CN106422923A - Solution preparation system and solution preparation method - Google Patents
Solution preparation system and solution preparation method Download PDFInfo
- Publication number
- CN106422923A CN106422923A CN201610421474.2A CN201610421474A CN106422923A CN 106422923 A CN106422923 A CN 106422923A CN 201610421474 A CN201610421474 A CN 201610421474A CN 106422923 A CN106422923 A CN 106422923A
- Authority
- CN
- China
- Prior art keywords
- solution
- compounding system
- reagent
- container
- solution compounding
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 239000003153 chemical reaction reagent Substances 0.000 claims abstract description 41
- 239000007787 solid Substances 0.000 claims abstract description 25
- 238000000034 method Methods 0.000 claims abstract description 12
- 239000007788 liquid Substances 0.000 claims abstract description 8
- 239000000126 substance Substances 0.000 claims description 13
- 150000001875 compounds Chemical class 0.000 claims description 6
- 238000007599 discharging Methods 0.000 claims description 3
- 239000007921 spray Substances 0.000 claims description 3
- 239000006185 dispersion Substances 0.000 claims description 2
- 238000007792 addition Methods 0.000 abstract description 3
- 230000001276 controlling effect Effects 0.000 abstract description 2
- 239000000243 solution Substances 0.000 description 39
- 239000003814 drug Substances 0.000 description 10
- 238000002156 mixing Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 238000010790 dilution Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000006166 lysate Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 229950000845 Politef Drugs 0.000 description 1
- 229940058401 Polytetrafluoroethylene Drugs 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000000875 corresponding Effects 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 239000003640 drug residue Substances 0.000 description 1
- 239000003480 eluent Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials 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- B01F31/00—Mixers with shaking, oscillating, or vibrating mechanisms
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F21/00—Dissolving
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- B—PERFORMING OPERATIONS; TRANSPORTING
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-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F31/00—Mixers with shaking, oscillating, or vibrating mechanisms
- B01F31/80—Mixing by means of high-frequency vibrations above one kHz, e.g. ultrasonic vibrations
- B01F31/89—Methodical aspects; Controlling
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C1/00—Crushing or disintegrating by reciprocating members
- B02C1/14—Stamping mills
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F2101/00—Mixing characterised by the nature of the mixed materials or by the application field
- B01F2101/23—Mixing of laboratory samples e.g. in preparation of analysing or testing properties of materials
Abstract
The invention discloses a solution preparation system and a solution preparation method. The system comprises: a container used as a solution preparation vessel and used for containing a prepared solution; a liquid adding device used for adding a reagent to the container and accurately controlling the addition amount of the reagent through a metering pump; and a control unit used for realizing automatic operation of the solution preparation system. The solution preparation system also comprises a tray and a solid crushing device matching with the tray, wherein the tray is used for containing a solid reagent; and the solid crushing device is used for crushing the solid reagent in the tray. The solution preparation system uses an automatic device to substitute a manual reagent preparation process, uses the metering pump to weigh reagents in the whole process and uses an infrared device to accurate quantify, so errors brought by various measuring vessels are prevented, and harms to environment and experiment personnel in the solution preparation process are also prevented.
Description
Technical field
The present invention relates to experimental apparatus technical field, relate more specifically to a kind of solution compounding system and compound method.
Background technology
The preparation of conventional reagent is the work that laboratory is frequently necessary to.When prepared by conventional soln, laboratory operation personnel
Substantial amounts of reagent, such as deionized water, acid, alkali or other reagent etc. need to be manually adding to, and to medicament stirring, dissolving, finally fixed
Hold.In operation, due to the impact of the weighing utensil of human users and use, it is readily incorporated personal error or system is missed
Difference, causes experimental result to deviate its actual concentration.
Currently for the automatic preparing device of sample, there is a kind of sample preparation platform, but it is relatively simple for structure, realize
Single function, is simply possible to use in the dilution of actual sample or standard sample, prepares a lot of steps during solution and still needs manual going
Complete, thus still in the face of above-mentioned technical problem.
Content of the invention
In view of this, present invention is primarily targeted at providing a kind of solution compounding system and compound method, to solve
At least one of above-mentioned technical problem.
To achieve these goals, as one aspect of the present invention, the invention provides a kind of solution compounding system, bag
Include：
Container, for as preparing the vessel of solution and hold the solution finally preparing；
Liquid-adding device, for adding reagent in described container, this liquid-adding device passes through dosing pump precise control reagent
Addition；
Control unit, is used for making this solution compounding system realize automation mechanized operation.
Preferably, described solution compounding system also includes pallet and the solid reducing mechanism supporting with described pallet；Its
In, described pallet is used for holding solid chemicals；Described solid reducing mechanism is used for the described solid chemicals that described pallet is held
Pulverized.
As another aspect of the present invention, present invention also offers a kind of solution compound method, wherein adopt as above institute
The preparation to carry out solution for the solution compounding system stated.
Understand, the solution compounding system of the present invention has the advantages that based on technique scheme：Using automatization
Equipment replaces the process of manual reagent preparation, and whole using dosage pump accurately measures reagent, the accurate constant volume of infrared facility, it is to avoid by
Measure the error that vessel bring in multiple, and it can be avoided that the harm to environment and experimenter in preparing solution processes.
Brief description
Fig. 1 is that the solution compounding system of the present invention carries out structural representation during sample comminution；
Fig. 2 is that the solution compounding system of the present invention carries out structural representation when a kind of reagent adds；
Fig. 3 is that the solution compounding system of the present invention carries out structural representation when plurality of reagents interpolation and sonic oscillation；
Fig. 4 is that the solution compounding system of the present invention carries out carrying out the structural representation of constant volume when a kind of reagent adds；
Fig. 5 is the overlooking the structure diagram of inside each device layout of the solution compounding system of the present invention.
Specific embodiment
For making the object, technical solutions and advantages of the present invention become more apparent, below in conjunction with specific embodiment, and reference
Accompanying drawing, the present invention is described in further detail.
The invention discloses a kind of solution compounding system, it is by liquid (not needing pulverization process step) or solid chemicals
(powder or lamellar need to grind to form to be easier to dissolved fine grained) is with, after reagent automatic dilution, ultrasonic dissolution disperses, then uses
Diluent is settled to required volume, is configured to the self-reacting device of certain density solution.
More specifically, the solution compounding system of the present invention, including：
Container, for as preparing solution hold the solution finally preparing；This container is, for example, quartzy constant volume cup；
Liquid-adding device, for adding the reagent for example as solvent in described container, this liquid-adding device passes through dosing pump
The addition of precise control reagent；
Control unit, is used for making this solution compounding system realize automation mechanized operation.
Preferably, this solution compounding system also includes pallet and the solid reducing mechanism supporting with described pallet；Wherein,
Described pallet is used for holding solid chemicals；Described solid reducing mechanism is used for the described solid chemicals that described pallet holds are carried out
Pulverize.
Preferably, this pallet can downwardly turn over, it is preferably able to 360 ° of rotations such that it is able to by the solid wherein holding
Medicament is poured in container.
Preferably, this liquid-adding device includes one or more spray discharging openings, for reagent is sprayed this pallet,
Thus by the solid chemicals shower on pallet in this container.
Preferably, this solution compounding system also includes Vltrasonic device, for supersound process is carried out to this container, make this appearance
Liquid dispersion in device uniformly, or makes solid chemicals fully dissolve in reagent.This Vltrasonic device is, for example, ultrasonic vibration set.
Preferably, this liquid-adding device includes multigroup reagent bottle holding reagent and matched dosing pump, Neng Goujing
Really control the interpolation of many group reagents.
Preferably, this solution compounding system also includes the volume fixing device in this container, volume fixing device is for example, red
Outer volume fixing device, liquid level detection device etc..
The invention also discloses a kind of solution compound method, wherein to be carried out molten using solution compounding system as above
The preparation of liquid.
Below so that the solution of solid chemicals is prepared as a example, to further illustrate Advantageous Effects and the advantage of the present invention.
The alternative traditional-handwork of the present invention configures reagent process, is run by software whole-course automation, solid medicine is pressed
The concentration needing is configured to solution.Instrument running is as follows：
1. load weighted medicine is transferred to conventional reagent to prepare in platform, and fixes corresponding position.Use polytetrafluoro
Ethylene dismembyator is ground to medicine, and the distance (grinding degree) between milling time and dismembyator and pallet can be by software
It is controlled.
2. fixed arm is rotatable arm, can rotate the pallet claiming to have medicine with 360 degree.Reagent spout is 360 degree
Swivel nozzle, and reagent flows into the optional different in flow rate of mode and different drip washing mode (as direct injection drip washing or pulsed are drenched
Wash mode) it is ensured that medicine can all dissolve and be transferred in lower reservoir, container is according to medicament configuration needs, optional glass
Or the container of quartz.
3. the lysate having been added to a certain amount of reagent is transferred to other reagent unit of interpolation, and adds one as needed
Other quantitative reagent.All reagent are added and after finishing, carries out supersound process, ultrasonic time and supersonic frequency can have software to enter
Row controls, and from 0～999min, supersonic frequency, from 40～100Hz, makes the medicine in lysate be completely dissolved to solution to ultrasonic time
In.
4. the reagent cup being completely dissolved medicine is transferred to mixing constant volume module.First eluent solution wall of cup, makes residual
The drug residue solution stayed on solution wall of cup merges.It is being suitably added reagent, the body required for being settled to by infrared equipment
Long-pending, infrared ray constant volume equipment can be by software set, and automatic lifting simultaneously selects constant volume, constant volume body according to the parameter request of input
Amass and may be selected from 100～1000ml.Solution is being mixed by evenly mixing device level (or stirring), is being finally completed process for preparation.
5. mix, in Vltrasonic device, mix and wherein can achieve that horizontal oscillations mix function, frequency of oscillation 30-100rpm, shake
Swing precision ± 1rpm, shock range Φ 8cm.Timing range 0～999min, temperature controlling range room temperature～60 DEG C, temperature-controlled precision
±1℃.
Preferably, the type selecting parameter of some equipment is as follows in the solution compounding system of the present invention：
1. dosing pump：Set pressure as 20bar, maximum flow is 4 ls/h per hour, peak frequency 160 stroke/point
Clock, it is 5ml that single goes out liquid minimum volume.
2. dismembyator edge and tray edge diameter of phi=4cm, radian is 2 radians (1 radian is equal to 57.3 °), rotatable
Fixed mount horizontal length is 1cm, and vertical length is 2cm.Pallet and fixed mount material can be all politef material, pallet
It is card slot type interface with fixed mount interface.
3. the inside and outside stainless steel all being processed using deactivation of dosing pump pump line.
4. diameter of phi=the 30cm of the mixing of Fig. 5, volume fixing device, shell is for the making of ABS engineering plastics, the full minute surface of cavity not
Rust steel assembly.
Particular embodiments described above, has carried out detailed further to the purpose of the present invention, technical scheme and beneficial effect
Describing in detail bright it should be understood that the foregoing is only the specific embodiment of the present invention, being not limited to the present invention, all
Within the spirit and principles in the present invention, any modification, equivalent substitution and improvement done etc., should be included in the protection of the present invention
Within the scope of.
Claims (10)
1. a kind of solution compounding system is it is characterised in that include：
Container, for as preparing the vessel of solution and hold the solution finally preparing；
Liquid-adding device, for adding reagent in described container, this liquid-adding device passes through the interpolation of dosing pump precise control reagent
Amount；
Control unit, is used for making this solution compounding system realize automation mechanized operation.
2. solution compounding system as claimed in claim 1 it is characterised in that described solution compounding system also include pallet and with
The supporting solid reducing mechanism of described pallet；Wherein, described pallet is used for holding solid chemicals；Described solid reducing mechanism is used for
The described solid chemicals that described pallet holds are pulverized.
3. solution compounding system as claimed in claim 2, it is characterised in that described pallet can downwardly turn over, is preferably able to
360 ° of rotations are such that it is able to pour the solid chemicals wherein holding in described container into.
4. solution compounding system as claimed in claim 2 is it is characterised in that described liquid-adding device includes one or more sprays
Discharging opening, for described reagent is sprayed described pallet, thus by the described solid chemicals shower holding on described pallet
To in described container；Wherein, described spray discharging opening is preferably 360 degree of swivel nozzles.
5. solution compounding system as claimed in claim 2 is it is characterised in that described solution compounding system also includes ultrasonic dress
Put, for supersound process is carried out to described container, make the liquid dispersion in described container uniform, or so that described solid chemicals is existed
Fully dissolve in described reagent.
6. solution compounding system as claimed in claim 5 is it is characterised in that described Vltrasonic device is ultrasonic vibration set.
7. solution compounding system as claimed in claim 1 is it is characterised in that described liquid-adding device includes multigroup reagent that holds
Reagent bottle and matched dosing pump, can accurately control the interpolation of many group reagents.
8. solution compounding system as claimed in claim 1 is it is characterised in that described solution compounding system is also included positioned at described
Volume fixing device in container.
9. solution compounding system as claimed in claim 8 is it is characterised in that described volume fixing device is infrared volume fixing device or liquid
Level detecting apparatus.
10. a kind of solution compound method is it is characterised in that prepare system using the solution as described in claim 1 to 9 any one
Unite and to carry out the preparation of solution.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610421474.2A CN106422923A (en) | 2016-06-14 | 2016-06-14 | Solution preparation system and solution preparation method |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610421474.2A CN106422923A (en) | 2016-06-14 | 2016-06-14 | Solution preparation system and solution preparation method |
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