CN106373902A - Detection method and detection mesh plate for detecting reliability of silver paste for solar cell - Google Patents

Detection method and detection mesh plate for detecting reliability of silver paste for solar cell Download PDF

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Publication number
CN106373902A
CN106373902A CN201510427174.0A CN201510427174A CN106373902A CN 106373902 A CN106373902 A CN 106373902A CN 201510427174 A CN201510427174 A CN 201510427174A CN 106373902 A CN106373902 A CN 106373902A
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CN
China
Prior art keywords
detection
silver paste
pierced pattern
web plate
reliability
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201510427174.0A
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Chinese (zh)
Inventor
潘熠霄
戚頔
刘玉杰
张愿成
吴新正
陆文婷
朱旭
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanghai Solar Energy Research Center Co Ltd
Original Assignee
Shanghai Solar Energy Research Center Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shanghai Solar Energy Research Center Co Ltd filed Critical Shanghai Solar Energy Research Center Co Ltd
Priority to CN201510427174.0A priority Critical patent/CN106373902A/en
Publication of CN106373902A publication Critical patent/CN106373902A/en
Pending legal-status Critical Current

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Classifications

    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L22/00Testing or measuring during manufacture or treatment; Reliability measurements, i.e. testing of parts without further processing to modify the parts as such; Structural arrangements therefor
    • H01L22/10Measuring as part of the manufacturing process
    • H01L22/14Measuring as part of the manufacturing process for electrical parameters, e.g. resistance, deep-levels, CV, diffusions by electrical means
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L22/00Testing or measuring during manufacture or treatment; Reliability measurements, i.e. testing of parts without further processing to modify the parts as such; Structural arrangements therefor
    • H01L22/10Measuring as part of the manufacturing process
    • H01L22/12Measuring as part of the manufacturing process for structural parameters, e.g. thickness, line width, refractive index, temperature, warp, bond strength, defects, optical inspection, electrical measurement of structural dimensions, metallurgic measurement of diffusions

Abstract

The invention provides a detection method and detection mesh plate for detecting reliability of a silver paste for a solar cell. The detection mesh plate includes a mesh plate base body; a first hollow-out pattern for relative resistivity detection, a second hollow-out pattern for tension detection, and a third hollow-out pattern for aluminum peeling detection at a junction part of a silver paste and an aluminium paste are arranged on the mesh plate base body. In addition, the detection mesh plate is used for realizing the detection method, thereby realizing silver paste reliability detection including relative resistivity detection of the silver paste, tension detection, and aluminum peeling detection at the junction part of the silver paste and the aluminium paste. Moreover, the operation means is simple; the testing cost is low; only the single type of testing mesh plate is provided; the reflected data are diversified; and the evaluation accuracy is high.

Description

The detection method of silver paste reliability used for solar batteries and detection web plate
Technical field
The present invention relates to photovoltaic technology, the detection method of more particularly, to a kind of silver paste reliability used for solar batteries And detection web plate.
Background technology
In photovoltaic industry, the unfailing performance of silver paste used for solar batteries is closely related with product.But it is reliable The evaluation and test high cost of performance, the reflection cycle of data is long, and the speed detecting with research and development of new product or shipment is seriously not Symbol, the experiment of some new products just can must be carried out after failtests data feedback before, serious shadow Ring the exploitation of experiment and the detection of OQC.
The method of reliability testing at present mainly has:
A, buy more a whole set of manufacture of solar cells equipment and carry out reliability assessment, this kind of method shortcoming is whole Complete equipment is with high costs, and utilization rate of equipment and installations is low, and high cost evaluated and tested by slurry, and advantage is failtests number Fast according to feedback, experiment progress is fast, meets OQC requirement.
B and solar battery sheet manufacturer cooperate to be fabricated to cell piece and carry out reliability assessment, Ci Zhongfang Method shortcoming is that experiment number is limited, and experimental amount is few, and experimental period is longer, and high cost evaluated and tested by slurry, excellent Point is to save the input cost of a whole set of manufacture of solar cells equipment.
C, it is fabricated to assembly and carries out reliability evaluating together with assembly, the shortcoming of this kind of method is experiment time Number is limited, and experimental cost is high, is easily affected final testing result by the data of other materials.Advantage is Save the input cost of a whole set of manufacture of solar cells equipment.
D, self-built method of testing, design test experiments, this kind of method the disadvantage is that, experimental procedure is loaded down with trivial details, In experimentation, slurry loss is larger, and advantage is, flexibly, data reflection speed is fast, and test just has for test To property, meet OQC requirement.
Content of the invention
The purpose of the present invention it is simply that in order to provide a kind of detection method of silver paste reliability used for solar batteries and Detection web plate.
In order to achieve the above object, present invention employs technical scheme below: a kind of silver paste used for solar batteries The detection method of reliability, including following measures:
First, one detection web plate of self-control, is provided with the first hollow out figure for carrying out relative resistivities detection Case, for carrying out the second pierced pattern of pull force calculation, and is used for carrying out silver-colored aluminium paste intersection and falls aluminum detection The 3rd pierced pattern;
2nd, solar battery front side silver paste is coated on homemade detection web plate;
3rd, with printer, solar battery front side silver paste is printed on 1/4 monocrystalline silicon piece, obtains and correspond to Silver paste printed patterns in each pierced pattern;
4th, the monocrystalline silicon piece after printing silver paste is sintered;
5th, with resistance meter to the printing figure corresponding to the first pierced pattern on the monocrystalline silicon piece after sintering The line resistance of case is tested, and obtains relative resistance rate score;
6th, use welding welding corresponding to the printed patterns of the second pierced pattern, and use puller system testing size Welding pulling force;
7th, by after silver paste is cleaned out on web plate, add aluminium paste in the 3rd pierced pattern part of detection web plate; Republish on 1/4 monocrystalline silicon piece, sinter after making aluminium paste and the silver paste boundary of corresponding position, then using glue Whether the silver-colored aluminium paste intersection of cloth test falls aluminum.
Described printer is Semi-automatic printer.
Described sintering furnace is high temperature sintering furnace.
Described resistance meter is micro- ω meter.
Described adhesive tape is normal transparent adhesive tape.
A kind of detection web plate for silver paste reliability used for solar batteries detection, including web plate matrix, in net Plate matrix is provided with the first pierced pattern for carrying out relative resistivities detection, for carrying out pull force calculation Second pierced pattern, and the 3rd pierced pattern of aluminum detection, each hollow out is fallen for carrying out silver-colored aluminium paste intersection It is provided with interval between pattern.
Described first pierced pattern includes two groups of symmetrically arranged multistage broken line shape grooves, between adjacent segment groove Turn back in 90 degree.
Described second pierced pattern includes four straight trough ditches, four straight trough ditch Parallel Symmetric settings two-by-two.
Described 3rd pierced pattern includes two articles of straight trough ditches, and two straight trough ditch interval settings are point-blank.
The width of the groove of the 3rd pierced pattern is more than the width of the groove of the second pierced pattern, the second hollow out figure The width of the groove of case is more than the width of the groove of the first pierced pattern.
The detection method of present invention silver paste used for solar batteries reliability and detection web plate are above due to employing Technical scheme so as to compared with prior art, has the following advantages that and feature:
1st, slurry sample preparation amount is the 10% of other means of testing.
2nd, test equipment input cost is little.
3rd, it is applied to a large amount of sample experiments.
4th, experimental data feedback cycle is short, and experimental data reference value is high.
5th, 3 big reliability detection projects are comprised.
Change web plate number of times when the 6th, testing few, save replacing construction, reduce the loss of slurry when changing web plate.
7th, cost of labor is little, and 1~2 people can a complete set of experiment.
Brief description
Fig. 1 is the structural representation of the detection web plate in the present invention.
Specific embodiment
Referring to Fig. 1, the detection web plate for silver paste reliability used for solar batteries detection in the present invention, bag Purse rope plate matrix 1, is provided with the first pierced pattern 11 for carrying out relative resistivities detection on web plate matrix, For carrying out the second pierced pattern 12 of pull force calculation, and fall aluminum detection for carrying out silver-colored aluminium paste intersection 3rd pierced pattern 13, is provided with interval between each pierced pattern.Wherein, the first pierced pattern includes two groups pairs Claim the multistage broken line shape groove of setting, turn back in 90 degree between adjacent segment groove.Second pierced pattern includes Article four, straight trough ditch, four straight trough ditch Parallel Symmetric settings two-by-two.3rd pierced pattern includes two articles of straight trough ditches, Article two, straight trough ditch interval setting is point-blank.And the width of the groove of the 3rd pierced pattern is more than second The width of the groove of pierced pattern, the width of the groove of the second pierced pattern is more than the groove of the first pierced pattern Width.
Using the detection web plate of the present invention, pull force calculation, relative resistivities detection and silver-colored aluminium paste can be carried out Intersection falls aluminum detection.Need in inspection to use Semi-automatic printer, 1/4 monocrystalline silicon piece, high temperature sintering furnace, Resistance meter, microscope, welding, measurer for pulling force, adhesive tape, computer.
Concrete grammar is as follows: solar battery front side silver paste is coated on homemade detection web plate;With print Solar battery front side silver paste is printed on 1/4 monocrystalline silicon piece brush machine, obtains corresponding to each pierced pattern Silver paste printed patterns;Then the monocrystalline silicon piece after printing silver paste is sintered;With resistance meter to burning The line resistance of the printed patterns corresponding to the first pierced pattern on the monocrystalline silicon piece after knot is tested, and obtains Relative resistance rate score;Weld the printed patterns corresponding to the second pierced pattern using welding, and use puller system The welding pulling force of testing size;After on web plate, silver paste is cleaned out, in the 3rd pierced pattern of detection web plate Part adds aluminium paste;Republish on 1/4 monocrystalline silicon piece, burn after making aluminium paste and the silver paste boundary of corresponding position Using adhesive plaster, knot, then tests whether silver-colored aluminium paste intersection falls aluminum.
Pattern as the detection web plate design in the present invention is different, and the content of test is also different, the method for test Also different.
Method of testing in the present invention is applied to any like product test.
Used in the present invention, printer minimum requirements is Semi-automatic printer.
Silicon chip used in the present invention is monocrystalline silicon piece.
Sintering furnace used in the present invention is high temperature sintering furnace.
Resistance meter used in the present invention is microhmmeter.
Puller system used in the present invention is automatic measurer for pulling force.
In the present invention, silver-colored aluminium paste intersection falls aluminum experiment and needs first to add aluminium paste after silver paste cleans out on web plate Republish once so as to sinter after having a common boundary with silver paste, and piece need to sinter after printing aluminium paste and test.

Claims (10)

1. a kind of detection method of silver paste reliability used for solar batteries is it is characterised in that include following arranging Apply:
First, one detection web plate of self-control, is provided with the first hollow out figure for carrying out relative resistivities detection Case, for carrying out the second pierced pattern of pull force calculation, and is used for carrying out silver-colored aluminium paste intersection and falls aluminum detection The 3rd pierced pattern;
2nd, solar battery front side silver paste is coated on homemade detection web plate;
3rd, with printer, solar battery front side silver paste is printed on 1/4 monocrystalline silicon piece, obtains and correspond to Silver paste printed patterns in each pierced pattern;
4th, the monocrystalline silicon piece after printing silver paste is sintered;
5th, with resistance meter to the printing figure corresponding to the first pierced pattern on the monocrystalline silicon piece after sintering The line resistance of case is tested, and obtains relative resistance rate score;
6th, use welding welding corresponding to the printed patterns of the second pierced pattern, and use puller system testing size Welding pulling force;
7th, by after silver paste is cleaned out on web plate, add aluminium paste in the 3rd pierced pattern part of detection web plate; Republish on 1/4 monocrystalline silicon piece, sinter after making aluminium paste and the silver paste boundary of corresponding position, then using glue Whether the silver-colored aluminium paste intersection of cloth test falls aluminum.
2. the detection method of silver paste reliability used for solar batteries as claimed in claim 1, its feature exists In: described printer is Semi-automatic printer.
3. the detection method of silver paste reliability used for solar batteries as claimed in claim 1, its feature exists In: described sintering furnace is high temperature sintering furnace.
4. the detection method of silver paste reliability used for solar batteries as claimed in claim 1, its feature exists In: described resistance meter is micro- ω meter.
5. the detection method of silver paste reliability used for solar batteries as claimed in claim 1, its feature exists In: described adhesive tape is normal transparent adhesive tape.
6. a kind of detection web plate for silver paste reliability used for solar batteries detection is it is characterised in that wrap Purse rope plate matrix, is provided with the first pierced pattern for carrying out relative resistivities detection on web plate matrix, uses In the second pierced pattern carrying out pull force calculation, and it is used for carrying out the 3rd that silver-colored aluminium paste intersection falls aluminum detection Pierced pattern, is provided with interval between each pierced pattern.
7. it is used for the detection web plate of silver paste reliability detection used for solar batteries as claimed in claim 6, its It is characterised by, described first pierced pattern includes two groups of symmetrically arranged multistage broken line shape grooves, adjacent segment groove Turn back in 90 degree between ditch.
8. it is used for the detection web plate of silver paste reliability detection used for solar batteries as claimed in claim 6, its It is characterised by, described second pierced pattern includes four straight trough ditches, four straight trough ditch Parallel Symmetric settings two-by-two.
9. it is used for the detection web plate of silver paste reliability detection used for solar batteries as claimed in claim 6, its It is characterised by, described 3rd pierced pattern includes two articles of straight trough ditches, two straight trough ditches are disposed on one directly On line.
10. it is used for the detection of silver paste reliability detection used for solar batteries as described in claim 7 or 8 or 9 Web plate is it is characterised in that the width of the groove of the 3rd pierced pattern is more than the width of the groove of the second pierced pattern Degree, the width of the groove of the second pierced pattern is more than the width of the groove of the first pierced pattern.
CN201510427174.0A 2015-07-20 2015-07-20 Detection method and detection mesh plate for detecting reliability of silver paste for solar cell Pending CN106373902A (en)

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Application Number Priority Date Filing Date Title
CN201510427174.0A CN106373902A (en) 2015-07-20 2015-07-20 Detection method and detection mesh plate for detecting reliability of silver paste for solar cell

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510427174.0A CN106373902A (en) 2015-07-20 2015-07-20 Detection method and detection mesh plate for detecting reliability of silver paste for solar cell

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109884392A (en) * 2017-12-06 2019-06-14 上海太阳能工程技术研究中心有限公司 A kind of silver aluminium paste intersection resistance value test method and test device
CN111463142A (en) * 2020-04-09 2020-07-28 浙江爱旭太阳能科技有限公司 Method for efficiently detecting corrosion of PERC aluminum paste
CN113960048A (en) * 2021-10-19 2022-01-21 广东斯特纳新材料有限公司 Solderability testing method of solder paste for MWT component
CN117330842A (en) * 2023-12-01 2024-01-02 长春黄金研究院有限公司 Preparation and detection device of silver powder pulping performance test piece

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20090255583A1 (en) * 2008-04-15 2009-10-15 E.I. Du Pont De Nemours And Company Aluminum pastes and use thereof in the production of silicon solar cells
CN102479568A (en) * 2010-11-30 2012-05-30 比亚迪股份有限公司 Conductive paste for solar cell and preparation method thereof
CN102555445A (en) * 2012-01-05 2012-07-11 天长吉阳新能源有限公司 Screen printing measurement method for crystalline silicon solar cell
CN104332423A (en) * 2014-10-24 2015-02-04 无锡帝科电子材料科技有限公司 Multifunctional comprehensive detection screen printing plate
CN204885093U (en) * 2015-07-20 2015-12-16 上海太阳能工程技术研究中心有限公司 A detect otter board that is used for solar cell to detect with silver thick liquid reliability

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20090255583A1 (en) * 2008-04-15 2009-10-15 E.I. Du Pont De Nemours And Company Aluminum pastes and use thereof in the production of silicon solar cells
CN102479568A (en) * 2010-11-30 2012-05-30 比亚迪股份有限公司 Conductive paste for solar cell and preparation method thereof
CN102555445A (en) * 2012-01-05 2012-07-11 天长吉阳新能源有限公司 Screen printing measurement method for crystalline silicon solar cell
CN104332423A (en) * 2014-10-24 2015-02-04 无锡帝科电子材料科技有限公司 Multifunctional comprehensive detection screen printing plate
CN204885093U (en) * 2015-07-20 2015-12-16 上海太阳能工程技术研究中心有限公司 A detect otter board that is used for solar cell to detect with silver thick liquid reliability

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109884392A (en) * 2017-12-06 2019-06-14 上海太阳能工程技术研究中心有限公司 A kind of silver aluminium paste intersection resistance value test method and test device
CN111463142A (en) * 2020-04-09 2020-07-28 浙江爱旭太阳能科技有限公司 Method for efficiently detecting corrosion of PERC aluminum paste
CN113960048A (en) * 2021-10-19 2022-01-21 广东斯特纳新材料有限公司 Solderability testing method of solder paste for MWT component
CN117330842A (en) * 2023-12-01 2024-01-02 长春黄金研究院有限公司 Preparation and detection device of silver powder pulping performance test piece
CN117330842B (en) * 2023-12-01 2024-02-27 长春黄金研究院有限公司 Preparation and detection device of silver powder pulping performance test piece

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Application publication date: 20170201