CN106621946A - High-viscosity carbon nanotube slurry premixing device - Google Patents

High-viscosity carbon nanotube slurry premixing device Download PDF

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Publication number
CN106621946A
CN106621946A CN201610784385.4A CN201610784385A CN106621946A CN 106621946 A CN106621946 A CN 106621946A CN 201610784385 A CN201610784385 A CN 201610784385A CN 106621946 A CN106621946 A CN 106621946A
Authority
CN
China
Prior art keywords
support
tank body
storage tank
motor
tank
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610784385.4A
Other languages
Chinese (zh)
Inventor
沈宇栋
顾灵锋
万仁涛
冯祺
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Wuxi Dongheng New Energy Technology Co Ltd
Original Assignee
Wuxi Dongheng New Energy Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Wuxi Dongheng New Energy Technology Co Ltd filed Critical Wuxi Dongheng New Energy Technology Co Ltd
Priority to CN201610784385.4A priority Critical patent/CN106621946A/en
Publication of CN106621946A publication Critical patent/CN106621946A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F29/00Mixers with rotating receptacles
    • B01F29/80Mixers with rotating receptacles rotating about a substantially vertical axis
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F29/00Mixers with rotating receptacles
    • B01F29/40Parts or components, e.g. receptacles, feeding or discharging means
    • B01F29/401Receptacles, e.g. provided with liners
    • B01F29/4011Receptacles, e.g. provided with liners characterised by the shape or cross-section of the receptacle, e.g. of Y-, Z -, S -, or X shape
    • B01F29/40113Conical, double-conicalor diabolo shapes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/40Mounting or supporting mixing devices or receptacles; Clamping or holding arrangements therefor
    • B01F35/43Supporting receptacles on frames or stands
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/71Feed mechanisms
    • B01F35/717Feed mechanisms characterised by the means for feeding the components to the mixer
    • B01F35/71805Feed mechanisms characterised by the means for feeding the components to the mixer using valves, gates, orifices or openings
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/75Discharge mechanisms
    • B01F35/754Discharge mechanisms characterised by the means for discharging the components from the mixer
    • B01F35/7547Discharge mechanisms characterised by the means for discharging the components from the mixer using valves, gates, orifices or openings

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Geometry (AREA)
  • Carbon And Carbon Compounds (AREA)

Abstract

The invention discloses a high-viscosity carbon nanotube slurry premixing device. The high-viscosity carbon nanotube slurry premixing device comprises a double-layer support, a second support is separably erected on a first support, a caster is arranged on a landing leg of the first support, a motor is detachably arranged on the first support, the motor is connected with a rotating shaft, and a storage tank is rotatably arranged on the rotating shaft in a rotating way; an air inlet valve, an air outlet valve and a charging and discharging valve are arranged on the storage tank body and communicate the exterior of the storage tank body with the interior of the storage tank body, the air inlet valve communicates the interior of the storage tank body with a protective gas source arranged outside the tank body, and the air outlet valve communicates the interior of the storage tank body with a vacuum pump arranged outside the tank body. When the high-viscosity carbon nanotube slurry premixing device is used for mixing materials, the motor drives the storage tank to rotate, so that the materials in the tank body are uniformly mixed; the tank body is arranged in the support when the storage tank rotates, so that the tank body can be prevented from impacting peripheral equipment, and certain protective effect is achieved; and the support is designed into a double-layer detachable structure, so that the motor and the tank body can be conveniently disassembled, and maintenance and disassembly are convenient.

Description

A kind of high viscosity carbon nano tube paste pre-mixing apparatus
Technical field
The present invention relates to the premix of slurry and caching technology field, particularly a kind of high viscosity carbon nano tube paste is loaded in mixture in advance Put.
Background technology
CNT, with excellent chemistry, physical property, is widely used in material as new nano-carbon material The fields such as material, the energy, biology.But carbon nanotube powder is with the presence of aggregate form, it is difficult to compatible with other materials, therefore needs CNT dispersion is obtained being applied again after carbon nano tube paste in organic solvent.CNT slurry in general workshop Material pre-compounding process requires humid control within 30%, particularly exists for the slurry humidity requirement control in lithium ion battery Within 10%, and carbon nanotube powder is very light, and dust is easily formed in atmosphere, causes the pollution of air and equipment, therefore whole Need to be carried out in dry behaviour and in the environment of sealing in the mixed process of individual slurry.
But currently without the pre-mixing apparatus produced particular for carbon nano tube paste, it is existing can generally plastics Tank, such as Patent No. CN03214298.6, the patent of entitled sealed plastic tank, but common sealed plastic tank institute Disposable lid mostly is with lid, it is impossible to reuse, and charging process can only be carried out in the case where lid is fully opened, CNT easily floats pollution peripheral equipment under open environment, while can also absorb large quantity of moisture, has a strong impact on slurry quality. It is also a kind of to select as sealing enamel reaction still, such as Application No. CN201520787146.5, entitled electronic type temperature The enamel reaction still of degree monitoring, but the equipment good airproof performance, but high cost, weight is big, not economical enough as slurry buffer tank It is practical.
The content of the invention
The technical problem to be solved in the present invention is to be directed to above-mentioned the deficiencies in the prior art, and provides a kind of CNT slurry Material pre-mixing apparatus.
To solve above-mentioned technical problem, the technical solution used in the present invention is:
A kind of high viscosity carbon nano tube paste pre-mixing apparatus, including double-layer scaffold, respectively first support and second support, second Support is detachable to be set up in first support, and castor is provided with the supporting leg of first support, detachable in first support to set Motor is equipped with, rotating shaft is connected with motor, storage tank is rotated and is arranged in the rotating shaft, rotates with rotating shaft;
Tank body is connected on storage tank and is outwardly and inwardly provided with intake valve, air outlet valve and charging/discharging valve, intake valve connection is deposited Storage tank tank interior and the shielding gas source of the gas being arranged at outside tank body, air outlet valve connects storage tank tank interior and is arranged at tank body Outside vavuum pump.
The edge of the above second support is provided with multiple suspension hooks.
The above first support and second support have four supporting legs.
The above motor can positive and negative alternate rotation, drive the positive and negative alternate rotation of storage tank.
The protective gas source of the above shielding gas source of the gas is nitrogen.
The present invention has the following technical effect that using after said structure:
Intake valve, air outlet valve and charging/discharging valve are provided with storage tank of the present invention, during charging, are discharged by the air outlet valve Air in the storage tank, by the intake valve to storage tank inject protective gas, to realize anhydrous, oxygen-free environment under plus Material, batch mixing and storage slurry, so as to avoiding raw material contaminated or polluting miscellaneous equipment.
During compound of the present invention, storage tank is driven to rotate by motor, tank when being well mixed material in tank, and rotating Body is arranged in support, can prevent tank body from surrounding devices are clashed into during rotation, plays certain protective role;Prop up and set up Count into double-layer detachable formula structure, convenient dismounting motor and tank body, convenient maintenance and dismounting.
Intake valve, air outlet valve and the charging/discharging valve of the present invention is all valve mechanism, therefore, when all in the vapor tight tank When air valve is all closed, the sealing of the vapor tight tank very well, can be with long storage time carbon nano tube paste.
Description of the drawings
Fig. 1 is the structural representation of the present invention.
Specific embodiment
In conjunction with the accompanying drawings, the present invention is further detailed explanation.These accompanying drawings are simplified schematic diagram, only with The basic structure of the illustration explanation present invention, therefore it only shows the composition relevant with the present invention.
The present invention proposes a kind of nanotube slurry pre-mixing apparatus, and it includes double-layer scaffold and the electricity being fixed in first support Machine and storage tank, are provided with intake valve, air outlet valve and charging/discharging valve on the storage tank, during charging, arranged by the air outlet valve The air gone out in the storage tank, by the intake valve to storage tank inject protective gas, to realize anhydrous, oxygen-free environment under Charging, batch mixing and storage slurry, so as to avoiding raw material contaminated or polluting miscellaneous equipment.
As shown in figure 1, for a kind of a kind of example structure of high viscosity carbon nano tube paste pre-mixing apparatus of the present invention, Including double-layer scaffold, respectively first support 1 and second support 2, second support 2 is detachable to be set up in first support 1, the Castor 3 is provided with the supporting leg of one support 1, it is detachable in first support 1 to be provided with motor 4, rotating shaft is connected with motor 4, Storage tank 5 is rotated and is arranged in the rotating shaft, is rotated with rotating shaft.
Tank body is connected on the tank body of storage tank 5 and is outwardly and inwardly provided with intake valve 7, air outlet valve 9 and charging/discharging valve 8, air inlet Valve 7 connects the tank interior of storage tank 5 and the shielding gas source of the gas 10 being arranged at outside tank body, in the connection tank body of storage tank 5 of air outlet valve 9 Portion and the vavuum pump 11 being arranged at outside tank body.
Storage tank lower rotation is arranged on machine shaft, and structure design is simple, can also be turned by arranging on support Axle, storage tank passes through sealing between bearing and the rotating shaft and rotates connection.
For the convenience for making and installing, the first support and second support have four supporting legs.
For the convenience of lifting, the edge of the second support is provided with multiple suspension hooks 6.
During in order to rotate, premix it is full and uniform, the motor 4 can positive and negative alternate rotation, drive the positive and negative friendship of storage tank 5 For rotation.
The protective gas source of the shielding gas source of the gas 10 is nitrogen.
The operation principle of the present invention:
The shielding gas source of the gas is connected with intake valve first, the vavuum pump is connected with the air outlet valve, then open into Air valve and air outlet valve, and start vavuum pump and Nitrogen source gases.The air outlet valve is passed through by the air in the tank body by vavuum pump Extract out, so as to form negative pressure in the inner chamber of the tank body, so that the nitrogen that the Nitrogen source gases are provided passes through the intake valve Flow in the tank body.When protective gas is full of in the inner chamber of the tank body, and in the presence of protective gas, input and output material is opened Valve, raw material such as CNT and organic solvent are added in the tank body by the charging/discharging valve.
After raw material is added, the charging/discharging valve is closed, intake valve, air outlet valve, Nitrogen source gases and vacuum are subsequently closed successively Pump.During adding raw material from the charging/discharging valve to the storage tank, it is passed through always in the inner chamber of the storage tank Protective gas, it can be ensured that the oxygen and moisture in tank body is extremely low, so as to realize being fed in the environment of anhydrous, anaerobic, it is to avoid Raw material is contaminated or pollutes miscellaneous equipment.
During compound of the present invention, storage tank is driven to rotate by motor, tank when being well mixed material in tank, and rotating Body is arranged in support, can prevent tank body from surrounding devices are clashed into during rotation, plays certain protective role;Prop up and set up Count into double-layer detachable formula structure, convenient dismounting motor and tank body, convenient maintenance and dismounting.
Mixing process is:The connection of the Nitrogen source gases and the intake valve is disconnected first, disconnects the vavuum pump and institute State the connection of air outlet valve.In the case where the intake valve, air outlet valve and charging/discharging valve valve are all closed, the storage tank is rotated, Premixed with the CNT and organic solvent in being positioned over the inner chamber of the tank body, obtain carbon nano tube paste, so as to Realize the batch mixing material in the environment of anhydrous, anaerobic, it is to avoid raw material is contaminated or pollutes miscellaneous equipment.
Because the intake valve on the storage tank, air outlet valve and charging/discharging valve are all valve mechanism, therefore, when described closed When all air valves in tank are all closed, the sealing of the vapor tight tank very well, can be with long storage time carbon nano tube paste.
With the above-mentioned desirable embodiment according to the present invention as enlightenment, by above-mentioned description, relevant staff is complete Entirely various change and modification can be carried out in the range of without departing from this invention technological thought.The technology of this invention Property scope is not limited to the content on specification, it is necessary to its technical scope is determined according to right.

Claims (5)

1. a kind of high viscosity carbon nano tube paste pre-mixing apparatus, it is characterised in that:Including double-layer scaffold, respectively first support (1)And second support(2), second support(2)It is detachable to be set up in first support(1)On, first support(1)Supporting leg on set It is equipped with castor(3), first support(1)It is above detachable to be provided with motor(4), motor(4)On be connected with rotating shaft, storage tank(5) Rotation is arranged in the rotating shaft, is rotated with rotating shaft;
Storage tank(5)Tank body is connected on tank body and is outwardly and inwardly provided with intake valve(7), air outlet valve(9)And charging/discharging valve(8), Intake valve(7)Connection storage tank(5)Tank interior and the shielding gas source of the gas being arranged at outside tank body(10), air outlet valve(9)Connection Storage tank(5)Tank interior and the vavuum pump being arranged at outside tank body(11).
2. high viscosity carbon nano tube paste pre-mixing apparatus according to claim 1, it is characterised in that:The second support (2)Edge be provided with multiple suspension hooks(6).
3. high viscosity carbon nano tube paste pre-mixing apparatus according to claim 1, it is characterised in that:The first support (1)And second support(2)There are four supporting legs.
4. high viscosity carbon nano tube paste pre-mixing apparatus according to claim 1, it is characterised in that:The motor(4)Energy Enough positive and negative alternate rotations, drive storage tank(5)Positive and negative alternate rotation.
5. high viscosity carbon nano tube paste pre-mixing apparatus according to claim 1, it is characterised in that:The shielding gas source of the gas (10)Protective gas source be nitrogen.
CN201610784385.4A 2016-08-31 2016-08-31 High-viscosity carbon nanotube slurry premixing device Pending CN106621946A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610784385.4A CN106621946A (en) 2016-08-31 2016-08-31 High-viscosity carbon nanotube slurry premixing device

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Application Number Priority Date Filing Date Title
CN201610784385.4A CN106621946A (en) 2016-08-31 2016-08-31 High-viscosity carbon nanotube slurry premixing device

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Publication Number Publication Date
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106345353A (en) * 2016-08-31 2017-01-25 无锡东恒新能源科技有限公司 Carbon nanotube paste stirring reactor

Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202893440U (en) * 2012-10-24 2013-04-24 无锡东恒新能源材料有限公司 Discharge system of ball grinder
CN202893264U (en) * 2012-10-24 2013-04-24 无锡东恒新能源材料有限公司 Nanotube slurry premixing and temporary storing device
CN202893471U (en) * 2012-10-24 2013-04-24 无锡东恒新能源材料有限公司 Slurry ball-milling and sand-milling production system
CN203710955U (en) * 2013-12-18 2014-07-16 安徽信远包装科技有限公司 Powder mixer
CN203886465U (en) * 2014-03-31 2014-10-22 中美上海施贵宝制药有限公司 Storage tank for mixing medicine materials
CN104275112A (en) * 2013-07-01 2015-01-14 中国科学院过程工程研究所 Square-tapered rotary mixer
CN204137638U (en) * 2014-08-07 2015-02-04 无锡东恒新能源科技有限公司 Highly viscous slurry preparation system and buffer memory bucket thereof
CN204865680U (en) * 2015-07-01 2015-12-16 江西格雷斯科技股份有限公司 Stirring compounding device
CN106345353A (en) * 2016-08-31 2017-01-25 无锡东恒新能源科技有限公司 Carbon nanotube paste stirring reactor
CN206082385U (en) * 2016-08-31 2017-04-12 无锡东恒新能源科技有限公司 Carbon nanotube paste premixing device

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202893440U (en) * 2012-10-24 2013-04-24 无锡东恒新能源材料有限公司 Discharge system of ball grinder
CN202893264U (en) * 2012-10-24 2013-04-24 无锡东恒新能源材料有限公司 Nanotube slurry premixing and temporary storing device
CN202893471U (en) * 2012-10-24 2013-04-24 无锡东恒新能源材料有限公司 Slurry ball-milling and sand-milling production system
CN104275112A (en) * 2013-07-01 2015-01-14 中国科学院过程工程研究所 Square-tapered rotary mixer
CN203710955U (en) * 2013-12-18 2014-07-16 安徽信远包装科技有限公司 Powder mixer
CN203886465U (en) * 2014-03-31 2014-10-22 中美上海施贵宝制药有限公司 Storage tank for mixing medicine materials
CN204137638U (en) * 2014-08-07 2015-02-04 无锡东恒新能源科技有限公司 Highly viscous slurry preparation system and buffer memory bucket thereof
CN204865680U (en) * 2015-07-01 2015-12-16 江西格雷斯科技股份有限公司 Stirring compounding device
CN106345353A (en) * 2016-08-31 2017-01-25 无锡东恒新能源科技有限公司 Carbon nanotube paste stirring reactor
CN206082385U (en) * 2016-08-31 2017-04-12 无锡东恒新能源科技有限公司 Carbon nanotube paste premixing device

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106345353A (en) * 2016-08-31 2017-01-25 无锡东恒新能源科技有限公司 Carbon nanotube paste stirring reactor

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Application publication date: 20170510