CN106306254A - Processing method of phoenix tree flower-chrysanthemum nankingense health care caffeine - Google Patents
Processing method of phoenix tree flower-chrysanthemum nankingense health care caffeine Download PDFInfo
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- CN106306254A CN106306254A CN201610734400.4A CN201610734400A CN106306254A CN 106306254 A CN106306254 A CN 106306254A CN 201610734400 A CN201610734400 A CN 201610734400A CN 106306254 A CN106306254 A CN 106306254A
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- flos firmianae
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- 241001412225 Firmiana simplex Species 0.000 title claims abstract description 13
- 238000003672 processing method Methods 0.000 title claims abstract description 13
- RYYVLZVUVIJVGH-UHFFFAOYSA-N caffeine Chemical compound CN1C(=O)N(C)C(=O)C2=C1N=CN2C RYYVLZVUVIJVGH-UHFFFAOYSA-N 0.000 title abstract description 10
- LPHGQDQBBGAPDZ-UHFFFAOYSA-N Isocaffeine Natural products CN1C(=O)N(C)C(=O)C2=C1N(C)C=N2 LPHGQDQBBGAPDZ-UHFFFAOYSA-N 0.000 title abstract 3
- 229960001948 caffeine Drugs 0.000 title abstract 3
- VJEONQKOZGKCAK-UHFFFAOYSA-N caffeine Natural products CN1C(=O)N(C)C(=O)C2=C1C=CN2C VJEONQKOZGKCAK-UHFFFAOYSA-N 0.000 title abstract 3
- 238000000855 fermentation Methods 0.000 claims abstract description 61
- 230000004151 fermentation Effects 0.000 claims abstract description 61
- 239000002994 raw material Substances 0.000 claims abstract description 55
- 240000005250 Chrysanthemum indicum Species 0.000 claims abstract description 9
- 235000007783 Chrysanthemum nankingense Nutrition 0.000 claims abstract description 9
- 235000013305 food Nutrition 0.000 claims abstract description 8
- 241000628997 Flos Species 0.000 claims description 126
- 238000001035 drying Methods 0.000 claims description 55
- 241001249699 Capitata Species 0.000 claims description 32
- 244000269722 Thea sinensis Species 0.000 claims description 32
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 32
- 235000013616 tea Nutrition 0.000 claims description 26
- 239000000203 mixture Substances 0.000 claims description 23
- 238000000605 extraction Methods 0.000 claims description 21
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- 238000010298 pulverizing process Methods 0.000 claims description 21
- 238000000034 method Methods 0.000 claims description 17
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 15
- 239000008367 deionised water Substances 0.000 claims description 15
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- 238000003306 harvesting Methods 0.000 claims description 7
- 239000000413 hydrolysate Substances 0.000 claims description 7
- 230000007062 hydrolysis Effects 0.000 claims description 7
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- 239000002245 particle Substances 0.000 claims description 7
- 238000003892 spreading Methods 0.000 claims description 7
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- XPCTZQVDEJYUGT-UHFFFAOYSA-N 3-hydroxy-2-methyl-4-pyrone Chemical compound CC=1OC=CC(=O)C=1O XPCTZQVDEJYUGT-UHFFFAOYSA-N 0.000 description 2
- 206010030113 Oedema Diseases 0.000 description 2
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 description 2
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- FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 description 1
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- 206010028980 Neoplasm Diseases 0.000 description 1
- 240000002834 Paulownia tomentosa Species 0.000 description 1
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- 235000006468 Thea sinensis Nutrition 0.000 description 1
- 206010053615 Thermal burn Diseases 0.000 description 1
- 241000130764 Tinea Species 0.000 description 1
- 208000002474 Tinea Diseases 0.000 description 1
- 240000001085 Trapa natans Species 0.000 description 1
- 241000700605 Viruses Species 0.000 description 1
- FPIPGXGPPPQFEQ-BOOMUCAASA-N Vitamin A Natural products OC/C=C(/C)\C=C\C=C(\C)/C=C/C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-BOOMUCAASA-N 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000975 bioactive effect Effects 0.000 description 1
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- 230000037304 dermatophytes Effects 0.000 description 1
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- 230000035619 diuresis Effects 0.000 description 1
- 208000001848 dysentery Diseases 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000003925 fat Substances 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
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- 231100000283 hepatitis Toxicity 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
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- 244000000010 microbial pathogen Species 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- VYQNWZOUAUKGHI-UHFFFAOYSA-N monobenzone Chemical compound C1=CC(O)=CC=C1OCC1=CC=CC=C1 VYQNWZOUAUKGHI-UHFFFAOYSA-N 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 235000008935 nutritious Nutrition 0.000 description 1
- 235000020333 oolong tea Nutrition 0.000 description 1
- NOOLISFMXDJSKH-UHFFFAOYSA-N p-menthan-3-ol Chemical compound CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 description 1
- 230000000144 pharmacologic effect Effects 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 239000003507 refrigerant Substances 0.000 description 1
- 235000009165 saligot Nutrition 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 230000035943 smell Effects 0.000 description 1
- UAJTZZNRJCKXJN-UHFFFAOYSA-M sodium;2-dodecoxy-2-oxoethanesulfonate Chemical compound [Na+].CCCCCCCCCCCCOC(=O)CS([O-])(=O)=O UAJTZZNRJCKXJN-UHFFFAOYSA-M 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
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- 150000003722 vitamin derivatives Chemical class 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/34—Tea substitutes, e.g. matè; Extracts or infusions thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Non-Alcoholic Beverages (AREA)
Abstract
The invention discloses a processing method of phoenix tree flower-chrysanthemum nankingense health care caffeine, and belongs to the field of food processing. The processing method is characterized in that phoenix tree flowers, tender stems and leaves of chrysanthemum nankingense and pubescent holly leaves are adopted, microwave fixation and enzyme deactivation and rolling are conducted to remove the green and astringent smell in the raw materials, wet fermentation is conducted after dry fermentation is conducted two times, therefore, the original faint scent of the raw materials is retained, the faint scent, obtained after fermentation, of the raw materials is increased, the mouthfeel of the caffeine product is improved, and the health care effects of clearing away heat and improving eyesight, regulating middle warmer and promoting appetite, reducing the blood pressure and the like are achieved.
Description
Technical field
The processing method that the present invention relates to a kind of caffein, especially relates to the processing of a kind of Flos Firmianae (Flow Flos firmianae) Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) health-protecting tea extract
Method.
Background technology
Firmiana platanifolia (Linn. f.) Marsili, has another name called blue or green paulownia, belongs to Sterculiaceae deciduous tree.Its root, skin, leaf and Huadu have certain medical value.Chinese parasol tree
Flos paulowniae, nature and flavor are sweet flat nontoxic, and people liver, kidney, lung three warp have the effects such as heat-clearing and toxic substances removing, expelling wind and removing dampness, inducing diuresis to remove edema.Cure mainly edema,
The disease such as tinea alba, burn and scald.At present, the domestic pharmacological action to Semen Firmianae, leaf and pollen all has research,.
Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui), also known as Folium chrysanthemi, LUBIANHUANG, is the cultivar based on young stem and leaf in Compositae Chrysanthemum, belongs to 1 year
Life or herbaceos perennial, containing nutrient substance such as rich in protein, fat, vitamin, cellulose, mineral, salt, its
Middle vitamin A and content of mineral substances are the most prominent.Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) has refrigerant, improving eyesight, in tune whet the appetite, also have removing toxic substances, blood pressure lowering it
Effect, to preventing and treating influenza, epidemic encephalitis, hepatitis, dysentery, suppression pathogenic microorganism, antibacterial and virus and dermatophytes growth are all played
Important function.Volatile oil contained by Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) is a kind of important bioactive substance, can maintain the normal function of blood capillary, clearly
Except free radical, suppress tumor.
Being of high nutritive value of Flos Firmianae (Flow Flos firmianae) and Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui), is used for being processed into Flos Firmianae (Flow Flos firmianae) Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) health-protecting tea extract, can realize former
The comprehensive utilization of material, improves its nutritive value and economic worth, and the most also the deep processing for Flos Firmianae (Flow Flos firmianae) and Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) product is opened up
One new approach.
Summary of the invention
The processing method that it is an object of the invention to provide a kind of Flos Firmianae (Flow Flos firmianae) Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) health-protecting tea extract, this method process stabilizing,
Simple to operate, be prone to grasp, Flos Firmianae (Flow Flos firmianae), Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) are fabricated to nutritious, drink convenient health-protecting tea extract, not only enrich
Product category, and improve the economic worth of Flos Firmianae (Flow Flos firmianae), Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui).
The present invention solves its technical problem and is adopted the technical scheme that:
The processing method of a kind of Flos Firmianae (Flow Flos firmianae) Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) health-protecting tea extract, is characterized in that, described manufacture method employing following steps:
(1) pretreatment of raw material: choose the fresh Flos Firmianae (Flow Flos firmianae) of harvesting, Dendranthema nankingense, Folium Ilicis Pubescentis, Fructus Trichosanthis young stem and leaf, the five tastes
Sub-tender leaf, after mix homogeneously, uses clear water drip washing, drains, then be placed in microwave green-killing device, and microwave operational frequencies is 180MHz,
Microwave output power is 12kw, and radiated time is 25min, and spreading for cooling is to room temperature；
(2) knead: the raw material after cooling is kneaded, raw material is placed in and rubs on plate, knead 15min, to raw material quality by hand
Deliquescing, distributes fragrance；It is re-fed in the drying room of 42 DEG C drying, is down to 12% to feed moisture content；
(3) fermentation: sent into by dried raw material in fermenting cellar, carries out dry fermentation 2 times under field conditions (factors), and the time is for the first time
2h, after drying, continues fermentation 4.5h；In the ratio of 1:0.1 raw material after dry fermentation adding green tea bacterium solution, fully after drying
Mix homogeneously, carries out wet fermentation, and the temperature of fermentation is 42 DEG C, and relative humidity is 40%, and fermentation time is 16h；
(4) extraction: the raw material after fermentation is carried out wall breaking pulverization, adds the deionized water of its weight 3.5 times, at 42 DEG C of constant temperature
Carry out backflow extraction 35min under water bath, be cooled to room temperature, filter to get filtrate and filtering residue, then filtering residue is added its weight 2 times
Deionized water under 55 DEG C of environment, carry out backflow extraction 25min, be cooled to room temperature, filter, merging filtrate, and at the ring of 65 DEG C
It is concentrated into the 18% of original volume under border, prepares Flos Firmianae (Flow Flos firmianae) lixiviating solution；By filtering residue dry after, waterproof pulverization be particle diameter be the Chinese parasol tree of 200 μm
Flos paulowniae mixed soil；
(5) Radix Glycyrrhizae pretreatment: choose fresh Radix Glycyrrhizae, is aided with Herba Hedyotis cantonensis, Cortex Moutan, cuts into slices after cleaning, and mix homogeneously puts into container
In, the pure water adding its weight 8 times soaks 5h, then uses break process, adds the cellulase and 0.2% of its weight 0.35%
Hemicellulose, be heated to 42 DEG C, united hydrolysis 55min, prepare Radix Glycyrrhizae hydrolysate；
(6) allotment: take the Flos Firmianae (Flow Flos firmianae) lixiviating solution of 25 weight portions, the Flos Firmianae (Flow Flos firmianae) mixed soil of 35 weight portions, the liquorice beverage of 20 weight portions
Solve thing, add the haw juice of 10 weight portions, the Semen Nelumbinis powder of 8 weight portions and the citric acid of 2 weight portions, after mix homogeneously, carry out
Vacuum and low temperature concentrates, and under the conditions of pressure 0.12MPa, temperature 48 DEG C, is concentrated into relative density 0.85g/cm3Concentrated solution；
(7) being dried: use syllogic to dry concentrated solution, first inferior to drying 25 minutes at 78 DEG C, second inferior to 50 DEG C at baking
Dry 35 minutes, drying 60 minutes at 42 DEG C for the third time, dry 30 minutes, interval between second time drying for the first time, for the second time
Dry and be spaced 35 minutes between third time drying, after pulverizing, prepare Flos Firmianae (Flow Flos firmianae) Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) health-protecting tea extract；
(8) packaging: after Flos Firmianae (Flow Flos firmianae) Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) health-protecting tea extract is arranged, pack with food stage packaging material, enter aeration-drying environment
Middle storage.
Beneficial effect: this method, by Flos Firmianae (Flow Flos firmianae), Dendranthema nankingense and Folium Ilicis Pubescentis, carries out microwave deactivation of enzyme enzyme denaturing, kneads,
Remove the not mature abnormal smells from the patient in raw material, then carry out wet fermentation after using 2 dry fermentations, make raw material both remain original delicate fragrance, also
Add the delicate fragrance after fermenting raw materials, improve the mouthfeel of product caffein, also there are appetizing, blood pressure lowering etc. in clearing away heat to improve acuity of vision, tune
Health-care effect.
Detailed description of the invention
Embodiment 1:
The processing method of a kind of Flos Firmianae (Flow Flos firmianae) Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) health-protecting tea extract, is characterized in that, described manufacture method employing following steps:
(1) pretreatment of raw material: choose the fresh Flos Firmianae (Flow Flos firmianae) of harvesting, Flos puerariae lobatae, Dendranthema nankingense, Francolini pintadeani Folium Camelliae sinensis, after mix homogeneously,
Using clear water drip washing, drain, then be placed in microwave green-killing device, microwave operational frequencies is 220MHz, and microwave output power is 18kw,
Radiated time is 20min, and spreading for cooling is to room temperature；
(2) knead: the raw material after cooling is kneaded, raw material is placed in and rubs on plate, knead 25min, to raw material quality by hand
Deliquescing, distributes fragrance；It is re-fed in the drying room of 45 DEG C drying, is down to 8% to feed moisture content；
(3) fermentation: sent into by dried raw material in fermenting cellar, carries out dry fermentation 2 times under field conditions (factors), and the time is for the first time
1h, after drying, continues fermentation 2.5h；In the ratio of 1:0.25 raw material after dry fermentation adds green tea bacterium solution after drying, fill
Dividing mix homogeneously, carry out wet fermentation, the temperature of fermentation is 32 DEG C, and relative humidity is 45%, and fermentation time is 10h；
(4) extraction: the raw material after fermentation is carried out wall breaking pulverization, adds the deionized water of its weight 6 times, at 48 DEG C of thermostatted waters
Carry out backflow extraction 25min under bath environment, be cooled to room temperature, filter to get filtrate and filtering residue, then filtering residue is added its weight 2.5 times
Deionized water under 58 DEG C of environment, carry out backflow extraction 15min, be cooled to room temperature, filter, merging filtrate, and at the ring of 80 DEG C
It is concentrated into the 22% of original volume under border, prepares Flos Firmianae (Flow Flos firmianae) lixiviating solution；By filtering residue dry after, waterproof pulverization be particle diameter be the Chinese parasol tree of 180 μm
Flos paulowniae mixed soil；
(5) Radix Glycyrrhizae pretreatment: choose fresh Radix Glycyrrhizae, is aided with Herba Hedyotis cantonensis, Herba Houttuyniae, Flos Citri Sarcodactylis, cuts into slices after cleaning, mix homogeneously,
Putting in container, the pure water adding its weight 4 times soaks 2h, then uses break process, adds the cellulose of its weight 0.28%
Enzyme and the hemicellulose of 0.12%, be heated to 45 DEG C, united hydrolysis 35min, prepares Radix Glycyrrhizae hydrolysate；
(6) allotment: take the Flos Firmianae (Flow Flos firmianae) lixiviating solution of 30 weight portions, the Flos Firmianae (Flow Flos firmianae) mixed soil of 40 weight portions, the liquorice beverage of 15 weight portions
Solve thing, add the Semen Hoveniae (Fructus Hoveniae) juice of 8 weight portions, the walnut powder of 6 weight portions and the citric acid of 1 weight portion, after mix homogeneously, carry out vacuum
Cryoconcentration, under the conditions of pressure 0.18MPa, temperature 52 DEG C, is concentrated into relative density 0.65g/cm3Concentrated solution；
(7) being dried: use syllogic to dry concentrated solution, first inferior to drying 18 minutes at 92 DEG C, second inferior to 68 DEG C at baking
Dry 25 minutes, drying 45 minutes at 55 DEG C for the third time, dry 20 minutes, interval between second time drying for the first time, for the second time
Dry and be spaced 15 minutes between third time drying, after pulverizing, prepare Flos Firmianae (Flow Flos firmianae) Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) health-protecting tea extract；
(8) packaging: after Flos Firmianae (Flow Flos firmianae) Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) health-protecting tea extract is arranged, pack with food stage packaging material, enter aeration-drying environment
Middle storage.
Embodiment 2:
The processing method of a kind of Flos Firmianae (Flow Flos firmianae) Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) health-protecting tea extract, is characterized in that, described manufacture method employing following steps:
(1) pretreatment of raw material: choose the fresh Flos Firmianae (Flow Flos firmianae) of harvesting, Dendranthema nankingense, calabash Folium Camelliae sinensis, Flos Lonicerae, mix homogeneously
After, to use clear water drip washing, drain, then be placed in microwave green-killing device, microwave operational frequencies is 260MHz, and microwave output power is
16kw, radiated time is 12min, and spreading for cooling is to room temperature；
(2) knead: the raw material after cooling is kneaded, raw material is placed in and rubs on plate, knead 20min, to raw material quality by hand
Deliquescing, distributes fragrance；It is re-fed in the drying room of 50 DEG C drying, is down to 5% to feed moisture content；
(3) fermentation: sent into by dried raw material in fermenting cellar, carries out dry fermentation 2 times under field conditions (factors), and the time is for the first time
3h, after drying, continues fermentation 6h；In the ratio of 1:0.35 raw material after dry fermentation adds pure water after drying, the most mixed
Closing uniformly, carry out wet fermentation, the temperature of fermentation is 48 DEG C, and relative humidity is 50%, and fermentation time is 8h；
(4) extraction: the raw material after fermentation is carried out wall breaking pulverization, adds the deionized water of its weight 5 times, at 35 DEG C of thermostatted waters
Carry out backflow extraction 55min under bath environment, be cooled to room temperature, filter to get filtrate and filtering residue, then filtering residue is added its weight 3 times
Deionized water carries out backflow extraction 35min under 48 DEG C of environment, is cooled to room temperature, filters, merging filtrate, and at the environment of 68 DEG C
Under be concentrated into the 28% of original volume, prepare Flos Firmianae (Flow Flos firmianae) lixiviating solution；By filtering residue dry after, waterproof pulverization be particle diameter be the Firmiana platanifolia (Linn. f.) Marsili of 160 μm
Flower mixed soil；
(5) Radix Glycyrrhizae pretreatment: choose fresh Radix Glycyrrhizae, is aided with Herba Hedyotis cantonensis, Herba Centellae, Mentholum, cuts into slices after cleaning, mix homogeneously,
Putting in container, the pure water adding its weight 3.5 times soaks 8h, then uses break process, adds the fiber of its weight 0.45%
Element enzyme and the hemicellulose of 0.06%, be heated to 46 DEG C, united hydrolysis 45min, prepares Radix Glycyrrhizae hydrolysate；
(6) allotment: take the Flos Firmianae (Flow Flos firmianae) lixiviating solution of 20 weight portions, the Flos Firmianae (Flow Flos firmianae) mixed soil of 45 weight portions, the liquorice beverage of 10 weight portions
Solve thing, add the sub-juice of car li, the water caltrop starch of 7 weight portions and the malic acid of 3 weight portions of 15 weight portions, after mix homogeneously, carry out
Vacuum and low temperature concentrates, and under the conditions of pressure 0.08MPa, temperature 42 DEG C, is concentrated into relative density 1.45g/cm3Concentrated solution；
(7) being dried: use syllogic to dry concentrated solution, first inferior to drying 10 minutes at 88 DEG C, second inferior to 76 DEG C at baking
Dry 20 minutes, drying 38 minutes at 61 DEG C for the third time, dry 12 minutes, interval between second time drying for the first time, for the second time
Dry and be spaced 25 minutes between third time drying, after pulverizing, prepare Flos Firmianae (Flow Flos firmianae) Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) health-protecting tea extract；
(8) packaging: after Flos Firmianae (Flow Flos firmianae) Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) health-protecting tea extract is arranged, pack with food stage packaging material, enter aeration-drying environment
Middle storage.
Embodiment 3:
The processing method of a kind of Flos Firmianae (Flow Flos firmianae) Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) health-protecting tea extract, is characterized in that, described manufacture method employing following steps:
(1) pretreatment of raw material: choose the fresh Flos Firmianae (Flow Flos firmianae) of harvesting, Dendranthema nankingense, oolong tea, loquat tender leaf, Flos Albiziae, mixed
After closing uniformly, using clear water drip washing, drain, then be placed in microwave green-killing device, microwave operational frequencies is 350MHz, microwave output work
Rate is 8kw, and radiated time is 12min, and spreading for cooling is to room temperature；
(2) knead: the raw material after cooling is kneaded, raw material is placed in and rubs on plate, knead 10min, to raw material quality by hand
Deliquescing, distributes fragrance；It is re-fed in the drying room of 65 DEG C drying, is down to 10% to feed moisture content；
(3) fermentation: sent into by dried raw material in fermenting cellar, carries out dry fermentation 2 times under field conditions (factors), and the time is for the first time
1.5h, after drying, continues fermentation 3.5h；In the ratio of 1:0.18 raw material after dry fermentation adds green tea bacterium solution after drying,
Being sufficiently mixed uniformly, carry out wet fermentation, the temperature of fermentation is 45 DEG C, and relative humidity is 50%, and fermentation time is 11h；
(4) extraction: the raw material after fermentation is carried out wall breaking pulverization, adds the deionized water of its weight 5 times, at 38 DEG C of thermostatted waters
Carry out backflow extraction 42min under bath environment, be cooled to room temperature, filter to get filtrate and filtering residue, then filtering residue is added its weight 2.5 times
Deionized water under 46 DEG C of environment, carry out backflow extraction 30min, be cooled to room temperature, filter, merging filtrate, and at the ring of 55 DEG C
It is concentrated into the 12% of original volume under border, prepares Flos Firmianae (Flow Flos firmianae) lixiviating solution；By filtering residue dry after, waterproof pulverization be particle diameter be the Chinese parasol tree of 280 μm
Flos paulowniae mixed soil；
(5) Radix Glycyrrhizae pretreatment: choose fresh Radix Glycyrrhizae, is aided with Herba Hedyotis cantonensis, tender Folium Nelumbinis, cuts into slices after cleaning, and mix homogeneously puts into container
In, the pure water adding its weight 3 times soaks 2h, then uses break process, adds the cellulase and 0.15% of its weight 0.5%
Hemicellulose, be heated to 48 DEG C, united hydrolysis 42min, prepare Radix Glycyrrhizae hydrolysate；
(6) allotment: take the Flos Firmianae (Flow Flos firmianae) lixiviating solution of 30 weight portions, the Flos Firmianae (Flow Flos firmianae) mixed soil of 45 weight portions, the liquorice beverage of 15 weight portions
Solve thing, add the Daharian rose fruit juice of 6 weight portions, the maltol of 2 weight portions and the citric acid of 2 weight portions, after mix homogeneously, carry out true
Empty cryoconcentration, under the conditions of pressure 0.15MPa, temperature 52 DEG C, is concentrated into relative density 1.25g/cm3Concentrated solution；
(7) being dried: use syllogic to dry concentrated solution, first inferior to drying 15 minutes at 86 DEG C, second inferior to 48 DEG C at baking
Dry 40 minutes, drying 55 minutes at 35 DEG C for the third time, dry 20 minutes, interval between second time drying for the first time, for the second time
Dry and be spaced 45 minutes between third time drying, after pulverizing, prepare Flos Firmianae (Flow Flos firmianae) Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) health-protecting tea extract；
(8) packaging: after Flos Firmianae (Flow Flos firmianae) Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) health-protecting tea extract is arranged, pack with food stage packaging material, enter aeration-drying environment
Middle storage.
Embodiment 4:
The processing method of a kind of Flos Firmianae (Flow Flos firmianae) Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) health-protecting tea extract, is characterized in that, described manufacture method employing following steps:
(1) pretreatment of raw material: choose the fresh Flos Firmianae (Flow Flos firmianae) of harvesting, Dendranthema nankingense, Fructus Trichosanthis young stem and leaf, green tea, Folium machili velutinae
Leaf, after mix homogeneously, uses clear water drip washing, drains, then be placed in microwave green-killing device, and microwave operational frequencies is 420MHz, microwave
Output is 22kw, and radiated time is 8min, and spreading for cooling is to room temperature；
(2) knead: the raw material after cooling is kneaded, raw material is placed in and rubs on plate, knead 25min, to raw material quality by hand
Deliquescing, distributes fragrance；It is re-fed in the drying room of 36 DEG C drying, is down to 20% to feed moisture content；
(3) fermentation: sent into by dried raw material in fermenting cellar, carries out dry fermentation 2 times under field conditions (factors), and the time is for the first time
0.5h, after drying, continues fermentation 2.5h；In the ratio of 1:0.28 raw material after dry fermentation adds green tea bacterium solution after drying,
Being sufficiently mixed uniformly, carry out wet fermentation, the temperature of fermentation is 37 DEG C, and relative humidity is 45%, and fermentation time is 8h；
(4) extraction: the raw material after fermentation is carried out wall breaking pulverization, adds the deionized water of its weight 6 times, at 32 DEG C of thermostatted waters
Carry out backflow extraction 40min under bath environment, be cooled to room temperature, filter to get filtrate and filtering residue, then filtering residue is added its weight 3.5 times
Deionized water under 52 DEG C of environment, carry out backflow extraction 30min, be cooled to room temperature, filter, merging filtrate, and at the ring of 67 DEG C
It is concentrated into the 16% of original volume under border, prepares Flos Firmianae (Flow Flos firmianae) lixiviating solution；By filtering residue dry after, waterproof pulverization be particle diameter be the Chinese parasol tree of 120 μm
Flos paulowniae mixed soil；
(5) Radix Glycyrrhizae pretreatment: choose fresh Radix Glycyrrhizae, is aided with Herba Hedyotis cantonensis, Flos Caryophylli, cuts into slices after cleaning, and mix homogeneously puts into container
In, the pure water adding its weight 2 times soaks 8h, then uses break process, add its weight 0.55% cellulase and
The hemicellulose of 0.16%, is heated to 30 DEG C, united hydrolysis 35min, prepares Radix Glycyrrhizae hydrolysate；
(6) allotment: take the Flos Firmianae (Flow Flos firmianae) lixiviating solution of 20 weight portions, the Flos Firmianae (Flow Flos firmianae) mixed soil of 45 weight portions, the liquorice beverage of 20 weight portions
Solve thing, add the real sub-juice of sweet oak, the egg albumen powder of 5 weight portions and the malic acid of 2 weight portions of 8 weight portions, after mix homogeneously, carry out true
Empty cryoconcentration, under the conditions of pressure 0.21MPa, temperature 55 DEG C, is concentrated into relative density 0.45g/cm3Concentrated solution；
(7) it is dried: by concentrated solution in microwave vacuum dryer, carry out low-temperature vacuum drying, in microwave power 360W, temperature 45
DEG C, be dried 45 minutes under the conditions of vacuum 28Pa, prepare Flos Firmianae (Flow Flos firmianae) Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) health-protecting tea extract after pulverizing；
(8) packaging: after Flos Firmianae (Flow Flos firmianae) Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) health-protecting tea extract is arranged, pack with food stage packaging material, enter aeration-drying environment
Middle storage.
Embodiment 5:
The processing method of a kind of Flos Firmianae (Flow Flos firmianae) Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) health-protecting tea extract, is characterized in that, described manufacture method employing following steps:
(1) pretreatment of raw material: choose the fresh Flos Firmianae (Flow Flos firmianae) of harvesting, Dendranthema nankingense, llex cornuta young stem and leaf, Cortex Lycii, mixing is all
After even, using clear water drip washing, drain, then be placed in microwave green-killing device, microwave operational frequencies is 260MHz, and microwave output power is
23kw, radiated time is 12min, and spreading for cooling is to room temperature；
(2) knead: the raw material after cooling is kneaded, raw material is placed in and rubs on plate, knead 5min by hand, become to raw material quality
Soft, distribute fragrance；It is re-fed in the drying room of 48 DEG C drying, is down to 25% to feed moisture content；
(3) fermentation: sent into by dried raw material in fermenting cellar, carries out dry fermentation 2 times under field conditions (factors), and the time is for the first time
1.5h, after drying, continues fermentation 5h；In the ratio of 1:0.4 raw material after dry fermentation adding deionized water, fully after drying
Mix homogeneously, carries out wet fermentation, and the temperature of fermentation is 48 DEG C, and relative humidity is 46%, and fermentation time is 12h；
(4) extraction: the raw material after fermentation is carried out wall breaking pulverization, adds the deionized water of its weight 4 times, at 38 DEG C of thermostatted waters
Carry out backflow extraction 40min under bath environment, be cooled to room temperature, filter to get filtrate and filtering residue, then filtering residue is added its weight 3 times
Deionized water carries out backflow extraction 30min under 45 DEG C of environment, is cooled to room temperature, filters, merging filtrate, and at the environment of 58 DEG C
Under be concentrated into the 22% of original volume, prepare Flos Firmianae (Flow Flos firmianae) lixiviating solution；By filtering residue dry after, waterproof pulverization be particle diameter be the Firmiana platanifolia (Linn. f.) Marsili of 180 μm
Flower mixed soil；
(5) Radix Glycyrrhizae pretreatment: choose fresh Radix Glycyrrhizae, is aided with Herba Hedyotis cantonensis, Cortex Moutan, cuts into slices after cleaning, and mix homogeneously puts into container
In, the pure water adding its weight 5 times soaks 3h, then uses break process, add its weight 0.85% cellulase and
The hemicellulose of 0.45%, is heated to 50 DEG C, united hydrolysis 35min, prepares Radix Glycyrrhizae hydrolysate；
(6) allotment: take the Flos Firmianae (Flow Flos firmianae) lixiviating solution of 25 weight portions, the Flos Firmianae (Flow Flos firmianae) mixed soil of 40 weight portions, the liquorice beverage of 15 weight portions
Solve thing, add the lantern fruit juice of 12 weight portions, the Fagopyrum esculentum Moench powder of 5 weight portions and the citric acid of 3 weight portions, after mix homogeneously, carry out
Vacuum and low temperature concentrates, and under the conditions of pressure 0.08MPa, temperature 42 DEG C, is concentrated into relative density 1.3g/cm3Concentrated solution；
(7) it is dried: concentrated solution is spray-dried, controls inlet temperature 102 DEG C, outlet temperature 88 DEG C, after pulverizing, prepare Chinese parasol tree
Flos paulowniae Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) health-protecting tea extract；
(8) packaging: after Flos Firmianae (Flow Flos firmianae) Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) health-protecting tea extract is arranged, pack with food stage packaging material, enter aeration-drying environment
Middle storage.
Part that the present invention does not relate to is the most same as the prior art maybe can use prior art to be realized.
Claims (1)
1. the processing method of a Flos Firmianae (Flow Flos firmianae) Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) health-protecting tea extract, it is characterised in that employing following steps:
(1) pretreatment of raw material: choose the fresh Flos Firmianae (Flow Flos firmianae) of harvesting, Dendranthema nankingense, Folium Ilicis Pubescentis, Fructus Trichosanthis young stem and leaf, the five tastes
Sub-tender leaf, after mix homogeneously, uses clear water drip washing, drains, then be placed in microwave green-killing device, and microwave operational frequencies is 180MHz,
Microwave output power is 12kw, and radiated time is 25min, and spreading for cooling is to room temperature；
(2) knead: the raw material after cooling is kneaded, raw material is placed in and rubs on plate, knead 15min, to raw material quality by hand
Deliquescing, distributes fragrance；It is re-fed in the drying room of 42 DEG C drying, is down to 12% to feed moisture content；
(3) fermentation: sent into by dried raw material in fermenting cellar, carries out dry fermentation 2 times under field conditions (factors), and the time is for the first time
2h, after drying, continues fermentation 4.5h；In the ratio of 1:0.1 raw material after dry fermentation adding green tea bacterium solution, fully after drying
Mix homogeneously, carries out wet fermentation, and the temperature of fermentation is 42 DEG C, and relative humidity is 40%, and fermentation time is 16h；
(4) extraction: the raw material after fermentation is carried out wall breaking pulverization, adds the deionized water of its weight 3.5 times, at 42 DEG C of constant temperature
Carry out backflow extraction 35min under water bath, be cooled to room temperature, filter to get filtrate and filtering residue, then filtering residue is added its weight 2 times
Deionized water under 55 DEG C of environment, carry out backflow extraction 25min, be cooled to room temperature, filter, merging filtrate, and at the ring of 65 DEG C
It is concentrated into the 18% of original volume under border, prepares Flos Firmianae (Flow Flos firmianae) lixiviating solution；By filtering residue dry after, waterproof pulverization be particle diameter be the Chinese parasol tree of 200 μm
Flos paulowniae mixed soil；
(5) Radix Glycyrrhizae pretreatment: choose fresh Radix Glycyrrhizae, is aided with Herba Hedyotis cantonensis, Cortex Moutan, cuts into slices after cleaning, and mix homogeneously puts into container
In, the pure water adding its weight 8 times soaks 5h, then uses break process, adds the cellulase and 0.2% of its weight 0.35%
Hemicellulose, be heated to 42 DEG C, united hydrolysis 55min, prepare Radix Glycyrrhizae hydrolysate；
(6) allotment: take the Flos Firmianae (Flow Flos firmianae) lixiviating solution of 25 weight portions, the Flos Firmianae (Flow Flos firmianae) mixed soil of 35 weight portions, the liquorice beverage of 20 weight portions
Solve thing, add the haw juice of 10 weight portions, the Semen Nelumbinis powder of 8 weight portions and the citric acid of 2 weight portions, after mix homogeneously, carry out
Vacuum and low temperature concentrates, and under the conditions of pressure 0.12MPa, temperature 48 DEG C, is concentrated into relative density 0.85g/cm3Concentrated solution；
(7) being dried: use syllogic to dry concentrated solution, first inferior to drying 25 minutes at 78 DEG C, second inferior to 50 DEG C at baking
Dry 35 minutes, drying 60 minutes at 42 DEG C for the third time, dry 30 minutes, interval between second time drying for the first time, for the second time
Dry and be spaced 35 minutes between third time drying, after pulverizing, prepare Flos Firmianae (Flow Flos firmianae) Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) health-protecting tea extract；
(8) packaging: after Flos Firmianae (Flow Flos firmianae) Dendranthemia capitata (Wall.) hutch. Hand (-Mazz.) X. D. Cui) health-protecting tea extract is arranged, pack with food stage packaging material, enter aeration-drying environment
Middle storage.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106879804A (en) * | 2017-03-17 | 2017-06-23 | 广西凌云县绿贵茶业有限公司 | A kind of preparation method of compound chrysanthemum tea |
| CN107518127A (en) * | 2017-08-22 | 2017-12-29 | 汪保华 | A kind of processing method of selfheal sophora flower tea |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105360838A (en) * | 2015-12-09 | 2016-03-02 | 郑州仁宏医药科技有限公司 | Rose beverage and preparation method thereof |
| CN105876027A (en) * | 2016-06-11 | 2016-08-24 | 彭超昀莉 | Making method of hawthorn fruit and anoectochilus roxburghii tea powder |
-
2016
- 2016-08-28 CN CN201610734400.4A patent/CN106306254A/en not_active Withdrawn
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105360838A (en) * | 2015-12-09 | 2016-03-02 | 郑州仁宏医药科技有限公司 | Rose beverage and preparation method thereof |
| CN105876027A (en) * | 2016-06-11 | 2016-08-24 | 彭超昀莉 | Making method of hawthorn fruit and anoectochilus roxburghii tea powder |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106879804A (en) * | 2017-03-17 | 2017-06-23 | 广西凌云县绿贵茶业有限公司 | A kind of preparation method of compound chrysanthemum tea |
| CN107518127A (en) * | 2017-08-22 | 2017-12-29 | 汪保华 | A kind of processing method of selfheal sophora flower tea |
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