CN106198125A - A kind of gas extraction and collection device - Google Patents

A kind of gas extraction and collection device Download PDF

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Publication number
CN106198125A
CN106198125A CN201610762022.0A CN201610762022A CN106198125A CN 106198125 A CN106198125 A CN 106198125A CN 201610762022 A CN201610762022 A CN 201610762022A CN 106198125 A CN106198125 A CN 106198125A
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collection
heat conduction
cup
gas extraction
collection device
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乔永平
赵林
姚继敏
庞强强
杜二计
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Northwest Institute of Eco Environment and Resources of CAS
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Cold and Arid Regions Environmental and Engineering Research Institute of CAS
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/22Devices for withdrawing samples in the gaseous state
    • G01N1/2273Atmospheric sampling
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/42Low-temperature sample treatment, e.g. cryofixation
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/22Devices for withdrawing samples in the gaseous state
    • G01N2001/2282Devices for withdrawing samples in the gaseous state with cooling means

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Engineering & Computer Science (AREA)
  • Biomedical Technology (AREA)
  • Molecular Biology (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

本发明公开了一种气体提取与收集装置,收集杯、导热板及冷阱,收集杯固定设置在导热板上,导热板设置于冷阱的顶端封口处;收集杯包括有杯体和顶盖,顶盖固定连接在杯体的顶端,导热板底端固定连接有若干导热管,导热管置于冷阱中。本发明中的气体提取与收集装置,设置导热板及多个导热管同时对收集杯进行制冷,效率更快;将收集杯设置成横截面为底边长顶边短的梯形,有利于增大收集杯与导热板的接触面积,缩短降温时间,提高工作效率,保护套的设置由于对收集杯进行制冷以后其表面温度较低,为了避免操作人员冻伤而通过保护套去拿去收集杯。

The invention discloses a gas extraction and collection device, a collection cup, a heat conduction plate and a cold trap, the collection cup is fixedly arranged on the heat conduction plate, and the heat conduction plate is arranged at the top seal of the cold trap; the collection cup includes a cup body and a top cover , the top cover is fixedly connected to the top of the cup body, the bottom of the heat conduction plate is fixedly connected with several heat conduction pipes, and the heat conduction pipes are placed in the cold trap. The gas extraction and collection device in the present invention is equipped with a heat conduction plate and a plurality of heat conduction tubes to cool the collection cup at the same time, and the efficiency is faster; the cross section of the collection cup is set as a trapezoid with a long bottom side and a short top side, which is beneficial to increase The contact area between the collection cup and the heat conduction plate shortens the cooling time and improves the work efficiency. The protective sleeve is installed because the surface temperature of the collection cup is lower after cooling. In order to avoid frostbite for the operator, take the collection cup through the protective sleeve.

Description

一种气体提取与收集装置A gas extraction and collection device

技术领域technical field

本发明涉及水汽收集技术领域,特别是涉及一种气体提取与收集装置。The invention relates to the technical field of water vapor collection, in particular to a gas extraction and collection device.

背景技术Background technique

水汽是指存在于大气中呈气态的水,其对全球生态、气候、环境具有重要意义。水汽的扩散与输送,是地球上水循环的重要环节,是将海水、陆地水与空中水联系在一起的纽带。正是通过扩散运动,使得海水和陆地水源源不断地蒸发升入空中,并随气流输送到全球各地,再凝结并以降水的形式回归到海洋和陆地。Water vapor refers to the gaseous water existing in the atmosphere, which is of great significance to the global ecology, climate and environment. The diffusion and transportation of water vapor is an important part of the water cycle on the earth, and it is the link that connects sea water, land water and air water. It is through the diffusion movement that the seawater and land water are continuously evaporated into the air, transported to all parts of the world with the air current, condensed and returned to the ocean and land in the form of precipitation.

在我国,水汽的提取与收集研究中,对青藏高原的寒冷及多年冰冻层的环境进行水汽的提取与收集研究具有更加重要的意义。但由于青藏高原环境的复杂,大型的气体提取与收集装置会给科考人员带来极大的不便,且现有的气体提取与收集装置收集效果较差,收集时间较长,从而降低了科研的效率。In my country, in the study of water vapor extraction and collection, it is more important to study the extraction and collection of water vapor in the cold and perennial frozen environment of the Qinghai-Tibet Plateau. However, due to the complex environment of the Qinghai-Tibet Plateau, large-scale gas extraction and collection devices will bring great inconvenience to scientific research personnel, and the existing gas extraction and collection devices have poor collection effect and long collection time, which reduces the scientific research. s efficiency.

因此,对于科研者来说,研制一种适用于青藏高原及其他寒冷地带的气体提取与收集装置,成为当前十分紧迫的需求。Therefore, for researchers, the development of a gas extraction and collection device suitable for the Qinghai-Tibet Plateau and other cold regions has become a very urgent demand at present.

发明内容Contents of the invention

本发明的目的是提供一种气体提取与收集装置,以解决上述现有技术存在的问题,使得该气体提取与收集装置加工制造简单,方便携带,同时具有较高的收集效率。The object of the present invention is to provide a gas extraction and collection device to solve the above-mentioned problems in the prior art, so that the gas extraction and collection device is easy to manufacture, easy to carry, and has high collection efficiency.

为实现上述目的,本发明提供了如下方案:本发明提供一种气体提取与收集装置,其特征在于:收集杯、导热板及冷阱,所述收集杯固定设置在所述导热板上,所述导热板设置于所述冷阱的顶端封口处;所述收集杯包括有杯体和顶盖,所述顶盖固定连接在所述杯体的顶端,所述导热板底端固定连接有若干导热管,所述导热管置于所述冷阱中。In order to achieve the above object, the present invention provides the following scheme: the present invention provides a gas extraction and collection device, which is characterized in that: a collection cup, a heat conduction plate and a cold trap, the collection cup is fixedly arranged on the heat conduction plate, the The heat conduction plate is arranged at the top seal of the cold trap; the collection cup includes a cup body and a top cover, the top cover is fixedly connected to the top of the cup body, and the bottom end of the heat conduction plate is fixedly connected with several A heat pipe, the heat pipe is placed in the cold trap.

可选的,所述收集杯的横截面为底边长顶边短的梯形。Optionally, the cross section of the collection cup is a trapezoid with a long bottom side and a short top side.

可选的,所述收集杯采用不锈钢材质。Optionally, the collection cup is made of stainless steel.

可选的,所述顶盖包括胶塞和手柄,所述手柄固定设置在所述胶塞顶端中央,所述杯体与所述顶盖的胶塞连接处设置有一密封圈。Optionally, the top cover includes a rubber plug and a handle, the handle is fixedly arranged at the center of the top end of the rubber plug, and a sealing ring is provided at the joint between the cup and the top cover.

可选的,所述导热板与所述导热管均采用紫铜材质。Optionally, both the heat conduction plate and the heat conduction pipe are made of red copper.

可选的,所述收集杯外侧包裹有一层保护套。Optionally, a protective sheath is wrapped on the outside of the collection cup.

可选的,所述冷阱的腔室内容置有冷介质。Optionally, a cold medium is placed in the chamber of the cold trap.

可选的,所述冷介质为液氮。Optionally, the cold medium is liquid nitrogen.

本发明相对于现有技术取得了以下技术效果:Compared with the prior art, the present invention has achieved the following technical effects:

本发明中的气体提取与收集装置,设置导热板及多个导热管同时对收集杯进行制冷,效率更快;将收集杯设置成横截面为底边长顶边短的梯形,有利于增大收集杯与导热板的接触面积,缩短降温时间,提高工作效率,保护套的设置由于对收集杯进行制冷以后其表面温度较低,为了避免操作人员冻伤而通过保护套去拿去收集杯。The gas extraction and collection device in the present invention is equipped with a heat conduction plate and a plurality of heat conduction tubes to cool the collection cup at the same time, and the efficiency is faster; the cross section of the collection cup is set as a trapezoid with a long bottom side and a short top side, which is beneficial to increase The contact area between the collection cup and the heat conduction plate shortens the cooling time and improves the work efficiency. The setting of the protective cover is because the surface temperature of the collection cup is lower after cooling.

附图说明Description of drawings

为了更清楚地说明本发明实施例或现有技术中的技术方案,下面将对实施例中所需要使用的附图作简单地介绍,显而易见地,下面描述中的附图仅仅是本发明的一些实施例,对于本领域普通技术人员来讲,在不付出创造性劳动性的前提下,还可以根据这些附图获得其他的附图。In order to more clearly illustrate the technical solutions in the embodiments of the present invention or the prior art, the following will briefly introduce the accompanying drawings required in the embodiments. Obviously, the accompanying drawings in the following description are only some of the present invention. Embodiments, for those of ordinary skill in the art, other drawings can also be obtained according to these drawings without paying creative labor.

图1为本发明气体提取与收集装置的整体结构示意图;Fig. 1 is the overall structure schematic diagram of the gas extraction and collection device of the present invention;

其中,1手柄;2胶塞;3保护套;4收集杯;5导热板;6导热管;7冷阱;8密封圈。Among them, 1 handle; 2 rubber plug; 3 protective cover; 4 collecting cup; 5 heat conducting plate; 6 heat conducting pipe; 7 cold trap; 8 sealing ring.

具体实施方式detailed description

下面将结合本发明实施例中的附图,对本发明实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本发明一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。The following will clearly and completely describe the technical solutions in the embodiments of the present invention with reference to the accompanying drawings in the embodiments of the present invention. Obviously, the described embodiments are only some, not all, embodiments of the present invention. Based on the embodiments of the present invention, all other embodiments obtained by persons of ordinary skill in the art without making creative efforts belong to the protection scope of the present invention.

本发明的目的是提供一种气体提取与收集装置,以解决上述现有技术存在的问题,使得该气体提取与收集装置加工制造简单,方便携带,同时具有较高的收集效率。The object of the present invention is to provide a gas extraction and collection device to solve the above-mentioned problems in the prior art, so that the gas extraction and collection device is easy to manufacture, easy to carry, and has high collection efficiency.

为使本发明的上述目的、特征和优点能够更加明显易懂,下面结合附图和具体实施方式对本发明作进一步详细的说明。In order to make the above objects, features and advantages of the present invention more comprehensible, the present invention will be further described in detail below in conjunction with the accompanying drawings and specific embodiments.

请参考图1,其中,图1为本发明气体提取与收集装置的整体结构示意图。Please refer to FIG. 1 , wherein FIG. 1 is a schematic diagram of the overall structure of the gas extraction and collection device of the present invention.

实施例一Embodiment one

如图1所示,本实施例提供一种气体提取与收集装置,收集杯4、导热板5及冷阱7,收集杯4固定设置在导热板5上,导热板5设置于冷阱7的顶端封口处;收集杯4包括有杯体和顶盖,顶盖固定连接在杯体的顶端,导热板5底端固定连接有若干导热管6,导热管6置于所述冷阱7中。As shown in Figure 1, the present embodiment provides a gas extraction and collection device, a collection cup 4, a heat conduction plate 5 and a cold trap 7, the collection cup 4 is fixedly arranged on the heat conduction plate 5, and the heat conduction plate 5 is arranged on the bottom of the cold trap 7 At the top seal; the collection cup 4 includes a cup body and a top cover, the top cover is fixedly connected to the top of the cup body, and the bottom end of the heat conducting plate 5 is fixedly connected with some heat conducting pipes 6, and the heat conducting pipes 6 are placed in the cold trap 7.

本实施例中的气体提取与收集装置,将收集杯4的顶盖固定密封的安装在杯体上以后,将收集杯4放置在导热板5上,通过冷阱7对导热板5进行制冷,多根导热管6的设置有助于快速地对导热板5进行制冷及冷传递,然后根据热传导的原理,收集杯4的温度也会随着导热板5温度的降低逐步降低,直到收集杯4的内壁及底面出现气体的液化;完成气体的提取与收集后,将收集杯4从导热板5上取下,打开收集杯4的顶盖,即可得到样品,操作人员可对样品进行后续的实验操作。In the gas extraction and collection device in this embodiment, after the top cover of the collection cup 4 is fixed and sealed on the cup body, the collection cup 4 is placed on the heat conduction plate 5, and the heat conduction plate 5 is refrigerated by the cold trap 7, The arrangement of a plurality of heat conducting pipes 6 helps to quickly cool and transfer heat to the heat conducting plate 5, and then according to the principle of heat conduction, the temperature of the collecting cup 4 will gradually decrease as the temperature of the heat conducting plate 5 decreases until the collecting cup 4 Liquefaction of gas occurs on the inner wall and bottom surface of the gas; after the extraction and collection of the gas is completed, the collection cup 4 is removed from the heat conduction plate 5, and the top cover of the collection cup 4 is opened to obtain the sample. Experimental operation.

实施例二Embodiment two

如图1所示,本实施例提供一种气体提取与收集装置,在实施例一的基础上,本实施例中的气体提取与收集装置还具有以下特点:As shown in Figure 1, this embodiment provides a gas extraction and collection device. On the basis of Embodiment 1, the gas extraction and collection device in this embodiment also has the following characteristics:

收集杯4的横截面为底边长顶边短的梯形,即增大收集杯4与导热板5的接触面积,加快能量的传递,实现收集杯4的快速降温。The cross-section of the collection cup 4 is a trapezoid with a long bottom and a short top side, which increases the contact area between the collection cup 4 and the heat conducting plate 5, speeds up the energy transfer, and realizes rapid cooling of the collection cup 4.

收集杯4采用不锈钢材质,收集杯4的杯壁为中空的,在收集杯4的中空腔室内添加有冷媒剂,对收集杯4的制冷起到一定的辅助作用,加快对收集杯4温度的降低。The collection cup 4 is made of stainless steel, and the wall of the collection cup 4 is hollow. A refrigerant agent is added in the hollow chamber of the collection cup 4, which plays a certain auxiliary role in the cooling of the collection cup 4 and accelerates the cooling of the collection cup 4 temperature. reduce.

顶盖包括胶塞2和手柄1,手柄1固定设置在胶塞2顶端中央,杯体与顶盖的胶塞2连接处设置有一密封圈8;胶塞2相对于螺纹连接其密封性更好,然后在杯体与胶塞2的连接处再设置一密封圈8起到二次密封作用,通过手柄1的设置,在气体收集完成后可以较容易的将胶塞2取下。The top cover includes a rubber plug 2 and a handle 1. The handle 1 is fixed at the center of the top of the rubber plug 2, and a sealing ring 8 is provided at the connection between the cup body and the top cover of the rubber plug 2; the rubber plug 2 has better sealing performance than the threaded connection. , and then set a sealing ring 8 at the connection between the cup body and the rubber plug 2 to play a secondary sealing role. Through the setting of the handle 1, the rubber plug 2 can be easily removed after the gas collection is completed.

导热板5与导热管6均采用紫铜材质。Both the heat conducting plate 5 and the heat conducting pipe 6 are made of red copper.

收集杯4外侧包裹有一层保护套3,由于在气体的收集过程中收集杯4温度降低,操作人员在气体收集完成后拿去收集杯4时保护套3起到保护作用,防止冻伤。The outside of the collection cup 4 is wrapped with a protective cover 3. Since the temperature of the collection cup 4 decreases during the gas collection process, the protective cover 3 plays a protective role when the operator removes the collection cup 4 after the gas collection is completed, preventing frostbite.

冷阱7的腔室内容置有冷介质,该冷介质采用液氮。A cold medium is housed in the chamber of the cold trap 7, and the cold medium adopts liquid nitrogen.

本发明中应用了具体个例对本发明的原理及实施方式进行了阐述,以上实施例的说明只是用于帮助理解本发明的方法及其核心思想;同时,对于本领域的一般技术人员,依据本发明的思想,在具体实施方式及应用范围上均会有改变之处。综上所述,本说明书内容不应理解为对本发明的限制。In the present invention, specific examples have been used to illustrate the principle and implementation of the present invention. The description of the above embodiments is only used to help understand the method and core idea of the present invention; meanwhile, for those of ordinary skill in the art, according to the present invention The idea of the invention will have changes in the specific implementation and scope of application. In summary, the contents of this specification should not be construed as limiting the present invention.

Claims (8)

1.一种气体提取与收集装置,其特征在于:收集杯、导热板及冷阱,所述收集杯固定设置在所述导热板上,所述导热板设置于所述冷阱的顶端封口处;所述收集杯包括有杯体和顶盖,所述顶盖固定连接在所述杯体的顶端,所述导热板底端固定连接有若干导热管,所述导热管置于所述冷阱中。1. A gas extraction and collection device, characterized in that: a collection cup, a heat conduction plate and a cold trap, the collection cup is fixedly arranged on the heat conduction plate, and the heat conduction plate is arranged at the top seal of the cold trap The collecting cup includes a cup body and a top cover, the top cover is fixedly connected to the top of the cup body, and the bottom end of the heat conducting plate is fixedly connected with some heat conducting pipes, and the heat conducting pipes are placed in the cold trap middle. 2.根据权利要求1所述的一种气体提取与收集装置,其特征在于:所述收集杯的横截面为底边长顶边短的梯形。2. A gas extraction and collection device according to claim 1, characterized in that: the cross section of the collection cup is a trapezoid with a long bottom side and a short top side. 3.根据权利要求1所述的一种气体提取与收集装置,其特征在于:所述收集杯采用不锈钢材质。3. A gas extraction and collection device according to claim 1, wherein the collection cup is made of stainless steel. 4.根据权利要求1所述的一种气体提取与收集装置,其特征在于:所述顶盖包括胶塞和手柄,所述手柄固定设置在所述胶塞顶端中央,所述杯体与所述顶盖的胶塞连接处设置有一密封圈。4. A gas extraction and collection device according to claim 1, characterized in that: the top cover includes a rubber plug and a handle, the handle is fixed at the center of the top of the rubber plug, and the cup body and the A sealing ring is arranged at the rubber plug joint of the top cover. 5.根据权利要求1所述的一种气体提取与收集装置,其特征在于:所述导热板与所述导热管均采用紫铜材质。5 . The gas extraction and collection device according to claim 1 , wherein the heat conduction plate and the heat conduction pipe are both made of red copper. 6 . 6.根据权利要求1所述的一种气体提取与收集装置,其特征在于:所述收集杯外侧包裹有一层保护套。6. A gas extraction and collection device according to claim 1, characterized in that: the outer side of the collection cup is wrapped with a protective sheath. 7.根据权利要求1所述的一种气体提取与收集装置,其特征在于:所述冷阱的腔室内容置有冷介质。7. A gas extraction and collection device according to claim 1, characterized in that: a cold medium is placed in the chamber of the cold trap. 8.根据权利要求7所述的一种气体提取与收集装置,其特征在于:所述冷介质为液氮。8. A gas extraction and collection device according to claim 7, characterized in that: the cold medium is liquid nitrogen.
CN201610762022.0A 2016-08-30 2016-08-30 A kind of gas extraction and collection device Pending CN106198125A (en)

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CN111479950A (en) * 2017-12-14 2020-07-31 安赛乐米塔尔公司 Vacuum deposition apparatus and method for coating a substrate
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KR20220080810A (en) * 2020-12-07 2022-06-15 (주)씨엠디엘 Apparatus for evaluating thermal characteristics of OLED materials
KR102477821B1 (en) 2020-12-07 2022-12-16 (주)씨엠디엘 Apparatus for evaluating thermal characteristics of OLED materials

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Application publication date: 20161207