CN106359771A - Precipitation-preventing concentrated extraction solution of waxberry herb tea and preparation method - Google Patents

Precipitation-preventing concentrated extraction solution of waxberry herb tea and preparation method Download PDF

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Publication number
CN106359771A
CN106359771A CN201611078374.0A CN201611078374A CN106359771A CN 106359771 A CN106359771 A CN 106359771A CN 201611078374 A CN201611078374 A CN 201611078374A CN 106359771 A CN106359771 A CN 106359771A
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pressure
extraction
obtains
herbal tea
fructus
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CN201611078374.0A
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Chinese (zh)
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上官星云
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广西百利乐生物科技有限公司
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Priority to CN201611078374.0A priority Critical patent/CN106359771A/en
Publication of CN106359771A publication Critical patent/CN106359771A/en

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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23FCOFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
    • A23F3/00Tea; Tea substitutes; Preparations thereof
    • A23F3/34Tea substitutes, e.g. matè; Extracts or infusions thereof

Abstract

The invention discloses a precipitation-preventing concentrated extraction solution of waxberry herb tea and a preparation method. The preparation method comprises the following steps that 1, raw material preparation is performed: waxberry juice, prunella vulgaris, chrysanthemum flowers and momordica grosvenori are prepared; 2, extraction is performed: impurity removal and cleaning are conducted on the raw materials except the waxberry juice, the raw materials are broken or crushed and put in an extraction tank, 7-8 parts of purified water by weight is added, decoction and extraction are performed for 1-2 times, 1-2 hours are needed each time, extraction solutions are mixed, the waxberry juice is added, and filtration is performed; 3, concentration is performed: the filtrate obtained in the step 2 is subjected to nanofiltration concentration to make the soluble solid content reach 15-16%; 4, pressurizing treatment is performed: a part of mannitol is added, by weight, to the material obtained in the step 3, the material is charged into a pressure-resistant and non-toxic flexible package bag, the bag is put in an airtight container, a pressurizing medium is water, pressurization is performed to reach 6-8 MPa, the pressure is kept for 60-90 seconds, and then the pressure is released to obtain the extraction solution. The quality stability of the concentrated extraction solution is ensured, and the obtained final product is clear and free of precipitate.

Description

Prevent the concentrated extracting solution of Fructus Myricae rubrae herbal tea and the preparation method precipitating
Technical field
The invention belongs to food processing technology field, more particularly, to prevent the concentrated extracting solution of Fructus Myricae rubrae herbal tea and the system precipitating Preparation Method.
Background technology
Fructus Myricae rubrae (myrica rubra (lour.) s.et zucc.) is the local product fruits of south China, and its fruit colour is gorgeous Beautiful, sweet mouthfeel, very popular.Fructus Myricae rubrae is not only delicious but also has very high nutritive value, except containing abundant carbon water Outside compound, vitamin c, organic acid, also contain abundant anthocyanidin and flavonoid components, there is stronger antioxidation, anti-ageing Old effect.Calcium in its fruit, phosphorus, the content of ferrum are more than ten times of common fruit.Because Fructus Myricae rubrae is unsuitable for storing and transports, tradition On be often processed into the products such as waxberry wine, preserved fruit so as to local flavor is suffered a loss greatly.
Fructus Myricae rubrae, Spica Prunellae (prunella vulgaris l), Flos Chrysanthemi (flos chrysanthemi) and Fructus Momordicae (siraitia grosvenorii) is conventional heat-clearing toxin-expelling functions plant, because toxic and side effects are minimum by China's health The plant list of portion row people " being food and medicine ", is widely used in various in China's tcm clinical practice and diet-therapy health-preserving among the people The treatment of heat symptom-complex.Fructus Myricae rubrae, nature and flavor sweet acid, temperature, enter lung, stomach, quench one's thirst of promoting the production of body fluid, stomach function regulating helps digestion;Spica Prunellae, the property of medicine is pungent, bitter, trembles with fear, Return liver, gallbladder meridian, clearing away heat-fire, improving eyesight, mass dissipating and swelling eliminating;Flos Chrysanthemi nature and flavor are sweet, bitter, be slightly cold, return lung, Liver Channel, have scattered wind heat clearing away, clearly The effect of liver improving eyesight;Fructus Momordicae sweet in the mouth is cool in nature, return lung, large intestine channel, has functions that nourishing the lung to arrest cough, promoting the production of body fluid to quench thirst, is applied to lung-heat Or the effects such as xeropulmonary cough, pertussis and summer-heat fluid deficiency and thirsty.Above 4 taste medicines are the main components as herbal tea.
Herbal tea is the common name of Han nationality's Chinese herbal medicine beverage.Herbal tea " neither cool, be not tea ".It is Guangdong, Hong Kong, The beverage that Macao Area conventional compound recipe among the people or single local products medical herbs decoct, by medium-height grass that is cold and cool for the property of medicine and can clearing up interior-heat Medicine is decocted water and is drunk as beverage, and to eliminate the summer heat in summer human body, or winter is dried the illness such as the throat pain causing.Herbal tea is people According to local weather, soil characteristics, during long-term prevention disease with health care, with tcm health preserving theoretical for instructing, With Chinese herbal medicine as raw material, eat, sum up a kind of have heat-clearing and toxic substances removing, promoting the production of body fluid to quench thirst, dispel fire dehumidifying the effects such as beverage.It There is specific term to instruct to be daily drunk by people, both no dose limitation, without physician guidance register.Guangdong herbal tea is that Han nationality passes The representative of system herbal tea culture.Herbal tea is water that is pan-fried for Chinese herbal medicine that is cold and cool for the property of medicine and can clearing up human body interior-heat to be cooked beverage drink, to eliminate Summer heat in summer human body, or treat the illness such as the throat pain that winter drying causes.On May 20th, 2006, herbal tea is through state affairs First national non-material cultural heritage is listed in institute's approval in.
At present, on market, herbal tea mainly has canned, Bottle & Can, Tetra Pak, herbal tea paving jorum dress and herbal tea dissolved granule several Plant packing and selling form, wherein mainly based on canned herbal tea.Send out according to State Statistics Bureau's China-styled Certain Industry Field enterprise information publishing center " 2012 the first three quarters China beverage industry operational application report " display of cloth, the sales volume of canned herbal tea exceed good to eat can The happy sales volume in China's Mainland, becomes " Chinese beverage first tank ", and is shown according to sales data before, it continuous 7 Year sales volume is leading, it can be seen that canned herbal tea deal in the market.It is compared to traditional herbal tea paving production model, existing The industrial big inevitable requirement product that produces of generationization can obtain seriality and guarantee property, to meeting wanting of consumer in quality Ask, obtain the trust of consumer.The leading level of production of existing herbal tea industry, mainly by advanced concentration technique, obtains draft Plant essence, then fill is allocated by subsidiary factory, thus ensureing stability and the concordance of herbal tea mouthfeel to greatest extent.Therefore, Quality control for herbal tea concentrated extracting solution is crucial.
Content of the invention
It is an object of the invention to provide preventing the brand-new preparation method of concentrated extracting solution of the Fructus Myricae rubrae herbal tea of precipitation, by cool The technical study of tea concentrated extracting solution is not it is ensured that the steady quality of concentrated extracting solution, the final products obtaining precipitate.
The present invention is achieved by the following technical solution:
Prevent the preparation method of the concentrated extracting solution of Fructus Myricae rubrae herbal tea of precipitation, comprise the steps:
1) raw material prepares: prepares red bayberry juice, Spica Prunellae, Flos Chrysanthemi, Fructus Momordicae;
2) extract: after the raw material in addition to red bayberry juice is removed impurity, cleans, smash or broken, put into extraction pot, add The pure water boiling and extraction of 7-8 times of weight portion 1-2 time, each 1-2 hour, united extraction liquid, add red bayberry juice, filter;
3) concentrate: by step 2) filtrate that obtains, it is 15-16% that nanofiltration is concentrated to soluble solid content;
4) pressurized treatments: by step 3) material that obtains, add the Mannitol of 0.001 weight portion, load pressure, nontoxic Soft packaging bag, puts in hermetic container, and pressure medium is water, is pressurized to 6-8mpa, keeps abrupt release pressure after 60-90s, obtains Arrive.
Step 1 of the present invention) described in red bayberry juice, Spica Prunellae, Flos Chrysanthemi, Fructus Momordicae, preferably according to 8-12:3-5:2-4: The weight ratio of 0.5-1.5, further preferably according to 10: 4:3:1 weight ratio;The preferably fresh Fructus Momordicae of Fructus Momordicae.
Step 4) described in nanofiltration concentrate, preferable temperature 28-30 DEG C, pressure 2.8-3.0mpa, membranous type number 474, can be by In mixing filtrate, soluble solid content brings up to 15-16% by 1.0-2.0%.
Present invention additionally comprises the concentrated extracting solution of the Fructus Myricae rubrae herbal tea of the high transmission rate being obtained using method made above.
Compared with prior art, the present invention has the advantage that
1st, in prior art, in order to prevent the precipitation of cool tea-based beverages, reach the purpose of clarification in other words, typically can be cool Add enzyme preparation or compound enzymic preparation in the production process of tea beverage, but add the relatively more suitable herbal raw material of enzyme preparation and carry Preparation, fill immediately after taking, for come large-scale production herbal tea discomfort using herb tea concentrated solution form as beverage host Close, because enzyme preparation has the scope of optimum ph value, and herb tea concentrated solution is as beverage host, the ph value of its ph value and final products Have any different, so, with the change of ph value, precipitation still can occur in end product.
2nd, the present invention, before pressurized treatments, adds Mannitol in concentrated solution, can keep osmotic pressure, prevent solubility The gathering of grain, reach the purpose preventing precipitating.
3rd, in prior art, the purpose to the high pressure such as food, beverage or ultra high pressure treatment is to sterilize or living Property constituents extraction, its pressure be 100-1000mpa, even more high, such HIGH PRESSURE TREATMENT be usually raw material the extraction stage. Herbal tea concentrated extracting solution is the mixed liquor after various raw material of Chinese medicine extract, it is easy to form polymerization now after different material mixings As if herbal tea concentrated extracting solution is processed with so high processing pressure, leading in the Chinese herbal medicine such as red bayberry juice, Fructus Momordicae Albumen, polysaccharose substance structure change, under conditions of long storage or cold preservation, freezing in can condense, form " cheese " shape Precipitation, produces quality problems, the mouthfeel of impact finished beverage, color and luster, outward appearance etc..The present invention to be processed herbal tea and to concentrate using pressurization The precipitation of extracting solution, clear up problems, pressure used, the far smaller than pressure limit of prior art, treated herbal tea is dense Contracting extracting solution, steady quality, precipitation will not be produced, also reached the purpose of sterilizing simultaneously.
Specific embodiment
With embodiment, the invention will be further described below, but the invention is not limited in these embodiments.
Embodiment 1:
Prevent the preparation method of the concentrated extracting solution of Fructus Myricae rubrae herbal tea of precipitation, comprise the steps:
1) raw material prepares: prepares red bayberry juice, Spica Prunellae, Flos Chrysanthemi, Fructus Momordicae, according to the weight ratio of 8:5:2:1.5;
2) extract: after the raw material in addition to red bayberry juice is removed impurity, cleans, smash or broken, put into extraction pot, add The pure water boiling and extraction of 7 times of weight portions 2 times, 1 hour every time, united extraction liquid, add red bayberry juice, filter;
3) concentrate: by step 2) filtrate that obtains, it is 15-16% that nanofiltration is concentrated to soluble solid content, nanofiltration temperature 28-30 DEG C of degree, pressure 2.8-3.0mpa, membranous type number 474;
4) pressurized treatments: by step 3) material that obtains, add the Mannitol of 0.001 weight portion, load pressure, nontoxic Soft packaging bag, puts in hermetic container, and pressure medium is water, is pressurized to 6-8mpa, keeps abrupt release pressure after 90s, obtains.
Embodiment 2:
Prevent the preparation method of the concentrated extracting solution of Fructus Myricae rubrae herbal tea of precipitation, comprise the steps:
1) raw material prepares: prepares red bayberry juice, Spica Prunellae, Flos Chrysanthemi, Fructus Momordicae, presses: the weight ratio of 12:3:4:0.5;
2) extract: after the raw material in addition to red bayberry juice is removed impurity, cleans, smash or broken, put into extraction pot, add The pure water boiling and extraction of 8 times of weight portions 1 time, 2 hours every time, united extraction liquid, add red bayberry juice, filter;
3) concentrate: by step 2) filtrate that obtains, it is 15-16% that nanofiltration is concentrated to soluble solid content, nanofiltration temperature 28-30 DEG C of degree, pressure 2.8-3.0mpa, membranous type number 474;
4) pressurized treatments: by step 3) material that obtains, add the Mannitol of 0.001 weight portion, load pressure, nontoxic Soft packaging bag, puts in hermetic container, and pressure medium is water, is pressurized to 6-8mpa, keeps abrupt release pressure after 80s, obtains.
Embodiment 3:
Prevent the preparation method of the concentrated extracting solution of Fructus Myricae rubrae herbal tea of precipitation, comprise the steps:
1) raw material prepares: prepares red bayberry juice, Spica Prunellae, Flos Chrysanthemi, Fructus Momordicae, presses: the weight ratio of 8:4:3:1;
2) extract: after the raw material in addition to red bayberry juice is removed impurity, cleans, smash or broken, put into extraction pot, add The pure water boiling and extraction of 7 times of weight portions 2 times, 1 hour every time, united extraction liquid, add red bayberry juice, filter;
3) concentrate: by step 2) filtrate that obtains, it is 15-16% that nanofiltration is concentrated to soluble solid content, nanofiltration temperature 28-30 DEG C of degree, pressure 2.8-3.0mpa, membranous type number 474;
4) pressurized treatments: by step 3) material that obtains, add the Mannitol of 0.001 weight portion, load pressure, nontoxic Soft packaging bag, puts in hermetic container, and pressure medium is water, is pressurized to 6-8mpa, keeps abrupt release pressure after 90s, obtains.
Comparative example 1:
1) raw material prepares: prepares red bayberry juice, Spica Prunellae, Flos Chrysanthemi, Fructus Momordicae, presses: the weight ratio of 8:4:3:1;
2) extract: after the raw material in addition to red bayberry juice is removed impurity, cleans, smash or broken, put into extraction pot, add The pure water boiling and extraction of 7 times of weight portions 2 times, 1 hour every time, united extraction liquid, add red bayberry juice, filter;
3) concentrate: by step 2) filtrate that obtains, it is 15-16% that nanofiltration is concentrated to soluble solid content, nanofiltration temperature 28-30 DEG C of degree, pressure 2.8-3.0mpa, membranous type number 474;
4) pressurized treatments: by step 3) material that obtains, load pressure, nontoxic soft packaging bag, put in hermetic container, Pressure medium is water, is pressurized to 6-8mpa, keeps abrupt release pressure after 90s, obtains.
Comparative example 2:
1) raw material prepares: prepares red bayberry juice, Spica Prunellae, Flos Chrysanthemi, Fructus Momordicae, presses: the weight ratio of 8:4:3:1;
2) extract: after the raw material in addition to red bayberry juice is removed impurity, cleans, smash or broken, put into extraction pot, add The pure water boiling and extraction of 7 times of weight portions 2 times, 1 hour every time, united extraction liquid, add red bayberry juice, filter;
3) concentrate: by step 2) filtrate that obtains, it is 15-16% that nanofiltration is concentrated to soluble solid content, nanofiltration temperature 28-30 DEG C of degree, pressure 2.8-3.0mpa, membranous type number 474;
4) pressurized treatments: by step 3) material that obtains, load pressure, nontoxic soft packaging bag, put in hermetic container, Obtain.
Comparative example 3:
1) raw material prepares: prepares red bayberry juice, Spica Prunellae, Flos Chrysanthemi, Fructus Momordicae, presses: the weight ratio of 8:4:3:1;
2) extract: after the raw material in addition to red bayberry juice is removed impurity, cleans, smash or broken, put into extraction pot, add The pure water boiling and extraction of 7 times of weight portions 2 times, 1 hour every time, united extraction liquid, add red bayberry juice, filter;
3) concentrate: by step 2) filtrate that obtains, it is 15-16% that nanofiltration is concentrated to soluble solid content, nanofiltration temperature 28-30 DEG C of degree, pressure 2.8-3.0mpa, membranous type number 474;
4) pressurized treatments: by step 3) material that obtains, add pectase 0.2% (w/v) and papain 0.3% (w/v) and 0.15% (w/v) citric acid, obtain.
Comparative example 4:
1) raw material prepares: prepares red bayberry juice, Spica Prunellae, Flos Chrysanthemi, Fructus Momordicae, presses: the weight ratio of 8:4:3:1;
2) extract: after the raw material in addition to red bayberry juice is removed impurity, cleans, smash or broken, put into extraction pot, add The pure water boiling and extraction of 7 times of weight portions 2 times, 1 hour every time, united extraction liquid, add red bayberry juice, filter;
3) concentrate: by step 2) filtrate that obtains, it is 15-16% that nanofiltration is concentrated to soluble solid content, nanofiltration temperature 28-30 DEG C of degree, pressure 2.8-3.0mpa, membranous type number 474;
4) pressurized treatments: by step 3) material that obtains, add the Mannitol of 0.001 weight portion and 0.006 weight portion Hydroxyethyl cellulose, loads pressure, nontoxic soft packaging bag, puts in hermetic container, and pressure medium is water, is pressurized to 80mpa, Keep abrupt release pressure after 90s, obtain.
Comparative example 5:
1) raw material prepares: prepares red bayberry juice, Spica Prunellae, Flos Chrysanthemi, Fructus Momordicae, presses: the weight ratio of 8:4:3:1;
2) extract: after the raw material in addition to red bayberry juice is removed impurity, cleans, smash or broken, put into extraction pot, add The pure water boiling and extraction of 7 times of weight portions 2 times, 1 hour every time, united extraction liquid, add red bayberry juice, filter;
3) concentrate: by step 2) filtrate that obtains, it is 15-16% that nanofiltration is concentrated to soluble solid content, nanofiltration temperature 28-30 DEG C of degree, pressure 2.8-3.0mpa, membranous type number 474;
4) pressurized treatments: by step 3) material that obtains, add the Mannitol of 0.001 weight portion and 0.006 weight portion Hydroxyethyl cellulose, loads pressure, nontoxic soft packaging bag, puts in hermetic container, and pressure medium is water, is pressurized to 150mpa, keeps abrupt release pressure after 90s, obtains.
Comparative example 6:
1) raw material prepares: prepares red bayberry juice, Spica Prunellae, Flos Chrysanthemi, Fructus Momordicae, presses: the weight ratio of 8:4:3:1;
2) extract: after the raw material in addition to red bayberry juice is removed impurity, cleans, smash or broken, put into extraction pot, add The pure water boiling and extraction of 7 times of weight portions 2 times, 1 hour every time, united extraction liquid, add red bayberry juice, filter;
3) concentrate: by step 2) filtrate that obtains, it is 15-16% that nanofiltration is concentrated to soluble solid content, nanofiltration temperature 28-30 DEG C of degree, pressure 2.8-3.0mpa, membranous type number 474;
4) pressurized treatments: by step 3) material that obtains, add the Mannitol of 0.001 weight portion and 0.006 weight portion Hydroxyethyl cellulose, loads pressure, nontoxic soft packaging bag, puts in hermetic container, and pressure medium is water, is pressurized to 300mpa, keeps abrupt release pressure after 90s, obtains.
Experimental example:
After the same storage condition of herb tea concentrated solution that embodiment 3 and comparative example are obtained is placed 6 months, synthetic beverage, Embodiment 3 and comparative example inspect 10 batches respectively by random samples, and each batch takes out 3 samples, and the beverage obtaining is compared by Acceleration study Precipitation status, count number of cases.
Conclusion: the sample result of embodiment 3 is better than comparative example.

Claims (5)

1. the preparation method preventing the concentrated extracting solution of Fructus Myricae rubrae herbal tea precipitating is it is characterised in that comprise the steps:
1) raw material prepares: prepares red bayberry juice, Spica Prunellae, Flos Chrysanthemi, Fructus Momordicae;
2) extract: after the raw material in addition to red bayberry juice is removed impurity, cleans, smash or broken, put into extraction pot, add 7-8 The pure water boiling and extraction of times weight portion 1-2 time, each 1-2 hour, united extraction liquid, add red bayberry juice, filter;
3) concentrate: by step 2) filtrate that obtains, it is 15-16% that nanofiltration is concentrated to soluble solid content;
4) pressurized treatments: by step 3) material that obtains, add the Mannitol of 0.001 weight portion, load pressure, nontoxic Soft Roll Pack, puts in hermetic container, and pressure medium is water, is pressurized to 6-8mpa, keeps abrupt release pressure after 60-90s, obtains.
2. according to claim 1 prevent precipitate the concentrated extracting solution of Fructus Myricae rubrae herbal tea preparation method it is characterised in that: Step 1) described in Fructus Momordicae charantiae, Flos Chrysanthemi, Fructus Momordicae, according to the weight ratio of 8-12:3-5:2-4:0.5-1.5.
3. according to claim 2 prevent precipitate the concentrated extracting solution of Fructus Myricae rubrae herbal tea preparation method it is characterised in that: Step 1) described in Fructus Momordicae charantiae, Flos Chrysanthemi, Fructus Momordicae, press: 10: 4:3:1 weight ratio.
4. according to claim 1 prevent precipitate the concentrated extracting solution of Fructus Myricae rubrae herbal tea preparation method it is characterised in that: Step 4) described in nanofiltration concentrate, its temperature be 28-30 DEG C, pressure 2.8-3.0mpa, membranous type number 474.
5. the concentrated extracting solution of the Fructus Myricae rubrae herbal tea of the high transmission rate that the preparation method any one of claim 1-4 obtains.
CN201611078374.0A 2016-11-30 2016-11-30 Precipitation-preventing concentrated extraction solution of waxberry herb tea and preparation method CN106359771A (en)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102793038A (en) * 2012-08-01 2012-11-28 广州王老吉药业股份有限公司 Concentrated solution of Chinese herbal tea and preparation method thereof
CN105901248A (en) * 2016-06-24 2016-08-31 广西百利乐生物科技有限公司 Juice-herbal tea beverage and preparation process thereof
CN105918573A (en) * 2016-06-24 2016-09-07 广西百利乐生物科技有限公司 Fruit juice and herbal tea drink and production method thereof
CN106107268A (en) * 2016-06-24 2016-11-16 广西百利乐生物科技有限公司 Fruit juice antipyretic beverage and preparation technology thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102793038A (en) * 2012-08-01 2012-11-28 广州王老吉药业股份有限公司 Concentrated solution of Chinese herbal tea and preparation method thereof
CN105901248A (en) * 2016-06-24 2016-08-31 广西百利乐生物科技有限公司 Juice-herbal tea beverage and preparation process thereof
CN105918573A (en) * 2016-06-24 2016-09-07 广西百利乐生物科技有限公司 Fruit juice and herbal tea drink and production method thereof
CN106107268A (en) * 2016-06-24 2016-11-16 广西百利乐生物科技有限公司 Fruit juice antipyretic beverage and preparation technology thereof

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