CN106525655A - A device and method for gas-liquid injection simulated oil displacement and fluid performance measurement - Google Patents

A device and method for gas-liquid injection simulated oil displacement and fluid performance measurement Download PDF

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CN106525655A
CN106525655A CN201610985253.8A CN201610985253A CN106525655A CN 106525655 A CN106525655 A CN 106525655A CN 201610985253 A CN201610985253 A CN 201610985253A CN 106525655 A CN106525655 A CN 106525655A
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pressure sensor
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CN106525655B (en
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刘宏生
韩培慧
陈广宇
孙刚
姜彬
吕昌森
郭松林
崔长玉
曹瑞波
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Petrochina Co Ltd
Daqing Oilfield Co Ltd
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Daqing Oilfield Co Ltd
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Abstract

本发明提供一种气液注入模拟驱油和流体性能测定装置及方法,所述装置包括模拟油藏的模型系统、向模型系统注入驱替介质的注入系统、对模型系统的流出液进行计量采集的流出液计量采集系统和用于获取岩心中流体性能的测定系统,所述测定系统包括:第一质量流量计和第一可视毛细管、第二质量流量计和第二可视毛细管。本发明装置通过设置可视毛细管、质量流量计和压差传感器,测定流体在进入岩心前、在岩心中不同层位不同位置以及流出岩心后的流体形态及运动粘度,有助于分析注入流体或注入流体与原油混合后在地层中的运动状态和速度,为研究流体运移规律和驱油机理提供技术支持;通过质量流量计准确计量气体、液体或气液混合物流体的流速及流量。

The invention provides a device and method for gas-liquid injection simulation of oil displacement and fluid performance measurement. The device includes a model system for simulating reservoirs, an injection system for injecting displacement medium into the model system, and metering and collection of effluent from the model system. The effluent metering collection system and the measurement system for obtaining fluid properties in the core, the measurement system includes: a first mass flow meter and a first visible capillary, a second mass flow meter and a second visible capillary. The device of the present invention measures the fluid form and kinematic viscosity of the fluid before entering the rock core, in different layers and different positions in the rock core, and after flowing out of the rock core by setting a visible capillary, a mass flow meter and a differential pressure sensor, which is helpful for analyzing the injected fluid or The movement state and speed of the injected fluid mixed with crude oil in the formation provide technical support for the study of fluid migration laws and oil displacement mechanisms; the flow velocity and flow rate of gas, liquid or gas-liquid mixture fluids are accurately measured by mass flowmeters.

Description

一种气液注入模拟驱油和流体性能测定装置及方法A device and method for gas-liquid injection simulated oil displacement and fluid performance measurement

技术领域technical field

本发明属于石油工程和工艺技术领域,具体涉及一种适用于实验室环境可实现气液交替注入或同时注入的气液注入模拟驱油的装置及方法,该模拟驱油装置和方法还能直接实现流体性能的测定。The invention belongs to the field of petroleum engineering and process technology, and specifically relates to a device and method for simulated oil displacement by gas-liquid injection, which is suitable for laboratory environments and can realize gas-liquid injection alternately or simultaneously. The simulated oil displacement device and method can also directly Realize the measurement of fluid properties.

背景技术Background technique

石油是不可再生的能源,经济有效地开发现有油田是永恒的课题。水驱可以提高采收率1/3-1/5,我国各大油田均已处于水驱后期,但有半数以上的石油地质储量仍残留在地下,需要开展有效的三次采油技术,可以使我国石油产量增加10%-20%。化学驱技术是在三次采油中应用最广泛最成熟的,而物理模拟驱油实验结果的好坏是判断化学驱能否在现场应用的主要依据。Petroleum is a non-renewable energy source, and economically and effectively developing existing oil fields is an eternal subject. Water flooding can increase the recovery rate by 1/3-1/5. All major oil fields in my country are in the late stage of water flooding, but more than half of the geological reserves of oil still remain underground. It is necessary to carry out effective tertiary oil recovery technology, which can make my country Oil production increased by 10%-20%. Chemical flooding technology is the most widely used and most mature technology in tertiary oil recovery, and the results of physical simulation flooding experiments are the main basis for judging whether chemical flooding can be applied in the field.

目前,物理模拟驱油实验装置主要针对聚合物驱、三元复合驱或气驱实验需要和特点设计的,而专门针对气液交替注入设计的物理模拟驱油装置很少,大部分都是由以上装置改造的,存在气液交替时压力波动大,气体流量计量不准确等问题。At present, physical simulation oil flooding experimental devices are mainly designed for the needs and characteristics of polymer flooding, ASP flooding or gas flooding experiments, while there are few physical simulation oil flooding devices specially designed for gas-liquid alternate injection, and most of them are made of The modification of the above devices has problems such as large pressure fluctuations when gas-liquid alternates, and inaccurate gas flow measurement.

发明内容Contents of the invention

本发明的目的是为了解决上述问题,提供一种适用于实验室环境适用于实验室环境可实现气液交替注入或同时注入的气液注入模拟驱油和流体性能测定装置。The object of the present invention is to solve the above problems and provide a gas-liquid injection simulated oil displacement and fluid performance measurement device suitable for laboratory environment, which can realize gas-liquid injection alternately or simultaneously.

本发明的上述目的是由以下技术方案来实现的:Above-mentioned purpose of the present invention is achieved by the following technical solutions:

一种气液注入模拟驱油和流体性能测定装置,包括模拟油藏的模型系统、向模型系统注入驱替介质的注入系统和对模型系统的流出液进行计量采集的流出液计量采集系统,所述模型系统包括岩心夹置器(A),还包括用于获取岩心中流体性能的测定系统,所述测定系统包括:A gas-liquid injection simulated oil displacement and fluid performance measurement device, including a model system for simulating reservoirs, an injection system for injecting displacement media into the model system, and an effluent metering and acquisition system for metering and collecting the effluent of the model system, the The model system includes a core holder (A), and also includes a measurement system for obtaining fluid properties in the core, and the measurement system includes:

第一质量流量计(H1)和第一可视毛细管(G5),二者串联连接在岩心夹置器(A)的岩心夹置器入口(A1)端,第一质量流量计(H1)的入口端处设置有第一压力传感器(P1);第一质量流量计(H1)的入口端连接到所述注入系统;The first mass flowmeter (H1) and the first visual capillary (G5), the two are connected in series at the core holder inlet (A1) end of the core holder (A), the first mass flowmeter (H1) The inlet end is provided with a first pressure sensor (P1); the inlet end of the first mass flow meter (H1) is connected to the injection system;

第二质量流量计(H2)和第二可视毛细管(G6),二者通过气动阀(K24)串联连接到岩心夹置器(A)的岩心夹置器出口(A8),并且岩心流体采集点(A2-A7)分别通过气动阀(K18-K23)连接到第二质量流量计(H2)的入口端,第二质量流量计(H2)入口端设置第五压力传感器(P7);第二可视毛细管(G6)的出口端连接到所述流出液计量采集系统。The second mass flow meter (H2) and the second visual capillary (G6), both are connected in series to the core holder outlet (A8) of the core holder (A) through the pneumatic valve (K24), and the core fluid collection The points (A2-A7) are respectively connected to the inlet port of the second mass flowmeter (H2) through the pneumatic valve (K18-K23), and the inlet port of the second mass flowmeter (H2) is provided with the fifth pressure sensor (P7); the second The outlet end of the visual capillary (G6) is connected to the effluent metering collection system.

上述气液注入模拟驱油和流体性能测定装置中,所述流出液计量采集系统包括第一回压阀(B1)、第二回压阀(B2)、气动阀(K3)、气动阀(K25)和油气水计量装置(D),第二可视毛细管(G6)的出口端依次通过第二回压阀(B2)、气动阀(K25)连接到油气水计量装置(D),岩心夹置器(A)的岩心夹置器出口(A8)依次通过第一回压阀(B1)、气动阀(K3)连接到油气水计量装置(D)。The above-mentioned gas-liquid is injected into the simulated oil displacement and fluid performance measurement device, and the effluent metering and collection system includes a first back pressure valve (B1), a second back pressure valve (B2), a pneumatic valve (K3), a pneumatic valve (K25 ) and the oil-gas-water metering device (D), the outlet end of the second visible capillary (G6) is connected to the oil-gas-water metering device (D) through the second back pressure valve (B2) and the pneumatic valve (K25) sequentially, and the core is clamped The outlet (A8) of the core holder (A) is connected to the oil, gas and water metering device (D) through the first back pressure valve (B1) and the pneumatic valve (K3) in sequence.

上述气液注入模拟驱油和流体性能测定装置中,所述第一可视毛细管(G5)位于岩心夹置器(A)的岩心夹置器入口(A1)端且与管线相连,沿第一可视毛细管(G5)长度方向平行的一侧设有第一光源(G3),另一侧设有第一高倍摄像机(G7),第一可视毛细管(G5)的入口和出口之间并联有第一压差传感器(P5)用以测量第一可视毛细管(G5)入口和出口之间的压力差。The above-mentioned gas-liquid is injected into the simulated oil displacement and fluid performance measurement device, the first visible capillary (G5) is located at the core holder inlet (A1) end of the core holder (A) and connected to the pipeline, along the first A first light source (G3) is arranged on one side parallel to the length direction of the visible capillary (G5), and a first high-power camera (G7) is arranged on the other side, and a parallel connection between the entrance and the outlet of the first visible capillary (G5) is provided. The first differential pressure sensor (P5) is used to measure the pressure difference between the inlet and outlet of the first visible capillary (G5).

上述气液注入模拟驱油和流体性能测定装置中,所述第二可视毛细管(G6)位于岩心夹置器出口(A8)端与管线相连,沿第二可视毛细管(G6)长度方向平行的一侧设有第二光源(G4),另一侧设有第二高倍摄像机(G8),第二可视毛细管(G6)的入口和出口之间并联有第二压差传感器(P6)。The above-mentioned gas-liquid is injected into the device for simulating oil displacement and fluid performance measurement, and the second visible capillary (G6) is located at the end of the outlet (A8) of the core holder and connected to the pipeline, parallel to the length direction of the second visible capillary (G6). One side is provided with a second light source (G4), the other side is provided with a second high-power camera (G8), and a second differential pressure sensor (P6) is connected in parallel between the inlet and outlet of the second visible capillary (G6).

上述气液注入模拟驱油和流体性能测定装置中,所述注入系统包括向模型系统注入气体的气体注入系统和向模型系统注入液体的液体注入系统。The above-mentioned gas-liquid injection into the device for simulating oil displacement and fluid performance measurement, the injection system includes a gas injection system for injecting gas into the model system and a liquid injection system for injecting liquid into the model system.

上述气液注入模拟驱油和流体性能测定装置中,所述气体注入系统包括:The above-mentioned gas-liquid injection simulates oil displacement and fluid performance measurement device, and the gas injection system includes:

并联连接的第一气体活塞容器L1和第二气体活塞容器L2,其中,A first gas piston container L1 and a second gas piston container L2 connected in parallel, wherein,

所述第一气体活塞容器(L1)的上端开口处设有气动阀(K10)和用于测量第一气体活塞容器(L1)内部气体压力的第三压力传感器(P3),第一气体活塞容器(L1)的上端开口通过气动阀(K11)与第一排空管(U1)相连通;第一气体活塞容器(L1)的下端开口通过气动阀(K14)连接到第二恒压恒速泵(R2)、通过气动阀(K16)连接到第三液体接收容器(F3);The upper opening of the first gas piston container (L1) is provided with a pneumatic valve (K10) and a third pressure sensor (P3) for measuring the internal gas pressure of the first gas piston container (L1). The upper opening of (L1) is connected to the first emptying pipe (U1) through the pneumatic valve (K11); the lower opening of the first gas piston container (L1) is connected to the second constant pressure and constant speed pump through the pneumatic valve (K14) (R2), connected to the third liquid receiving container (F3) through a pneumatic valve (K16);

第二气体活塞容器(L2)的上端开口处设有气动阀(K9)和用于测量第二气体活塞容器(L2)内部气体压力的第四压力传感器(P4),第二气体活塞容器(L2)的上端开口通过气动阀(K12)与第二排空管(U2)相连通;第二气体活塞容器(L2)的下端开口通过气动阀(K13)连接到第三恒压恒速泵(R3)、通过气动阀(K17)连接到第三液体接收容器(F3);The upper opening of the second gas piston container (L2) is provided with a pneumatic valve (K9) and a fourth pressure sensor (P4) for measuring the internal gas pressure of the second gas piston container (L2), and the second gas piston container (L2 ) through the pneumatic valve (K12) and the second emptying pipe (U2); the lower end of the second gas piston container (L2) is connected to the third constant pressure constant speed pump (R3) through the pneumatic valve (K13) ), connected to the third liquid receiving container (F3) through a pneumatic valve (K17);

用于存储高压气体的高压气瓶(N),所述高压气瓶(N)通过气动阀(K8)连接到一气体增压泵(M),所述气体增压泵(M)通过气动阀(K7)连接到气动阀(K9)和气动阀(K10)的交接处,气动阀(K7、K9、K10)的交接处通过气动阀(K6)连接到第一质量流量计(H1)的入口端。A high-pressure gas cylinder (N) for storing high-pressure gas, the high-pressure gas cylinder (N) is connected to a gas booster pump (M) through a pneumatic valve (K8), and the gas booster pump (M) is connected to a gas booster pump (M) through a pneumatic valve (K7) is connected to the junction of pneumatic valve (K9) and pneumatic valve (K10), and the junction of pneumatic valve (K7, K9, K10) is connected to the inlet of the first mass flow meter (H1) through pneumatic valve (K6) end.

上述气液注入模拟驱油和流体性能测定装置中,所述液体注入系统包括液体活塞容器(E),所述液体活塞容器(E)的上端入口处设置有用于测量液体活塞容器(E)中液体压力的第二压力传感器(P2),液体活塞容器(E)的上端开口分别通过气动阀(K2)与第一液体接收器(F1)相连以及通过气动阀(K5)连接到第一质量流量计(H1)的入口端;所述液体活塞容器(E)的下端开口通过气动阀(K4)与第一恒压恒速泵(R1)相连,并通过气动阀(K15)与第二液体接收容器(F2)相连。The above-mentioned gas-liquid injection simulated oil displacement and fluid performance measurement device, the liquid injection system includes a liquid piston container (E), and the upper end inlet of the liquid piston container (E) is provided with a device for measuring the liquid piston container (E). The second pressure sensor (P2) for liquid pressure, the upper opening of the liquid piston container (E) is respectively connected to the first liquid receiver (F1) via a pneumatic valve (K2) and to the first mass flow rate via a pneumatic valve (K5). The inlet end of the gauge (H1); the lower opening of the liquid piston container (E) is connected to the first constant pressure constant speed pump (R1) through the pneumatic valve (K4), and is connected to the second liquid receiving port through the pneumatic valve (K15). Containers (F2) are connected.

上述气液注入模拟驱油和流体性能测定装置中,所述岩心夹置器(A)、第一回压阀(B1)、第二回压阀(B2)、油气水计量装置(D)、液体活塞容器(E)、液体接收容器(F1)、第一质量流量计(H1)、第二质量流量计(H2)、第一气体活塞容器(L1)、第二气体活塞容器(L2)以及第一不透光箱(G1)和第二不透光箱(G2)均置于恒温箱(Q)中。The above-mentioned gas-liquid is injected into the simulated oil displacement and fluid performance measurement device, the core holder (A), the first back pressure valve (B1), the second back pressure valve (B2), the oil, gas and water metering device (D), Liquid piston container (E), liquid receiving container (F1), first mass flow meter (H1), second mass flow meter (H2), first gas piston container (L1), second gas piston container (L2) and Both the first light-tight box (G1) and the second light-tight box (G2) are placed in the thermostatic box (Q).

上述气液注入模拟驱油和流体性能测定装置中,所述第一质量流量计(H1)、第二质量流量计(H2)、气动阀(K1-K25)、各压力传感器(P1-P4,P7)、各压差传感器(P4,P5)、恒温箱(Q)、各恒压恒速泵(R1-R3)、第一光源(G3)、第二光源(G4)、第一高倍摄像机(G7)、第二高倍摄像机(G8)、气体增压泵M均电连接到计算机(W)。The above-mentioned gas-liquid is injected into the simulated oil displacement and fluid performance measurement device, the first mass flowmeter (H1), the second mass flowmeter (H2), the pneumatic valve (K1-K25), each pressure sensor (P1-P4, P7), each differential pressure sensor (P4, P5), constant temperature box (Q), each constant pressure and constant speed pump (R1-R3), the first light source (G3), the second light source (G4), the first high-power camera ( G7), the second high power camera (G8), and the gas booster pump M are all electrically connected to the computer (W).

本发明还提供一种气液注入模拟驱油和流体性能测定方法,该方法采用上述气液注入模拟驱油和流体性能测定装置进行气液注入模拟驱油实验以及对岩心中流体性能进行测定,包括以下步骤:The present invention also provides a gas-liquid injection simulated oil displacement and a method for measuring fluid performance. The method uses the above-mentioned gas-liquid injection simulated oil displacement and fluid performance measurement device to perform a gas-liquid injection simulated oil displacement experiment and measure the fluid performance in the core. Include the following steps:

步骤一:将三层非均质含油岩心放入岩心夹置器(A)中,液体装入液体活塞容器(E)中,高压气瓶(N)中气体种类满足所述模拟驱油实验的设计,第一气体活塞容器(L1)和第二气体活塞容器(L2)中的活塞位于顶部,所有气动阀均处于关闭状态,计算机(W)控制恒温箱(Q)加热至模拟驱油实验预设温度;计算机(W)控制第一光源(G3)和第二光源(G4)开启,并控制第一高倍摄像机(G7)和第二高倍摄像机(G8)开启;Step 1: Put the three-layer heterogeneous oil-bearing core into the core holder (A), put the liquid into the liquid piston container (E), and the gas type in the high-pressure gas cylinder (N) meets the requirements of the simulated oil displacement experiment. Design, the pistons in the first gas piston container (L1) and the second gas piston container (L2) are located at the top, all pneumatic valves are closed, and the computer (W) controls the thermostat (Q) to heat up to the pre-simulation oil displacement experiment. Set the temperature; the computer (W) controls the opening of the first light source (G3) and the second light source (G4), and controls the opening of the first high-power camera (G7) and the second high-power camera (G8);

步骤二:计算机(W)控制气动阀(K8,K7,K10,K16)开启,高压气瓶(N)中的气体通过气体增压泵(M)和气动阀(K8,K7,K10)进入第一气体活塞容器(L1)中,当第一气体活塞容器(L1)中的活塞被推到底部,计算机(W)控制气动阀(K10,K16)关闭;计算机(W)控制气动阀(K9,K17)开启,高压气瓶(N)中的气体通过增压泵(M)和气动阀(K8,K7,K9)进入第二气体活塞容器(L2)中,当第二气体活塞容器(L2)中的活塞被推到底部,计算机(W)控制气动阀(K8,K7,K9,K17)关闭;Step 2: The computer (W) controls the opening of the pneumatic valves (K8, K7, K10, K16), and the gas in the high-pressure cylinder (N) enters the first stage through the gas booster pump (M) and the pneumatic valves (K8, K7, K10). In a gas piston container (L1), when the piston in the first gas piston container (L1) is pushed to the bottom, the computer (W) controls the pneumatic valves (K10, K16) to close; the computer (W) controls the pneumatic valves (K9, K17) is opened, the gas in the high-pressure cylinder (N) enters the second gas piston container (L2) through the booster pump (M) and the pneumatic valve (K8, K7, K9), when the second gas piston container (L2) The piston in the cylinder is pushed to the bottom, and the computer (W) controls the pneumatic valves (K8, K7, K9, K17) to close;

步骤三:根据模拟驱油实验设计的回压设定第一回压阀(B1)的压力值,计算机(W)控制气动阀(K4,K13,K14)开启,计算机(W)控制第一恒压恒速泵(R1)、第二恒压恒速泵(R2)和第三恒压恒速泵(R3)分别对液体活塞容器(E)、第一气体活塞容器(L1)、第二气体活塞容器(L2)加压,当第二压力传感器(P2)、第三压力传感器(P3)或第四压力传感器(P4)的压力值与第一回压阀(B1)的压力值相等时,计算机(W)控制相应的恒压恒速泵停止;Step 3: Set the pressure value of the first back pressure valve (B1) according to the back pressure designed in the simulated oil displacement experiment, the computer (W) controls the opening of the pneumatic valves (K4, K13, K14), and the computer (W) controls the first constant The pressure and constant speed pump (R1), the second constant pressure and constant speed pump (R2) and the third constant pressure and constant speed pump (R3) respectively control the liquid piston container (E), the first gas piston container (L1), the second gas The piston container (L2) is pressurized, when the pressure value of the second pressure sensor (P2), the third pressure sensor (P3) or the fourth pressure sensor (P4) is equal to the pressure value of the first back pressure valve (B1), The computer (W) controls the corresponding constant pressure constant speed pump to stop;

步骤四:采用气液交替注入方式或气液同时注入方式向岩心夹置器(A)中的含油岩心中注入驱油介质,在注入过程中,计算机(W)通过第一高倍摄像机(G7)和第一光源(G3)观测气体、液体或气液混合物的流动状态,同时结合第一质量流量计(H1)和第一压差传感器(P5)的数值计算出气体、液体或气液混合物的运动粘度;计算机(W)控制气动阀(K18-K24)中的一个开启,设定回压阀(B2)的压力等于第五压力传感器(P7)的压力值,通过第二高倍摄像机(G8)和第二光源(G4)可观测对应三层非均质岩心流体采集点(A2-A7)及岩心夹置器出口(A8)的流体流动状态,同样结合第二质量流量计(H2)和第二压差传感器(P6)的数值计算出该采集点流体的运动粘度,直到满足模拟驱油实验设计的注入时间为止。Step 4: Inject the oil-displacing medium into the oil-bearing core in the core holder (A) by means of alternate gas-liquid injection or simultaneous gas-liquid injection. During the injection process, the computer (W) passes through the first high-power camera (G7) and the first light source (G3) to observe the flow state of the gas, liquid or gas-liquid mixture, and at the same time combine the values of the first mass flow meter (H1) and the first differential pressure sensor (P5) to calculate the flow rate of the gas, liquid or gas-liquid mixture Kinematic viscosity; the computer (W) controls one of the pneumatic valves (K18-K24) to open, and sets the pressure of the back pressure valve (B2) equal to the pressure value of the fifth pressure sensor (P7), through the second high-power camera (G8) And the second light source (G4) can observe the fluid flow state corresponding to the three-layer heterogeneous core fluid collection point (A2-A7) and the core holder outlet (A8), also combined with the second mass flowmeter (H2) and the first The numerical value of the second pressure difference sensor (P6) calculates the kinematic viscosity of the fluid at the collection point until the injection time designed for the simulated oil displacement experiment is met.

上述气液注入模拟驱油和流体性能测定方法中,步骤四中的气液同时注入方式包括以下步骤:In the above gas-liquid injection simulated oil displacement and fluid performance measurement method, the gas-liquid simultaneous injection method in step 4 includes the following steps:

计算机(W)控制气动阀(K3,K5,K6,K10)开启,计算机(W)控制第一恒压恒速泵(R1)、第二恒压恒速泵(R2)以模拟驱油实验设计的气液比、注入速度注入液体和气体,当满足模拟驱油实验设计的注入时间后,计算机(W)控制气动阀(K3,K5,K6,K10)关闭并停止第一恒压恒速泵(R1)和第二恒压恒速泵(R2);在实验过程中计算机(W)记录第一压力传感器(P1)的压力值及第一质量流量计(H1)泡沫流体的流速和注入时间,并实时记录油气水计量装置(D)中油、气、水体积。The computer (W) controls the opening of the pneumatic valves (K3, K5, K6, K10), and the computer (W) controls the first constant-pressure constant-speed pump (R1) and the second constant-pressure constant-speed pump (R2) to simulate oil displacement experimental design The gas-liquid ratio and injection speed are used to inject liquid and gas. When the injection time of the simulated oil displacement experiment is met, the computer (W) controls the pneumatic valves (K3, K5, K6, K10) to close and stop the first constant pressure and constant speed pump. (R1) and the second constant pressure and constant speed pump (R2); during the experiment, the computer (W) records the pressure value of the first pressure sensor (P1) and the flow rate and injection time of the first mass flow meter (H1) foam fluid , and record the volume of oil, gas and water in the oil, gas and water metering device (D) in real time.

上述气液注入模拟驱油和流体性能测定方法中,步骤四中的气液交替注入方式包括交替进行的以下步骤:In the above gas-liquid injection simulated oil displacement and fluid performance measurement method, the gas-liquid alternate injection method in step 4 includes the following steps alternately:

(1)注入液体时,计算机(W)控制气动阀(K3,K4,K5)开启,计算机(W)控制第一恒压恒速泵(R1)以恒定的模拟驱油实验设计的速度注入液体,当满足模拟驱油实验设计的注入时间后,计算机(W)控制气动阀(K5)关闭,并停止第一恒压恒速泵(R1);计算机(W)同时记录液体注入时的第一压力传感器(P1)的值、液体注入时间和速度,通过第一质量流量计(H1)测量的液体注入速度校正通过第一恒压恒速泵(R1)记录的注入速度;(1) When liquid is injected, the computer (W) controls the opening of the pneumatic valves (K3, K4, K5), and the computer (W) controls the first constant pressure and constant speed pump (R1) to inject the liquid at a constant speed designed for the simulated oil flooding experiment , when the injection time designed for the simulated oil displacement experiment is met, the computer (W) controls the pneumatic valve (K5) to close, and stops the first constant-pressure constant-speed pump (R1); the computer (W) simultaneously records the first time when the liquid is injected The value of the pressure sensor (P1), the liquid injection time and speed, the liquid injection speed measured by the first mass flow meter (H1) corrects the injection speed recorded by the first constant pressure constant speed pump (R1);

在注入液体过程中,计算机(W)同时控制气动阀(K13,K14)开启,并分别比较第三压力传感器(P3)、第四压力传感器(P4)的压力值与第一压力传感器(P1)的压力值的大小,即当第三压力传感器(P3)的压力值大于第一压力传感器(P1)的压力值时,计算机(W)控制气动阀(K11)开启,气体从第一排空管(U1)排出,直到第三压力传感器(P3)的压力值等于第一压力传感器(P1)的压力值为止,关闭气动阀(K11);当第三压力传感器(P3)的压力值小于第一压力传感器(P1)的压力值时,计算机(W)控制第二恒压恒速泵(R2)对第一气体活塞容器(L1)加压,直到第三压力传感器(P3)的压力值等于第一压力传感器(P1)的压力值为止,停止第二恒压恒速泵(R2)加压;同样,当第四压力传感器(P4)的压力值大于第一压力传感器(P1)的压力值,计算机(W)控制气动阀(K12)开启,气体从第二排空管(U2)排出,直到第四压力传感器(P4)的压力值等于第一压力传感器(P1)的压力值为止,关闭气动阀(K12);当第四压力传感器(P4)的压力值小于第一压力传感器(P1)的压力值时,计算机(W)控制第三恒压恒速泵(R3)对第二气体活塞容器(L2)加压,直到第四压力传感器(P4)的压力值等于第一压力传感器(P1)的压力值为止,停止第三恒压恒速泵(R3)加压,直到液体注入完毕;During the liquid injection process, the computer (W) simultaneously controls the pneumatic valves (K13, K14) to open, and respectively compares the pressure values of the third pressure sensor (P3), the fourth pressure sensor (P4) with the first pressure sensor (P1) The size of the pressure value, that is, when the pressure value of the third pressure sensor (P3) is greater than the pressure value of the first pressure sensor (P1), the computer (W) controls the pneumatic valve (K11) to open, and the gas is discharged from the first exhaust pipe (U1) discharge until the pressure value of the third pressure sensor (P3) is equal to the pressure value of the first pressure sensor (P1), close the pneumatic valve (K11); when the pressure value of the third pressure sensor (P3) is less than the first When the pressure value of the pressure sensor (P1), the computer (W) controls the second constant pressure constant speed pump (R2) to pressurize the first gas piston container (L1), until the pressure value of the third pressure sensor (P3) is equal to the first Until the pressure value of the first pressure sensor (P1), stop the pressurization of the second constant pressure constant speed pump (R2); similarly, when the pressure value of the fourth pressure sensor (P4) is greater than the pressure value of the first pressure sensor (P1), The computer (W) controls the pneumatic valve (K12) to open, and the gas is discharged from the second exhaust pipe (U2) until the pressure value of the fourth pressure sensor (P4) is equal to the pressure value of the first pressure sensor (P1), and the pneumatic valve is closed. Valve (K12); when the pressure value of the fourth pressure sensor (P4) was less than the pressure value of the first pressure sensor (P1), the computer (W) controlled the third constant pressure constant speed pump (R3) to the second gas piston container (L2) Pressurize until the pressure value of the fourth pressure sensor (P4) is equal to the pressure value of the first pressure sensor (P1), stop the third constant pressure constant speed pump (R3) to pressurize until the liquid is injected;

(2)注入气体时,计算机(W)控制气动阀(K3,K6,K10)开启,计算机(W)控制第二恒压恒速泵(R2)以模拟驱油实验设计的速度注入气体,当满足模拟驱油实验设计的注入时间后,计算机(W)控制气动阀(K6,K10)关闭并停止第二恒压恒速泵(R2);计算机(W)记录气体注入时的第一压力传感器(P1)的值、气体注入速度和时间,通过第一质量流量计(H1)测量的气体注入速度校正通过第二恒压恒速泵(R2)记录的注入速度;(2) When injecting gas, the computer (W) controls the opening of the pneumatic valves (K3, K6, K10), and the computer (W) controls the second constant pressure and constant speed pump (R2) to inject gas at the speed designed for the simulated oil displacement experiment. After satisfying the injection time designed for the simulated oil displacement experiment, the computer (W) controls the pneumatic valves (K6, K10) to close and stops the second constant pressure and constant speed pump (R2); the computer (W) records the first pressure sensor when the gas is injected The value of (P1), gas injection rate and time, the gas injection rate measured by the first mass flow meter (H1) corrects the injection rate recorded by the second constant pressure constant speed pump (R2);

在注入气体过程中,计算机(W)比较第四压力传感器(P4)的压力值与第一压力传感器(P1)的压力值的大小,当第四压力传感器(P4)的压力值大于第一压力传感器(P1)的压力值,计算机(W)控制气动阀(K12)开启,气体从第二排空管(U2)排出,直到第四压力传感器(P4)的压力值等于第一压力传感器(P1)的压力值为止,关闭气动阀(K12);当第四压力传感器(P4)的压力值小于第一压力传感器(P1)的压力值,计算机(W)控制第三恒压恒速泵(R3)对第二气体活塞容器(L2)加压,直到第四压力传感器(P4)的压力值等于第一压力传感器(P1)的压力值为止,停止第三恒压恒速泵(R3)加压,直到气体注入完毕,或当第一气体活塞容器(L1)中气体体积用完时,计算机(W)控制气动阀(K9)开启,控制气动阀(K10)关闭并停止第二恒压恒速泵(R2),计算机(W)控制第三恒压恒速泵(R3)以同样的模拟驱油实验设计的速度继续注入气体,当满足模拟驱油实验设计的注入时间后,计算机W控制气动阀(K6,K9)关闭和停止第三恒压恒速泵(R3);During the gas injection process, the computer (W) compares the pressure value of the fourth pressure sensor (P4) with the pressure value of the first pressure sensor (P1), when the pressure value of the fourth pressure sensor (P4) is greater than the first pressure The pressure value of the sensor (P1), the computer (W) controls the pneumatic valve (K12) to open, and the gas is discharged from the second emptying pipe (U2), until the pressure value of the fourth pressure sensor (P4) is equal to the pressure value of the first pressure sensor (P1 ), close the pneumatic valve (K12); when the pressure value of the fourth pressure sensor (P4) is less than the pressure value of the first pressure sensor (P1), the computer (W) controls the third constant pressure constant speed pump (R3 ) Pressurize the second gas piston container (L2) until the pressure value of the fourth pressure sensor (P4) is equal to the pressure value of the first pressure sensor (P1), stop the third constant pressure constant speed pump (R3) pressurization , until the gas injection is completed, or when the gas volume in the first gas piston container (L1) is used up, the computer (W) controls the pneumatic valve (K9) to open, controls the pneumatic valve (K10) to close and stops the second constant pressure constant speed The pump (R2), the computer (W) controls the third constant pressure constant speed pump (R3) to continue injecting gas at the same speed designed for the simulated oil flooding experiment, and when the injection time of the simulated oil flooding experiment design is satisfied, the computer W controls the pneumatic Valves (K6, K9) close and stop the third constant pressure constant speed pump (R3);

在注入气体过程中,计算机(W)同时比较第二压力传感器(P2)的压力值与第一压力传感器(P1)的压力值的大小,当第二压力传感器(P2)的压力值大于第一压力传感器(P1)的压力值时,计算机(W)控制气动阀(K2)开启,排出多余液体到第一液体接收容器(F1)中,直到第二压力传感器(P2)的压力值等于第一压力传感器(P1)的压力值为止,关闭气动阀(K2);当第二压力传感器(P2)的压力值小于第一压力传感器(P1)的压力值,计算机(W)控制第一恒压恒速泵(R1)对液体活塞容器(E)加压,直到第二压力传感器(P2)的压力值等于第一压力传感器(P1)的压力值为止,停止第一恒压恒速泵(R1),直到气体注入完毕。During the gas injection process, the computer (W) compares the pressure value of the second pressure sensor (P2) with the pressure value of the first pressure sensor (P1) at the same time, when the pressure value of the second pressure sensor (P2) is greater than the first When the pressure value of the pressure sensor (P1) is reached, the computer (W) controls the pneumatic valve (K2) to open and discharge excess liquid into the first liquid receiving container (F1) until the pressure value of the second pressure sensor (P2) is equal to the first Close the pneumatic valve (K2) until the pressure value of the pressure sensor (P1); when the pressure value of the second pressure sensor (P2) is lower than the pressure value of the first pressure sensor (P1), the computer (W) controls the first constant pressure constant The speed pump (R1) pressurizes the liquid piston container (E) until the pressure value of the second pressure sensor (P2) is equal to the pressure value of the first pressure sensor (P1), then the first constant pressure constant speed pump (R1) is stopped , until the gas injection is complete.

采用上述技术方案,本发明的技术效果是:本发明装置通过设置可视毛细管、质量流量计和压差传感器,可观测流体在进入岩心前、在岩心中不同层位不同位置以及流出岩心后的流体形态及运动粘度,在模拟驱油的同时直接实现流体性能的测定,有助于分析注入流体或注入流体与原油混合后在地层中的运动状态和速度,为研究流体运移规律和驱油机理提供技术支持;通过第二、第三恒速恒压泵实时控制第一气体活塞容器、第二气体活塞容器中注入气体的压力,使第一气体活塞容器、第二气体活塞容器中注入气体的压力与岩心夹置器入口注入压力相同,实现了气液注入过程中气体注入压力平稳,控制精度高;通过第一恒速恒压泵实时控制液体活塞容器中注入液体的压力,使液体活塞容器中注入液体的压力与岩心夹置器入口注入压力相同,实现了气液注入过程中液体注入压力平稳,控制精度高;通过质量流量计准确计量气体、液体或气液混合物流体的流速及流量。By adopting the above technical scheme, the technical effect of the present invention is: the device of the present invention can observe the flow of fluid before entering the rock core, in different layers and different positions in the rock core, and after flowing out of the rock core by setting a visible capillary, a mass flow meter and a differential pressure sensor. Fluid form and kinematic viscosity can directly measure fluid properties while simulating oil displacement, which is helpful to analyze the movement state and speed of injected fluid or injected fluid mixed with crude oil in the formation. The mechanism provides technical support; through the second and third constant speed and constant pressure pumps, the pressure of the gas injected into the first gas piston container and the second gas piston container is controlled in real time, so that the gas is injected into the first gas piston container and the second gas piston container The pressure is the same as the injection pressure at the inlet of the core holder, which realizes stable gas injection pressure and high control precision during the gas-liquid injection process; the pressure of the liquid injected into the liquid piston container is controlled in real time by the first constant speed and constant pressure pump, so that the liquid piston The pressure of the liquid injected in the container is the same as the injection pressure at the inlet of the core holder, which realizes the stable liquid injection pressure and high control precision during the gas-liquid injection process; the flow rate and flow rate of gas, liquid or gas-liquid mixture fluid are accurately measured by the mass flow meter .

附图说明Description of drawings

图1是本发明的整体结构示意图。Fig. 1 is a schematic diagram of the overall structure of the present invention.

图中附图标记表示为:The reference signs in the figure represent:

A:岩心夹置器,A1:岩心夹置器入口,A8:岩心夹置器出口。A2-A7:岩心流体采集点;A: core holder, A1: core holder inlet, A8: core holder outlet. A2-A7: core fluid collection points;

B1:第一回压阀,B2:第二回压阀;D:油气水计量装置;G1:第一不透光密封箱,G2:第二不透光密封箱;G3:第一光源,G4:第二光源;G5:第一可视毛细管,G6:第二可视毛细管;G7:第一高倍摄像机,G8:第二高倍摄像机;H1:第一质量流量计,H2:第二质量流量计;B1: first back pressure valve, B2: second back pressure valve; D: oil, gas and water metering device; G1: first light-tight sealing box, G2: second light-tight sealing box; G3: first light source, G4 : the second light source; G5: the first visible capillary, G6: the second visible capillary; G7: the first high-power camera, G8: the second high-power camera; H1: the first mass flow meter, H2: the second mass flow meter ;

E:液体活塞容器;F1:第一液体接收器,F2:第二液体接收器,F3:第三液体接收器;K1-K25:气动阀;L1:第一气体活塞容器,L2:第二气体活塞容器;M:气体增压泵;N:高压气瓶;U1:第一排空管,U2:第二排空管;P1:第一压力传感器,P2:第二压力传感器,P3:第三压力传感器,P4:第四压力传感器;P5:第一压差传感器,P6:第二压差传感器;P7:第五压力传感器;Q:恒温箱;E: liquid piston container; F1: first liquid receiver, F2: second liquid receiver, F3: third liquid receiver; K1-K25: pneumatic valve; L1: first gas piston container, L2: second gas Piston container; M: gas booster pump; N: high pressure cylinder; U1: first emptying pipe, U2: second emptying pipe; P1: first pressure sensor, P2: second pressure sensor, P3: third Pressure sensor, P4: fourth pressure sensor; P5: first differential pressure sensor, P6: second differential pressure sensor; P7: fifth pressure sensor; Q: constant temperature box;

R1:第一恒压恒速泵,R2:第二恒压恒速泵,R3:第三恒压恒速泵;W:计算机。R1: the first constant pressure and constant speed pump, R2: the second constant pressure and constant speed pump, R3: the third constant pressure and constant speed pump; W: computer.

具体实施方式detailed description

以下结合附图和具体实施例,对本发明的气液注入模拟驱油和流体性能测定装置及方法进行详细说明。The gas-liquid injection simulated oil displacement and fluid performance measurement device and method of the present invention will be described in detail below in conjunction with the accompanying drawings and specific embodiments.

气液注入模拟驱油和流体性能测定装置Gas-liquid injection simulated oil displacement and fluid performance measurement device

如图1所示,为本发明的气液注入模拟驱油和流体性能测定装置的实施例,该装置是一种适用于实验室环境的模拟及测定装置(粗线表示物理管道连接,细线表示电连接),包括模拟油藏的模型系统、向模型系统注入气体的气体注入系统、向模型系统注入液体的液体注入系统、对模型系统的流出液进行计量采集的流出液计量采集系统以及用于获取岩心中流体性能的测定系统,其中:As shown in Figure 1, it is the embodiment of the gas-liquid injection simulated oil displacement and fluid performance measurement device of the present invention, which is a kind of simulation and measurement device suitable for laboratory environment (thick line represents physical pipeline connection, thin line Indicates the electrical connection), including the model system for simulating the oil reservoir, the gas injection system for injecting gas into the model system, the liquid injection system for injecting liquid into the model system, the effluent metering and acquisition system for metering and collecting the effluent of the model system, and the A measurement system for obtaining fluid properties in rock cores, wherein:

本实施例中的模型系统为岩心夹置器A用于制作不同含油级别的岩心样品以及作为放置样品的容器,它具有与气体注入系统、液体注入系统、测定系统相连通的岩心夹置器入口A1、与测定系统相连通的岩心夹置器出口A8。置于岩心夹置器A中的岩心为上中下三层非均质岩心,三层非均质岩心共用同一岩心夹置器入口A1注入流体、同一岩心夹置器出口A8采出流体,上中下三层非均质岩心每层分别在位于岩心长度方向的三分之一位置设置岩心流体采集点A2-A7,用于辅助研究流体运移规律和驱油机理。The model system in this embodiment is the core holder A used to make rock core samples of different oil levels and as a container for placing samples. It has a core holder inlet connected to the gas injection system, liquid injection system and measurement system. A1, the outlet A8 of the core holder connected to the measurement system. The cores placed in the core holder A are the upper, middle and lower layers of heterogeneous cores. The three layers of heterogeneous cores share the same core holder inlet A1 to inject fluid and the same core holder outlet A8 to produce fluid. For each layer of the heterogeneous core in the middle and lower three layers, core fluid collection points A2-A7 are set at one-third of the core length direction, which are used to assist in the study of fluid migration laws and oil displacement mechanisms.

本实施例中的气体注入系统包括用于存储高压气体的高压气瓶N以及并联连接的第一气体活塞容器L1和第二气体活塞容器L2,第一气体活塞容器L1的上端开口处设有第三压力传感器P3,用于测量第一气体活塞容器L1内部的气体压力;第一气体活塞容器L1的上端开口通过气动阀K11与第一排空管U1相连通,用于排出气体,降低第一气体活塞容器L1中气体的压力;第一气体活塞容器L1的上端开口处还设有气动阀K10,用于控制第一气体活塞容器L1与其他部件的连通;第一气体活塞容器L1的下端开口处通过气动阀K14连接到第二恒压恒速泵R2、通过气动阀K16连接到第三液体接收容器F3,第三液体接收容器F3用于接收第一、第二气体活塞容器中活塞下部的液体,可使气体活塞容器充入高压气体。The gas injection system in this embodiment includes a high-pressure gas cylinder N for storing high-pressure gas, and a first gas piston container L1 and a second gas piston container L2 connected in parallel. The upper end opening of the first gas piston container L1 is provided with a second Three pressure sensors P3 are used to measure the gas pressure inside the first gas piston container L1; the upper opening of the first gas piston container L1 communicates with the first emptying pipe U1 through the pneumatic valve K11 to discharge gas and reduce the first The pressure of the gas in the gas piston container L1; the upper opening of the first gas piston container L1 is also provided with a pneumatic valve K10, which is used to control the communication between the first gas piston container L1 and other components; the lower end opening of the first gas piston container L1 connected to the second constant pressure and constant speed pump R2 through the pneumatic valve K14, and connected to the third liquid receiving container F3 through the pneumatic valve K16, and the third liquid receiving container F3 is used to receive the lower part of the piston in the first and second gas piston containers Liquid, allowing the gas piston container to be filled with high pressure gas.

同理,第二气体活塞容器L2的上端开口处设有第四压力传感器P4,用于测量第二气体活塞容器L2内部的气体压力;第二气体活塞容器L2的上端开口通过气动阀K12与第二排空管U2相连通,用于排出气体,降低第二气体活塞容器L2中气体的压力;第二气体活塞容器L2的上端开口处还设有气动阀K9,用于控制第二气体活塞容器L2与其他部件的连通;第二气体活塞容器L2的下端开口通过气动阀K13连接到第三恒压恒速泵R3、通过气动阀K17连接到第三液体接收容器F3,第三恒压恒速泵R3用于控制第二气体活塞容器L2中气体流速和压力。Similarly, the upper opening of the second gas piston container L2 is provided with a fourth pressure sensor P4 for measuring the gas pressure inside the second gas piston container L2; The two emptying pipes U2 are connected to each other, and are used to discharge gas and reduce the pressure of the gas in the second gas piston container L2; the upper opening of the second gas piston container L2 is also provided with a pneumatic valve K9, which is used to control the second gas piston container The communication between L2 and other components; the lower end opening of the second gas piston container L2 is connected to the third constant pressure and constant speed pump R3 through the pneumatic valve K13, connected to the third liquid receiving container F3 through the pneumatic valve K17, and the third constant pressure and constant speed pump R3. The pump R3 is used to control the gas flow rate and pressure in the second gas piston container L2.

高压气瓶N通过气动阀K8连接到一气体增压泵M,气体增压泵M用于提高气体压力,其通过气动阀K7连接到气动阀K9和气动阀K10的交接处,气动阀K7、K9、K10的交接处通过气动阀K6连接到第一质量流量计H1的入口端。The high-pressure gas cylinder N is connected to a gas booster pump M through a pneumatic valve K8. The gas booster pump M is used to increase the gas pressure. It is connected to the junction of the pneumatic valve K9 and the pneumatic valve K10 through the pneumatic valve K7. The pneumatic valve K7, The junction of K9 and K10 is connected to the inlet port of the first mass flow meter H1 through the pneumatic valve K6.

本实施例中的液体注入系统包括液体活塞容器E,该液体活塞容器E的上端入口处设置有第二压力传感器P2,用于测量液体活塞容器E中液体的压力,液体活塞容器E的上端开口分别通过气动阀K2与第一液体接收器F1相连以及通过气动阀K5连接到第一质量流量计H1的入口端,第一液体接收器F1用于接收液体活塞容器E中的液体。液体活塞容器E的下端开口通过气动阀K4与第一恒压恒速泵R1相连、通过气动阀K15与第二液体接收容器F2相连,其中,第一恒压恒速泵R1控制液体活塞容器E中液体的流速和压力,第二液体接收容器F2接收液体活塞容器E中活塞下部的液体。The liquid injection system in this embodiment includes a liquid piston container E, the upper end of the liquid piston container E is provided with a second pressure sensor P2 for measuring the pressure of the liquid in the liquid piston container E, the upper end of the liquid piston container E is open The first liquid receiver F1 is connected to the first liquid receiver F1 through the pneumatic valve K2 and connected to the inlet port of the first mass flow meter H1 through the pneumatic valve K5 respectively. The first liquid receiver F1 is used to receive the liquid in the liquid piston container E. The lower end opening of the liquid piston container E is connected to the first constant pressure and constant speed pump R1 through the pneumatic valve K4, and connected to the second liquid receiving container F2 through the pneumatic valve K15, wherein the first constant pressure and constant speed pump R1 controls the liquid piston container E The flow rate and pressure of the liquid in the liquid, the second liquid receiving container F2 receives the liquid in the lower part of the piston in the liquid piston container E.

本实施例中的测定系统包括第一质量流量计H1、第二质量流量计H2、第一可视毛细管G5和第二可视毛细管G6,其中,第一质量流量计H1和第一可视毛细管G5串联连接在岩心夹置器A的岩心夹置器入口A1端,第一质量流量计H1的入口端处设置有第一压力传感器P1,第一质量流量计H1的入口端连接到气体注入系统和液体注入系统,用于测量注入气体、液体或气液混合物的流速,第一压力传感器P1测量第一质量流量计H1入口端的压力;第二质量流量计H2和第二可视毛细管G6通过气动阀K24串联连接到岩心夹置器A的岩心夹置器出口A8,并且岩心流体采集点A2-A7分别通过气动阀K18-K23连接到第二质量流量计H2的入口端,第二质量流量计H2入口端设置第五压力传感器P7,第二质量流量计H2用于测量岩心流体采集点流出的气体、液体或气液混合物的流速。第二可视毛细管G6的出口端连接到流出液计量采集系统。The measurement system in this embodiment includes a first mass flowmeter H1, a second mass flowmeter H2, a first visible capillary G5 and a second visible capillary G6, wherein the first mass flowmeter H1 and the first visible capillary G5 is connected in series to the core holder inlet A1 end of the core holder A, the first pressure sensor P1 is arranged at the inlet end of the first mass flowmeter H1, and the inlet end of the first mass flowmeter H1 is connected to the gas injection system And liquid injection system, used to measure the flow rate of injected gas, liquid or gas-liquid mixture, the first pressure sensor P1 measures the pressure at the inlet port of the first mass flowmeter H1; the second mass flowmeter H2 and the second visual capillary G6 pass through the pneumatic The valve K24 is connected in series to the core holder outlet A8 of the core holder A, and the core fluid collection points A2-A7 are respectively connected to the inlet port of the second mass flowmeter H2 through the pneumatic valves K18-K23, and the second mass flowmeter The fifth pressure sensor P7 is set at the inlet end of H2, and the second mass flow meter H2 is used to measure the flow rate of gas, liquid or gas-liquid mixture flowing out of the core fluid collection point. The outlet end of the second visible capillary G6 is connected to the effluent metering collection system.

第一可视毛细管G5位于岩心夹置器A的岩心夹置器入口A1处与管线相连(可视毛细管不是套在管线上的,他是单独的设备,与管线连接的),沿第一可视毛细管G5长度方向平行的一侧设有第一光源G3,另一侧设有第一高倍摄像机G7,第一可视毛细管G5的入口和出口之间并联有第一压差传感器P5,用于测量第一可视毛细管G5入口和出口之间的压力差,第一可视毛细管G5、第一光源G3、第一高倍摄像机G7以及第一压差传感器P5均置于第一不透光密封箱G1的箱体内,目的是避免外界光线干扰,使摄像机拍摄更加清晰稳定,保持温度恒定,提高测量精度;同样,第二可视毛细管G6位于岩心夹置器出口A8侧与管线相连,沿第二可视毛细管G6长度方向平行的一侧设有第二光源G4,另一侧设有第二高倍摄像机G8,第二可视毛细管G6的入口和出口之间并联有第二压差传感器P6,第二可视毛细管G6、第二光源G4、第二高倍摄像机G8以及第二压差传感器P6均在不透光密封箱体G2中。The first visible capillary G5 is located at the entrance A1 of the core holder A of the core holder A and is connected to the pipeline (the visible capillary is not set on the pipeline, it is a separate device connected to the pipeline), along the first visible A first light source G3 is provided on one side parallel to the length direction of the visual capillary G5, a first high-power camera G7 is provided on the other side, and a first differential pressure sensor P5 is connected in parallel between the inlet and outlet of the first visible capillary G5 for Measure the pressure difference between the inlet and outlet of the first visible capillary G5, the first visible capillary G5, the first light source G3, the first high-power camera G7 and the first differential pressure sensor P5 are all placed in the first light-tight sealed box In the box of G1, the purpose is to avoid external light interference, make the camera shooting more clear and stable, keep the temperature constant, and improve the measurement accuracy; similarly, the second visible capillary G6 is located at the side of the core holder outlet A8 and connected with the pipeline, along the second One side parallel to the length direction of the visible capillary G6 is provided with a second light source G4, and the other side is provided with a second high-power camera G8, and a second differential pressure sensor P6 is connected in parallel between the inlet and outlet of the second visible capillary G6. The two visible capillaries G6, the second light source G4, the second high-power camera G8 and the second differential pressure sensor P6 are all in the light-tight sealed box G2.

本实施例中的流出液计量采集系统包括第一回压阀B1、第二回压阀B2、气动阀K3、气动阀K25和油气水计量装置D,第二可视毛细管G6的出口端依次通过第二回压阀B2、气动阀K25连接到油气水计量装置D,岩心夹置器A的岩心夹置器出口A8依次通过第一回压阀B1、气动阀K3连接到油气水计量装置D,第一回压阀B1和第二回压阀B2分别用于控制岩心夹置器出口A8和第二可视毛细管G6的出口压力,油气水计量装置D用于计量不同时间油、气、水的采出体积。The effluent metering and collection system in this embodiment includes a first back pressure valve B1, a second back pressure valve B2, a pneumatic valve K3, a pneumatic valve K25 and an oil, gas and water metering device D, and the outlet end of the second visual capillary G6 passes through the The second back pressure valve B2 and the pneumatic valve K25 are connected to the oil, gas and water metering device D, and the outlet A8 of the core holder A of the core holder A is connected to the oil, gas and water metering device D through the first back pressure valve B1 and the pneumatic valve K3 in turn, The first back pressure valve B1 and the second back pressure valve B2 are used to control the outlet pressure of the core holder outlet A8 and the second visible capillary G6 respectively, and the oil, gas and water metering device D is used to measure oil, gas and water at different times Extracted volume.

岩心夹置器A、第一回压阀B1、第二回压阀B2、油气水计量装置D、液体活塞容器E、液体接收容器F1、第一质量流量计H1、第二质量流量计H2、第一气体活塞容器L1、第二气体活塞容器L2以及第一不透光箱G1和第二不透光箱G2均置于恒温箱Q中,目的是保持实验过程中注入流体温度恒定,提高实验精度,恒温箱加热温度范围为25℃-200℃。而其它部件不放入恒温箱Q中是为了防止仪器老化,提高仪器寿命及安全性。Core holder A, first back pressure valve B1, second back pressure valve B2, oil, gas and water metering device D, liquid piston container E, liquid receiving container F1, first mass flow meter H1, second mass flow meter H2, The first gas piston container L1, the second gas piston container L2, the first light-tight box G1 and the second light-tight box G2 are all placed in the constant temperature box Q, the purpose is to keep the temperature of the injected fluid constant during the experiment, and improve the temperature of the experiment. Accuracy, the heating temperature range of the incubator is 25°C-200°C. And other components are not put into the incubator Q in order to prevent the aging of the instrument and improve the service life and safety of the instrument.

第一质量流量计H1、第二质量流量计H2、气动阀K1-K25、各压力传感器P1-P6、恒温箱Q、各恒压恒速泵R1-R3、第一光源G3、第二光源G4、第一高倍摄像机G7、第二高倍摄像机G8、气体增压泵M均电连接到计算机W,由计算机W采集相应部件的数据、设定相应部件的参数以及控制相应部件的执行。First mass flowmeter H1, second mass flowmeter H2, pneumatic valves K1-K25, pressure sensors P1-P6, constant temperature box Q, constant pressure and constant speed pumps R1-R3, first light source G3, second light source G4 , the first high-power camera G7, the second high-power camera G8, and the gas booster pump M are all electrically connected to the computer W, and the computer W collects the data of the corresponding components, sets the parameters of the corresponding components, and controls the execution of the corresponding components.

以上各部件按照上述连接关系形成本发明的气液注入模拟驱油和流体性能测定装置,该装置中接触到气体介质和/或液体介质的各部件以及连接各部件的管线均耐酸碱腐蚀,且耐压在50MPa以上;第一质量流量计H1和第二质量流量计H2可选择福克斯波罗公司的产品,该产品可测量气相、液相和气液两相的质量流量,第一可视毛细管G5和第二可视毛细管G6可为蓝宝石材质,耐压50MPa以上、耐温200℃以上;第一气体活塞容器L1和第二气体活塞容器L2容积为2000mL或3000mL,根据岩心夹置器中的岩心孔隙体积来选定,岩心孔隙体积小于200mL,选用2000mL,岩心孔隙体积大于200mL,选用3000mL,液体活塞容器E容积为500mL或1000mL,根据岩心夹置器中的岩心孔隙体积来选定,岩心孔隙体积小于200mL,选用500mL,岩心孔隙体积大于200mL,选用1000mL。The above components form the gas-liquid injection simulated oil displacement and fluid performance measuring device of the present invention according to the above-mentioned connection relationship. In the device, each component that contacts the gas medium and/or liquid medium and the pipelines connecting the components are all resistant to acid and alkali corrosion. And the withstand pressure is above 50MPa; the first mass flowmeter H1 and the second mass flowmeter H2 can choose Foxboro's products, which can measure the mass flow of gas phase, liquid phase and gas-liquid two-phase, the first visible capillary G5 and the second visible capillary G6 can be made of sapphire, with a pressure resistance of more than 50MPa and a temperature resistance of more than 200°C; the volume of the first gas piston container L1 and the second gas piston container L2 is 2000mL or 3000mL. The core pore volume is selected according to the core pore volume. If the core pore volume is less than 200mL, 2000mL is selected. If the core pore volume is greater than 200mL, 3000mL is selected. The volume of the liquid piston container E is 500mL or 1000mL, which is selected according to the core pore volume in the core holder. If the pore volume is less than 200mL, 500mL is selected, and if the core pore volume is greater than 200mL, 1000mL is selected.

气液注入模拟驱油和流体性能测定方法Gas-liquid injection simulated oil displacement and fluid performance measurement method

采用上述装置可以进行气液注入模拟驱油实验以及对岩心中流体性能进行测定,具体的气液注入模拟驱油和流体性能测定方法包括以下步骤:The above-mentioned device can be used to carry out gas-liquid injection simulated oil displacement experiments and to measure the fluid performance in the core. The specific gas-liquid injection simulated oil displacement and fluid performance measurement methods include the following steps:

步骤一:将三层非均质含油岩心放入岩心夹置器A中,液体装入液体活塞容器E中,高压气瓶N中气体种类满足实验的设计,第一气体活塞容器L1和第二气体活塞容器L2中的活塞位于顶部,所有气动阀均处于关闭状态,计算机W控制恒温箱Q加热至实验预设温度;计算机W控制第一光源G3和第二光源G4开启,并控制第一高倍摄像机G7和第二高倍摄像机G8开启并记录整个实验过程中毛细管内流体的影像(以获得流体的流动状态)。Step 1: Put the three-layer heterogeneous oil-bearing core into the core holder A, put the liquid into the liquid piston container E, and the gas type in the high-pressure gas cylinder N meets the design of the experiment, the first gas piston container L1 and the second gas piston container The piston in the gas piston container L2 is at the top, all pneumatic valves are closed, and the computer W controls the thermostat Q to be heated to the experimental preset temperature; the computer W controls the first light source G3 and the second light source G4 to be turned on, and controls the first high-magnification The camera G7 and the second high-power camera G8 are turned on and record images of the fluid in the capillary during the whole experiment (to obtain the flow state of the fluid).

步骤二:计算机W控制气动阀K8、K7、K10、K16开启,高压气瓶N中的气体通过气体增压泵M和气动阀K8、K7、K10进入第一气体活塞容器L1中,当第一气体活塞容器L1中的活塞被推到底部,计算机W控制气动阀K10、K16关闭;计算机W控制气动阀K9、K17开启,高压气瓶N中的气体通过增压泵M和气动阀K8、K7、K9进入第二气体活塞容器L2中,当第二气体活塞容器L2中的活塞被推到底部,计算机W控制气动阀K8、K7、K9、K17关闭。Step 2: The computer W controls the opening of the pneumatic valves K8, K7, K10, and K16, and the gas in the high-pressure cylinder N enters the first gas piston container L1 through the gas booster pump M and the pneumatic valves K8, K7, and K10. The piston in the gas piston container L1 is pushed to the bottom, the computer W controls the closing of the pneumatic valves K10 and K16; the computer W controls the opening of the pneumatic valves K9 and K17, and the gas in the high-pressure cylinder N passes through the booster pump M and the pneumatic valves K8 and K7 , K9 into the second gas piston container L2, when the piston in the second gas piston container L2 is pushed to the bottom, the computer W controls the pneumatic valves K8, K7, K9, K17 to close.

步骤三:根据模拟驱油实验设计的回压设定第一回压阀B1的压力值,计算机W控制气动阀K4、K13、K14开启,计算机W控制第一恒压恒速泵R1、第二恒压恒速泵R2和第三恒压恒速泵R3分别对液体活塞容器E、第一气体活塞容器L1、第二气体活塞容器L2加压,当第二压力传感器P2、第三压力传感器P3或第四压力传感器P4的压力值与第一回压阀B1的压力值相等时,计算机W控制相应的恒压恒速泵停止。Step 3: Set the pressure value of the first back pressure valve B1 according to the back pressure designed in the simulated oil displacement experiment, the computer W controls the opening of the pneumatic valves K4, K13, and K14, and the computer W controls the first constant pressure and constant speed pump R1, the second The constant pressure and constant speed pump R2 and the third constant pressure and constant speed pump R3 pressurize the liquid piston container E, the first gas piston container L1 and the second gas piston container L2 respectively, when the second pressure sensor P2 and the third pressure sensor P3 Or when the pressure value of the fourth pressure sensor P4 is equal to the pressure value of the first back pressure valve B1, the computer W controls the corresponding constant pressure constant speed pump to stop.

第四步:采用气液交替注入方式或气液同时注入方式向岩心夹置器A中的含油岩心中注入驱油介质,在注入过程中,计算机W通过第一高倍摄像机G7和第一光源G3观测气体、液体或气液混合物的流动状态,同时结合第一质量流量计H1数值(进入岩心前的流体流速)和第一压差传感器P5数值(第一可视毛细管G5两端的差压)计算出气体、液体或气液混合物的运动粘度;计算机W控制气动阀K18-K24中的一个开启,设定回压阀B2的压力等于第五压力传感器P7的压力值(岩心流体采集点A2-A7中任一采集点处流出岩心后的压力),通过第二高倍摄像机G8和第二光源G4观测对应三层非均质岩心流体采集点A2-A7及岩心夹置器出口A8的流体流动状态,测量岩心夹置器出口A8的流体性质时需要关闭气动阀K3,同样结合第二质量流量计H2(流出岩心后的流体流速)和第二压差传感器P6数值(第二可视毛细管G6两端的差压)计算出该采集点流体的运动粘度,直到满足模拟驱油实验设计的注入时间为止。Step 4: Inject the oil-displacing medium into the oil-bearing core in the core holder A by using the gas-liquid alternate injection method or the gas-liquid simultaneous injection method. During the injection process, the computer W passes the first high-power camera G7 and the first light source G3 Observe the flow state of gas, liquid or gas-liquid mixture, and combine the value of the first mass flowmeter H1 (fluid flow rate before entering the core) and the value of the first differential pressure sensor P5 (the differential pressure at both ends of the first visible capillary G5) to calculate Kinematic viscosity of gas, liquid or gas-liquid mixture; computer W controls one of pneumatic valve K18-K24 to open, and the pressure of setting back pressure valve B2 is equal to the pressure value of the fifth pressure sensor P7 (core fluid collection point A2-A7 The pressure after flowing out of the core at any collection point), through the second high-power camera G8 and the second light source G4 to observe the fluid flow state corresponding to the three-layer heterogeneous core fluid collection points A2-A7 and the outlet A8 of the core holder, When measuring the fluid properties of the core holder outlet A8, it is necessary to close the pneumatic valve K3, and also combine the second mass flowmeter H2 (fluid flow rate after flowing out of the core) and the second differential pressure sensor P6 value (the two ends of the second visible capillary G6 differential pressure) to calculate the kinematic viscosity of the fluid at the collection point until the injection time designed for the simulated oil displacement experiment is met.

步骤四中的气液同时注入方式包括以下步骤:The gas-liquid simultaneous injection method in step 4 includes the following steps:

计算机W控制气动阀K3、K5、K6、K10开启,计算机W控制第一恒压恒速泵R1、第二恒压恒速泵R2以模拟驱油实验设计的气液比、注入速度注入液体和气体,当满足模拟驱油实验设计的注入时间后,计算机W控制气动阀K3、K5、K6、K10关闭并停止第一恒压恒速泵R1和第二恒压恒速泵R2;在实验过程中计算机W记录第一压力传感器P1的压力值及第一质量流量计H1泡沫流体的流速和注入时间,并实时记录油气水计量装置D中油气水体积。The computer W controls the opening of the pneumatic valves K3, K5, K6, and K10, and the computer W controls the first constant-pressure constant-speed pump R1 and the second constant-pressure constant-speed pump R2 to simulate the gas-liquid ratio and injection speed designed in the oil displacement experiment. Gas, when the injection time of the simulated oil displacement experiment design is satisfied, the computer W controls the pneumatic valves K3, K5, K6, and K10 to close and stop the first constant-pressure constant-speed pump R1 and the second constant-pressure constant-speed pump R2; The central computer W records the pressure value of the first pressure sensor P1 and the flow rate and injection time of the foam fluid of the first mass flowmeter H1, and records the volume of oil, gas and water in the oil, gas and water metering device D in real time.

步骤四中气液交替注入方式包括交替进行的以下步骤:The gas-liquid alternate injection method in step 4 includes the following steps carried out alternately:

(1)注入液体时,计算机W控制气动阀K3、K4、K5开启,计算机W控制第一恒压恒速泵R1以恒定的模拟驱油实验设计的速度注入液体,当满足模拟驱油实验设计的注入时间后,模拟驱油计算机W控制气动阀K5关闭、停止第一恒压恒速泵R1;计算机W同时记录液体注入时的第一压力传感器P1的值、液体注入时间和速度(注入量=注入时间×注入速度),计算机W通过第一质量流量计H1测量的液体注入速度校正通过第一恒压恒速泵R1记录的注入速度,保证注入速度的准确。(1) When injecting the liquid, the computer W controls the opening of the pneumatic valves K3, K4, and K5, and the computer W controls the first constant-pressure constant-speed pump R1 to inject the liquid at a constant speed designed for the simulated oil displacement experiment. After the injection time, the simulated oil displacement computer W controls the pneumatic valve K5 to close and stops the first constant pressure and constant speed pump R1; the computer W simultaneously records the value of the first pressure sensor P1 when the liquid is injected, and the liquid injection time and speed (injection volume = injection time × injection speed), the computer W corrects the injection speed recorded by the first constant pressure and constant speed pump R1 through the liquid injection speed measured by the first mass flowmeter H1 to ensure the accuracy of the injection speed.

在注入液体过程中,计算机W同时控制气动阀K13、K14开启,并分别比较第三压力传感器P3、第四压力传感器P4的压力值与第一压力传感器P1的压力值的大小,即当第三压力传感器P3的压力值大于第一压力传感器P1的压力值时,计算机W控制气动阀K11开启,气体从第一排空管U1排出,直到第三压力传感器P3的压力值等于第一压力传感器P1的压力值为止,关闭气动阀K11;当第三压力传感器P3的压力值小于第一压力传感器P1的压力值时,计算机W控制第二恒压恒速泵R2对第一气体活塞容器L1加压,直到第三压力传感器P3的压力值等于第一压力传感器P1的压力值为止,停止第二恒压恒速泵R2加压;同样,当第四压力传感器P4的压力值大于第一压力传感器P1的压力值,计算机W控制气动阀K12开启,气体从第二排空管U2排出,直到第四压力传感器P4的压力值等于第一压力传感器P1的压力值为止,关闭气动阀K12;当第四压力传感器P4的压力值小于第一压力传感器P1的压力值时,计算机W控制第三恒压恒速泵R3对第二气体活塞容器L2加压,直到第四压力传感器P4的压力值等于第一压力传感器P1的压力值为止,停止第三恒压恒速泵R3加压,直到液体注入完毕。During the liquid injection process, the computer W simultaneously controls the pneumatic valves K13 and K14 to open, and respectively compares the pressure values of the third pressure sensor P3 and the fourth pressure sensor P4 with the pressure value of the first pressure sensor P1, that is, when the third When the pressure value of the pressure sensor P3 is greater than the pressure value of the first pressure sensor P1, the computer W controls the opening of the pneumatic valve K11, and the gas is discharged from the first emptying pipe U1 until the pressure value of the third pressure sensor P3 is equal to that of the first pressure sensor P1 close the pneumatic valve K11; when the pressure value of the third pressure sensor P3 is lower than the pressure value of the first pressure sensor P1, the computer W controls the second constant pressure and constant speed pump R2 to pressurize the first gas piston container L1 , until the pressure value of the third pressure sensor P3 is equal to the pressure value of the first pressure sensor P1, stop the second constant pressure constant speed pump R2 pressurization; similarly, when the pressure value of the fourth pressure sensor P4 is greater than the pressure value of the first pressure sensor P1 The computer W controls the pneumatic valve K12 to open, and the gas is discharged from the second exhaust pipe U2 until the pressure value of the fourth pressure sensor P4 is equal to the pressure value of the first pressure sensor P1, and the pneumatic valve K12 is closed; when the fourth pressure sensor P4 is equal to the pressure value of the first pressure sensor P1 When the pressure value of the pressure sensor P4 is lower than the pressure value of the first pressure sensor P1, the computer W controls the third constant pressure constant speed pump R3 to pressurize the second gas piston container L2 until the pressure value of the fourth pressure sensor P4 is equal to the first Stop the third constant pressure and constant speed pump R3 to pressurize until the pressure value of the pressure sensor P1 is reached until the liquid injection is completed.

(2)注入气体时,计算机W控制气动阀K3、K6、K10开启,计算机W控制第二恒压恒速泵R2以模拟驱油实验设计的速度注入气体,当满足模拟驱油实验设计的注入时间后,模拟驱油计算机W控制气动阀K6、K10关闭并停止第二恒压恒速泵R2;计算机W记录气体注入时的第一压力传感器P1的值、气体注入速度和时间,计算机W通过第一质量流量计H1测量的气体注入速度校正通过第二恒压恒速泵R2记录的注入速度,保证注入速度的准确。(2) When injecting gas, the computer W controls the pneumatic valves K3, K6, and K10 to open, and the computer W controls the second constant-pressure constant-speed pump R2 to inject gas at the speed designed for the simulated oil displacement experiment. After a period of time, the simulated oil displacement computer W controls the pneumatic valves K6 and K10 to close and stops the second constant pressure and constant speed pump R2; the computer W records the value of the first pressure sensor P1, the gas injection speed and time when the gas is injected, and the computer W passes through The gas injection rate measured by the first mass flow meter H1 corrects the injection rate recorded by the second constant pressure constant speed pump R2 to ensure the accuracy of the injection rate.

在注入气体过程中,计算机W比较第四压力传感器P4的压力值与第一压力传感器P1的压力值的大小,当第四压力传感器P4的压力值大于第一压力传感器P1的压力值,计算机W控制气动阀K12开启,气体从第二排空管U2排出,直到第四压力传感器P4的压力值等于第一压力传感器P1的压力值为止,关闭气动阀K12;当第四压力传感器P4的压力值小于第一压力传感器P1的压力值,计算机W控制第三恒压恒速泵R3对第二气体活塞容器L2加压,直到第四压力传感器P4的压力值等于第一压力传感器P1的压力值为止,停止第三恒压恒速泵R3加压,直到气体注入完毕,或当第一气体活塞容器L1中气体体积用完时,计算机W控制气动阀K9开启,控制气动阀K10关闭并停止第二恒压恒速泵R2,计算机W控制第三恒压恒速泵R3以同样的模拟驱油实验要求速度继续注入气体,当注入气体时间满足模拟驱油实验要求后,计算机W自动控制气动阀K6、K9关闭和停止第三恒压恒速泵R3。During the gas injection process, the computer W compares the pressure value of the fourth pressure sensor P4 with the pressure value of the first pressure sensor P1, and when the pressure value of the fourth pressure sensor P4 is greater than the pressure value of the first pressure sensor P1, the computer W Control the opening of the pneumatic valve K12, and the gas is discharged from the second emptying pipe U2 until the pressure value of the fourth pressure sensor P4 is equal to the pressure value of the first pressure sensor P1, then close the pneumatic valve K12; when the pressure value of the fourth pressure sensor P4 If the pressure value of the first pressure sensor P1 is lower than the pressure value of the first pressure sensor P1, the computer W controls the third constant pressure constant speed pump R3 to pressurize the second gas piston container L2 until the pressure value of the fourth pressure sensor P4 is equal to the pressure value of the first pressure sensor P1 , stop the third constant pressure and constant speed pump R3 to pressurize until the gas injection is complete, or when the gas volume in the first gas piston container L1 is used up, the computer W controls the opening of the pneumatic valve K9, controls the closing of the pneumatic valve K10 and stops the second The constant pressure and constant speed pump R2, the computer W controls the third constant pressure and constant speed pump R3 to continue injecting gas at the same speed required by the simulated oil flooding experiment. When the gas injection time meets the requirements of the simulated oil flooding experiment, the computer W automatically controls the pneumatic valve K6 , K9 closes and stops the third constant-pressure constant-speed pump R3.

在注入气体过程中,计算机W同时比较第二压力传感器P2的压力值与第一压力传感器P1的压力值的大小,当第二压力传感器P2的压力值大于第一压力传感器P1的压力值时,计算机W控制气动阀K2开启,排出多余液体到第一液体接收容器F1中,直到第二压力传感器P2的压力值等于第一压力传感器P1的压力值为止,关闭气动阀K2;当第二压力传感器P2的压力值小于第一压力传感器P1的压力值,计算机W控制第一恒压恒速泵R1对液体活塞容器E加压,直到第二压力传感器P2的压力值等于第一压力传感器P1的压力值为止,停止第一恒压恒速泵R1,直到气体注入完毕。During the gas injection process, the computer W simultaneously compares the pressure value of the second pressure sensor P2 with the pressure value of the first pressure sensor P1, and when the pressure value of the second pressure sensor P2 is greater than the pressure value of the first pressure sensor P1, The computer W controls the opening of the pneumatic valve K2, discharges excess liquid into the first liquid receiving container F1, and closes the pneumatic valve K2 until the pressure value of the second pressure sensor P2 is equal to the pressure value of the first pressure sensor P1; when the second pressure sensor The pressure value of P2 is less than the pressure value of the first pressure sensor P1, the computer W controls the first constant pressure and constant speed pump R1 to pressurize the liquid piston container E until the pressure value of the second pressure sensor P2 is equal to the pressure of the first pressure sensor P1 value, stop the first constant pressure and constant speed pump R1 until the gas injection is complete.

气液注入模拟驱油和流体性能测定方法中气液交替注入时岩心入口压力平稳,流速恒定,不出现波动。质量流量计可以测量微量气体、液体、气液混合物的流速。In gas-liquid injection simulated oil displacement and fluid performance measurement method, the core inlet pressure is stable, the flow rate is constant, and there is no fluctuation when the gas-liquid is alternately injected. Mass flow meters can measure the flow rate of trace gases, liquids, and gas-liquid mixtures.

气液注入模拟驱油和流体性能测定方法中获取的流体性能参数包括:流体状态(由上述步骤四中第一高倍摄像机G7和第二高倍摄像机G8记录)、流体流速(在步骤四中由第一质量流量计H1和第二质量流量计H2记录)、流体运动粘度(在步骤四中用下述算式计算得到)、压力(第一压力传感器P1和第五压力传感器P7记录)。The fluid performance parameters obtained in the gas-liquid injection simulated oil displacement and fluid performance measurement methods include: fluid state (recorded by the first high-power camera G7 and the second high-power camera G8 in the above step four), fluid velocity (in step four by the first high-power camera G8) A mass flow meter H1 and a second mass flow meter H2 record), fluid kinematic viscosity (calculated using the following formula in step 4), pressure (recorded by the first pressure sensor P1 and the fifth pressure sensor P7).

通过公式泊肃叶定律计算运动粘度。流体运动粘度计算公式为: Kinematic viscosity is calculated by the formula Poiseuille's law. The formula for calculating fluid kinematic viscosity is:

式中μ为流体粘度,Q为流体的流量,L为可视毛细管的长度,r为可视毛细管的半径,△P为可视毛细管两端的差压,K为可视毛细管常数。In the formula, μ is the viscosity of the fluid, Q is the flow rate of the fluid, L is the length of the visible capillary, r is the radius of the visible capillary, ΔP is the differential pressure at both ends of the visible capillary, and K is the constant of the visible capillary.

气液注入模拟驱油和流体性能测定方法可以获取岩心夹置器的注入液体流动性质和出口液体流动性质。岩心夹置器在上中下三层设置A2-A7六个流体采集点,可以测定同一层位不同位置流体的性质,不同层位相同位置流体的性质。即可测定流体在岩心中不同位置、层位的流体性质。如果岩心含油,可以测定油对不同位置流体性能的影响。The gas-liquid injection simulated oil displacement and fluid performance measurement methods can obtain the flow properties of the injected liquid and the outlet liquid of the core holder. The core holder sets six fluid collection points A2-A7 in the upper, middle and lower layers, which can measure the properties of fluids in different positions in the same layer and the properties of fluids in the same positions in different layers. The fluid properties of the fluid at different positions and layers in the core can be determined. If the core contains oil, the effect of the oil on the fluid properties at different locations can be determined.

上述获得的流体性能数据可用于驱油机理的研究(参见实验验证部分)。The fluid performance data obtained above can be used to study the oil displacement mechanism (see the experimental verification section).

另外,如果实验还有其它特殊要求,可根据实际情况,调整注入流程,以满足实验要求。In addition, if there are other special requirements for the experiment, the injection process can be adjusted according to the actual situation to meet the experimental requirements.

实验验证Experimental verification

实验温度45℃,岩心上、中、下层渗透率分别为200、800、1000md,岩心孔隙体积为256mL,含油饱和度为71%;实验设计回压为5MPa,气液同时注入,气液比为1:1,二氧化碳气体注入速度0.9mL/min,起泡剂注入速度0.9mL/min,注入时间72min,起泡剂组成为:磺基甜菜碱硅表面活性剂0.5wt%、十二烷基二甲基氧化按0.2wt%、部分水解聚丙烯酰胺(分子量为1660万,水解度为23%)0.1wt%、余量为水。第一可视毛细管G5、第二可视毛细管G6的长度为80cm,内径为1mm,可视毛细管常数K为0.756。The experimental temperature is 45°C, the permeability of the upper, middle and lower layers of the core is 200, 800, and 1000md respectively, the pore volume of the core is 256mL, and the oil saturation is 71%. 1:1, carbon dioxide gas injection rate 0.9mL/min, foaming agent injection rate 0.9mL/min, injection time 72min, foaming agent composition: sulfobetaine silicon surfactant 0.5wt%, dodecyl di Methyl oxidation is 0.2wt%, partially hydrolyzed polyacrylamide (molecular weight is 16.6 million, hydrolysis degree is 23%) is 0.1wt%, and the balance is water. The first visible capillary G5 and the second visible capillary G6 have a length of 80 cm, an inner diameter of 1 mm, and a visible capillary constant K of 0.756.

表1模拟驱油实验参数表Table 1. Parameter table of simulated oil displacement experiment

分析流体在岩心中不同时间、不同位置的流动状态和粘度参数为分析驱油机理提供依据。随时间变化A4,A7采集点流体粘度发生很大变化,并观测到含油泡沫,说明这两点位置附近泡沫形成了有效驱替,且这两点位置附近的油被驱替出来,说明泡沫在中高渗透层形成了有效驱替。在注入40min,A2采集点粘度较低,观测到少量含油泡沫,表明低渗透层泡沫没有形成有效驱替,需要再采取其它驱替方法来提高低渗透层的驱替效率。在注入70min,A8采集点粘度较低,且只观察到少量含油泡沫,表明发泡剂在岩心中吸附损失较大、泡沫耐油性较差,需要提高发泡剂的耐油性和注入时间。Analyzing the flow state and viscosity parameters of the fluid at different times and locations in the core provides a basis for analyzing the oil displacement mechanism. The viscosity of the fluid at collection points A4 and A7 changes greatly with time, and oil-containing foam is observed, indicating that the foam near these two points has formed an effective displacement, and the oil near these two points has been displaced, indicating that the foam is in the The medium-high permeability layer forms an effective displacement. After 40 minutes of injection, the viscosity at the A2 collection point was low, and a small amount of oily foam was observed, indicating that the foam in the low-permeability layer did not form effective displacement, and other displacement methods were needed to improve the displacement efficiency of the low-permeability layer. At 70 minutes after injection, the viscosity of the A8 collection point was low, and only a small amount of oily foam was observed, indicating that the foaming agent had a large adsorption loss in the core and the oil resistance of the foam was poor, so it is necessary to increase the oil resistance of the foaming agent and the injection time.

本领域技术人员应当理解,这些实施例或实施方式仅用于说明本发明而不限制本发明的范围,对本发明所做的各种等价变型和修改均属于本发明公开内容。Those skilled in the art should understand that these examples or implementations are only for illustrating the present invention and not limiting the scope of the present invention, and various equivalent variations and modifications to the present invention belong to the disclosure content of the present invention.

Claims (12)

1.一种气液注入模拟驱油和流体性能测定装置,包括模拟油藏的模型系统、向模型系统注入驱替介质的注入系统和对模型系统的流出液进行计量采集的流出液计量采集系统,所述模型系统包括岩心夹置器(A),其特征在于,还包括用于获取岩心中流体性能的测定系统,所述测定系统包括:1. A gas-liquid injection simulated oil displacement and fluid performance measurement device, including a model system for simulating reservoirs, an injection system for injecting displacement media into the model system, and an effluent metering and acquisition system for metering and collecting the effluent of the model system , the model system includes a core holder (A), characterized in that it also includes a measurement system for obtaining fluid properties in the core, and the measurement system includes: 第一质量流量计(H1)和第一可视毛细管(G5),二者串联连接在岩心夹置器(A)的岩心夹置器入口(A1)端,第一质量流量计(H1)的入口端处设置有第一压力传感器(P1);第一质量流量计(H1)的入口端连接到所述注入系统;The first mass flowmeter (H1) and the first visual capillary (G5), the two are connected in series at the core holder inlet (A1) end of the core holder (A), the first mass flowmeter (H1) The inlet end is provided with a first pressure sensor (P1); the inlet end of the first mass flow meter (H1) is connected to the injection system; 第二质量流量计(H2)和第二可视毛细管(G6),二者通过气动阀(K24)串联连接到岩心夹置器(A)的岩心夹置器出口(A8),并且岩心流体采集点(A2-A7)分别通过气动阀(K18-K23)连接到第二质量流量计(H2)的入口端,第二质量流量计(H2)入口端设置第五压力传感器(P7);第二可视毛细管(G6)的出口端连接到所述流出液计量采集系统。The second mass flow meter (H2) and the second visual capillary (G6), both are connected in series to the core holder outlet (A8) of the core holder (A) through the pneumatic valve (K24), and the core fluid collection The points (A2-A7) are respectively connected to the inlet port of the second mass flowmeter (H2) through the pneumatic valve (K18-K23), and the inlet port of the second mass flowmeter (H2) is provided with the fifth pressure sensor (P7); the second The outlet end of the visual capillary (G6) is connected to the effluent metering collection system. 2.根据权利要求1所述的气液注入模拟驱油和流体性能测定装置,其特征在于,所述流出液计量采集系统包括第一回压阀(B1)、第二回压阀(B2)、气动阀(K3)、气动阀(K25)和油气水计量装置(D),第二可视毛细管(G6)的出口端依次通过第二回压阀(B2)、气动阀(K25)连接到油气水计量装置(D),岩心夹置器(A)的岩心夹置器出口(A8)依次通过第一回压阀(B1)、气动阀(K3)连接到油气水计量装置(D)。2. The gas-liquid injection simulated oil displacement and fluid performance measuring device according to claim 1, characterized in that, the effluent metering and collection system comprises a first back pressure valve (B1), a second back pressure valve (B2) , pneumatic valve (K3), pneumatic valve (K25) and oil, gas and water metering device (D), the outlet end of the second visual capillary (G6) is connected to the The oil-gas-water metering device (D), the core holder outlet (A8) of the core holder (A) is connected to the oil-gas-water metering device (D) through the first back pressure valve (B1) and the pneumatic valve (K3) in sequence. 3.根据权利要求2所述的气液注入模拟驱油和流体性能测定装置,其特征在于,所述第一可视毛细管(G5)位于岩心夹置器(A)的岩心夹置器入口(A1)端且与管线相连,沿第一可视毛细管(G5)长度方向平行的一侧设有第一光源(G3),另一侧设有第一高倍摄像机(G7),第一可视毛细管(G5)的入口和出口之间并联有第一压差传感器(P5)用以测量第一可视毛细管(G5)入口和出口之间的压力差。3. gas-liquid injection simulated oil displacement and fluid performance measuring device according to claim 2, is characterized in that, described first visible capillary (G5) is positioned at the rock core holder inlet (A) of rock core holder (A) A1) end and connected to the pipeline, a first light source (G3) is provided on one side parallel to the length direction of the first visible capillary (G5), a first high-power camera (G7) is provided on the other side, and the first visible capillary A first differential pressure sensor (P5) is connected in parallel between the inlet and outlet of (G5) to measure the pressure difference between the inlet and outlet of the first visible capillary (G5). 4.根据权利要求2或3所述的气液注入模拟驱油和流体性能测定装置,其特征在于,所述第二可视毛细管(G6)位于岩心夹置器出口(A8)端与管线相连,沿第二可视毛细管(G6)长度方向平行的一侧设有第二光源(G4),另一侧设有第二高倍摄像机(G8),第二可视毛细管(G6)的入口和出口之间并联有第二压差传感器(P6)。4. The gas-liquid injection simulated oil displacement and fluid performance measuring device according to claim 2 or 3, characterized in that, the second visible capillary (G6) is located at the end of the core holder outlet (A8) and is connected to the pipeline , a second light source (G4) is provided on one side parallel to the length direction of the second visible capillary (G6), a second high-power camera (G8) is provided on the other side, and the entrance and exit of the second visible capillary (G6) A second differential pressure sensor (P6) is connected in parallel between them. 5.根据权利要求4所述的气液注入模拟驱油和流体性能测定装置,其特征在于,所述注入系统包括向模型系统注入气体的气体注入系统和向模型系统注入液体的液体注入系统。5. The gas-liquid injection simulated oil displacement and fluid performance measurement device according to claim 4, wherein the injection system includes a gas injection system for injecting gas into the model system and a liquid injection system for injecting liquid into the model system. 6.根据权利要求5所述的气液注入模拟驱油和流体性能测定装置,其特征在于,所述气体注入系统包括:6. The gas-liquid injection simulated oil displacement and fluid performance measuring device according to claim 5, wherein the gas injection system comprises: 并联连接的第一气体活塞容器L1和第二气体活塞容器L2,其中,A first gas piston container L1 and a second gas piston container L2 connected in parallel, wherein, 所述第一气体活塞容器(L1)的上端开口处设有气动阀(K10)和用于测量第一气体活塞容器(L1)内部气体压力的第三压力传感器(P3),第一气体活塞容器(L1)的上端开口通过气动阀(K11)与第一排空管(U1)相连通;第一气体活塞容器(L1)的下端开口通过气动阀(K14)连接到第二恒压恒速泵(R2)、通过气动阀(K16)连接到第三液体接收容器(F3);The upper opening of the first gas piston container (L1) is provided with a pneumatic valve (K10) and a third pressure sensor (P3) for measuring the internal gas pressure of the first gas piston container (L1). The upper opening of (L1) is connected to the first emptying pipe (U1) through the pneumatic valve (K11); the lower opening of the first gas piston container (L1) is connected to the second constant pressure and constant speed pump through the pneumatic valve (K14) (R2), connected to the third liquid receiving container (F3) through a pneumatic valve (K16); 第二气体活塞容器(L2)的上端开口处设有气动阀(K9)和用于测量第二气体活塞容器(L2)内部气体压力的第四压力传感器(P4),第二气体活塞容器(L2)的上端开口通过气动阀(K12)与第二排空管(U2)相连通;第二气体活塞容器(L2)的下端开口通过气动阀(K13)连接到第三恒压恒速泵(R3)、通过气动阀(K17)连接到第三液体接收容器(F3);The upper opening of the second gas piston container (L2) is provided with a pneumatic valve (K9) and a fourth pressure sensor (P4) for measuring the internal gas pressure of the second gas piston container (L2), and the second gas piston container (L2 ) through the pneumatic valve (K12) and the second emptying pipe (U2); the lower end of the second gas piston container (L2) is connected to the third constant pressure constant speed pump (R3) through the pneumatic valve (K13) ), connected to the third liquid receiving container (F3) through a pneumatic valve (K17); 用于存储高压气体的高压气瓶(N),所述高压气瓶(N)通过气动阀(K8)连接到一气体增压泵(M),所述气体增压泵(M)通过气动阀(K7)连接到气动阀(K9)和气动阀(K10)的交接处,气动阀(K7、K9、K10)的交接处通过气动阀(K6)连接到第一质量流量计(H1)的入口端。A high-pressure gas cylinder (N) for storing high-pressure gas, the high-pressure gas cylinder (N) is connected to a gas booster pump (M) through a pneumatic valve (K8), and the gas booster pump (M) is connected to a gas booster pump (M) through a pneumatic valve (K7) is connected to the junction of pneumatic valve (K9) and pneumatic valve (K10), and the junction of pneumatic valve (K7, K9, K10) is connected to the inlet of the first mass flow meter (H1) through pneumatic valve (K6) end. 7.根据权利要求5所述的气液注入模拟驱油和流体性能测定装置,其特征在于,所述液体注入系统包括液体活塞容器(E),所述液体活塞容器(E)的上端入口处设置有用于测量液体活塞容器(E)中液体压力的第二压力传感器(P2),液体活塞容器(E)的上端开口分别通过气动阀(K2)与第一液体接收器(F1)相连以及通过气动阀(K5)连接到第一质量流量计(H1)的入口端;所述液体活塞容器(E)的下端开口通过气动阀(K4)与第一恒压恒速泵(R1)相连,并通过气动阀(K15)与第二液体接收容器(F2)相连。7. gas-liquid injection simulated oil displacement and fluid performance measuring device according to claim 5, is characterized in that, described liquid injection system comprises liquid piston container (E), and the upper end entrance of described liquid piston container (E) A second pressure sensor (P2) for measuring the liquid pressure in the liquid piston container (E) is provided, and the upper end opening of the liquid piston container (E) is respectively connected with the first liquid receiver (F1) through a pneumatic valve (K2) and through The pneumatic valve (K5) is connected to the inlet port of the first mass flow meter (H1); the lower end opening of the liquid piston container (E) is connected to the first constant-pressure constant-speed pump (R1) through the pneumatic valve (K4), and It is connected to the second liquid receiving container (F2) through a pneumatic valve (K15). 8.根据权利要求5或6所述的气液注入模拟驱油和流体性能测定装置,其特征在于,所述岩心夹置器(A)、第一回压阀(B1)、第二回压阀(B2)、油气水计量装置(D)、液体活塞容器(E)、液体接收容器(F1)、第一质量流量计(H1)、第二质量流量计(H2)、第一气体活塞容器(L1)、第二气体活塞容器(L2)以及第一不透光箱(G1)和第二不透光箱(G2)均置于恒温箱(Q)中。8. The gas-liquid injection simulated oil displacement and fluid performance measuring device according to claim 5 or 6, characterized in that, the core clamp (A), the first back pressure valve (B1), the second back pressure Valve (B2), oil, gas and water metering device (D), liquid piston container (E), liquid receiving container (F1), first mass flow meter (H1), second mass flow meter (H2), first gas piston container (L1), the second gas piston container (L2), and the first light-tight box (G1) and the second light-tight box (G2) are all placed in the thermostatic box (Q). 9.根据权利要求5或6所述的气液注入模拟驱油和流体性能测定装置,其特征在于,所述第一质量流量计(H1)、第二质量流量计(H2)、气动阀(K1-K25)、各压力传感器(P1-P4,P7)、各压差传感器(P4,P5)、恒温箱(Q)、各恒压恒速泵(R1-R3)、第一光源(G3)、第二光源(G4)、第一高倍摄像机(G7)、第二高倍摄像机(G8)、气体增压泵M均电连接到计算机(W)。9. according to claim 5 or 6 described gas-liquid injection simulated oil flooding and fluid property measuring device, it is characterized in that, described first mass flow meter (H1), the second mass flow meter (H2), pneumatic valve ( K1-K25), each pressure sensor (P1-P4, P7), each differential pressure sensor (P4, P5), constant temperature box (Q), each constant pressure constant speed pump (R1-R3), the first light source (G3) , the second light source (G4), the first high-power camera (G7), the second high-power camera (G8), and the gas booster pump M are all electrically connected to the computer (W). 10.一种气液注入模拟驱油和流体性能测定方法,所述方法采用权利要求1至9任一项所述的气液注入模拟驱油和流体性能测定装置进行气液注入模拟驱油实验以及对岩心中流体性能进行测定,包括以下步骤:10. A gas-liquid injection simulated oil displacement and fluid performance measurement method, said method adopts the gas-liquid injection simulated oil displacement and fluid performance measurement device according to any one of claims 1 to 9 to carry out the gas-liquid injection simulated oil displacement experiment And measuring the fluid properties in the core, including the following steps: 步骤一:将三层非均质含油岩心放入岩心夹置器(A)中,液体装入液体活塞容器(E)中,高压气瓶(N)中气体种类满足所述模拟驱油实验的设计,第一气体活塞容器(L1)和第二气体活塞容器(L2)中的活塞位于顶部,所有气动阀均处于关闭状态,计算机(W)控制恒温箱(Q)加热至模拟驱油实验预设温度;计算机(W)控制第一光源(G3)和第二光源(G4)开启,并控制第一高倍摄像机(G7)和第二高倍摄像机(G8)开启;Step 1: Put the three-layer heterogeneous oil-bearing core into the core holder (A), put the liquid into the liquid piston container (E), and the gas type in the high-pressure gas cylinder (N) meets the requirements of the simulated oil displacement experiment. Design, the pistons in the first gas piston container (L1) and the second gas piston container (L2) are located at the top, all pneumatic valves are closed, and the computer (W) controls the thermostat (Q) to heat up to the pre-simulation oil displacement experiment. Set the temperature; the computer (W) controls the opening of the first light source (G3) and the second light source (G4), and controls the opening of the first high-power camera (G7) and the second high-power camera (G8); 步骤二:计算机(W)控制气动阀(K8,K7,K10,K16)开启,高压气瓶(N)中的气体通过气体增压泵(M)和气动阀(K8,K7,K10)进入第一气体活塞容器(L1)中,当第一气体活塞容器(L1)中的活塞被推到底部,计算机(W)控制气动阀(K10,K16)关闭;计算机(W)控制气动阀(K9,K17)开启,高压气瓶(N)中的气体通过增压泵(M)和气动阀(K8,K7,K9)进入第二气体活塞容器(L2)中,当第二气体活塞容器(L2)中的活塞被推到底部,计算机(W)控制气动阀(K8,K7,K9,K17)关闭;Step 2: The computer (W) controls the opening of the pneumatic valves (K8, K7, K10, K16), and the gas in the high-pressure cylinder (N) enters the first stage through the gas booster pump (M) and the pneumatic valves (K8, K7, K10). In a gas piston container (L1), when the piston in the first gas piston container (L1) is pushed to the bottom, the computer (W) controls the pneumatic valves (K10, K16) to close; the computer (W) controls the pneumatic valves (K9, K17) is opened, the gas in the high-pressure cylinder (N) enters the second gas piston container (L2) through the booster pump (M) and the pneumatic valve (K8, K7, K9), when the second gas piston container (L2) The piston in the cylinder is pushed to the bottom, and the computer (W) controls the pneumatic valves (K8, K7, K9, K17) to close; 步骤三:根据模拟驱油实验设计的回压设定第一回压阀(B1)的压力值,计算机(W)控制气动阀(K4,K13,K14)开启,计算机(W)控制第一恒压恒速泵(R1)、第二恒压恒速泵(R2)和第三恒压恒速泵(R3)分别对液体活塞容器(E)、第一气体活塞容器(L1)、第二气体活塞容器(L2)加压,当第二压力传感器(P2)、第三压力传感器(P3)或第四压力传感器(P4)的压力值与第一回压阀(B1)的压力值相等时,计算机(W)控制相应的恒压恒速泵停止;Step 3: Set the pressure value of the first back pressure valve (B1) according to the back pressure designed in the simulated oil displacement experiment, the computer (W) controls the opening of the pneumatic valves (K4, K13, K14), and the computer (W) controls the first constant The pressure and constant speed pump (R1), the second constant pressure and constant speed pump (R2) and the third constant pressure and constant speed pump (R3) respectively control the liquid piston container (E), the first gas piston container (L1), the second gas The piston container (L2) is pressurized, when the pressure value of the second pressure sensor (P2), the third pressure sensor (P3) or the fourth pressure sensor (P4) is equal to the pressure value of the first back pressure valve (B1), The computer (W) controls the corresponding constant pressure constant speed pump to stop; 步骤四:采用气液交替注入方式或气液同时注入方式向岩心夹置器(A)中的含油岩心中注入驱油介质,在注入过程中,计算机(W)通过第一高倍摄像机(G7)和第一光源(G3)观测气体、液体或气液混合物的流动状态,同时结合第一质量流量计(H1)和第一压差传感器(P5)的数值计算出气体、液体或气液混合物的运动粘度;计算机(W)控制气动阀(K18-K24)中的一个开启,设定回压阀(B2)的压力等于第五压力传感器(P7)的压力值,通过第二高倍摄像机(G8)和第二光源(G4)观测对应三层非均质岩心流体采集点(A2-A7)及岩心夹置器出口(A8)的流体流动状态,同样结合第二质量流量计(H2)和第二压差传感器(P6)的数值计算出该采集点流体的运动粘度,直到满足模拟驱油实验设计的注入时间为止。Step 4: Inject the oil-displacing medium into the oil-bearing core in the core holder (A) by means of alternate gas-liquid injection or simultaneous gas-liquid injection. During the injection process, the computer (W) passes through the first high-power camera (G7) and the first light source (G3) to observe the flow state of the gas, liquid or gas-liquid mixture, and at the same time combine the values of the first mass flow meter (H1) and the first differential pressure sensor (P5) to calculate the flow rate of the gas, liquid or gas-liquid mixture Kinematic viscosity; the computer (W) controls one of the pneumatic valves (K18-K24) to open, and sets the pressure of the back pressure valve (B2) equal to the pressure value of the fifth pressure sensor (P7), through the second high-power camera (G8) and the second light source (G4) to observe the fluid flow state corresponding to the three-layer heterogeneous core fluid collection points (A2-A7) and the outlet of the core holder (A8), also combined with the second mass flowmeter (H2) and the second The value of the differential pressure sensor (P6) calculates the kinematic viscosity of the fluid at the collection point until the injection time designed for the simulated oil displacement experiment is met. 11.根据权利要求10所述的气液注入模拟驱油和流体性能测定方法,其特征在于,步骤四中的气液同时注入方式包括以下步骤:11. gas-liquid injection simulated oil displacement and fluid performance measurement method according to claim 10, is characterized in that, the gas-liquid simultaneous injection mode in step 4 comprises the following steps: 计算机(W)控制气动阀(K3,K5,K6,K10)开启,计算机(W)控制第一恒压恒速泵(R1)、第二恒压恒速泵(R2)以模拟驱油实验设计的气液比、注入速度注入液体和气体,当满足模拟驱油实验设计的注入时间后,计算机(W)控制气动阀(K3,K5,K6,K10)关闭并停止第一恒压恒速泵(R1)和第二恒压恒速泵(R2);在实验过程中计算机(W)记录第一压力传感器(P1)的压力值及第一质量流量计(H1)泡沫流体的流速和注入时间,并实时记录油气水计量装置(D)中油、气、水体积。The computer (W) controls the opening of the pneumatic valves (K3, K5, K6, K10), and the computer (W) controls the first constant-pressure constant-speed pump (R1) and the second constant-pressure constant-speed pump (R2) to simulate oil displacement experimental design The gas-liquid ratio and injection speed are used to inject liquid and gas. When the injection time of the simulated oil displacement experiment is met, the computer (W) controls the pneumatic valves (K3, K5, K6, K10) to close and stop the first constant pressure and constant speed pump. (R1) and the second constant pressure and constant speed pump (R2); during the experiment, the computer (W) records the pressure value of the first pressure sensor (P1) and the flow rate and injection time of the first mass flow meter (H1) foam fluid , and record the volume of oil, gas and water in the oil, gas and water metering device (D) in real time. 12.根据权利要求10所述的气液注入模拟驱油和流体性能测定方法,其特征在于,步骤四中的气液交替注入方式包括交替进行的以下步骤:12. The gas-liquid injection simulated oil displacement and fluid performance measurement method according to claim 10, wherein the gas-liquid alternate injection method in step 4 comprises the following steps carried out alternately: (1)注入液体时,计算机(W)控制气动阀(K3,K4,K5)开启,计算机(W)控制第一恒压恒速泵(R1)以恒定的模拟驱油实验设计的速度注入液体,当满足模拟驱油实验设计的注入时间后,计算机(W)控制气动阀(K5)关闭,并停止第一恒压恒速泵(R1);计算机(W)同时记录液体注入时的第一压力传感器(P1)的值、液体注入时间和速度,通过第一质量流量计(H1)测量的液体注入速度校正通过第一恒压恒速泵(R1)记录的注入速度;(1) When liquid is injected, the computer (W) controls the opening of the pneumatic valves (K3, K4, K5), and the computer (W) controls the first constant pressure and constant speed pump (R1) to inject the liquid at a constant speed designed for the simulated oil flooding experiment , when the injection time designed for the simulated oil displacement experiment is met, the computer (W) controls the pneumatic valve (K5) to close, and stops the first constant-pressure constant-speed pump (R1); the computer (W) simultaneously records the first time when the liquid is injected The value of the pressure sensor (P1), the liquid injection time and speed, the liquid injection speed measured by the first mass flow meter (H1) corrects the injection speed recorded by the first constant pressure constant speed pump (R1); 在注入液体过程中,计算机(W)同时控制气动阀(K13,K14)开启,并分别比较第三压力传感器(P3)、第四压力传感器(P4)的压力值与第一压力传感器(P1)的压力值的大小,即当第三压力传感器(P3)的压力值大于第一压力传感器(P1)的压力值时,计算机(W)控制气动阀(K11)开启,气体从第一排空管(U1)排出,直到第三压力传感器(P3)的压力值等于第一压力传感器(P1)的压力值为止,关闭气动阀(K11);当第三压力传感器(P3)的压力值小于第一压力传感器(P1)的压力值时,计算机(W)控制第二恒压恒速泵(R2)对第一气体活塞容器(L1)加压,直到第三压力传感器(P3)的压力值等于第一压力传感器(P1)的压力值为止,停止第二恒压恒速泵(R2)加压;同样,当第四压力传感器(P4)的压力值大于第一压力传感器(P1)的压力值,计算机(W)控制气动阀(K12)开启,气体从第二排空管(U2)排出,直到第四压力传感器(P4)的压力值等于第一压力传感器(P1)的压力值为止,关闭气动阀(K12);当第四压力传感器(P4)的压力值小于第一压力传感器(P1)的压力值时,计算机(W)控制第三恒压恒速泵(R3)对第二气体活塞容器(L2)加压,直到第四压力传感器(P4)的压力值等于第一压力传感器(P1)的压力值为止,停止第三恒压恒速泵(R3)加压,直到液体注入完毕;During the liquid injection process, the computer (W) simultaneously controls the pneumatic valves (K13, K14) to open, and respectively compares the pressure values of the third pressure sensor (P3), the fourth pressure sensor (P4) with the first pressure sensor (P1) The size of the pressure value, that is, when the pressure value of the third pressure sensor (P3) is greater than the pressure value of the first pressure sensor (P1), the computer (W) controls the pneumatic valve (K11) to open, and the gas is discharged from the first exhaust pipe (U1) discharge until the pressure value of the third pressure sensor (P3) is equal to the pressure value of the first pressure sensor (P1), close the pneumatic valve (K11); when the pressure value of the third pressure sensor (P3) is less than the first When the pressure value of the pressure sensor (P1), the computer (W) controls the second constant pressure constant speed pump (R2) to pressurize the first gas piston container (L1), until the pressure value of the third pressure sensor (P3) is equal to the first Until the pressure value of the first pressure sensor (P1), stop the pressurization of the second constant pressure constant speed pump (R2); similarly, when the pressure value of the fourth pressure sensor (P4) is greater than the pressure value of the first pressure sensor (P1), The computer (W) controls the pneumatic valve (K12) to open, and the gas is discharged from the second exhaust pipe (U2) until the pressure value of the fourth pressure sensor (P4) is equal to the pressure value of the first pressure sensor (P1), and the pneumatic valve is closed. Valve (K12); when the pressure value of the fourth pressure sensor (P4) was less than the pressure value of the first pressure sensor (P1), the computer (W) controlled the third constant pressure constant speed pump (R3) to the second gas piston container (L2) Pressurize until the pressure value of the fourth pressure sensor (P4) is equal to the pressure value of the first pressure sensor (P1), stop the third constant pressure constant speed pump (R3) to pressurize until the liquid is injected; (2)注入气体时,计算机(W)控制气动阀(K3,K6,K10)开启,计算机(W)控制第二恒压恒速泵(R2)以模拟驱油实验设计的速度注入气体,当满足模拟驱油实验设计的注入时间后,计算机(W)控制气动阀(K6,K10)关闭并停止第二恒压恒速泵(R2);计算机(W)记录气体注入时的第一压力传感器(P1)的值、气体注入速度和时间,通过第一质量流量计(H1)测量的气体注入速度校正通过第二恒压恒速泵(R2)记录的注入速度;(2) When injecting gas, the computer (W) controls the opening of the pneumatic valves (K3, K6, K10), and the computer (W) controls the second constant pressure and constant speed pump (R2) to inject gas at the speed designed for the simulated oil displacement experiment. After satisfying the injection time designed for the simulated oil displacement experiment, the computer (W) controls the pneumatic valves (K6, K10) to close and stops the second constant pressure and constant speed pump (R2); the computer (W) records the first pressure sensor when the gas is injected The value of (P1), gas injection rate and time, the gas injection rate measured by the first mass flow meter (H1) corrects the injection rate recorded by the second constant pressure constant speed pump (R2); 在注入气体过程中,计算机(W)比较第四压力传感器(P4)的压力值与第一压力传感器(P1)的压力值的大小,当第四压力传感器(P4)的压力值大于第一压力传感器(P1)的压力值,计算机(W)控制气动阀(K12)开启,气体从第二排空管(U2)排出,直到第四压力传感器(P4)的压力值等于第一压力传感器(P1)的压力值为止,关闭气动阀(K12);当第四压力传感器(P4)的压力值小于第一压力传感器(P1)的压力值,计算机(W)控制第三恒压恒速泵(R3)对第二气体活塞容器(L2)加压,直到第四压力传感器(P4)的压力值等于第一压力传感器(P1)的压力值为止,停止第三恒压恒速泵(R3)加压,直到气体注入完毕,或当第一气体活塞容器(L1)中气体体积用完时,计算机(W)控制气动阀(K9)开启,控制气动阀(K10)关闭并停止第二恒压恒速泵(R2),计算机(W)控制第三恒压恒速泵(R3)以同样的模拟驱油实验设计的速度继续注入气体,当满足模拟驱油实验设计的注入时间后,计算机W控制气动阀(K6,K9)关闭和停止第三恒压恒速泵(R3);During the gas injection process, the computer (W) compares the pressure value of the fourth pressure sensor (P4) with the pressure value of the first pressure sensor (P1), when the pressure value of the fourth pressure sensor (P4) is greater than the first pressure The pressure value of the sensor (P1), the computer (W) controls the pneumatic valve (K12) to open, and the gas is discharged from the second emptying pipe (U2), until the pressure value of the fourth pressure sensor (P4) is equal to the pressure value of the first pressure sensor (P1 ), close the pneumatic valve (K12); when the pressure value of the fourth pressure sensor (P4) is less than the pressure value of the first pressure sensor (P1), the computer (W) controls the third constant pressure constant speed pump (R3 ) Pressurize the second gas piston container (L2) until the pressure value of the fourth pressure sensor (P4) is equal to the pressure value of the first pressure sensor (P1), stop the third constant pressure constant speed pump (R3) pressurization , until the gas injection is completed, or when the gas volume in the first gas piston container (L1) is used up, the computer (W) controls the pneumatic valve (K9) to open, controls the pneumatic valve (K10) to close and stops the second constant pressure constant speed The pump (R2), the computer (W) controls the third constant pressure constant speed pump (R3) to continue injecting gas at the same speed designed for the simulated oil flooding experiment, and when the injection time of the simulated oil flooding experiment design is satisfied, the computer W controls the pneumatic Valves (K6, K9) close and stop the third constant pressure constant speed pump (R3); 在注入气体过程中,计算机(W)同时比较第二压力传感器(P2)的压力值与第一压力传感器(P1)的压力值的大小,当第二压力传感器(P2)的压力值大于第一压力传感器(P1)的压力值时,计算机(W)控制气动阀(K2)开启,排出多余液体到第一液体接收容器(F1)中,直到第二压力传感器(P2)的压力值等于第一压力传感器(P1)的压力值为止,关闭气动阀(K2);当第二压力传感器(P2)的压力值小于第一压力传感器(P1)的压力值,计算机(W)控制第一恒压恒速泵(R1)对液体活塞容器(E)加压,直到第二压力传感器(P2)的压力值等于第一压力传感器(P1)的压力值为止,停止第一恒压恒速泵(R1),直到气体注入完毕。During the gas injection process, the computer (W) compares the pressure value of the second pressure sensor (P2) with the pressure value of the first pressure sensor (P1) at the same time, when the pressure value of the second pressure sensor (P2) is greater than the first When the pressure value of the pressure sensor (P1) is reached, the computer (W) controls the pneumatic valve (K2) to open and discharge excess liquid into the first liquid receiving container (F1) until the pressure value of the second pressure sensor (P2) is equal to the first Close the pneumatic valve (K2) until the pressure value of the pressure sensor (P1); when the pressure value of the second pressure sensor (P2) is lower than the pressure value of the first pressure sensor (P1), the computer (W) controls the first constant pressure constant The speed pump (R1) pressurizes the liquid piston container (E) until the pressure value of the second pressure sensor (P2) is equal to the pressure value of the first pressure sensor (P1), then the first constant pressure constant speed pump (R1) is stopped , until the gas injection is complete.
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