CN106495482A - A kind of ceramic glaze and preparation method thereof - Google Patents
A kind of ceramic glaze and preparation method thereof Download PDFInfo
- Publication number
- CN106495482A CN106495482A CN201610833569.5A CN201610833569A CN106495482A CN 106495482 A CN106495482 A CN 106495482A CN 201610833569 A CN201610833569 A CN 201610833569A CN 106495482 A CN106495482 A CN 106495482A
- Authority
- CN
- China
- Prior art keywords
- parts
- glaze
- ceramic glaze
- preparation
- sio
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/02—Frit compositions, i.e. in a powdered or comminuted form
- C03C8/04—Frit compositions, i.e. in a powdered or comminuted form containing zinc
Abstract
The invention belongs to ceramic glaze technical field, and in particular to a kind of ceramic glaze and preparation method thereof, a kind of ceramic glaze, it are prepared from by the raw material of following parts by weight：SiO280 to 100 parts, Al2O36 to 9 parts, 4 to 8 parts of CaO, CaCO320 to 30 parts, B2O34 to 10 parts, Na2SiO312 to 15 parts, 5 to 8 parts of ZnO, 5 to 8 parts of CuO, 8 to 12 parts of MnO, Na25 to 10 parts of 3 to 8 parts of O, MgO, K24 to 8 parts of O, the applied range of the preparation method of the ceramic glaze disclosed by the invention and it can be readily appreciated that goodish effect is all played in the reduction to production cost and the training to technical staff.
Description
Technical field
The invention belongs to ceramic glaze technical field, and in particular to a kind of ceramic glaze and preparation method thereof.
Background technology
In existing ceramic sintering process, the formula of ceramic glaze generally using Anhydrite, quartz, limestone, Calcium Carbonate,
The powder of the natural mineral matters such as lead makees solvent or the suspension of increase glaze is used, and presses 3% to 70% typically in the formula of glaze
Ratio add, but industry is contrary to the presence of multiple factors unfavorable to long-run development using traditional natural crystal
Long time scientific develops, such as, natural minerals belong to non-renewable resources, long-term a large amount of exploitations, are unfavorable for the development being longer than；With
When, natural minerals distribution throughout the country and quality all levels uneven, the development of extensive style also can be caused to natural environment
Destruction；If the above-mentioned mineral for using directly are used to generally require and are milled to the fineness that can cross 250 to 350 mesh sieve reticular densitys, make
The bigger price of fineness is also higher, and the technique from mining to ball milling for finished product is loaded down with trivial details, and the extensive style ball milling work of manufacturer
Skill also generally requires the Ball-milling Time of 20 to 30 hours, its machine cost and time cost also at a relatively high and waste；Above-mentioned or
The processed rear purity of similar natural minerals is all higher, and for the modulation and exploitation of art ceramic glaze, which lacks more
Wide probability, fires effect to glaze and causes certain limitation etc., also, more famous in traditional ceramicses technique and should
With the wider crystalline glaze of scope be fired into because be after the crystalline material melting in product sintering process in glaze in saturation,
Crystallize is produced using the control to annealing process, so as to separate out the crystallization of various decorative patterns.Zinc oxide, lead, lithium are usually adopted
The mineral such as type oxide add the material proportion in glaze formula or the urgency in sintering procedure using local temperature section by increase
The acute process for heating up or lowering the temperature obtains effect, but these traditional techniques need higher material cost or to firing master worker
Technological level and firing experience have a higher requirement, but be between master and apprentice among the people development since ancient times more due to the art pottery
Teach privately, cause the utilization to material never to obtain too big change, and the country for burning process training and
Education is also at stage for more falling behind, thus preferably can grasp the master worker of these burning process also majority be older and
The few indivedual crowds of quantity, the above are not meet demand for development and actual demand of the society to industry now.
Content of the invention
For the deficiencies in the prior art, the present invention proposes a kind of ceramic glaze and preparation method thereof, solves or alleviate
Problem mentioned above.
The technical scheme is that and be achieved in that：A kind of ceramic glaze, it are by the raw material system of following parts by weight
Standby：SiO280 to 100 parts, Al2O36 to 9 parts, 4 to 8 parts of CaO, CaCO320 to 30 parts, B2O34 to 10 parts,
Na2SiO312 to 15 parts, 5 to 8 parts of ZnO, 5 to 8 parts of CuO, 8 to 12 parts of MnO, Na25 to 10 parts of 3 to 8 parts of O, MgO, K2O
4 to 8 parts.
It is prepared from by the raw material of following parts by weight：SiO290 parts, Al2O38 parts, 6 parts of CaO, CaCO325
Part, B2O38 parts, Na2SiO314 parts, 6 parts of ZnO, 6 parts of CuO, 10 parts of MnO, Na28 parts of 6 parts of O, MgO, K26 parts of O.
Its preparation method is as follows：
1）The each component of above-mentioned weight portion is chosen, mix homogeneously obtains compound；
2）Compound is crossed after 80 mesh sieves, 1 to 1 .5 hours of melting at 900 to 1000 DEG C, then at 1300 to 1500 DEG C,
Melting 2 hours, then water quenching obtain block glaze；
3）By block glaze through wet ball grinding after, remove impurity of sieving obtains glaze slip, and the concentration of glaze slip is 1 .5 to 1.8g/mL, by glaze
Slurry imposes on billet surface, dries after being less than 1% to the moisture in glaze slip, respectively at 1000 to 1100 DEG C and 1200 to 1250 DEG C
Alternately fire 2 times, each firing time is 20 to 30 minutes, after cooling, obtains ceramic glaze.
Described drying is dried at 80 to 160 DEG C.
Described melting is carried out in box siliconits resistance furnace.
Described it is cooled to naturally cool to room temperature with stove.
The present invention has following beneficial effect：The range of application of the preparation method of the ceramic glaze disclosed by the invention
Wide and it can be readily appreciated that goodish effect is all played in the reduction to production cost and the training to technical staff；The pottery of the present invention
In preparation process, fusion process adopts stagewise to glaze, and sintering procedure is alternately fired using high and low temperature, by this shape
The melting of formula and firing ensure that each component is effectively combined, and then obtain the preferable ceramic glaze of the uniformity；The ceramic glaze of the present invention
Material can quickly reach antibacterial effect, rapid-action, and antibiotic property can keep the long period.Prepared by the ceramic glaze of the present invention
Ceramics sample to hold the most long resistance to deteriorating time of milk be also conventional ceramic glaze product far superior on market.
Specific embodiment
A kind of ceramic glaze, it are prepared from by the raw material of following parts by weight：SiO280 to 100 parts, Al2O36
To 9 parts, 4 to 8 parts of CaO, CaCO320 to 30 parts, B2O34 to 10 parts, Na2SiO312 to 15 parts, 5 to 8 parts of ZnO, CuO 5 to
8 parts, 8 to 12 parts of MnO, Na25 to 10 parts of 3 to 8 parts of O, MgO, K24 to 8 parts of O.It is by the raw material system of following parts by weight
Standby：SiO290 parts, Al2O38 parts, 6 parts of CaO, CaCO325 parts, B2O38 parts, Na2SiO314 parts, 6 parts of ZnO, CuO
6 parts, 10 parts of MnO, Na28 parts of 6 parts of O, MgO, K26 parts of O.Its preparation method is as follows：1）The each component of above-mentioned weight portion is chosen,
Mix homogeneously, obtains compound；2）Compound is crossed after 80 mesh sieves, at 900 to 1000 DEG C, 1 to 1 .5 hours of melting, then exist
At 1300 to 1500 DEG C, melting 2 hours, then water quenching obtain block glaze；3）By block glaze through wet ball grinding after, sieve
Remove impurity obtains glaze slip, and the concentration of glaze slip is 1 .5 to 1.8g/mL, glaze slip is imposed on billet surface, is dried to the moisture in glaze slip
After less than 1%, alternately fire 2 times at 1000 to 1100 DEG C and 1200 to 1250 DEG C respectively, each firing time is 20 to 30
Minute, after cooling, obtain ceramic glaze.Described drying is dried at 80 to 160 DEG C.Described melting is in box silicon-carbon
Carry out in rod resistance furnace.Described it is cooled to naturally cool to room temperature with stove.
Embodiment 1：Take SiO280 kg, Al2O34 kg of 6 kg, CaO, CaCO320 kg, B2O34 kg, Na2SiO312
5 kg of 5 kg of kg, ZnO, CuO, 8 kg of MnO, Na23 kg of O, MgO 5 kg, K24 kg of O, their mix homogeneously are obtained mixed
Material is closed, compound is crossed after 80 mesh sieves, 1 to 1 .5 hours of melting at 900 to 1000 DEG C, then at 1300 to 1500 DEG C,
Melting 2 hours, then water quenching obtain block glaze；By block glaze through wet ball grinding after, remove impurity of sieving obtains glaze slip, glaze slip
Concentration be 1 .5 to 1.8g/mL, glaze slip is imposed on billet surface, dry to the moisture in glaze slip less than 1% after, exist respectively
Alternately fire 2 times at 1000 to 1100 DEG C and 1200 to 1250 DEG C, each firing time is 20 to 30 minutes, after cooling, obtains
Ceramic glaze.Described drying is dried at 80 to 160 DEG C.Described melting is carried out in box siliconits resistance furnace
's.Described it is cooled to naturally cool to room temperature with stove.
Embodiment 2：Take SiO2100 kg, Al2O38 kg of 9 kg, CaO, CaCO330 kg, B2O310 kg, Na2SiO3
8 kg of 8 kg of 15 kg, ZnO, CuO, 12 kg of MnO, Na28 kg of O, MgO 10 kg, K28 kg of O, by their mix homogeneously,
Compound is obtained, compound is crossed after 80 mesh sieves, 1 to 1 .5 hours of melting at 900 to 1000 DEG C, then at 1300 to 1500 DEG C
Under, melting 2 hours, then water quenching obtain block glaze；By block glaze through wet ball grinding after, remove impurity of sieving obtains glaze slip, glaze
The concentration of slurry is 1 .5 to 1.8g/mL, and glaze slip is imposed on billet surface, dries after being less than 1% to the moisture in glaze slip, exists respectively
Alternately fire 2 times at 1000 to 1100 DEG C and 1200 to 1250 DEG C, each firing time is 20 to 30 minutes, after cooling, obtains
Ceramic glaze.Described drying is dried at 80 to 160 DEG C.Described melting is carried out in box siliconits resistance furnace
's.Described it is cooled to naturally cool to room temperature with stove.
Embodiment 3：Take SiO290 kg, Al2O36 kg of 8 kg, CaO, CaCO325 kg, B2O38 kg, Na2SiO314
6 kg of 6 kg of kg, ZnO, CuO, 10 kg of MnO, Na26 kg of O, MgO 8 kg, K26 kg of O, their mix homogeneously are obtained mixed
Material is closed, compound is crossed after 80 mesh sieves, 1 to 1 .5 hours of melting at 900 to 1000 DEG C, then at 1300 to 1500 DEG C,
Melting 2 hours, then water quenching obtain block glaze；By block glaze through wet ball grinding after, remove impurity of sieving obtains glaze slip, glaze slip
Concentration be 1 .5 to 1.8g/mL, glaze slip is imposed on billet surface, dry to the moisture in glaze slip less than 1% after, exist respectively
Alternately fire 2 times at 1000 to 1100 DEG C and 1200 to 1250 DEG C, each firing time is 20 to 30 minutes, after cooling, obtains
Ceramic glaze.Described drying is dried at 80 to 160 DEG C.Described melting is carried out in box siliconits resistance furnace
's.Described it is cooled to naturally cool to room temperature with stove.
Claims (6)
1. a kind of ceramic glaze, it is characterised in that it is prepared from by the raw material of following parts by weight：SiO280 to 100
Part, Al2O36 to 9 parts, 4 to 8 parts of CaO, CaCO320 to 30 parts, B2O34 to 10 parts, Na2SiO312 to 15 parts, ZnO 5 to 8
Part, 5 to 8 parts of CuO, 8 to 12 parts of MnO, Na25 to 10 parts of 3 to 8 parts of O, MgO, K24 to 8 parts of O.
2. ceramic glaze according to claim 1, it is characterised in that it is prepared from by the raw material of following parts by weight
's：SiO290 parts, Al2O38 parts, 6 parts of CaO, CaCO325 parts, B2O38 parts, Na2SiO314 parts, 6 parts of ZnO, 6 parts of CuO,
10 parts of MnO, Na28 parts of 6 parts of O, MgO, K26 parts of O.
3. a kind of preparation method of ceramic glaze as claimed in claim 1 or 2, it is characterised in that its preparation method is as follows：
1）The each component of above-mentioned weight portion is chosen, mix homogeneously obtains compound；
2）Compound is crossed after 80 mesh sieves, 1 to 1 .5 hours of melting at 900 to 1000 DEG C, then at 1300 to 1500 DEG C,
Melting 2 hours, then water quenching obtain block glaze；
3）By block glaze through wet ball grinding after, remove impurity of sieving obtains glaze slip, and the concentration of glaze slip is 1 .5 to 1.8g/mL, by glaze
Slurry imposes on billet surface, dries after being less than 1% to the moisture in glaze slip, respectively at 1000 to 1100 DEG C and 1200 to 1250 DEG C
Alternately fire 2 times, each firing time is 20 to 30 minutes, after cooling, obtains ceramic glaze.
4. the preparation method of ceramic glaze according to claim 3, it is characterised in that described drying is 80 to 160
Dry at DEG C.
5. the preparation method of ceramic glaze according to claim 3, it is characterised in that described melting is in box silicon-carbon
Carry out in rod resistance furnace.
6. the preparation method of ceramic glaze according to claim 3, it is characterised in that described being cooled to is naturally cold with stove
But to room temperature.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610833569.5A CN106495482A (en) | 2016-09-20 | 2016-09-20 | A kind of ceramic glaze and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610833569.5A CN106495482A (en) | 2016-09-20 | 2016-09-20 | A kind of ceramic glaze and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106495482A true CN106495482A (en) | 2017-03-15 |
Family
ID=58290846
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610833569.5A Pending CN106495482A (en) | 2016-09-20 | 2016-09-20 | A kind of ceramic glaze and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106495482A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107628751A (en) * | 2017-09-30 | 2018-01-26 | 浙江工业大学之江学院 | A kind of apple green crystalline glaze material and the method for firing apple green crystalline glaze |
| CN108218233A (en) * | 2018-02-07 | 2018-06-29 | 盐城工业职业技术学院 | Semi-conducting glaze for higfh-tension ceramics and preparation method thereof |
| CN110217991A (en) * | 2019-07-02 | 2019-09-10 | 山东华浩陶瓷有限公司 | A kind of high strength china glaze and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101786795A (en) * | 2009-12-31 | 2010-07-28 | 深圳市永丰源实业有限公司 | Enamel glaze and preparation process thereof |
-
2016
- 2016-09-20 CN CN201610833569.5A patent/CN106495482A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101786795A (en) * | 2009-12-31 | 2010-07-28 | 深圳市永丰源实业有限公司 | Enamel glaze and preparation process thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107628751A (en) * | 2017-09-30 | 2018-01-26 | 浙江工业大学之江学院 | A kind of apple green crystalline glaze material and the method for firing apple green crystalline glaze |
| CN108218233A (en) * | 2018-02-07 | 2018-06-29 | 盐城工业职业技术学院 | Semi-conducting glaze for higfh-tension ceramics and preparation method thereof |
| CN110217991A (en) * | 2019-07-02 | 2019-09-10 | 山东华浩陶瓷有限公司 | A kind of high strength china glaze and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US5091345A (en) | Glass composition | |
| CN105693202B (en) | A kind of Gao Baigao high-intensitive medium temperature hard fine porcelain and preparation method thereof thoroughly | |
| CN105315015B (en) | A kind of preparation method of building decoration transmutation art pottery ceramic tile | |
| CN102249738B (en) | Furnace transmutation glaze dolomitic pottery and preparation technique thereof | |
| CN111943724A (en) | Method for manufacturing matt transparent glazed ceramic chip | |
| CN102923958A (en) | Novel microcrystal glass ceramic composite board and preparation method thereof | |
| CN106495482A (en) | A kind of ceramic glaze and preparation method thereof | |
| CN110510876A (en) | A kind of matting glaze and preparation method thereof | |
| CN101767985A (en) | Shadowy blue ware and preparation method thereof | |
| CN103342467B (en) | Novel nucleated glass ceramic clad plate and preparation method thereof | |
| CN106430974B (en) | A kind of ox blood color copper red ceramic glaze and preparation method thereof | |
| CN108147665A (en) | Microcrystal grain glaze and preparation method thereof | |
| CN105294091B (en) | A kind of same kiln fires the production method of dual gauge Antique Imitation Tiles | |
| CN107244807B (en) | Leaf green spot glaze and preparation method thereof | |
| CN106477884A (en) | A kind of rust red glaze and preparation method thereof | |
| CN103332965A (en) | Golden yellow crystallized dry-granular glaze and using method thereof | |
| CN105461284B (en) | A kind of Antique Imitation Tiles | |
| CN102010232A (en) | Building ceramic aventurine glaze and preparation method thereof | |
| US3846098A (en) | Manufacture of a white porcelain body of high translucency and high strength | |
| CN103304277B (en) | Microcrystal glass ceramic composite plate and one-time rapid sintering method thereof | |
| CN107601897A (en) | The preparation method of the ceramic light yellow glaze of high temperature light | |
| CN107619191B (en) | Green-bottom silver flake grain high-temperature crystalline glaze and preparation method thereof | |
| CN105330147A (en) | Preparation method of zinc silicate crystal glaze for bone china | |
| CN104418336B (en) | Synthetic wollastonite, protein porcelain containing the same and manufacturing method thereof | |
| CN103539486B (en) | Ceramic flower leopard print glaze composite mineralizing agent and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170315 |