CN106220905B - 一种提高烟用滴丸稳定性的滴丸包裹材料及其制备方法 - Google Patents
一种提高烟用滴丸稳定性的滴丸包裹材料及其制备方法 Download PDFInfo
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- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
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Abstract
本发明提供一种提高烟用滴丸稳定性的滴丸包裹材料及其制备方法。所述滴丸包裹材料是将海藻酸钠、明胶、阿拉伯胶用75±5℃的水搅拌0.5~2小时溶解,然后将过氧化物溶解在25±5℃的水中,搅拌0.5~2小时溶解,最后将溶解后的全部物料与过氧化物水溶液添加剩下的水混合均匀,置于具有加热夹层的反应罐中搅拌,夹层用蒸汽加热到75±5℃,搅拌1~2小时后,混合物充分互溶,再保温1~2小时,静置保温75±5℃条件下过滤,所得滤液即为能够提高烟用滴丸稳定性的滴丸包裹材料。本发明不易吸潮、脆性好、强度优,能够有效提高滴丸产品的外观质量和产品品质。
Description
技术领域
本发明属于卷烟技术领域,具体涉及一种提高烟用滴丸稳定性、用于烟用添加剂滴丸的包裹材料及其制备方法。
背景技术
现有技术中,本申请人专利申报“烟用添加剂滴丸包裹材料及用其包裹的滴丸及滴丸的应用”(CN102485777),“烟用添加剂滴丸的改进型包裹材料”(CN102485777),提供了一种能将烟用添加剂包裹起来的包裹材料,用它包裹添加剂制成滴丸,再将此滴丸应用于滤嘴棒中,制得一种含有烟用添加剂,能由消费者自行决定释放的滤嘴棒。上述专利申请经一段时间试用后,发现其存在缺陷:滴丸在成型后添加到卷烟滤棒中,经存储、流通等多个环节后到消费者手中,一般会至少经历3-6个月时间,这段时间滴丸容易受到环境的影响,吸收水分而变软。一方面,滴丸表现得脆性减弱,不易捏破;另一方面,滴丸在滤棒中不易寻找,影响消费者的感官体验。
自由基引发剂,简称引发剂。指一类容易受热分解成自由基(即初级自由基)的化合物,可用于引发烯类、双烯类单体的自由基聚合和共聚合反应,也可用于不饱和聚酯的交联固化和高分子交联反应。自由基聚合是研究最早、工业化应用最广泛的聚合反应。与其他聚合历程相比,自由基聚合具有单体来源广泛、工艺简单、价格低廉、产品丰富的特点,因而一直受到人们的重视。
自由基引发剂(initiators for free radical polymerization)的分类,有多种分类方法,按引发剂的分子结构,可以分为偶氮类、过氧类和氧化还原类。也可以按照其溶解性能分为水溶性引发剂(如无机类的过硫酸盐、过氧化氢、水溶偶氮引发剂等)和油溶性(溶于单体或有机溶剂)的有机类引发剂。
过氧化合物是含有过氧基(—O—O—)的一类化合物,受热后—O—O—键断裂,分裂成两个相应的自由基,从而引发单体聚合,称为过氧化物引发剂。分无机过氧化物和有机过氧物两类。无机过氧化物引发剂,有过氧化氢、过硫酸铵或过硫酸钾等,可溶于水,用作水溶液聚合、乳液聚合的引发剂。
发明内容
针对现有技术的上述不足,本发明要解决的技术问题是提供一种提高烟用添加剂滴丸稳定性的滴丸包裹材料及其制备方法,该包裹材料是滴丸配方中添加一种过氧化物引发剂,通过产生氧化聚合反应,将滴丸胶皮的分子量聚合增大,从而产生大分子的聚合物。大分子聚合物对环境的适应性要明显优于小分子的明胶等物质,不易吸潮、脆性好、强度优,能够有效提高滴丸产品的外观质量和产品品质。
本发明的技术方案是:一种提高烟用滴丸稳定性的滴丸包裹材料,是由以下组份和重量份的原料组成:
上述物质的总重量份数为100份。
其中,所述过氧化物包括:过氧化氢、过氧化钠、过氧化钾、过氧化钙、过氧化镁、过氧化锌、过硫酸氢钾、过氧化锶、过硫酸铵、过硫酸钾、过碳酸钠中的任意一种或几种;
所述的海藻酸钠的粘度为5~50mPa.s;
所述的阿拉伯胶的粘度为50~150mPa.s;
所述的明胶的粘度为20~80mPa.s。
所述水为纯净水。
本发明提供一种提高烟用滴丸稳定性的滴丸包裹材料的制备方法,其特征在于具体步骤如下:
(1)将上述配方中的2~20重量份的海藻酸钠、2~20重量份的明胶和2~20重量份的阿拉伯胶采用20~40重量份的75±5℃水中,搅拌0.5~2小时溶解成胶液;
(2)将上述配方中的0.5~5重量份的过氧化物加入5~10重量份的25±5℃水中,搅拌0.5~2小时溶解成过氧化物水溶液;
(3)将步骤(1)中溶解后的全部胶液与步骤(2)中的过氧化物水溶液添加25~40重量份的水混合均匀,置于具有加热夹层的反应罐中搅拌,夹层用蒸汽加热到75±5℃,搅拌1~2小时后,混合物充分互溶,再保温1~2小时,静置,待泡沫上浮后,保温75±5℃条件下过滤,所得滤液即为能够提高烟用滴丸稳定性的滴丸包裹材料。
本发明较优的技术方案:所述步骤(1)中的胶液,是将海藻酸钠、明胶和阿拉伯胶分别采用75±5℃水、搅拌0.5~2小时溶解形成海藻酸钠溶液、明胶溶液和阿拉伯胶溶液,或将海藻酸钠、明胶和阿拉伯胶同时加入75±5℃的水中、搅拌0.5~2小时溶解形成混合胶溶液。
本发明的优点:本发明在滴丸配方中添加一种过氧化物引发剂,通过产生氧化聚合反应,将滴丸胶皮的分子量聚合增大,从而产生大分子的聚合物,大分子聚合物对环境的适应性要明显优于小分子的明胶等物质,不易吸潮、脆性好、强度优,能够有效提高滴丸产品的外观质量和产品品质。采用本发明中的配方滴制得到的滴丸在硬度、脆度及环境适应性方面具有极大改善,显著提高了产品外观及物理性能品质。
具体实施方式
下面结合实施例对本发明的具体实施方式作进一步详细的描述。以下实施例均为实验室数据。
实施例1:一种提高烟用滴丸稳定性的滴丸包裹材料,具体配方如下:
其制备方法为:首先将上述配方中的10重量份的海藻酸钠、10重量份的明胶和10重量份的阿拉伯胶用30重量份、75±5℃的水搅拌0.5小时溶解,然后将0.5重量份的过硫酸铵溶解在5重量份、25±5℃的水中,搅拌0.5小时,最后将溶解后的全部物料与过硫酸铵水溶液添加34.5重量份的水混合均匀,置于具有加热夹层的反应罐中搅拌,夹层用蒸汽加热到75±5℃,搅拌1小时后,混合物充分互溶,再保温1小时,静置,待泡沫上浮后,保温75±5℃条件下过滤,所得滤液即为能够提高烟用滴丸稳定性的滴丸包裹材料。使用DWJSYJ-I型小胶丸滴丸机滴制出滴丸。本发明所使用的滴制机是现有技术已有的,本发明借用其完成本发明的任务。
实施例2:一种提高烟用滴丸稳定性的滴丸包裹材料,具体配方如下:
名称 | 规格 | 比例份数 |
海藻酸钠 | 粘度(mpa.s)30 | 5 |
明胶 | 粘度(mpa.s)40 | 8 |
阿拉伯胶 | 粘度(mpa.s)100 | 9 |
过硫酸铵 | 食品级 | 1 |
过氧化氢 | 食品级 | 2 |
水 | 纯净水 | 75 |
其制备方法为:首先将上述配方中的5重量份的海藻酸钠、8重量份的明胶和9重量份的阿拉伯胶分别用10重量份、75±5℃的水搅拌1小时溶解,然后将1重量份的过硫酸铵和2重量份的过氧化氢溶解在10重量份、25±5℃的水中,搅拌1小时,最后将溶解后的全部物料与过氧化物水溶液添加35重量份的水混合均匀,置于具有加热夹层的反应罐中搅拌,夹层用蒸汽加热到75±5℃,搅拌1小时后,混合物充分互溶,再保温1小时,静置,待泡沫上浮后,保温75±5℃条件下过滤,所得滤液即为能够提高烟用滴丸稳定性的滴丸包裹材料。使用DWJSYJ-I型小胶丸滴丸机滴制出滴丸。本发明所使用的滴制机是现有技术已有的,本发明借用其完成本发明的任务。
实施例3:一种提高烟用滴丸稳定性的滴丸包裹材料,具体配方如下:
名称 | 规格 | 比例份数 |
海藻酸钠 | 粘度(mpa.s)40 | 9 |
明胶 | 粘度(mpa.s)40 | 5 |
阿拉伯胶 | 粘度(mpa.s)120 | 9 |
过硫酸铵 | 食品级 | 2 |
过氧化钠 | 食品级 | 3 |
过氧化氢 | 食品级 | 2 |
水 | 纯净水 | 70 |
其制备方法为:首先将上述配方中的9重量份的海藻酸钠、5重量份的明胶和9重量份的阿拉伯胶采用40重量份、75±5℃的水搅拌2小时溶解,然后将2重量份的过硫酸铵、3重量份的过硫酸铵和2重量份的过氧化氢溶解在10重量份、25±5℃的水中,搅拌2小时,最后将溶解后的全部物料与过氧化物水溶液添加20重量份的水混合均匀,置于具有加热夹层的反应罐中搅拌,夹层用蒸汽加热到75±5℃,搅拌2小时后,混合物充分互溶,再保温2小时,静置,待泡沫上浮后,保温75±5℃条件下过滤,所得滤液即为能够提高烟用滴丸稳定性的滴丸包裹材料。使用DWJSYJ-I型小胶丸滴丸机滴制出滴丸。本发明所使用的滴制机是现有技术已有的,本发明借用其完成本发明的任务。
上述实施例中制得的滴丸脆性较好,硬度较高,依据2007年明胶空心胶囊标准与2010年版《中国药典》方法进行测定,具体结果如下:
序号 | 硬度 | 脆度值 |
原产品 | 4N | 60% |
实施例1 | 5.2N | 85% |
实施例2 | 5.0N | 80% |
实施例3 | 5.3N | 90% |
按照上述实施例制备的滴丸在温度20℃±2℃,湿度80%的恒温恒湿箱中放置48小时,水分由常温常湿条件下的1.0%分别上升为1.25%、1.27%、1.08%,原产品水分由1.0%上升为3.5%,烟用滴丸对环境的适应性和稳定性明显提升。滴丸在破裂时,发出清脆“啪”的声音。
Claims (3)
1.一种提高烟用滴丸稳定性的滴丸包裹材料,是由以下组份和重量份的原料组成:
其中,所述过氧化物包括:过氧化氢、过氧化钠、过氧化钾、过氧化钙、过氧化镁、过氧化锌、过硫酸氢钾、过氧化锶、过硫酸铵、过硫酸钾、过碳酸钠中的任意一种或几种;
所述的海藻酸钠的粘度为5~50mPa.s;
所述的阿拉伯胶的粘度为50~150mPa.s;
所述的明胶的粘度为20~80mPa.s。
2.一种权利要求1中所述的提高烟用滴丸稳定性的滴丸包裹材料的制备方法,其特征在于具体步骤如下:
(1)将上述配方中的2~20重量份的海藻酸钠、2~20重量份的明胶和2~20重量份的阿拉伯胶采用20~40重量份的75±5℃水中,搅拌0.5~2小时溶解成胶液;
(2)将上述配方中的0.5~5重量份的过氧化物加入5~10重量份的25±5℃水中,搅拌0.5~2小时溶解成过氧化物水溶液;
(3)将步骤(1)中溶解后的全部胶液与步骤(2)中的过氧化物水溶液添加25~40重量份的水混合均匀,置于具有加热夹层的反应罐中搅拌,夹层用蒸汽加热到75±5℃,搅拌1~2小时后,混合物充分互溶,再保温1~2小时,静置,待泡沫上浮后,保温75±5℃条件下过滤,所得滤液即为能够提高烟用滴丸稳定性的滴丸包裹材料。
3.根据权利要求2所述的一种提高烟用滴丸稳定性的滴丸包裹材料的制备方法,其特征在于:所述步骤(1)中的胶液,是将海藻酸钠、明胶和阿拉伯胶分别采用75±5℃水、搅拌0.5~2小时溶解形成海藻酸钠溶液、明胶溶液和阿拉伯胶溶液,或将海藻酸钠、明胶和阿拉伯胶同时加入75±5℃的水中、搅拌0.5~2小时溶解形成混合胶溶液。
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