CN106166804A - A kind of reclaimed rubber thick refining plasticizing system and thick smelting method thereof - Google Patents

A kind of reclaimed rubber thick refining plasticizing system and thick smelting method thereof Download PDF

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Publication number
CN106166804A
CN106166804A CN201610384680.0A CN201610384680A CN106166804A CN 106166804 A CN106166804 A CN 106166804A CN 201610384680 A CN201610384680 A CN 201610384680A CN 106166804 A CN106166804 A CN 106166804A
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CN
China
Prior art keywords
micelle
puddler
stirring
steam
elevator
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Granted
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CN201610384680.0A
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Chinese (zh)
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CN106166804B (en
Inventor
陈立奇
王冠楠
陈东军
王溥宁
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Suqian Jingxian Technology Co ltd
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JIANGSU HUAXING RUBBER SCIENCE & TECHNOLOGY Co Ltd
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Priority to CN201610384680.0A priority Critical patent/CN106166804B/en
Publication of CN106166804A publication Critical patent/CN106166804A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29BPREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00Mixing; Kneading
    • B29B7/74Mixing; Kneading using other mixers or combinations of mixers, e.g. of dissimilar mixers ; Plant
    • B29B7/7476Systems, i.e. flow charts or diagrams; Plants
    • B29B7/748Plants
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29BPREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00Mixing; Kneading
    • B29B7/02Mixing; Kneading non-continuous, with mechanical mixing or kneading devices, i.e. batch type
    • B29B7/06Mixing; Kneading non-continuous, with mechanical mixing or kneading devices, i.e. batch type with movable mixing or kneading devices
    • B29B7/10Mixing; Kneading non-continuous, with mechanical mixing or kneading devices, i.e. batch type with movable mixing or kneading devices rotary
    • B29B7/18Mixing; Kneading non-continuous, with mechanical mixing or kneading devices, i.e. batch type with movable mixing or kneading devices rotary with more than one shaft
    • B29B7/20Mixing; Kneading non-continuous, with mechanical mixing or kneading devices, i.e. batch type with movable mixing or kneading devices rotary with more than one shaft with intermeshing devices, e.g. screws
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29BPREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00Mixing; Kneading
    • B29B7/74Mixing; Kneading using other mixers or combinations of mixers, e.g. of dissimilar mixers ; Plant
    • B29B7/7476Systems, i.e. flow charts or diagrams; Plants
    • B29B7/7495Systems, i.e. flow charts or diagrams; Plants for mixing rubber
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29BPREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00Mixing; Kneading
    • B29B7/80Component parts, details or accessories; Auxiliary operations
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29BPREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B7/00Mixing; Kneading
    • B29B7/80Component parts, details or accessories; Auxiliary operations
    • B29B7/88Adding charges, i.e. additives
    • B29B7/94Liquid charges
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J11/00Recovery or working-up of waste materials
    • C08J11/04Recovery or working-up of waste materials of polymers
    • C08J11/10Recovery or working-up of waste materials of polymers by chemically breaking down the molecular chains of polymers or breaking of crosslinks, e.g. devulcanisation
    • C08J11/18Recovery or working-up of waste materials of polymers by chemically breaking down the molecular chains of polymers or breaking of crosslinks, e.g. devulcanisation by treatment with organic material
    • C08J11/20Recovery or working-up of waste materials of polymers by chemically breaking down the molecular chains of polymers or breaking of crosslinks, e.g. devulcanisation by treatment with organic material by treatment with hydrocarbons or halogenated hydrocarbons
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2317/00Characterised by the use of reclaimed rubber
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/50Reuse, recycling or recovery technologies
    • Y02W30/62Plastics recycling; Rubber recycling

Abstract

A kind of reclaimed rubber thick refining plasticizing system and thick smelting method thereof, wherein, including trough, the first elevator, pretreatment blender, micelle connecting gear, desulfurizing machine, the second elevator and receiving vat, before manufacture waste rubber powder is carried out pretreatment, use special rabbling mechanism that it is broken up, tentatively realize waste rubber powder and change to graininess micelle;By special micelle connecting gear, synchronize spray water steam and softening agent, realize rubber powder granule, do not crack and fully admix softening agent during transmitting.Use the multiple thick smelting method of twice stirring, twice softening, twice desulfurization, thus be continuously finished micelle macromolecules cross-linking network structure opening and stoping anti-process to short chain molecule structure, be greatly promoted properties of product.Improve using effect.

Description

A kind of reclaimed rubber thick refining plasticizing system and thick smelting method thereof
Technical field
The present invention relates to the thick refining plasticizing system of a kind of reclaimed rubber and thick smelting method thereof.
Background technology
At present, China is the rubber-consumer big country that the world is the first, but domestic rubber sources is the deficientest, more than 70% Natural rubber dependence on import, the recycling utilization of waste old is significant to the scarcity filling up rubber sources.Screw Extrusion Method is a kind of Novel waste rubber regeneration method, utilize screw extruder make rubber powder through mechanical shearing, regenerative agent, activator comprehensive Effect, obtains higher flexibility at short notice, so that scrap rubber regeneration, its production technology is simple, does not produce new pollution, It is easily achieved industrialization, and regenerating waste or used rubber effect is preferable.
Currently used Plasticator all takes the mode of cage to de-connect rubber powder, does not carry out rubber powder before de-connecting Pretreatment, therefore rubber powder realizes graininess shapewear when changing in cage, and cage easily occurs as high-temperature space machinery Phenomenon viscous, stifled, constrains enterprises production efficiency.
In process of production, owing to there is air, micelle and air contact inside machine, splitting easily occurs in high temperature micelle The phenomenon solving, aoxidizing;In waste rubber powder regenerative process, rubber powder needs chain rupture, softening, it is therefore desirable to be quantitatively adding softening agent, mesh The method of front employing is to spray softening agent at charging aperture, but in use finds that the use of this kind of mode can not be good Admix with micelle, finally finished product is impacted.
Summary of the invention
For overcoming the defect of prior art, it is an object of the invention to provide the thick refining plasticizing system of a kind of reclaimed rubber and Thick smelting method, carries out pretreatment to waste rubber powder before manufacture, uses special rabbling mechanism to break up it, the most in fact Existing waste rubber powder changes to graininess micelle;By special micelle connecting gear, synchronize spray water steam and softening agent, passing Realize rubber powder granule during sending, do not crack and fully admix softening agent.
The present invention solves technical problem and adopts the following technical scheme that
A kind of reclaimed rubber is with slightly refining plasticizing system, and wherein, including two retable unit and receiving vats, described plasticizing unit includes putting Hopper, the first elevator, pretreatment blender, micelle connecting gear, desulfurizing machine and the second elevator, described second retable The receiving vat of unit is positioned at below the second elevator discharging opening of the first retable unit, the second lifting of the second retable unit Being provided with receiving vat below machine discharging opening, described trough is chamfered edge bench-type structure, described trough connects described first and promotes Machine, described first elevator is provided with elevator discharging opening, and described pretreatment blender is positioned at orientation under described first elevator Put;
Described pretreatment blender includes blender housing and rabbling mechanism, the described cylindrical structure of blender housing bottom, Top is outward-dipping, opening-like;Described rabbling mechanism quantity is two, is symmetricly set in described blender housing both sides, institute State rabbling mechanism and include shaft, stirring motor, the first puddler, the second puddler, the 3rd puddler and connecting rod;Described electricity Machine quantity is two, is installed on described blender hull outside both sides, and described shaft one end connects described motor, and the other end is stretched Entering blender enclosure interior and connect the center of described first puddler, described connecting rod one end connects the first puddler, separately One end connects the 3rd puddler, and described second puddler is connected in described connecting rod, and described second puddler is positioned at described the Between three puddlers and the first puddler;The two ends of described first, second, third puddler are equipped with stirring flanging, described in stir Mix flanging to be inclined to set, described stirring flanging and described first puddler, the second puddler, the 3rd puddler angle A It it is 120 degree;Being provided with agitating plate in the middle of described 3rd puddler, described agitating plate presents narrow structure under width, and its top is provided with triangle Groove;Described pretreatment blender one side bottom is provided with stirring discharging opening, described stirring discharging opening and described micelle connecting gear Bottom connects;
Described micelle connecting gear is inclined to set, and including cylinder shell and conveyor screw, described conveyor screw is positioned at described cylinder Inside body case, described cylinder shell is provided with oil injection mechanism and steam spraying mechanism, and described oil injection mechanism includes spray bar Road and atomizer, described oil spout pipeline is two, is symmetricly set in both sides in described cylinder shell housing, described atomizer quantity For 20-30, it is arranged in cylinder shell internal side wall, is connected with described oil spout pipeline bottom described atomizer, described spray Oil nozzle is provided with oil injection plate, and described oil injection plate is provided with the first nozzle opening and the second nozzle opening, and described first nozzle opening is in oil spout Quantity on plate is six, is positioned at oil injection plate center, ringwise structure distribution;Described second oil spout fluid apertures is on oil injection plate Quantity be 6, be centered around the first nozzle opening outer rim surrounding ringwise;It is provided with the first spray bar on described first nozzle opening; The second spray bar it is provided with, described first spray bar and the second spray bar is inclined on oil injection plate sets on described second nozzle opening Put;Described steam spraying mechanism includes steam pipeline and steam outlet nozzle, and described steam pipeline is two, right Claiming to be arranged at both sides in described cylinder shell housing, described steam outlet nozzle quantity is 15-20, is arranged in cylinder shell On portion's sidewall, it is connected with described steam pipeline bottom described steam outlet nozzle, in side bottom described steam outlet nozzle Shape body, top is that circular arc extends out structure;Described oil spout duct bottom connects air pump;Described oil spout pipeline is by pipe even Connect softening agent holding vessel;Described steam duct bottom is connected by pipe steam evaporator;Described micelle connecting gear Top exit connects desulfurizing machine charging aperture;Described desulfurizing machine bottom discharge mouth connects the second elevator, on described second elevator It is provided with elevator discharging opening;
Described receiving vat is square tube structure, is positioned at the lower section of described second elevator discharging opening.
Above-mentioned a kind of reclaimed rubber is with slightly refining plasticizing system, wherein, and the rounded plate body of described oil injection plate.
Above-mentioned a kind of reclaimed rubber is with slightly refining plasticizing system, wherein, and described first spray bar and described oil injection plate angle B It it is 48 degree.
Above-mentioned a kind of reclaimed rubber is with slightly refining plasticizing system, wherein, and described second spray bar and described oil injection plate angle C It it is 62 degree.
A kind of thick smelting method of reclaimed rubber, wherein, its step is as follows:
1, stirring for the first time, waste rubber powder is put into blender stirring, stir speed (S.S.) is 45r/min, and mixing time is 20- 30min;
2, micelle softens for the first time, by the rubber powder after stirring by screw conveyer, uniformly sprays softening agent during transmitting, softens Agent fountain height is 10-25g/min, and is passed through steam in screw rod, and steam intake is 5-8L/min;
3, desulfurization processes, and the micelle after softening is passed through desulfurizing machine, regulation desulfurizing machine each district temperature:
Desulfurizing machine Heating Zone Temperature is 320-450 DEG C;
Desulfurizing machine heat preservation zone temperature is 300-350 DEG C;
Desulfurizing machine cooling zone temperature is 80-150 DEG C;
4, being again stirring for, put into by the micelle after first desulfurization and continue stirring in blender, stir speed (S.S.) is 65r/min, stirring Time is 10-20min;
5, micelle softens again, and the rubber powder after being again stirring for passes through screw conveyer, uniformly sprays softening agent during transmitting, Softening agent fountain height is 8-15g/min, and is passed through steam in screw rod, and steam intake is 5-8L/min;
6, desulfurization processes again, and the micelle after again softening is passed through desulfurizing machine, regulation desulfurizing machine each district temperature:
Desulfurizing machine Heating Zone Temperature is 320-450 DEG C;
Desulfurizing machine heat preservation zone temperature is 300-350 DEG C;
Desulfurizing machine cooling zone temperature is 80-150 DEG C;
Discharging after desulfurization.
Above-mentioned a kind of thick smelting method of reclaimed rubber, wherein, described softening agent is aromatic naphtha, paraffin oil, vaseline, naphthenic oil In two or more mixture.
Above-mentioned a kind of thick smelting method of reclaimed rubber, wherein, described softening agent is aromatic naphtha, paraffin oil, vaseline, naphthenic oil Mixture with the mass ratio mixing gained of 3:4:1:5.
Compared with the prior art, beneficial effects of the present invention is embodied in:
1, before manufacture waste rubber powder is carried out pretreatment, use special rabbling mechanism that it is broken up, tentatively realize Waste rubber powder changes to graininess micelle;Pretreatment blender uses becomes privileged design, internal symmetrically arranged is stirred by two Mix mechanism, waste rubber powder, unique rabbling mechanism design can be broken up uniformly, use three puddlers to be stirred simultaneously.Can It is greatly promoted stirring efficiency;The length of three puddlers uses the design of the length of side the most successively on rabbling mechanism, can make Sizing material bottom blender is more easy to mixing and breaks up, bottom is not easy to deposit on rubber powder, and puddler and uses stirring flanging, can pin Multiple directions are stirred, accomplish that Multi-angle omnibearing stirs, maximum lift mixing evenness.Real through up to ten thousand science Testing, when stirring flanging and the first puddler, the second puddler, the 3rd puddler angle A be when being 120 degree, and mixing effect is Good.
2, by special micelle connecting gear, internal distinctive steam pipeline steams with steam outlet nozzle spray water Gas.Micelle and air is isolated, it is ensured that the micelle of the condition of high temperature do not cracks, not oxygen with the steam of a certain amount of full high-temperature space Change.Particularly steam outlet nozzle design, uses top arc shape to extend out structure, and beneficially steam quickly spreads, and strengthens water Steam isolation effect.Quantitatively softening agent it is sprayed in the rubber powder of motion by fueling injection equipment and vaporizes so that it is uniformly admixing, full Foot rubber powder softens, the needs of chain rupture;Particularly atomizer design, multiple oil spout pipelines carry out spraying softening agent from multiple angles, Accomplish to cover comprehensively, uniformly spray;And spray bar uses unique 62 degree, 48 degree to be obliquely installed, can effectively ensure that spray area Maximize.
3, the thick smelting method of special reclaimed rubber, makes rubber powder be placed in the high-temperature space of motion, meets and opens strand Temperature-time requirement;Use the multiple thick smelting method of twice stirring, twice softening, twice desulfurization, thus it is big to be continuously finished micelle Molecule cross-linked structure opening and stoping anti-process to short chain molecule structure, is greatly promoted properties of product.Improve and use Effect.
Accompanying drawing explanation
Fig. 1 is the schematic diagram of the present invention.
The pretreatment blender schematic internal view of Fig. 2 present invention.
The rabbling mechanism schematic diagram of Fig. 3 present invention.
The micelle connecting gear longitudinal direction partial sectional view of Fig. 4 present invention.
The horizontal partial sectional view of micelle connecting gear of Fig. 5 present invention.
The micelle conveyer shell side view of Fig. 6 present invention.
The atomizer schematic diagram of Fig. 7 present invention.
The oil injection plate schematic diagram of Fig. 8 present invention.
Detailed description of the invention
The invention will be further described below in conjunction with the accompanying drawings.
Desulfurizing machine used in the embodiment of the present invention is purchased from Jiangsu Hong Ding environmental protection equipment Science and Technology Ltd., product type For HD-B-13.
Softening agent in the embodiment of the present invention is that aromatic naphtha, paraffin oil, vaseline, naphthenic oil are with the mass ratio of 3:4:1:5 The mixture of mixing gained.Used aromatic naphtha is purchased from Dezhou Ming Sheng Chemical Co., Ltd., and product type is TDAE.Used To paraffin oil and naphthenic oil be purchased from Changzhou mesochite lubricating oil company limited, paraffin oil product type is 150 environment-friendly types;Ring Alkane oil product model is KNH4006.
In the present embodiment, correlation indices is as follows:
First retable unit the 13, second retable unit 14, receiving vat 7, trough the 1, first elevator the 2, first elevator Discharging opening 21, pretreatment blender 3, micelle connecting gear 4, desulfurizing machine the 5, second elevator the 6, second elevator discharging opening 61, Blender housing 31, rabbling mechanism 32, shaft 321, stirring motor the 322, first puddler the 323, second puddler 324, Three puddlers 325, connecting rod 326, stirring flanging 327, agitating plate 328, triangle groove 329, stirring discharging opening 33, cylinder shell 41, conveyor screw 42, oil injection mechanism 43, oil spout pipeline 431, atomizer 432, oil injection plate the 8, first nozzle opening the 81, second oil spout Hole the 82, first spray bar the 83, second spray bar 84, steam spraying mechanism 44, steam pipeline 441, steam outlet nozzle 442, pipe 10, softening agent holding vessel 11, steam evaporator 12, air pump 9.
A kind of reclaimed rubber is with slightly refining plasticizing system, and wherein, a kind of reclaimed rubber is with slightly refining plasticizing system, wherein, including two groups Plasticizing unit 13,14 and receiving vat 7, described plasticizing unit includes trough the 1, first elevator 2, pretreatment blender 3, micelle Connecting gear 4, desulfurizing machine the 5, second elevator 6, the receiving vat 1 of described second retable unit 14 is positioned at the first retable unit Below the second elevator discharging opening 61 of 14, below the second elevator discharging opening 61 of the second retable unit 14, it is provided with receiving vat 7, described trough 1, in chamfered edge bench-type structure, described trough 1 connects described first elevator, on described first elevator Being provided with the first elevator discharging opening 21, described pretreatment blender 3 is positioned at described first elevator lower position;
Described pretreatment blender 3 includes blender housing 31 and rabbling mechanism 32, and described blender housing bottom is cylindrical Structure, top is outward-dipping, opening-like;Described rabbling mechanism quantity is two, is symmetricly set in described blender housing two Side, described rabbling mechanism 32 includes that shaft 321, stirring motor the 322, first puddler the 323, second puddler the 324, the 3rd stir Mix bar 325 and connecting rod 326;Described number of motors is two, is installed on described blender hull outside both sides, described shaft One end connects described motor, and the other end stretches into blender enclosure interior and connects the center of described first puddler, described company Extension bar one end connects the first puddler, and the other end connects the 3rd puddler, and described second puddler is connected in described connecting rod, Described second puddler is between described 3rd puddler and the first puddler;The two of described first, second, third puddler End is equipped with stirring flanging 327, and described stirring flanging is inclined to set, described stirring flanging and described first puddler, second Puddler, the 3rd puddler angle A are 120 degree;Agitating plate 328, described agitating plate it is provided with in the middle of described 3rd puddler Presenting narrow structure under width, its top is provided with triangle groove 329;Described pretreatment blender one side bottom is provided with stirring discharging opening 33, described stirring discharging opening is connected bottom described micelle connecting gear;
Described micelle connecting gear is inclined to set, and including cylinder shell 41 and conveyor screw 42, described conveyor screw is positioned at institute Stating inside cylinder shell, described cylinder shell is provided with oil injection mechanism 43 and steam spraying mechanism 44, described oil injection mechanism 43 Including oil spout pipeline 431 and atomizer 432, described oil spout pipeline is two, is symmetricly set in described cylinder shell housing two Side, described atomizer quantity is 26, is arranged in cylinder shell internal side wall, with described oil spout pipeline bottom described atomizer Being connected, described atomizer is provided with oil injection plate 8, and described oil injection plate 8 is provided with the first nozzle opening 81 and the second nozzle opening 82, institute Stating first nozzle opening quantity on oil injection plate is six, is positioned at oil injection plate center, ringwise structure distribution;Described second Oil spout fluid apertures quantity on oil injection plate is 6, is centered around the first nozzle opening outer rim surrounding ringwise;On described first nozzle opening It is provided with the first spray bar 83;The second spray bar 84, described first spray bar and the second spray it is provided with on described second nozzle opening Oil pipe is inclined to set on oil injection plate;Described steam spraying mechanism 44 includes steam pipeline 441 and steam outlet nozzle 442, described steam pipeline is two, is symmetricly set in both sides in described cylinder shell housing, and described steam is given vent to anger Unrounded number is 16, is arranged in cylinder shell internal side wall, with described steam pipeline phase bottom described steam outlet nozzle Connecting, be square bottom described steam outlet nozzle body, and top is that circular arc extends out structure;Described oil spout duct bottom connects There is air pump 9;Described oil spout pipeline connects softening agent holding vessel 11 by pipe 10;Described steam duct bottom passes through pipe 10 Connect and have steam evaporator 12;Described micelle connecting gear top connects desulfurizing machine 5 charging aperture;
Described desulfurizing machine bottom discharge mouth connects the second elevator, and described second elevator is provided with the second elevator discharging opening 61。
Described receiving vat is square tube structure, is positioned under the second elevator discharging opening of described second plasticizing unit Side;The rounded plate body of described oil injection plate.Described first spray bar and described oil injection plate angle B are 48 degree.Described second spray Oil pipe and described oil injection plate angle C are 62 degree.
Embodiment 1
A kind of thick smelting method of reclaimed rubber, wherein, its step is as follows:
1, stirring for the first time, waste rubber powder is put into blender stirring, stir speed (S.S.) is 45r/min, and mixing time is 20min;
2, micelle softens for the first time, by the rubber powder after stirring by screw conveyer, uniformly sprays softening agent during transmitting, softens Agent fountain height is 10g/min, and is passed through steam in screw rod, and steam intake is 5L/min;
3, desulfurization processes, and the micelle after softening is passed through desulfurizing machine, regulation desulfurizing machine each district temperature:
Desulfurizing machine Heating Zone Temperature is 320 DEG C;
Desulfurizing machine heat preservation zone temperature is 300 DEG C;
Desulfurizing machine cooling zone temperature is 80 DEG C;
4, being again stirring for, put into by the micelle after first desulfurization and continue stirring in blender, stir speed (S.S.) is 65r/min, stirring Time is 10min;
5, micelle softens again, and the rubber powder after being again stirring for passes through screw conveyer, uniformly sprays softening agent during transmitting, Softening agent fountain height is 8g/min, and is passed through steam in screw rod, and steam intake is 5L/min;
6, desulfurization processes again, and the micelle after again softening is passed through desulfurizing machine, regulation desulfurizing machine each district temperature:
Desulfurizing machine Heating Zone Temperature is 320 DEG C;
Desulfurizing machine heat preservation zone temperature is 300 DEG C;
Desulfurizing machine cooling zone temperature is 80 DEG C;
Discharging after desulfurization.
Embodiment 2
A kind of thick smelting method of reclaimed rubber, wherein, its step is as follows:
1, stirring for the first time, waste rubber powder is put into blender stirring, stir speed (S.S.) is 45r/min, and mixing time is 30min;
2, micelle softens for the first time, by the rubber powder after stirring by screw conveyer, uniformly sprays softening agent during transmitting, softens Agent fountain height is 25g/min, and is passed through steam in screw rod, and steam intake is 8L/min;
3, desulfurization processes, and the micelle after softening is passed through desulfurizing machine, regulation desulfurizing machine each district temperature:
Desulfurizing machine Heating Zone Temperature is 450 DEG C;
Desulfurizing machine heat preservation zone temperature is 350 DEG C;
Desulfurizing machine cooling zone temperature is 150 DEG C;
4, being again stirring for, put into by the micelle after first desulfurization and continue stirring in blender, stir speed (S.S.) is 65r/min, stirring Time is 20min;
5, micelle softens again, and the rubber powder after being again stirring for passes through screw conveyer, uniformly sprays softening agent during transmitting, Softening agent fountain height is 15g/min, and is passed through steam in screw rod, and steam intake is 8L/min;
6, desulfurization processes again, and the micelle after again softening is passed through desulfurizing machine, regulation desulfurizing machine each district temperature:
Desulfurizing machine Heating Zone Temperature is 450 DEG C;
Desulfurizing machine heat preservation zone temperature is 350 DEG C;
Desulfurizing machine cooling zone temperature is 150 DEG C;
Discharging after desulfurization.
Embodiment 3
A kind of thick smelting method of reclaimed rubber, wherein, its step is as follows:
1, stirring for the first time, waste rubber powder is put into blender stirring, stir speed (S.S.) is 45r/min, and mixing time is 25min;
2, micelle softens for the first time, by the rubber powder after stirring by screw conveyer, uniformly sprays softening agent during transmitting, softens Agent fountain height is 15g/min, and is passed through steam in screw rod, and steam intake is 7L/min;
3, desulfurization processes, and the micelle after softening is passed through desulfurizing machine, regulation desulfurizing machine each district temperature:
Desulfurizing machine Heating Zone Temperature is 380 DEG C;
Desulfurizing machine heat preservation zone temperature is 320 DEG C;
Desulfurizing machine cooling zone temperature is 120 DEG C;
4, being again stirring for, put into by the micelle after first desulfurization and continue stirring in blender, stir speed (S.S.) is 65r/min, stirring Time is 16min;
5, micelle softens again, and the rubber powder after being again stirring for passes through screw conveyer, uniformly sprays softening agent during transmitting, Softening agent fountain height is 11g/min, and is passed through steam in screw rod, and steam intake is 6L/min;
6, desulfurization processes again, and the micelle after again softening is passed through desulfurizing machine, regulation desulfurizing machine each district temperature:
Desulfurizing machine Heating Zone Temperature is 350 DEG C;
Desulfurizing machine heat preservation zone temperature is 310 DEG C;
Desulfurizing machine cooling zone temperature is 90 DEG C;
Discharging after desulfurization.
Compared with the prior art, beneficial effects of the present invention is embodied in:
1, before manufacture waste rubber powder is carried out pretreatment, use special rabbling mechanism that it is broken up, tentatively realize Waste rubber powder changes to graininess micelle;Pretreatment blender uses becomes privileged design, internal symmetrically arranged is stirred by two Mix mechanism, waste rubber powder, unique rabbling mechanism design can be broken up uniformly, use three puddlers to be stirred simultaneously.Can It is greatly promoted stirring efficiency;The length of three puddlers uses the design of the length of side the most successively on rabbling mechanism, can make Sizing material bottom blender is more easy to mixing and breaks up, bottom is not easy to deposit on rubber powder, and puddler and uses stirring flanging, can pin Multiple directions are stirred, accomplish that Multi-angle omnibearing stirs, maximum lift mixing evenness.Real through up to ten thousand science Testing, when stirring flanging and the first puddler, the second puddler, the 3rd puddler angle A be when being 120 degree, and mixing effect is Good.
2, by special micelle connecting gear, internal distinctive steam pipeline steams with steam outlet nozzle spray water Gas.Micelle and air is isolated, it is ensured that the micelle of the condition of high temperature do not cracks, not oxygen with the steam of a certain amount of full high-temperature space Change.Particularly steam outlet nozzle design, uses top arc shape to extend out structure, and beneficially steam quickly spreads, and strengthens water Steam isolation effect.Quantitatively softening agent it is sprayed in the rubber powder of motion by fueling injection equipment and vaporizes so that it is uniformly admixing, full Foot rubber powder softens, the needs of chain rupture;Particularly atomizer design, multiple oil spout pipelines carry out spraying softening agent from multiple angles, Accomplish to cover comprehensively, uniformly spray;And spray bar uses unique 62 degree, 48 degree to be obliquely installed, can effectively ensure that spray area Maximize.
3, the thick smelting method of special reclaimed rubber, makes rubber powder be placed in the high-temperature space of motion, meets and opens strand Temperature-time requirement;Use the multiple thick smelting method of twice stirring, twice softening, twice desulfurization, thus it is big to be continuously finished micelle Molecule cross-linked structure opening and stoping anti-process to short chain molecule structure, is greatly promoted properties of product.Improve and use Effect.
The above, the only present invention preferably detailed description of the invention, but protection scope of the present invention is not limited thereto, Any those familiar with the art in the technical scope that the invention discloses, the change that can readily occur in or replacement, All should contain within the scope of the present invention.Therefore, protection scope of the present invention should be with the protection domain of claims It is as the criterion.

Claims (5)

1. a reclaimed rubber is with slightly refining plasticizing system, it is characterised in that include two retable unit and receiving vats, described Plasticator Group includes trough, the first elevator, pretreatment blender, micelle connecting gear, desulfurizing machine and the second elevator, described The receiving vat of two retable units is positioned at below the second elevator discharging opening of the first retable unit, the second retable unit Being provided with receiving vat below second elevator discharging opening, described trough is chamfered edge bench-type structure, described trough connects described First elevator, described first elevator is provided with elevator discharging opening, and described pretreatment blender is positioned at described first and promotes Machine lower position;
Described pretreatment blender includes blender housing and rabbling mechanism, the described cylindrical structure of blender housing bottom, Top is outward-dipping, opening-like;Described rabbling mechanism quantity is two, is symmetricly set in described blender housing both sides, institute State rabbling mechanism and include shaft, stirring motor, the first puddler, the second puddler, the 3rd puddler and connecting rod;Described electricity Machine quantity is two, is installed on described blender hull outside both sides, and described shaft one end connects described motor, and the other end is stretched Entering blender enclosure interior and connect the center of described first puddler, described connecting rod one end connects the first puddler, separately One end connects the 3rd puddler, and described second puddler is connected in described connecting rod, and described second puddler is positioned at described the Between three puddlers and the first puddler;The two ends of described first, second, third puddler are equipped with stirring flanging, described in stir Mix flanging to be inclined to set, described stirring flanging and described first puddler, the second puddler, the 3rd puddler angle A It it is 120 degree;Being provided with agitating plate in the middle of described 3rd puddler, described agitating plate presents narrow structure under width, and its top is provided with triangle Groove;Described pretreatment blender one side bottom is provided with stirring discharging opening, described stirring discharging opening and described micelle connecting gear Bottom connects;
Described micelle connecting gear is inclined to set, and including cylinder shell and conveyor screw, described conveyor screw is positioned at described cylinder Inside body case, described cylinder shell is provided with oil injection mechanism and steam spraying mechanism, and described oil injection mechanism includes spray bar Road and atomizer, described oil spout pipeline is two, is symmetricly set in both sides in described cylinder shell housing, described atomizer quantity For 20-30, it is arranged in cylinder shell internal side wall, is connected with described oil spout pipeline bottom described atomizer, described spray Oil nozzle is provided with oil injection plate, and described oil injection plate is provided with the first nozzle opening and the second nozzle opening, and described first nozzle opening is in oil spout Quantity on plate is six, is positioned at oil injection plate center, ringwise structure distribution;Described second oil spout fluid apertures is on oil injection plate Quantity be 6, be centered around the first nozzle opening outer rim surrounding ringwise;It is provided with the first spray bar on described first nozzle opening; The second spray bar it is provided with, described first spray bar and the second spray bar is inclined on oil injection plate sets on described second nozzle opening Put;Described steam spraying mechanism includes steam pipeline and steam outlet nozzle, and described steam pipeline is two, right Claiming to be arranged at both sides in described cylinder shell housing, described steam outlet nozzle quantity is 15-20, is arranged in cylinder shell On portion's sidewall, it is connected with described steam pipeline bottom described steam outlet nozzle, in side bottom described steam outlet nozzle Shape body, top is that circular arc extends out structure;Described oil spout duct bottom connects air pump;Described oil spout pipeline is by pipe even Connect softening agent holding vessel;Described steam duct bottom is connected by pipe steam evaporator;Described micelle connecting gear Top exit connects desulfurizing machine charging aperture;Described desulfurizing machine bottom discharge mouth connects the second elevator, on described second elevator It is provided with elevator discharging opening;
Described receiving vat is square tube structure, is positioned at the lower section of described second elevator discharging opening.
2. a kind of reclaimed rubber as claimed in claim 1 is with slightly refining plasticizing system, it is characterised in that the rounded plate of described oil injection plate Body.
3. a kind of reclaimed rubber as claimed in claim 1 is with slightly refining plasticizing system, it is characterised in that described first spray bar and institute Stating oil injection plate angle B is 48 degree.
4. a kind of reclaimed rubber as claimed in claim 1 is with slightly refining plasticizing system, it is characterised in that described second spray bar and institute Stating oil injection plate angle C is 62 degree.
5. the thick smelting method of reclaimed rubber, it is characterised in that its step is as follows:
1) stirring for the first time, waste rubber powder is put into blender stirring, stir speed (S.S.) is 45r/min, and mixing time is 20- 30min;
2) micelle softens for the first time, by the rubber powder after stirring by screw conveyer, uniformly sprays softening agent during transmitting, softens Agent fountain height is 10-25g/min, and is passed through steam in screw rod, and steam intake is 5-8L/min;
3) desulfurization processes, and the micelle after softening is passed through desulfurizing machine, regulation desulfurizing machine each district temperature:
Desulfurizing machine Heating Zone Temperature is 320-450 DEG C;
Desulfurizing machine heat preservation zone temperature is 300-350 DEG C;
Desulfurizing machine cooling zone temperature is 80-150 DEG C;
4) being again stirring for, put into by the micelle after first desulfurization and continue stirring in blender, stir speed (S.S.) is 65r/min, stirring Time is 10-20min;
5) micelle softens again, and the rubber powder after being again stirring for passes through screw conveyer, uniformly sprays softening agent during transmitting, Softening agent fountain height is 8-15g/min, and is passed through steam in screw rod, and steam intake is 5-8L/min;
6) desulfurization processes again, and the micelle after again softening is passed through desulfurizing machine, regulation desulfurizing machine each district temperature:
Desulfurizing machine Heating Zone Temperature is 320-450 DEG C;
Desulfurizing machine heat preservation zone temperature is 300-350 DEG C;
Desulfurizing machine cooling zone temperature is 80-150 DEG C;
Discharging after desulfurization.
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