CN106166441A - There is solid air purification smell removal agent and the preparation method of degradation property - Google Patents
There is solid air purification smell removal agent and the preparation method of degradation property Download PDFInfo
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- CN106166441A CN106166441A CN201610271586.4A CN201610271586A CN106166441A CN 106166441 A CN106166441 A CN 106166441A CN 201610271586 A CN201610271586 A CN 201610271586A CN 106166441 A CN106166441 A CN 106166441A
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- air purification
- removal agent
- degradation property
- solid air
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
- B01D53/81—Solid phase processes
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/46—Removing components of defined structure
- B01D53/48—Sulfur compounds
- B01D53/52—Hydrogen sulfide
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/46—Removing components of defined structure
- B01D53/54—Nitrogen compounds
- B01D53/58—Ammonia
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/46—Removing components of defined structure
- B01D53/72—Organic compounds not provided for in groups B01D53/48 - B01D53/70, e.g. hydrocarbons
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2257/00—Components to be removed
- B01D2257/70—Organic compounds not provided for in groups B01D2257/00 - B01D2257/602
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2257/00—Components to be removed
- B01D2257/70—Organic compounds not provided for in groups B01D2257/00 - B01D2257/602
- B01D2257/702—Hydrocarbons
- B01D2257/7027—Aromatic hydrocarbons
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2257/00—Components to be removed
- B01D2257/70—Organic compounds not provided for in groups B01D2257/00 - B01D2257/602
- B01D2257/708—Volatile organic compounds V.O.C.'s
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2258/00—Sources of waste gases
- B01D2258/06—Polluted air
Abstract
A kind of solid air purification smell removal agent with degradation property and preparation method, according to part by weight, include 4A zeolite, kieselguhr and tartaric acid, by tartaric acid and 4A zeolite and the chemical reaction of diatomaceous mixture, form the crystalline solid with poroid body, owing to 4A zeolite and kieselguhr are mineral, 4A zeolite and kieselguhr can incinerate, it is achieved that have the air cleaning eliminating smell agent of degradation property through using for a long time.
Description
One, technical field
The present invention relates to a kind of solid air purification smell removal agent and preparation method, a kind of solid-state sky with degradation property
Gas purification smell removal agent and preparation method.
Two, background technology
But there is the material meetings such as various pollutant, formaldehyde, benzene-like compounds, ammoniac compounds, voc in the federation that indoor are more or less
To air born pollution, contaminated air has various abnormal flavour, and make that people produces a feeling is sick of and healthy product to people
Raw infringement, there is also the microorganism such as various antibacterial and virus in air, therefore the agent of solid air purification smell removal is a kind of important
Environmentally-friendly sanitary articles for use, in existing solid air purification smell removal agent, the product unicity purposes of Environment control air pollution,
Especially indoor air purification is administered, there is no a kind of comprehensive product, it is possible to removing the product of various foreign odor taste, function is uneven
Entirely, and complex process, production cost is higher, especially single to liquid type eliminating smell agent purposes, and activated carbon deodorant exists secondary
Pollute, it is often more important that use the cycle short, currently there are no a kind of solid air purification smell removal agent with degradation property and system
Preparation Method.
Three, summary of the invention
The object of the present invention is a kind of solid air purification smell removal agent with degradation property,
The object of the present invention is the preparation method of a kind of solid air purification smell removal agent with degradation property.
In order to overcome above-mentioned technical disadvantages, it is an object of the invention to provide a kind of solid air with degradation property and purify
Eliminating smell agent and preparation method, it is achieved that have the air cleaning eliminating smell agent of degradation property.
For reaching above-mentioned purpose, the present invention adopts the technical scheme that: a kind of solid air with degradation property purifies
Eliminating smell agent, according to part by weight, includes 4A zeolite, kieselguhr and tartaric acid.
Owing to devising 4A zeolite, kieselguhr and tartaric acid, by tartaric acid and 4A zeolite and diatomaceous mixture
Chemical reaction, forms the crystalline solid with poroid body, owing to 4A zeolite and kieselguhr are mineral, 4A zeolite and kieselguhr warp
Cross to use for a long time and can incinerate, it is achieved that have the air cleaning eliminating smell agent of degradation property.
The present invention devises, include formed have poroid body a diameter of 0.58 ~ 0.7nm crystalline solid 4A zeolite,
Kieselguhr and tartaric acid.
The present invention devises, and also includes phosphoric acid and potassium permanganate.
The present invention devises, and according to part by weight, includes 50 ~ 70 parts of 4A zeolite, 5 ~ 10 parts of tartaric acid, phosphoric acid 3.2
~ 4.8 parts, 2 ~ 10 parts of potassium permanganate, 10 ~ 40 parts of kieselguhr.
The present invention devises, and 4A zeolite and kieselguhr are set to food stage, and tartaric acid, phosphoric acid and potassium permanganate are set to doctor
Treat sanitation-grade.
According to part by weight, include 55 parts of 4A zeolite, 8 parts of tartaric acid, phosphatase 24 part, 3 parts of potassium permanganate, kieselguhr 30
Part.
The present invention devises, the preparation method of a kind of solid air purification smell removal agent with degradation property, the steps include:
4A zeolite and diatomaceous mixture are reacted with tartaric acid, then reaction is obtained thing carries out drying and pulverization process,
The reaction of powder obtains thing and carries out ripening with phosphoric acid and potassium permanganate, then carries out pelletize and drying and processing, obtains solid-state
Air cleaning eliminating smell agent finished product.
The present invention devises, and the steps include:
4A zeolite and kieselguhr are mixed to form intermedium I according to part by weight,
Adding the tartaric acid solution that concentration is 18-22% in intermedium I and form mixed solution, the PH adjusting mixed solution is 7-
9, make mixed solution carry out chemical reaction 2.8-3.2h and obtain intermedium II,
Intermedium II is carried out drying and processing in 380-420 DEG C of environment and obtains the powder of 80 ~ 120 mesh through pulverization process
Agent,
According to part by weight, phosphoric acid and potassium permanganate are carried out mixing and add suitable quantity of water with powder to mix homogeneously, then enter
The ripening of row 0.8-1.2h waits until intermedium III,
Intermedium III, through prilling granulator shaped granule, carries out drying and processing in the environment of 118-122 DEG C and obtains solid air
Purification smell removal agent finished product.
The present invention devises, and shaped granule is set to 3 ~ 5mm spherosome.
The present invention devises, and the diameter of the poroid body of shaped granule is set to 0.58 ~ 0.7nm.
Reaction mechanism in the technical program:
(CH3CH2)2N + H3PO4 →(CH3CH2)2N·H3PO4
NH3 + H3PO4 → (NH3)2HPO4
H2S + CaO → CaS + H2O
HCHO + O2→ HCOOH + O2→H2O + CO2↑
C7H8 + O2→CO2↑ +H2O
CH3CH2OH + O2→CO2↑ + H2O
C6H5OH + O2→CO2↑ + H2O
In the technical program, 4A zeolite, kieselguhr and tartaric acid are important technical characteristic, empty in the solid-state with degradation property
In the technical field of gas purification smell removal agent and preparation method, there is novelty, creativeness and practicality, in the technical program
Term is all can to explain with patent documentation in the art and understand.
Four, detailed description of the invention
According to guidelines for examination, to used in the present invention such as " having ", " comprising " and " including " term should be understood to not
Allot other element one or more or the existence of a combination thereof or interpolation.
Below in conjunction with in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely retouched
State, it is clear that described embodiment is only a part of embodiment of the present invention rather than whole embodiments.Based on the present invention
In embodiment, the every other enforcement that those of ordinary skill in the art are obtained under not making creative work premise
Example, broadly falls into the scope of protection of the invention.
In describing the invention, it should be noted that term " " center ", " on ", D score, "left", "right", " vertically ",
The orientation of the instruction such as " level ", " interior ", " outward " or position relationship are based on general shown orientation or position relationship, merely to
Be easy to describe the present invention and simplifying describe rather than instruction or the hint device of indication or element must have specific orientation,
With specific azimuth configuration and operation, therefore it is not considered as limiting the invention.Additionally, term " first ", " second ",
" the 3rd " is only used for describing purpose, and it is not intended that indicate or hint relative importance.
In describing the invention, it should be noted that unless otherwise clearly defined and limited, term " is installed ", " phase
Even ", " connection " should be interpreted broadly, for example, it may be fixing connection, it is also possible to be to removably connect, or be integrally connected；Can
To be mechanical connection, it is also possible to be electrical connection；Can be to be joined directly together, it is also possible to be indirectly connected to by intermediary, Ke Yishi
The connection of two element internals.For the ordinary skill in the art, can understand that above-mentioned term is at this with concrete condition
Concrete meaning in invention.
If additionally, the most non-structure of technical characteristic involved in invention described below difference embodiment
Become conflict just can be combined with each other.
A kind of solid air purification smell removal agent with degradation property, in conjunction with illustrating the present embodiment, first enforcement
Example, according to part by weight, includes 50 parts of 4A zeolite, 5 parts of tartaric acid, phosphoric acid 3.2 parts, 2 parts of potassium permanganate, 10 parts of kieselguhr.
In the present embodiment, 4A zeolite and kieselguhr are set to food stage, and tartaric acid, phosphoric acid and potassium permanganate are set to doctor
Treat sanitation-grade.
A kind of solid air purification smell removal agent with degradation property, second embodiment, according to part by weight, include
70 parts of 4A zeolite, 10 parts of tartaric acid, phosphatase 24 .8 part, 10 parts of potassium permanganate, 40 parts of kieselguhr.
A kind of solid air purification smell removal agent with degradation property, the 3rd embodiment, according to part by weight, include
50 ~ 70 parts of 4A zeolite, 5 ~ 10 parts of tartaric acid, phosphoric acid 3.2 ~ 4.8 parts, 2 ~ 10 parts of potassium permanganate, 10 ~ 40 parts of kieselguhr.
A kind of solid air purification smell removal agent with degradation property, the 4th embodiment, according to part by weight, include
60 parts of 4A zeolite, 7.5 parts of tartaric acid, phosphatase 24 .0 part, 6 parts of potassium permanganate, 25 parts of kieselguhr.
A kind of solid air purification smell removal agent with degradation property, the 5th embodiment, according to part by weight, include
55 parts of 4A zeolite, 8 parts of tartaric acid, phosphatase 24 part, 3 parts of potassium permanganate, 30 parts of kieselguhr.
The most suitable due to 4A zeolite and diatomaceous ratio in the present embodiment, the intensity of the granule of formation preferably and
The incineration shortest time of granule.
Below in conjunction with embodiment, further describing the present invention, following example are intended to illustrate rather than this
The further restriction of invention.A kind of preparation method of the solid air purification smell removal agent with degradation property, first embodiment,
The steps include:
4A zeolite and kieselguhr are mixed to form intermedium I according to part by weight,
Adding the tartaric acid solution that concentration is 18% in intermedium I and form mixed solution, the PH adjusting mixed solution is 7, makes to mix
Conjunction solution carries out chemical reaction 2.8h and obtains intermedium II,
Intermedium II is carried out drying and processing in 380 DEG C of environment and obtains the powder of 80 mesh through pulverization process,
According to part by weight, phosphoric acid and potassium permanganate are carried out mixing and add suitable quantity of water with powder to mix homogeneously, then enter
The ripening of row 0.8h waits until intermedium III,
Intermedium III, through prilling granulator shaped granule, carries out drying and processing in the environment of 118 DEG C and obtains solid air purification
Eliminating smell agent finished product.
In the present embodiment, shaped granule is set to 3mm spherosome.
In the present embodiment, the diameter of the poroid body of shaped granule is set to 0.58nm.
Testing the present embodiment, its result of the test is:
A kind of preparation method of the solid air purification smell removal agent with degradation property, second embodiment, the steps include:
4A zeolite and kieselguhr are mixed to form intermedium I according to part by weight,
Adding the tartaric acid solution that concentration is 22% in intermedium I and form mixed solution, the PH adjusting mixed solution is 9, makes to mix
Conjunction solution carries out chemical reaction 3.2h and obtains intermedium II,
Intermedium II is carried out drying and processing in 420 DEG C of environment and obtains the powder of 120 mesh through pulverization process,
According to part by weight, phosphoric acid and potassium permanganate are carried out mixing and add suitable quantity of water with powder to mix homogeneously, then enter
The ripening of row 1.2h waits until intermedium III,
Intermedium III, through prilling granulator shaped granule, carries out drying and processing in the environment of 122 DEG C and obtains solid air purification
Eliminating smell agent finished product.
In the present embodiment, shaped granule is set to 5mm spherosome.
In the present embodiment, the diameter of the poroid body of shaped granule is set to 0.7nm.
A kind of preparation method of the solid air purification smell removal agent with degradation property, the 3rd embodiment, the steps include:
4A zeolite and kieselguhr are mixed to form intermedium I according to part by weight,
Adding the tartaric acid solution that concentration is 18-22% in intermedium I and form mixed solution, the PH adjusting mixed solution is 7-
9, make mixed solution carry out chemical reaction 2.8-3.2h and obtain intermedium II,
Intermedium II is carried out drying and processing in 380-420 DEG C of environment and obtains the powder of 80 ~ 120 mesh through pulverization process
Agent,
According to part by weight, phosphoric acid and potassium permanganate are carried out mixing and add suitable quantity of water with powder to mix homogeneously, then enter
The ripening of row 0.8-1.2h waits until intermedium III,
Intermedium III, through prilling granulator shaped granule, carries out drying and processing in the environment of 118-122 DEG C and obtains solid air
Purification smell removal agent finished product.
In the present embodiment, shaped granule is set to 3 ~ 5mm spherosome.
In the present embodiment, the diameter of the poroid body of shaped granule is set to 0.58 ~ 0.7nm.
A kind of preparation method of the solid air purification smell removal agent with degradation property, the 4th embodiment, the steps include:
4A zeolite and kieselguhr are mixed to form intermedium I according to part by weight,
Adding the tartaric acid solution that concentration is 20% in intermedium I and form mixed solution, the PH adjusting mixed solution is 8, makes to mix
Conjunction solution carries out chemical reaction 3.0h and obtains intermedium II,
Intermedium II is carried out drying and processing in 400 DEG C of environment and obtains the powder of 100 mesh through pulverization process,
According to part by weight, phosphoric acid and potassium permanganate are carried out mixing and add suitable quantity of water with powder to mix homogeneously, then enter
The ripening of row 1.0h waits until intermedium III,
Intermedium III, through prilling granulator shaped granule, carries out drying and processing in the environment of 120 DEG C and obtains solid air purification
Eliminating smell agent finished product.
In the present embodiment, shaped granule is set to 4mm spherosome.
In the present embodiment, the diameter of the poroid body of shaped granule is set to 0.64nm.
A kind of preparation method of the solid air purification smell removal agent with degradation property, the 5th embodiment, the steps include:
4A zeolite and kieselguhr are mixed to form intermedium I according to part by weight,
Adding the tartaric acid solution that concentration is 21% in intermedium I and form mixed solution, the PH adjusting mixed solution is 7.8, makes
Mixed solution carries out chemical reaction 3.2h and obtains intermedium II,
Intermedium II is carried out drying and processing in 410 DEG C of environment and obtains the powder of 90 mesh through pulverization process,
According to part by weight, phosphoric acid and potassium permanganate are carried out mixing and add suitable quantity of water with powder to mix homogeneously, then enter
The ripening of row 1.1h waits until intermedium III,
Intermedium III, through prilling granulator shaped granule, carries out drying and processing in the environment of 121 DEG C and obtains solid air purification
Eliminating smell agent finished product.
In the present embodiment, shaped granule is set to 3.8mm spherosome.
In the present embodiment, the diameter of the poroid body of shaped granule is set to 0.68nm.
The present invention has a lower feature:
1, owing to devising 4A zeolite, kieselguhr and tartaric acid, by tartaric acid and 4A zeolite and the change of diatomaceous mixture
Learning reaction, form the crystalline solid with poroid body, owing to 4A zeolite and kieselguhr are mineral, 4A zeolite and kieselguhr pass through
Use for a long time and can incinerate, it is achieved that have the air cleaning eliminating smell agent of degradation property.
2, owing to devising phosphoric acid and potassium permanganate, by phosphoric acid and potassium permanganate and formaldehyde, ammonia, hydrogen sulfide, benzene, TVOC
Etc. carrying out chemical reaction, thus eliminate.
3, owing to devising 4A zeolite, kieselguhr, phosphoric acid, potassium permanganate and tartaric acid, the crystalline solid of formation has physics
Absorption and chemisorbed dual-use function, the degree of depth fixes absorption and oxidation, the formaldehyde neutralized in air, ammonia, hydrogen sulfide, benzene etc. to be had
Poison, deleterious molecular, non-secondary pollution.
4, owing to devising 4A zeolite, kieselguhr, phosphoric acid, potassium permanganate and tartaric acid, by twice drying and processing, formed
The minimum-value aperture 0.58 ~ 0.7nm of poroid body of crystalline solid, can be in the air such as active adsorption formaldehyde (molecular diameter 0.37nm)
Foul smell molecule, has high-performance biological activity and mithridatism.
5, owing to devising 4A zeolite, kieselguhr, phosphoric acid, potassium permanganate and tartaric acid, by the granule of 80 ~ 120 mesh, shape
The crystalline solid become has the performance that absorption affinity is strong and specific surface area is big.
6, planform has been carried out the restriction of numerical range owing to devising, the technical side making numerical range be the present invention
Technical characteristic in case, calculates or is tested by limited number of time the technical characteristic drawn not by formula, and test shows this numerical value
The technical characteristic of scope achieves good technique effect.
7, owing to devising the technical characteristic of the present invention, in the effect of the set individually and each other of technical characteristic,
Being shown by test, the property indices of the present invention is at least 1.7 times of existing property indices, is had by assessment
There is good market value.
Also having technical characteristic as other same or like with 4A zeolite, kieselguhr and tartaric acid is all the reality of the present invention
Execute one of example, and each technical characteristic of embodiment described above can combine arbitrarily, for meeting Patent Law, patent in fact
Execute the requirement of detailed rules and regulations and guidelines for examination, the no longer embodiment to all possible combination of each technical characteristic in above-described embodiment
All it is described.
Above-described embodiment is the solid air purification smell removal agent with degradation property provided by the present invention and preparation side
A kind of way of realization of method, according to other deformation of scheme provided by the present invention, increases or reduces composition therein or step
Suddenly, or the present invention is used for other the technical field close with the present invention, belongs to protection scope of the present invention.
Claims (10)
1. there is a solid air purification smell removal agent for degradation property, it is characterized in that: according to part by weight, include 4A boiling
Stone, kieselguhr and tartaric acid.
The solid air purification smell removal agent with degradation property the most according to claim 1, is characterized in that: include formation
There is 4A zeolite, kieselguhr and the tartaric acid of the crystalline solid of a diameter of 0.58 ~ 0.7nm of poroid body.
The solid air purification smell removal agent with degradation property the most according to claim 1, is characterized in that: also include phosphorus
Acid and potassium permanganate.
The solid air purification smell removal agent with degradation property the most according to claim 3, is characterized in that: according to weight ratio
Example, includes 50 ~ 70 parts of 4A zeolite, 5 ~ 10 parts of tartaric acid, phosphoric acid 3.2 ~ 4.8 parts, 2 ~ 10 parts of potassium permanganate, kieselguhr 10
~ 40 parts.
The solid air purification smell removal agent with degradation property the most according to claim 1, is characterized in that: according to weight ratio
Example, includes 55 parts of 4A zeolite, 8 parts of tartaric acid, phosphatase 24 part, 3 parts of potassium permanganate, 30 parts of kieselguhr.
The solid air purification smell removal agent with degradation property the most according to claim 1, is characterized in that: 4A zeolite and silicon
Diatomaceous earth is set to food stage, and tartaric acid, phosphoric acid and potassium permanganate are set to health care level.
7. there is a preparation method for the solid air purification smell removal agent of degradation property, it is characterized in that: the steps include: 4A to boil
Stone and diatomaceous mixture react with tartaric acid, then reaction is obtained thing carry out drying and pulverization process, powder
Reaction obtain thing and phosphoric acid and potassium permanganate carries out ripening, then carry out pelletize and drying and processing, obtain solid air clean
Change eliminating smell agent finished product.
The preparation method of the solid air purification smell removal agent with degradation property the most according to claim 7, is characterized in that:
The steps include:
4A zeolite and kieselguhr are mixed to form intermedium I according to part by weight,
Adding the tartaric acid solution that concentration is 18-22% in intermedium I and form mixed solution, the PH adjusting mixed solution is 7-
9, make mixed solution carry out chemical reaction 2.8-3.2h and obtain intermedium II,
Intermedium II is carried out drying and processing in 380-420 DEG C of environment and obtains the powder of 80 ~ 120 mesh through pulverization process
Agent,
According to part by weight, phosphoric acid and potassium permanganate are carried out mixing and add suitable quantity of water with powder to mix homogeneously, then enter
The ripening of row 0.8-1.2h waits until intermedium III,
Intermedium III, through prilling granulator shaped granule, carries out drying and processing in the environment of 118-122 DEG C and obtains solid air
Purification smell removal agent finished product.
The preparation method of the solid air purification smell removal agent with degradation property the most according to claim 7, is characterized in that:
Shaped granule is set to 3 ~ 5mm spherosome.
The preparation method of the solid air purification smell removal agent with degradation property the most according to claim 7, its feature
It is: the diameter of the poroid body of shaped granule is set to 0.58 ~ 0.7nm.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107252613A (en) * | 2017-07-27 | 2017-10-17 | 嘉兴市九分钟生物科技有限公司 | It is a kind of to remove ammonia and the material for air purification of deodorization and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107252613A (en) * | 2017-07-27 | 2017-10-17 | 嘉兴市九分钟生物科技有限公司 | It is a kind of to remove ammonia and the material for air purification of deodorization and preparation method thereof |
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