CN106348844B - A kind of deodorant and preparation method thereof in seaweed digest process - Google Patents
A kind of deodorant and preparation method thereof in seaweed digest process Download PDFInfo
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- CN106348844B CN106348844B CN201610691263.0A CN201610691263A CN106348844B CN 106348844 B CN106348844 B CN 106348844B CN 201610691263 A CN201610691263 A CN 201610691263A CN 106348844 B CN106348844 B CN 106348844B
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
Abstract
The invention discloses a kind of deodorants and preparation method thereof in seaweed digest process, the product has the advantages such as production is simple, use cost is lower, function and effect are significant, help to solve presently, there are the decomposed odor contamination problem of seaweed, improve the decomposed effect of seaweed.The invention has the advantages that making full use of the synergistic effect of compound Chinese herb and probiotics fermention, further includes the strong suction-operated of adsorbent, the NH in seaweed digest process can be effectively removed3、H2S、CH4Deng more than 10 kinds of foul gas, not only existing foul gas molecule can be removed by chemical reaction, and the generation of new foul smell molecule can be inhibited, the harm of foul gas can be eliminated from source, it is avoided using the natural products ingredient extracted in plant and probiotics using the deficiency contained in traditional deodorant to human body, environment harmful, effect is preferable, penetrating power is strong, volatility is low, the lasting effect time is long, maintenance energy is good with de-tasting, and does not have adverse effect to the decomposed microbial activities of seaweed.
Description
Technical field
The present invention relates to a kind of deodorants and preparation method thereof in seaweed digest process, belong to marine biotechnology neck
Domain.
Background technique
With organic agriculture, green agriculture, Nuisance Free Agricultural Development, as the novel alga fertilizer of efficient ecological environmental protection,
Nutrition, volume increase, degeneration-resistant, cold-resistant, drought resisting, in terms of have remarkable result, be developed rapidly.In recent years, with
Alga fertilizer upsurge is sprung up, and many middle-size and small-size fertilizer enterprises increase one after another or change the line of production marine alga fertilizer, according to incompletely statistics, China at present
Alga fertilizer manufacturing enterprise is at 300 or more.Although marine alga fertilizer production technology multiplicity, the extraction of seaweed functional active components is must
Indispensable, current extracting method has fermentation method, enzymatic isolation method, acid hydrolyzation, alkaline hydrolysiss etc., and wherein solid fermentation process has been at present
A kind of major way extracted as pretreatment and active constituent.In addition, the sudden algae in the oceans such as Enteromorpha is lasting quick-fried in recent years
Hair, although having developed package deal, harmless treatment process, the Enteromorpha part after collecting can not be dried or blueness
Storage, have to carry out decomposed processing.To sum up, the decomposed important step for having become marine algae resourceization comprehensive utilization of seaweed.
Although decomposed technique is of great significance to fertilizer production, a large amount of foul gas is generated in digest process, is given
Environment brings huge pollution, this is also that the green production of seaweed bio organic fertilizer brings serious challenge;It is easy simultaneously
Nearby residents are caused to suffer from respiratory disease.With the raising of people's environmental protection concern consciousness, domestic foul gas complains event
Frequently occur, complaint amount occupies second in entire tip-offs about environmental issues, at serious society, an environmental problem.
There are many research that nowadays China handles foul gas, de-tasted at present for China the state of development of technology come
It sees, bioanalysis will become following development trend.However, increasingly complicated, the life of the ingredient with the decomposed foul gas of seaweed
Object method also some aspects need perfect, such as find more stable, efficient, economic microorganism to improve the removal of foul gas
Efficiency;How more efficient biofilter filler is selected, and the specific surface area of filler can be increased by making it not only, can also be enhanced
Its adsorption capacity;Consider to cooperate other methods to use on the basis of single treatment mode, preferably removes stench to reach
Effect;More energy efficient, efficient unit etc. is developed, these problems all will be solution required for we will study from now on.
Summary of the invention
It is de-tasted in technology to overcome the shortcomings of that existing seaweed is decomposed, the purpose of the present invention is to provide one kind for sea
Deodorant and preparation method thereof in algae digest process, the product is simple with production, use cost is lower, function and effect are significant
Etc. advantages, help to solve presently, there are the decomposed odor contamination problem of seaweed, improve the decomposed effect of seaweed.
Above-mentioned purpose of the present invention is achieved by the following technical programs:
The present invention provides a kind of deodorant in seaweed digest process, it is characterised in that makes full use of compound medium-height grass
The synergistic effect of medicine, probiotics fermention and adsorbent effectively removes the decomposed penetrating odor of seaweed.
The present invention provides a kind of deodorant and preparation method thereof in seaweed digest process, it is characterised in that described multiple
The mass component of square Chinese herbal medicine are as follows: 20~30 parts of luffa, 18~22 parts of cinnamomum camphora, 20~25 parts of peppermint, 15~20 parts of purple perilla, Ah
15~20 parts of Wei, 10~15 parts of agalloch eaglewood, 8~12 parts of Rhizoma Chuanxiong, 8~12 parts of thyme, 6~10 parts of Radix Glycyrrhizae, 6~10 parts of the tuber of stemona, chaste tree
3~5 parts of mustard.
The present invention provides a kind of deodorant and preparation method thereof in seaweed digest process, it is characterised in that the benefit
Raw bacterium be candida utili, EM bacteria agent, nitrobacteria, bacillus megaterium and lactobacillus plantarum mix bacterium agent.
The present invention provides a kind of deodorant and preparation method thereof in seaweed digest process, it is characterised in that by such as
Lower step preparation:
(1) Chinese herbal medicine pre-processes: herbal raw material being sorted, crushing sieves with 100 mesh sieve;
(2) ingredient: accurate feed proportioning according to the above ratio is uniformly mixed, and the pure of 3 times of mass ratioes of herbal raw material is added
Water;
(3) 3~5% cellulase of herbal raw material mass ratio, 2~3% non-starch polysaccharide ultrasound-assisted enzymolysis: is added
Enzyme, digests 30~60min under ultrasonic wave subsidiary conditions, and hydrolysis temperature is controlled at 40~60 DEG C;
(4) prepared by bio-fermentation agent: taking 10~15 parts of rice brans, 10~15 portions of corn flour, 3~5 parts of rape cakes, 8~10 parts
Wheat bran, 4~6 parts of fermented bean dregs, 3~5 parts of calcium dihydrogen phosphates, 3~5 parts of EM bacteria agents, 2~3 parts of candida utili, 1~2 part of plant
Object lactobacillus, 2~3 parts of bacillus megateriums, 1~2 part of nitrobacteria, are mixed evenly;Then with the water containing 2% molasses
Moisture is adjusted to 3~5d of anaerobic fermentation at 35~40%, 25~30 DEG C by solution;
(5) it ferments: 2~3 parts of bio-fermentation agents of addition into step (3) Chinese herbal medicine enzymolysis liquid, ventilating fermentation 30~
60min, then 4~6h of anaerobic fermentation control 28~35 DEG C of temperature, and periodic agitation in fermentation process;
(6) it compounds: 20 parts of adsorbents will be added in the culture medium after step (5) fermentation;
(7) dry: to carry out being drying to obtain that seaweed is decomposed to use deodorant after compounding.
Adsorbent described in above-mentioned steps (6) is one or more of zeolite, active carbon, bentonite, vermiculite.
The present invention provides a kind of deodorant and preparation method thereof in seaweed digest process, it is characterised in that deodorant
Application method are as follows: deodorant is mixed into seaweed in the ratio of decomposed seaweed mass ratio 2~5%, be uniformly mixed.
Beneficial effects of the present invention: first is that the present invention makes full use of the association of compound Chinese herb, probiotics fermention and adsorbent
Same-action, the chemical reaction between existing Chinese herbal medicine active constituent and foul gas, and profitable probliotics biodegrade and absorption are made
With further including the strong suction-operated of adsorbent, the NH in seaweed digest process can be effectively removed3、H2S、CH4Deng more than 10 kinds
It is preferable to de-taste effect for foul gas;Second is that containing candida utili, lactobacillus plantarum, bacillus megaterium, nitre in deodorant
Change the probiotics such as bacterium, the decomposed effect of seaweed can be obviously improved, shorten the decomposed effect of seaweed, practice result is proved to use and is somebody's turn to do
Apply shortening 3d or more in the decomposed practice of the condition of identical decomposed effect when deodorant;Third is that the deodorant can not only pass through chemistry
Reaction removes existing foul gas molecule, and can inhibit the generation of new foul smell molecule, and effluvium can be eliminated from source
The harm of body;Fourth is that the deodorant penetrating power is strong, overcome traditional deodorant due to permeance property difference and cannot sufficiently with sea
The shortcomings that algae contacts;Fifth is that safety is higher, avoided using the natural products ingredient extracted in plant and probiotics using tradition
Contain the deficiency (nitrate, phosphate etc.) to human body, environment harmful in deodorant;Sixth is that product volatility is low, Ke Yichang
Time lasting effect, maintenance energy is good, and does not have adverse effect to the decomposed microbial activities of seaweed.
Different Chinese herbal medicine nature and flavor are different, and there is huge differences for effect, and there is multiple after different Chinese herbal medicine combinations
Miscellaneous interaction relationship, and the proportion between Chinese herbal medicine is closer, it is real that different ratio will also be such that monarch relationship occurs
The variation of matter, to make the relationship of composite Chinese herbal that substantive change occur.The present invention provides a kind of decomposed for seaweed
Deodorant in the process and preparation method thereof, following strictly the monarch and his subjects makes the combination principle of assistant, passes through scientific compatibility luffa, perfume (or spice)
The Chinese herbal medicines such as camphor tree, peppermint, purple perilla, asafoetide, agalloch eaglewood, Rhizoma Chuanxiong, thyme, Radix Glycyrrhizae, the tuber of stemona, schizonepeta pass through answering between Chinese herbal medicine
Miscellaneous phase mutual relation makes the application product achieve the technical effect that technical staff fail to predict under routine test.Test knot
Fruit shows to change Chinese herbal medicine composition or significantly reduces product function and effect (P < 0.01) than regular meeting.
Specific embodiment
Below with reference to embodiment, the present invention will be further described.
Embodiment 1:
A kind of deodorant and preparation method thereof in seaweed digest process, is prepared by following steps:
(1) Chinese herbal medicine pre-processes: herbal raw material being sorted, crushing sieves with 100 mesh sieve;
(2) 30 parts of luffa, 18 parts of cinnamomum camphora, 25 parts of peppermint, 15 parts of purple perilla, 20 parts of asafoetide, 10 parts of agalloch eaglewood, river ingredient: are pressed
5 parts of 12 parts of rhizome of chuanxiong, 8 parts of thyme, 10 parts of Radix Glycyrrhizae, 6 parts of the tuber of stemona, schizonepeta ratio accurate feed proportionings are uniformly mixed, and Chinese herbal medicine original is added
Expect the pure water of 3 times of mass ratioes;
(3) ultrasound-assisted enzymolysis: being added 5% cellulase of herbal raw material mass ratio, 3% non-starch polysaccharide enzyme, super
30min is digested under sound wave subsidiary conditions, hydrolysis temperature is controlled at 40~60 DEG C;
(4) prepared by bio-fermentation agent: taking 15 parts of rice brans, 10 portions of corn flour, 5 parts of rape cakes, 8 parts of wheat brans, 6 parts of fermentation beans
The dregs of rice, 3 parts of calcium dihydrogen phosphates, 5 parts of EM bacteria agents, 3 parts of candida utili, 2 parts of lactobacillus plantarums, 3 parts of bacillus megateriums, 2 parts
Nitrobacteria is mixed evenly;Then moisture is adjusted at 35~40%, 25~30 DEG C with the aqueous solution containing 2% molasses
Anaerobic fermentation 3d;
(5) it ferments: 3 parts of bio-fermentation agents being added into step (3) Chinese herbal medicine enzymolysis liquid, then ventilating fermentation 30min detests
Aerobe fermentation 4h controls 28~35 DEG C of temperature, and periodic agitation in fermentation process;
(6) it compounds: 20 parts of zeolites will be added in the culture medium after step (5) fermentation;
(7) dry: to carry out being drying to obtain that seaweed is decomposed to use deodorant after compounding.
Embodiment 2:
A kind of deodorant and preparation method thereof in seaweed digest process, is prepared by following steps:
(1) Chinese herbal medicine pre-processes: herbal raw material being sorted, crushing sieves with 100 mesh sieve;
(2) 20 parts of luffa, 22 parts of cinnamomum camphora, 20 parts of peppermint, 20 parts of purple perilla, 15 parts of asafoetide, 15 parts of agalloch eaglewood, river ingredient: are pressed
3 parts of 8 parts of rhizome of chuanxiong, 12 parts of thyme, 6 parts of Radix Glycyrrhizae, 10 parts of the tuber of stemona, schizonepeta ratio accurate feed proportionings are uniformly mixed, and Chinese herbal medicine original is added
Expect the pure water of 3 times of mass ratioes;
(3) ultrasound-assisted enzymolysis: being added 3% cellulase of herbal raw material mass ratio, 2% non-starch polysaccharide enzyme, super
60min is digested under sound wave subsidiary conditions, hydrolysis temperature is controlled at 40~60 DEG C;
(4) prepared by bio-fermentation agent: taking 10 parts of rice brans, 15 portions of corn flour, 3 parts of rape cakes, 10 parts of wheat brans, 4 parts of fermentation beans
The dregs of rice, 5 parts of calcium dihydrogen phosphates, 3 parts of EM bacteria agents, 2 parts of candida utili, 1 part of lactobacillus plantarum, 2 parts of bacillus megateriums, 1 part
Nitrobacteria is mixed evenly;Then moisture is adjusted at 35~40%, 25~30 DEG C with the aqueous solution containing 2% molasses
Anaerobic fermentation 5d;
(5) it ferments: 2 parts of bio-fermentation agents being added into step (3) Chinese herbal medicine enzymolysis liquid, then ventilating fermentation 60min detests
Aerobe fermentation 6h controls 28~35 DEG C of temperature, and periodic agitation in fermentation process;
(6) it compounds: 20 parts of active carbons will be added in the culture medium after step (5) fermentation;
(7) dry: to carry out being drying to obtain that seaweed is decomposed to use deodorant after compounding.
Embodiment 3:
A kind of deodorant and preparation method thereof in seaweed digest process, is prepared by following steps:
(1) Chinese herbal medicine pre-processes: herbal raw material being sorted, crushing sieves with 100 mesh sieve;
(2) 25 parts of luffa, 20 parts of cinnamomum camphora, 23 parts of peppermint, 18 parts of purple perilla, 18 parts of asafoetide, 12 parts of agalloch eaglewood, river ingredient: are pressed
4 parts of 10 parts of rhizome of chuanxiong, 10 parts of thyme, 8 parts of Radix Glycyrrhizae, 8 parts of the tuber of stemona, schizonepeta ratio accurate feed proportionings are uniformly mixed, and Chinese herbal medicine original is added
Expect the pure water of 3 times of mass ratioes;
(3) 4% cellulase of herbal raw material mass ratio, 2.5% non-starch polysaccharide enzyme, In ultrasound-assisted enzymolysis: is added
45min is digested under ultrasonic wave subsidiary conditions, hydrolysis temperature is controlled at 40~60 DEG C;
(4) bio-fermentation agent prepare: take 12 parts of rice brans, 12 portions of corn flour, 4 parts of rape cakes, 9 parts of wheat brans, 5 parts of fermented bean dregs,
4 parts of calcium dihydrogen phosphates, 4 parts of EM bacteria agents, 2.5 parts of candida utili, 1.5 parts of lactobacillus plantarums, 2.5 parts of bacillus megateriums,
1.5 parts of nitrobacterias, are mixed evenly;Then moisture is adjusted to 35~40%, 25~30 with the aqueous solution containing 2% molasses
Anaerobic fermentation 4d at DEG C;
(5) it ferments: 2.5 parts of bio-fermentation agents of addition into step (3) Chinese herbal medicine enzymolysis liquid, ventilating fermentation 45min, then
Anaerobic fermentation 5h controls 28~35 DEG C of temperature, and periodic agitation in fermentation process;
(6) it compounds: 20 parts of bentonites will be added in the culture medium after step (5) fermentation;
(7) dry: to carry out being drying to obtain that seaweed is decomposed to use deodorant after compounding.
The technical effect of the invention obtained is illustrated with test data below:
Test group | H2S removal rate (%) | Ammonia nitrogen removal frank (%) | Methyl mercaptan removal rate (%) |
Embodiment 1 | 99.41 | 98.08 | 94.82 |
Embodiment 2 | 99.03 | 97.96 | 93.97 |
Embodiment 3 | 99.37 | 98.24 | 94.54 |
Change I group of test of Chinese herbal medicine composition | 85.02 | 82.62 | 76.46 |
Change II group of test of Chinese herbal medicine composition | 84.81 | 81.95 | 80.79 |
Without probiotics fermention group | 66.76 | 61.03 | 50.28 |
Change I group of test of composite bacteria agent composition | 83.90 | 80.68 | 79.51 |
Change II group of test of composite bacteria agent composition | 82.80 | 73.63 | 70.66 |
Without compound Chinese herb test group | 76.13 | 70.17 | 62.27 |
The above examples are only used to illustrate the technical scheme of the present invention, rather than is limited;Although referring to aforementioned reality
It applies example to be described in detail to by invention, but for those of ordinary skill in the art, it still can be to aforementioned reality
Technical solution documented by example is applied to modify or equivalent replacement of some of the technical features;And to these modifications
Or replacement, the spirit and scope for claimed technical solution of the invention that it does not separate the essence of the corresponding technical solution.
Claims (2)
1. a kind of deodorant in seaweed digest process, it is characterised in that make full use of compound Chinese herb, probiotics fermention
And the synergistic effect of adsorbent, effectively remove the decomposed penetrating odor of seaweed;Specifically, described in seaweed digest process
Deodorant is made by the steps:
(1) Chinese herbal medicine pre-processes: herbal raw material being sorted, crushing sieves with 100 mesh sieve;
(2) ingredient: by 20~30 parts of luffa, 18~22 parts of cinnamomum camphora, 20~25 parts of peppermint, 15~20 parts of purple perilla, asafoetide 15~
20 parts, 10~15 parts of agalloch eaglewood, 8~12 parts of Rhizoma Chuanxiong, 8~12 parts of thyme, 6~10 parts of Radix Glycyrrhizae, 6~10 parts of the tuber of stemona, schizonepeta 3~5
Part ratio accurate feed proportioning, is uniformly mixed, and the pure water of 3 times of mass ratioes of herbal raw material is added;
(3) 3~5% cellulase of herbal raw material mass ratio, 2~3% non-starch polysaccharide enzymes, In ultrasound-assisted enzymolysis: is added
30~60min is digested under ultrasonic wave subsidiary conditions, hydrolysis temperature is controlled at 40~60 DEG C;
(4) bio-fermentation agent prepare: take 10~15 parts of rice brans, 10~15 portions of corn flour, 3~5 parts of rape cakes, 8~10 parts of wheat brans,
4~6 parts of fermented bean dregs, 3~5 parts of calcium dihydrogen phosphates, 3~5 parts of EM bacteria agents, 2~3 parts of candida utili, 1~2 part of plant cream
Bacillus, 2~3 parts of bacillus megateriums, 1~2 part of nitrobacteria, are mixed evenly;Then with the aqueous solution containing 2% molasses
Moisture is adjusted to 3~5d of anaerobic fermentation at 35~40%, 25~30 DEG C;
(5) it ferments: 2~3 parts of bio-fermentation agents of addition into step (3) Chinese herbal medicine enzymolysis liquid, 30~60min of ventilating fermentation, so
4~6h of anaerobic fermentation afterwards controls 28~35 DEG C of temperature, and periodic agitation in fermentation process;
(6) it compounds: 20 parts of adsorbents will be added in the culture medium after step (5) fermentation;The adsorbent be zeolite, active carbon,
The composition of one or more of bentonite, vermiculite;
(7) dry: to carry out being drying to obtain that seaweed is decomposed to use deodorant after compounding.
2. a kind of deodorant in seaweed digest process as described in claim 1, it is characterised in that the deodorant
Application method are as follows: deodorant is mixed into seaweed in the ratio of decomposed seaweed mass ratio 2~5%, is uniformly mixed.
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CN107963795A (en) * | 2017-12-01 | 2018-04-27 | 广西晨康力食品股份有限公司 | A kind of special deodorant in pig farm and preparation method thereof |
CN109876644A (en) * | 2019-02-18 | 2019-06-14 | 王玉廷 | A kind of biological deodorant and the preparation method and application thereof |
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