percentage
Number calculates, and the content of the alkyl benzene sulphonate or its salt is 1%~5%.
Preferably, the foam cleaning and sterilizing agent further includes stabilizer, calculated according to mass percent, the stabilizer
Content is 0~1%.
Preferably, the stabilizer is at least one of EDTA, PAA, HEDP, EDTMP, NTA.
Another object of the present invention is provide a kind of method using foam cleaning and sterilizing agent as described above, the method packet
Include step:
(1) the foam cleaning and sterilizing agent is diluted；
(2) the foam cleaning and sterilizing agent after dilution is foamed；And
(3) the foam cleaning and sterilizing agent after foaming covers cleaning and sterilizing object surface.
Preferably, the application method further includes step (4): rinsing the foam on cleaning and sterilizing object surface.
Another object of the present invention is to provide a kind of application of foam cleaning and sterilizing agent as described above, and the foam is clear
Decontamination venom is applied to cleaning and sterilizing food manufacturing apparatus, factory, hospital or irrigation canals and ditches.
The prior art is compared, the foam cleaning and sterilizing agent of the present invention containing Peracetic acid, and its advantages include:
The Peracetic acid that acetic acid of the invention and hydrogen peroxide generate has efficient Disinfection Effect, and surfactant adds
Enter may make disinfectant that there is foaming effect and better cleaning effect.The foam cleaning disinfection liquid can generate stable bubble
Foam, so as to carry out the cleaning and sterilizing of foam coverage to the body surface for having tilt angle or vertical object surface, foam disappears
Poison more saves disinfectant consumption than immersion or fountain disinfection, can be used for equipment surface, inclined surface, irrigation canals and ditches, rough earth
Deng foam disinfectant, and sterilize while can play cleaning action.
Peracetic acid has strong oxidizing property, and the addition of conventional surfactants is easily decomposed, and decomposable process consumption is big
The Peracetic acid of amount influences the Disinfection Effect of product.Alkyl benzene sulphonate or its salt, oxidation amine surfactants resistance to oxidation, no
Easily by decomposition of peracetic acid.However, the additional amount of alkyl benzene sulphonate or its salt be it is a small amount of, less than oxidation amine surfactants
Additive amount, so that the foam cleaning disinfection liquid is more stable.Stabilizer can also be added in the foam cleaning agent, stabilizer can chelate miscellaneous
Matter, unhindered amina, metal ion etc. are catalyzed the substance of Peracetic acid reaction, further increase the stability of foam cleaning disinfection liquid.
Alkyl benzene sulphonate or its salt belong to anionic surfactant, there is a good cleaning effect, and amine-oxides class surfactant can be with
Foaming, and it is able to maintain the adhesive force increase that foam is more stable, on object surface.The compounding of the two so that foam cleaning disinfection liquid both
Cleaning effect is enhanced, and there is frothing function, new usage mode is made it have, is easy to execute-in-place, expand its application
Range.
Specific embodiment
The present invention is intended to provide a kind of foam cleaning and sterilizing agent containing Peracetic acid, the foam cleaning and sterilizing agent can save
Disinfectant consumption, foam wall built-up effect is good, can play cleaning action while disinfection.
Foam cleaning and sterilizing agent includes acetic acid, hydrogen peroxide, surfactant and water, is calculated according to mass percent, bubble
Foam cleaning and sterilizing agent includes following components:
Preferably, surfactant includes oxidation amine surfactants and alkyl benzene sulphonate or its salt.
Preferably, oxidation amine surfactants are N- dimethyl-alkyl amine oxide, calculated according to mass percent, oxygen
The content for changing amine surfactants is 1%~9%.
Preferably, alkylbenzene sulfonate is alkyl benzene sulphonate sodium salt or benzene sulfonamide acid potassium salt, according to mass percentage
It calculates, the content of alkyl benzene sulphonate or its salt is 1%~5%.
Preferably, foam cleaning and sterilizing agent further includes stabilizer, calculated according to mass percent, the content of stabilizer is 0
~1%.
Preferably, stabilizer is at least one of EDTA, PAA, HEDP, EDTMP, NTA.
Using the method for foam cleaning and sterilizing agent as above, method comprising steps of
(1) agent of foam cleaning and sterilizing is diluted；
(2) the foam cleaning and sterilizing agent after dilution is foamed；
(3) the foam cleaning and sterilizing agent after foaming covers cleaning and sterilizing object surface；And
(4) foam on cleaning and sterilizing object surface is rinsed.
Foam cleaning disinfection liquid is applied to cleaning and sterilizing food manufacturing apparatus, factory, hospital or irrigation canals and ditches.
The present invention is further elaborated for following specific embodiments, but not as a limitation of the invention.
Embodiment 1
A kind of Peracetic acid foam cleaning and sterilizing agent is made of by weight percent following raw material, and preparation process is as follows:
7 parts of water are added in plastic bottle, 1 part of acetic acid, 1 part of hydrogen peroxide, is uniformly mixed；Cetyl sulfonic acid is added
0.02 part of sodium, it is 0.2 part that N- dimethyl-cetyl amine oxide content, which is added, and it is 0.02 part that EDTA, which is added,；More than being added after stirring
Measure water.Product is stored at room temperature 1-7 days, the use of quick measurement test paper measurement peroxyacetic acid concentration is 0.28%.
Embodiment 2
A kind of Peracetic acid foam cleaning and sterilizing agent is made of by weight percent following raw material, and preparation process is as follows:
5 parts of water are added in plastic bottle, 3.5 parts of acetic acid, 2 parts of hydrogen peroxide, is uniformly mixed；Xylene monosulfonic acid is added
0.05 part of sodium, it is 0.3 part that N- dimethyl-cetyl amine oxide content, which is added, and it is 0.02 part that NTA, which is added,；More than being added after stirring
Measure water.Product is stored at room temperature 1-7 days, the use of quick measurement test paper measurement peroxyacetic acid concentration is 3.5%.
Embodiment 3
A kind of Peracetic acid foam cleaning and sterilizing agent is made of by weight percent following raw material, and preparation process is as follows:
3 parts of water are added in plastic bottle, 4 parts of acetic acid, 2.5 parts of hydrogen peroxide, is uniformly mixed；Xylene monosulfonic acid is added
0.05 part of sodium, it is 0.4 part that N- dimethyl-cetyl amine oxide content, which is added, and it is 0.04 part that EDTA, which is added,；More than being added after stirring
Measure water.Product is stored at room temperature 1-7 days, the use of quick measurement test paper measurement peroxyacetic acid concentration is 5.4%.
Comparative example 1
A kind of Peracetic acid is made of without alveolitoid disinfectant following raw material by weight percent, and preparation process is as follows:
3 parts of water are added in plastic bottle, 4 parts of acetic acid, 2.5 parts of hydrogen peroxide, is uniformly mixed；Xylene monosulfonic acid is added
0.05 part of sodium, it is 0.04 part that EDTA, which is added,；Excess water is added after stirring.Product is stored at room temperature 1-7 days, uses quick measurement test paper
Measuring peroxyacetic acid concentration is 5.4%.
Thimerosal prepared by Example 1~3 and comparative example 1 is by test method according to " disinfection technology standard " (2002 editions)
It is required that carrying out, using suspension quantitative bacteric idal experiment.
The bactericidal effect of foam cleaning and sterilizing agent
It is 1000mg/L, disinfection time 30S-60S, experimental result such as table 1 that sample, which is diluted to Peracetic acid content,
It is shown.
The bactericidal effect of 1 foam cleaning disinfection liquid of table
Foam cleaning disinfection liquid of the present invention has good inhibiting effect to common germ as can be seen from Table 1, can
Killing rate is up to 100%, and sterilizing time can be as short as 1min.Examples 1 to 3 foam is stablized, long with object table time of contact, more right
Ratio 1 has better bactericidal effect.
The measurement of foam cleaning and sterilizing agent frostproof froth n
500ml peracetic acid soln (Peracetic acid is diluted to 1000mg/L) is set to flow to same solution from 450mm height
After solution surface, foam volume that Roche foam meter measures at room temperature.
2 sample foams performance test one of table
| Sample number into spectrum | Initial foam cm | 3min foam | 10min foam |
| Embodiment 1 | 68 | 52 | 33 |
| Embodiment 2 | 49 | 42 | 24 |
| Embodiment 3 | 36 | 28 | 18 |
| Comparative example 1 | 6 | 0 | 0 |
Foam cleaning and sterilizing agent foam stablizes the time
Test method, with foaming machine by the sample 500g foaming to stainless steel plate after dilution, stainless steel plate area is 1 flat
Square rice tilts 45 degree angles, on foam uniform fold to panel, foam that below the panel collection slides from stainless steel faceplate.On time
Between weigh slide foam weight.
3 sample foams performance test two of table
| Sample number into spectrum | 1min | 2min | 5min | 10min |
| Embodiment 1 | 193 | 374 | 425 | 459 |
| Embodiment 2 | 247 | 396 | 432 | 470 |
| Embodiment 3 | 253 | 401 | 450 | 472 |
| Comparative example 1 | 442 | 468 | 472 | 473 |
Frostproof froth n measurement, foam are stablized two measurements of time while being illustrated, embodiment 1, embodiment 2, and embodiment 3 has
Preferable foaming effect, foam have certain stability, and foaming machine can be used and normally foamed, it can be achieved that foam disinfectant.
The foam stability of comparative example 1 is very poor, foaming machine cannot be used normally to be foamed, sample, which does not foam, directly to be wandered to face
Below plate.
The prior art is compared, the foam cleaning and sterilizing agent of the present invention containing Peracetic acid, and its advantages include:
The Peracetic acid that acetic acid of the invention and hydrogen peroxide generate has efficient Disinfection Effect, and surfactant adds
Enter may make disinfectant that there is foaming effect and better cleaning effect.The foam cleaning disinfection liquid can generate stable bubble
Foam, so as to carry out the cleaning and sterilizing of foam coverage to the body surface for having tilt angle or vertical object surface, foam disappears
Poison more saves disinfectant consumption than immersion or fountain disinfection, can be used for equipment surface, inclined surface, irrigation canals and ditches, rough earth
Deng foam disinfectant, and sterilize while can play cleaning action.
Peracetic acid has strong oxidizing property, and the addition of conventional surfactants is easily decomposed, and decomposable process consumption is big
The Peracetic acid of amount influences the Disinfection Effect of product.Alkyl benzene sulphonate or its salt, oxidation amine surfactants resistance to oxidation, no
Easily by decomposition of peracetic acid.However, the additional amount of alkyl benzene sulphonate or its salt be it is a small amount of, less than oxidation amine surfactants
Additive amount, so that the foam cleaning disinfection liquid is more stable.Stabilizer can also be added in the foam cleaning agent, stabilizer can chelate miscellaneous
Matter, unhindered amina, metal ion etc. are catalyzed the substance of Peracetic acid reaction, further increase the stability of foam cleaning disinfection liquid.
Alkyl benzene sulphonate or its salt belong to anionic surfactant, there is a good cleaning effect, and amine-oxides class surfactant can be with
Foaming, and it is able to maintain the adhesive force increase that foam is more stable, on object surface.The compounding of the two so that foam cleaning disinfection liquid both
Cleaning effect is enhanced, and there is frothing function, new usage mode is made it have, is easy to execute-in-place, expand its application
Range.
Above disclosed is only presently preferred embodiments of the present invention, cannot limit the right of the present invention with this certainly
Range, therefore according to equivalent variations made by scope of the present invention patent, it is still within the scope of the present invention.
Claims (6)
1. a kind of foam cleaning and sterilizing agent containing Peracetic acid, which is characterized in that for have the body surface of tilt angle or
Vertical object surface carries out cleaning and sterilizing, calculates according to mass percent, the foam cleaning and sterilizing agent includes following components:
The surfactant includes oxidation amine surfactants and alkyl benzene sulphonate or its salt, and the oxidation amine surface is living
Property agent be N- dimethyl-alkyl amine oxide, it is described oxidation amine surfactants content be 1%~9%, the benzene sulfonamide
The content of acid or its salt is 1%~5%, and the content of the alkyl benzene sulphonate or its salt is less than the oxidation amine surfactants
Content.
2. the foam cleaning and sterilizing agent containing Peracetic acid as described in claim 1, which is characterized in that the foam cleaning disappears
Toxic agent further includes stabilizer, is calculated according to mass percent, and the content of the stabilizer is 0~1%.
3. the foam cleaning and sterilizing agent containing Peracetic acid as claimed in claim 2, which is characterized in that the stabilizer is
At least one of EDTA, PAA, HEDP, EDTMP, NTA.
4. a kind of method using foam cleaning and sterilizing agent as claimed in any one of claims 1 to 3, which is characterized in that described
Method comprising steps of
(1) the foam cleaning and sterilizing agent is diluted；
(2) the foam cleaning and sterilizing agent after dilution is foamed；And
(3) the foam cleaning and sterilizing agent after foaming covers cleaning and sterilizing object surface.
5. application method as claimed in claim 4, which is characterized in that further include that step (4) rinse cleaning and sterilizing object surface
Foam.
6. a kind of application of foam cleaning and sterilizing agent as claimed in any one of claims 1 to 3, by the foam cleaning disinfection liquid
Applied to cleaning and sterilizing food manufacturing apparatus, factory, hospital or irrigation canals and ditches.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611185724.3A CN106665570B (en) | 2016-12-20 | 2016-12-20 | A kind of agent of foam cleaning and sterilizing and its application containing Peracetic acid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611185724.3A CN106665570B (en) | 2016-12-20 | 2016-12-20 | A kind of agent of foam cleaning and sterilizing and its application containing Peracetic acid |
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| CN106665570A CN106665570A (en) | 2017-05-17 |
| CN106665570B true CN106665570B (en) | 2019-09-03 |
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Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108047113B (en) * | 2017-12-14 | 2018-11-23 | 广州中冠动物药业有限公司 | A kind of synthesis technology of Peracetic acid |
| CN111165478A (en) * | 2020-02-11 | 2020-05-19 | 南通大学 | Foam type sterilization, disinfection and air purification agent and preparation method and application thereof |
| CN111264555A (en) * | 2020-03-06 | 2020-06-12 | 吉林云飞医药有限公司 | Hydrogen peroxide disinfectant and preparation method and application thereof |
| CN111494870B (en) * | 2020-03-18 | 2021-11-19 | 中国人民解放军陆军防化学院 | Disinfection method |
| CN112956475A (en) * | 2021-01-25 | 2021-06-15 | 海韵一剑大卫生科技有限公司 | Foam type peroxyacetic acid disinfectant, and preparation method and use method thereof |
| CN115486445B (en) * | 2021-11-02 | 2024-03-26 | 上海柯珑清洁技术有限公司 | Cleaning disinfectant and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4263177A (en) * | 1979-06-27 | 1981-04-21 | Sherex Chemical Company, Inc. | Amine oxide foam stabilizers for alkyl benzene sulfonate foaming agents |
| CN1711845A (en) * | 2004-06-25 | 2005-12-28 | 殷生章 | Disinfectant for killing coronary virus |
| CN101507430A (en) * | 2009-03-31 | 2009-08-19 | 中国检验检疫科学研究院 | Freezeproof foam disinfectant and preparation method thereof |
| CN102090393A (en) * | 2010-12-29 | 2011-06-15 | 广东环凯微生物科技有限公司 | Stable peroxyacetic acid disinfectant |
-
2016
- 2016-12-20 CN CN201611185724.3A patent/CN106665570B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4263177A (en) * | 1979-06-27 | 1981-04-21 | Sherex Chemical Company, Inc. | Amine oxide foam stabilizers for alkyl benzene sulfonate foaming agents |
| CN1711845A (en) * | 2004-06-25 | 2005-12-28 | 殷生章 | Disinfectant for killing coronary virus |
| CN101507430A (en) * | 2009-03-31 | 2009-08-19 | 中国检验检疫科学研究院 | Freezeproof foam disinfectant and preparation method thereof |
| CN102090393A (en) * | 2010-12-29 | 2011-06-15 | 广东环凯微生物科技有限公司 | Stable peroxyacetic acid disinfectant |
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