CN1061054A - The manufacture method of additive for KCL galvanizing electrolyte - Google Patents
The manufacture method of additive for KCL galvanizing electrolyte Download PDFInfo
- Publication number
- CN1061054A CN1061054A CN 90108749 CN90108749A CN1061054A CN 1061054 A CN1061054 A CN 1061054A CN 90108749 CN90108749 CN 90108749 CN 90108749 A CN90108749 A CN 90108749A CN 1061054 A CN1061054 A CN 1061054A
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- CN
- China
- Prior art keywords
- peregal
- additive
- kcl
- manufacture
- galvanizing electrolyte
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000000654 additive Substances 0.000 title claims abstract description 13
- 230000000996 additive Effects 0.000 title claims abstract description 12
- 238000005246 galvanizing Methods 0.000 title claims abstract description 12
- 239000003792 electrolyte Substances 0.000 title claims abstract description 10
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M potassium chloride Chemical compound data:image/svg+xml;base64,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 data:image/svg+xml;base64,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 [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 title claims abstract description 10
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 6
- 239000001211 (E)-4-phenylbut-3-en-2-one Substances 0.000 claims abstract description 6
- BWHOZHOGCMHOBV-BQYQJAHWSA-N Benzylideneacetone Chemical group 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CC(=O)\C=C\C1=CC=CC=C1 BWHOZHOGCMHOBV-BQYQJAHWSA-N 0.000 claims abstract description 6
- 229930008407 benzylideneacetone Natural products 0.000 claims abstract description 6
- WXMKPNITSTVMEF-UHFFFAOYSA-M Sodium benzoate Chemical compound 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[Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims abstract description 5
- 235000010234 sodium benzoate Nutrition 0.000 claims abstract description 5
- 239000004299 sodium benzoate Substances 0.000 claims abstract description 5
- 229920000191 poly(N-vinyl pyrrolidone) Polymers 0.000 claims description 12
- 238000010438 heat treatment Methods 0.000 claims description 6
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- 239000007788 liquid Substances 0.000 description 2
- HLBBKKJFGFRGMU-UHFFFAOYSA-M Sodium formate Chemical compound 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[Na+].[O-]C=O HLBBKKJFGFRGMU-UHFFFAOYSA-M 0.000 description 1
- NWONKYPBYAMBJT-UHFFFAOYSA-L Zinc sulfate Chemical compound 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[Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000003863 ammonium salts Chemical class 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- XFXPMWWXUTWYJX-UHFFFAOYSA-N cyanide Chemical compound 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- 238000005265 energy consumption Methods 0.000 description 1
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- QDPYDWXGZVHLMJ-UHFFFAOYSA-K potassium;zinc;trichloride Chemical compound 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[Cl-].[Cl-].[Cl-].[K+].[Zn+2] QDPYDWXGZVHLMJ-UHFFFAOYSA-K 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
Abstract
A kind of manufacture method of additive for KCL galvanizing electrolyte, it is made up of carrier and lacquer.Used lacquer is benzylideneacetone and Sodium Benzoate.Adopt the prepared additive of method of the present invention, can improve the performance of zinc-plated tank liquor, play the effect that improves covering power, covering power, light and cut down the consumption of energy, and overcome the deficiency of A, two kinds of solution-type additives of B, make use more convenient.
Description
The present invention relates to electroplate and used tank liquor class particularly zinc-plated tank liquor class.
The galvanizing flux that generally adopts is the zincic acid salt plating liquor of DE type additive at present.The current efficiency of this galvanizing flux is lower, the power consumption is higher, covering power, covering power, light is all relatively poor, current density range is narrower etc.In recent years, the potassium chloride zinc plating process that develops on the ammonium salt basis has promptly overcome some shortcomings of zincate, has solved the galvanized pollution problem of prussiate again, has saved the energy simultaneously widely.Though occurred polytype additive for KCL galvanizing electrolyte, but all be in secret experimental stage, their common deficiency is to be divided into two kinds of solution of A, B, adds and daily adding when joining groove, bring trouble to the operator, also influenced the stability of tank liquor.
The object of the present invention is to provide a kind ofly be convenient to operate, the additive for KCL galvanizing electrolyte of good stability.
The object of the present invention is achieved like this, and its composition is:
8701 or the sulfonated bodies 160～320g/l of peregal
Peregal (A-20) 70～150g/l
Benzylideneacetone 25～50g/l
Sodium Benzoate 38～75g/l
Its compound method is that above four kinds of components are mixed the post-heating dissolving, adds hot water to prescribed volume, 70 ℃ down insulation to fully dissolving, continued heating 6 hours or heat three 1 hour, middle naturally cooling.8701 or sulfonated bodies, the peregal (A-20) of peregal promptly be elementary brightening agent, be again the carrier of main brightener benzylideneacetone and sodium formiate, make that the dispersion of brightening agent in plating bath is more even.
The invention has the advantages that:
1, in KCL galvanizing electrolyte, uses this additive can improve the performances such as light, covering power, current efficiency of plating bath, the Application Areas of KCL galvanizing electrolyte is enlarged more, alleviate environmental pollution.
2, this additive is a kind of single-liquid type, easy to operate, be convenient to safeguard, the good stability of solution.
3, energy consumption reduction, fractional energy savings can reach 20～50%.
For example the utility model is described in detail below:
1, by every liter 8,701 240 gram, the proportioning of peregal (A-20) 110 grams, benzylideneacetone 40 grams, Sodium Benzoate 50 grams, mix heating for dissolving after having got medicine, add the volume of hot water to regulation, insulation is 6 hours under 70 ℃ of temperature, and make (or heat continuously 31 hour, naturally cooling between hour).A kind of pale brown look oily transparent liquid.
2, will go up 8701 described in the example and change following reflection into:
The peregal and the excessive vitriol oil reacted 60 minutes under 30 ℃～40 ℃ temperature, constantly stirred simultaneously, transferred PH=7 with 10% sodium hydroxide solution then, extracted with 1: 1 ethanolic soln, got the emulsus resultant.Other is with example 1.
Claims (3)
1, a kind of manufacture method of additive for KCL galvanizing electrolyte is characterized in that its composition is:
8701 or the sulfonated bodies 160～320g/l of peregal
Peregal (A-20) 70～150g/l
Benzylideneacetone 25～50g/l
Sodium Benzoate 38～75g/l
Four kinds of components are mixed the post-heating dissolving, add hot water to prescribed volume, 70 ℃ down insulation continued heating 6 hours or continued heating 1 hour to fully dissolving, naturally cooling, reheat 1 hour, naturally cooling again, reheat 1 hour.
2, the manufacture method of additive for KCL galvanizing electrolyte according to claim 1 is characterized in that best group becomes:
8701 or the sulfonated bodies 240g/l of peregal
Peregal (A-20) 110g/l
Benzylideneacetone 40g/l
Sodium Benzoate 50g/l
3, according to the manufacture method of claim 1,2 described additive for KCL galvanizing electrolyte, the sulfonated bodies that it is characterized in that described peregal is made by following method: the peregal and the excessive vitriol oil reacted 60 minutes under 30 ℃～40 ℃ temperature, constantly stir simultaneously, transfer PH=7 with 10% sodium hydroxide solution then, with ethanolic soln extraction in 1: 1, get the emulsus resultant.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 90108749 CN1061054A (en) | 1990-10-26 | 1990-10-26 | The manufacture method of additive for KCL galvanizing electrolyte |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 90108749 CN1061054A (en) | 1990-10-26 | 1990-10-26 | The manufacture method of additive for KCL galvanizing electrolyte |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1061054A true CN1061054A (en) | 1992-05-13 |
Family
ID=4881118
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 90108749 Pending CN1061054A (en) | 1990-10-26 | 1990-10-26 | The manufacture method of additive for KCL galvanizing electrolyte |
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| CN (1) | CN1061054A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101063219B (en) * | 2007-05-22 | 2010-08-25 | 昆明理工大学 | Technique for preparing zinc and Zn-Fe alloy electroplating brightener |
| CN101063220B (en) * | 2007-05-22 | 2010-09-22 | 昆明理工大学 | Zinc and Zn-Fe alloy electroplating brightener |
| CN101063216B (en) * | 2007-05-22 | 2010-09-22 | 昆明理工大学 | Zinc and Zn-Fe alloy electroplating bright technique |
-
1990
- 1990-10-26 CN CN 90108749 patent/CN1061054A/en active Pending
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101063219B (en) * | 2007-05-22 | 2010-08-25 | 昆明理工大学 | Technique for preparing zinc and Zn-Fe alloy electroplating brightener |
| CN101063220B (en) * | 2007-05-22 | 2010-09-22 | 昆明理工大学 | Zinc and Zn-Fe alloy electroplating brightener |
| CN101063216B (en) * | 2007-05-22 | 2010-09-22 | 昆明理工大学 | Zinc and Zn-Fe alloy electroplating bright technique |
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