CN106621946A - High-viscosity carbon nanotube slurry premixing device - Google Patents
High-viscosity carbon nanotube slurry premixing device Download PDFInfo
- Publication number
- CN106621946A CN106621946A CN201610784385.4A CN201610784385A CN106621946A CN 106621946 A CN106621946 A CN 106621946A CN 201610784385 A CN201610784385 A CN 201610784385A CN 106621946 A CN106621946 A CN 106621946A
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- CN
- China
- Prior art keywords
- support
- tank body
- storage tank
- motor
- tank
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F29/00—Mixers with rotating receptacles
- B01F29/80—Mixers with rotating receptacles rotating about a substantially vertical axis
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F29/00—Mixers with rotating receptacles
- B01F29/40—Parts or components, e.g. receptacles, feeding or discharging means
- B01F29/401—Receptacles, e.g. provided with liners
- B01F29/4011—Receptacles, e.g. provided with liners characterised by the shape or cross-section of the receptacle, e.g. of Y-, Z -, S -, or X shape
- B01F29/40113—Conical, double-conicalor diabolo shapes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/40—Mounting or supporting mixing devices or receptacles; Clamping or holding arrangements therefor
- B01F35/43—Supporting receptacles on frames or stands
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/71—Feed mechanisms
- B01F35/717—Feed mechanisms characterised by the means for feeding the components to the mixer
- B01F35/71805—Feed mechanisms characterised by the means for feeding the components to the mixer using valves, gates, orifices or openings
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/75—Discharge mechanisms
- B01F35/754—Discharge mechanisms characterised by the means for discharging the components from the mixer
- B01F35/7547—Discharge mechanisms characterised by the means for discharging the components from the mixer using valves, gates, orifices or openings
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physics & Mathematics (AREA)
- Geometry (AREA)
- Carbon And Carbon Compounds (AREA)
Abstract
The invention discloses a high-viscosity carbon nanotube slurry premixing device. The high-viscosity carbon nanotube slurry premixing device comprises a double-layer support, a second support is separably erected on a first support, a caster is arranged on a landing leg of the first support, a motor is detachably arranged on the first support, the motor is connected with a rotating shaft, and a storage tank is rotatably arranged on the rotating shaft in a rotating way; an air inlet valve, an air outlet valve and a charging and discharging valve are arranged on the storage tank body and communicate the exterior of the storage tank body with the interior of the storage tank body, the air inlet valve communicates the interior of the storage tank body with a protective gas source arranged outside the tank body, and the air outlet valve communicates the interior of the storage tank body with a vacuum pump arranged outside the tank body. When the high-viscosity carbon nanotube slurry premixing device is used for mixing materials, the motor drives the storage tank to rotate, so that the materials in the tank body are uniformly mixed; the tank body is arranged in the support when the storage tank rotates, so that the tank body can be prevented from impacting peripheral equipment, and certain protective effect is achieved; and the support is designed into a double-layer detachable structure, so that the motor and the tank body can be conveniently disassembled, and maintenance and disassembly are convenient.
Description
Technical field
The present invention relates to the premix of slurry and caching technology field, particularly a kind of high viscosity carbon nano tube paste is loaded in mixture in advance
Put.
Background technology
CNT, with excellent chemistry, physical property, is widely used in material as new nano-carbon material
The fields such as material, the energy, biology.But carbon nanotube powder is with the presence of aggregate form, it is difficult to compatible with other materials, therefore needs
CNT dispersion is obtained being applied again after carbon nano tube paste in organic solvent.CNT slurry in general workshop
Material pre-compounding process requires humid control within 30%, particularly exists for the slurry humidity requirement control in lithium ion battery
Within 10%, and carbon nanotube powder is very light, and dust is easily formed in atmosphere, causes the pollution of air and equipment, therefore whole
Need to be carried out in dry behaviour and in the environment of sealing in the mixed process of individual slurry.
But currently without the pre-mixing apparatus produced particular for carbon nano tube paste, it is existing can generally plastics
Tank, such as Patent No. CN03214298.6, the patent of entitled sealed plastic tank, but common sealed plastic tank institute
Disposable lid mostly is with lid, it is impossible to reuse, and charging process can only be carried out in the case where lid is fully opened,
CNT easily floats pollution peripheral equipment under open environment, while can also absorb large quantity of moisture, has a strong impact on slurry quality.
It is also a kind of to select as sealing enamel reaction still, such as Application No. CN201520787146.5, entitled electronic type temperature
The enamel reaction still of degree monitoring, but the equipment good airproof performance, but high cost, weight is big, not economical enough as slurry buffer tank
It is practical.
The content of the invention
The technical problem to be solved in the present invention is to be directed to above-mentioned the deficiencies in the prior art, and provides a kind of CNT slurry
Material pre-mixing apparatus.
To solve above-mentioned technical problem, the technical solution used in the present invention is:
A kind of high viscosity carbon nano tube paste pre-mixing apparatus, including double-layer scaffold, respectively first support and second support, second
Support is detachable to be set up in first support, and castor is provided with the supporting leg of first support, detachable in first support to set
Motor is equipped with, rotating shaft is connected with motor, storage tank is rotated and is arranged in the rotating shaft, rotates with rotating shaft;
Tank body is connected on storage tank and is outwardly and inwardly provided with intake valve, air outlet valve and charging/discharging valve, intake valve connection is deposited
Storage tank tank interior and the shielding gas source of the gas being arranged at outside tank body, air outlet valve connects storage tank tank interior and is arranged at tank body
Outside vavuum pump.
The edge of the above second support is provided with multiple suspension hooks.
The above first support and second support have four supporting legs.
The above motor can positive and negative alternate rotation, drive the positive and negative alternate rotation of storage tank.
The protective gas source of the above shielding gas source of the gas is nitrogen.
The present invention has the following technical effect that using after said structure:
Intake valve, air outlet valve and charging/discharging valve are provided with storage tank of the present invention, during charging, are discharged by the air outlet valve
Air in the storage tank, by the intake valve to storage tank inject protective gas, to realize anhydrous, oxygen-free environment under plus
Material, batch mixing and storage slurry, so as to avoiding raw material contaminated or polluting miscellaneous equipment.
During compound of the present invention, storage tank is driven to rotate by motor, tank when being well mixed material in tank, and rotating
Body is arranged in support, can prevent tank body from surrounding devices are clashed into during rotation, plays certain protective role;Prop up and set up
Count into double-layer detachable formula structure, convenient dismounting motor and tank body, convenient maintenance and dismounting.
Intake valve, air outlet valve and the charging/discharging valve of the present invention is all valve mechanism, therefore, when all in the vapor tight tank
When air valve is all closed, the sealing of the vapor tight tank very well, can be with long storage time carbon nano tube paste.
Description of the drawings
Fig. 1 is the structural representation of the present invention.
Specific embodiment
In conjunction with the accompanying drawings, the present invention is further detailed explanation.These accompanying drawings are simplified schematic diagram, only with
The basic structure of the illustration explanation present invention, therefore it only shows the composition relevant with the present invention.
The present invention proposes a kind of nanotube slurry pre-mixing apparatus, and it includes double-layer scaffold and the electricity being fixed in first support
Machine and storage tank, are provided with intake valve, air outlet valve and charging/discharging valve on the storage tank, during charging, arranged by the air outlet valve
The air gone out in the storage tank, by the intake valve to storage tank inject protective gas, to realize anhydrous, oxygen-free environment under
Charging, batch mixing and storage slurry, so as to avoiding raw material contaminated or polluting miscellaneous equipment.
As shown in figure 1, for a kind of a kind of example structure of high viscosity carbon nano tube paste pre-mixing apparatus of the present invention,
Including double-layer scaffold, respectively first support 1 and second support 2, second support 2 is detachable to be set up in first support 1, the
Castor 3 is provided with the supporting leg of one support 1, it is detachable in first support 1 to be provided with motor 4, rotating shaft is connected with motor 4,
Storage tank 5 is rotated and is arranged in the rotating shaft, is rotated with rotating shaft.
Tank body is connected on the tank body of storage tank 5 and is outwardly and inwardly provided with intake valve 7, air outlet valve 9 and charging/discharging valve 8, air inlet
Valve 7 connects the tank interior of storage tank 5 and the shielding gas source of the gas 10 being arranged at outside tank body, in the connection tank body of storage tank 5 of air outlet valve 9
Portion and the vavuum pump 11 being arranged at outside tank body.
Storage tank lower rotation is arranged on machine shaft, and structure design is simple, can also be turned by arranging on support
Axle, storage tank passes through sealing between bearing and the rotating shaft and rotates connection.
For the convenience for making and installing, the first support and second support have four supporting legs.
For the convenience of lifting, the edge of the second support is provided with multiple suspension hooks 6.
During in order to rotate, premix it is full and uniform, the motor 4 can positive and negative alternate rotation, drive the positive and negative friendship of storage tank 5
For rotation.
The protective gas source of the shielding gas source of the gas 10 is nitrogen.
The operation principle of the present invention:
The shielding gas source of the gas is connected with intake valve first, the vavuum pump is connected with the air outlet valve, then open into
Air valve and air outlet valve, and start vavuum pump and Nitrogen source gases.The air outlet valve is passed through by the air in the tank body by vavuum pump
Extract out, so as to form negative pressure in the inner chamber of the tank body, so that the nitrogen that the Nitrogen source gases are provided passes through the intake valve
Flow in the tank body.When protective gas is full of in the inner chamber of the tank body, and in the presence of protective gas, input and output material is opened
Valve, raw material such as CNT and organic solvent are added in the tank body by the charging/discharging valve.
After raw material is added, the charging/discharging valve is closed, intake valve, air outlet valve, Nitrogen source gases and vacuum are subsequently closed successively
Pump.During adding raw material from the charging/discharging valve to the storage tank, it is passed through always in the inner chamber of the storage tank
Protective gas, it can be ensured that the oxygen and moisture in tank body is extremely low, so as to realize being fed in the environment of anhydrous, anaerobic, it is to avoid
Raw material is contaminated or pollutes miscellaneous equipment.
During compound of the present invention, storage tank is driven to rotate by motor, tank when being well mixed material in tank, and rotating
Body is arranged in support, can prevent tank body from surrounding devices are clashed into during rotation, plays certain protective role;Prop up and set up
Count into double-layer detachable formula structure, convenient dismounting motor and tank body, convenient maintenance and dismounting.
Mixing process is:The connection of the Nitrogen source gases and the intake valve is disconnected first, disconnects the vavuum pump and institute
State the connection of air outlet valve.In the case where the intake valve, air outlet valve and charging/discharging valve valve are all closed, the storage tank is rotated,
Premixed with the CNT and organic solvent in being positioned over the inner chamber of the tank body, obtain carbon nano tube paste, so as to
Realize the batch mixing material in the environment of anhydrous, anaerobic, it is to avoid raw material is contaminated or pollutes miscellaneous equipment.
Because the intake valve on the storage tank, air outlet valve and charging/discharging valve are all valve mechanism, therefore, when described closed
When all air valves in tank are all closed, the sealing of the vapor tight tank very well, can be with long storage time carbon nano tube paste.
With the above-mentioned desirable embodiment according to the present invention as enlightenment, by above-mentioned description, relevant staff is complete
Entirely various change and modification can be carried out in the range of without departing from this invention technological thought.The technology of this invention
Property scope is not limited to the content on specification, it is necessary to its technical scope is determined according to right.
Claims (5)
1. a kind of high viscosity carbon nano tube paste pre-mixing apparatus, it is characterised in that:Including double-layer scaffold, respectively first support
(1)And second support(2), second support(2)It is detachable to be set up in first support(1)On, first support(1)Supporting leg on set
It is equipped with castor(3), first support(1)It is above detachable to be provided with motor(4), motor(4)On be connected with rotating shaft, storage tank(5)
Rotation is arranged in the rotating shaft, is rotated with rotating shaft;
Storage tank(5)Tank body is connected on tank body and is outwardly and inwardly provided with intake valve(7), air outlet valve(9)And charging/discharging valve(8),
Intake valve(7)Connection storage tank(5)Tank interior and the shielding gas source of the gas being arranged at outside tank body(10), air outlet valve(9)Connection
Storage tank(5)Tank interior and the vavuum pump being arranged at outside tank body(11).
2. high viscosity carbon nano tube paste pre-mixing apparatus according to claim 1, it is characterised in that:The second support
(2)Edge be provided with multiple suspension hooks(6).
3. high viscosity carbon nano tube paste pre-mixing apparatus according to claim 1, it is characterised in that:The first support
(1)And second support(2)There are four supporting legs.
4. high viscosity carbon nano tube paste pre-mixing apparatus according to claim 1, it is characterised in that:The motor(4)Energy
Enough positive and negative alternate rotations, drive storage tank(5)Positive and negative alternate rotation.
5. high viscosity carbon nano tube paste pre-mixing apparatus according to claim 1, it is characterised in that:The shielding gas source of the gas
(10)Protective gas source be nitrogen.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201610784385.4A CN106621946A (en) | 2016-08-31 | 2016-08-31 | High-viscosity carbon nanotube slurry premixing device |
Applications Claiming Priority (1)
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CN201610784385.4A CN106621946A (en) | 2016-08-31 | 2016-08-31 | High-viscosity carbon nanotube slurry premixing device |
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Publication Number | Publication Date |
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CN106621946A true CN106621946A (en) | 2017-05-10 |
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CN201610784385.4A Pending CN106621946A (en) | 2016-08-31 | 2016-08-31 | High-viscosity carbon nanotube slurry premixing device |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106345353A (en) * | 2016-08-31 | 2017-01-25 | 无锡东恒新能源科技有限公司 | Carbon nanotube paste stirring reactor |
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CN202893264U (en) * | 2012-10-24 | 2013-04-24 | 无锡东恒新能源材料有限公司 | Nanotube slurry premixing and temporary storing device |
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CN204865680U (en) * | 2015-07-01 | 2015-12-16 | 江西格雷斯科技股份有限公司 | Stirring compounding device |
CN106345353A (en) * | 2016-08-31 | 2017-01-25 | 无锡东恒新能源科技有限公司 | Carbon nanotube paste stirring reactor |
CN206082385U (en) * | 2016-08-31 | 2017-04-12 | 无锡东恒新能源科技有限公司 | Carbon nanotube paste premixing device |
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2016
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Patent Citations (10)
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CN202893440U (en) * | 2012-10-24 | 2013-04-24 | 无锡东恒新能源材料有限公司 | Discharge system of ball grinder |
CN202893264U (en) * | 2012-10-24 | 2013-04-24 | 无锡东恒新能源材料有限公司 | Nanotube slurry premixing and temporary storing device |
CN202893471U (en) * | 2012-10-24 | 2013-04-24 | 无锡东恒新能源材料有限公司 | Slurry ball-milling and sand-milling production system |
CN104275112A (en) * | 2013-07-01 | 2015-01-14 | 中国科学院过程工程研究所 | Square-tapered rotary mixer |
CN203710955U (en) * | 2013-12-18 | 2014-07-16 | 安徽信远包装科技有限公司 | Powder mixer |
CN203886465U (en) * | 2014-03-31 | 2014-10-22 | 中美上海施贵宝制药有限公司 | Storage tank for mixing medicine materials |
CN204137638U (en) * | 2014-08-07 | 2015-02-04 | 无锡东恒新能源科技有限公司 | Highly viscous slurry preparation system and buffer memory bucket thereof |
CN204865680U (en) * | 2015-07-01 | 2015-12-16 | 江西格雷斯科技股份有限公司 | Stirring compounding device |
CN106345353A (en) * | 2016-08-31 | 2017-01-25 | 无锡东恒新能源科技有限公司 | Carbon nanotube paste stirring reactor |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN106345353A (en) * | 2016-08-31 | 2017-01-25 | 无锡东恒新能源科技有限公司 | Carbon nanotube paste stirring reactor |
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Application publication date: 20170510 |