CN105967146A - Gas distribution graphite component for hydrochloric acid synthesis furnace - Google Patents

Gas distribution graphite component for hydrochloric acid synthesis furnace Download PDF

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Publication number
CN105967146A
CN105967146A CN201610537837.9A CN201610537837A CN105967146A CN 105967146 A CN105967146 A CN 105967146A CN 201610537837 A CN201610537837 A CN 201610537837A CN 105967146 A CN105967146 A CN 105967146A
Authority
CN
China
Prior art keywords
chlorine
graphite
guide
hydrogen
module
Prior art date
Application number
CN201610537837.9A
Other languages
Chinese (zh)
Inventor
刘仍礼
缪世阳
陆俊
冯亮
张龙
Original Assignee
南通星球石墨设备有限公司
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 南通星球石墨设备有限公司 filed Critical 南通星球石墨设备有限公司
Priority to CN201610537837.9A priority Critical patent/CN105967146A/en
Publication of CN105967146A publication Critical patent/CN105967146A/en

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Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00Halogens; Halogen acids
    • C01B7/01Chlorine; Hydrogen chloride
    • C01B7/012Preparation of hydrogen chloride from the elements

Abstract

The invention relates to a gas distribution graphite component for a hydrochloric acid synthesis furnace. The gas distribution graphite component is characterized by comprising a hydrogen module and a chloride module; a plurality of hydrogen guiding holes and chloride guiding holes are respectively formed in the hydrogen module and the chloride module, so that when hydrogen and chloride pass through the hydrogen module and the chloride module and then are mixed, both the hydrogen and the chloride spirally and rotationally rise and are contacted more sufficiently in the synthesis furnace, and a hydrogenation reaction during synthesis is more sufficient.

Description

A kind of hydrochloric acid synthetic furnace gas distribution graphite components
Technical field
The present invention relates to crystal vessel field, particularly relate to a kind of hydrochloric acid synthetic furnace gas distribution graphite components.
Background technology
In chemical industry synthetic furnace be primarily used to sulfuration, nitrification, hydrogenation, hydrocarbonylation, be polymerized, the pressure vessel of the process engineering such as condensation, principle is to be stirred by agitator by the various liquid in synthetic furnace, makes material dispersion uniform, reacts;General needs to be passed through in a kettle. by hydrogen and chlorine gas in synthetic furnace in the synthetic reaction of HCl gas, hydrogen and chlorine needed, by one section of graphite guide pipe, to enter back in synthetic furnace through graphite guide pipe and react before entering synthetic furnace.
General hydrogen and chlorine are directly entered in synthetic furnace by graphite guide pipe, so cause the reaction in synthetic furnace of hydrogen and chlorine insufficient, and substantial amounts of mixed gas can not the most thoroughly be reacted, and causes synthetic effect undesirable.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of hydrochloric acid synthetic furnace gas distribution graphite components, it is possible to makes hydrogen and chlorine increase through assembly rear screw between synthesis and is sufficiently stirred for, mix homogeneously so that hydrogenation is more abundant.
For solving above-mentioned technical problem, the technical scheme is that a kind of hydrochloric acid synthetic furnace gas distribution graphite components, its innovative point is: this is that graphite components includes: hydrogen module and chlorine module;
Described hydrogen module includes module bodies and graphite hydrogen guide;Described module bodies is ring type, and outward flange is the hypotenuse from the most outward-dipping extension of extreme direction on earth of module bodies top, and inwall is the circular contour limit of vertical direction;Described graphite hydrogen guide is cylindric, and the outer wall of graphite hydrogen guide and the inwall of module bodies are connected by resin glue and graphite hydrogen guide uses interference fit with module bodies;
The centre of described graphite hydrogen guide has through hole, inwall at graphite hydrogen guide has some groups of equally spaced hydrogen pilot holes, described hydrogen pilot hole is obliquely installed on graphite hydrogen guide, and the axis direction of hydrogen pilot hole and horizontal direction are 30 ° of angles;Described hydrogen pilot hole connects with the inwall of graphite hydrogen guide;
Described chlorine module top closure bottom end opening, chlorine module top is embedded in the through hole arranged in the middle of graphite hydrogen guide, and chlorine module includes chlorine conduit and graphite chlorine guide;Described graphite chlorine guide is arranged on the top of chlorine conduit and forms the top closed, graphite chlorine guide and chlorine conduit integral die-cast molding;The outline of described graphite chlorine guide is parabolic shape, offers several chlorine pilot holes on graphite chlorine guide;Described chlorine pilot hole is obliquely installed on graphite chlorine guide, and the axis of chlorine pilot hole and chlorine conduit axis direction are 30 ° of angles.
Further, the graphite chlorine guide on described chlorine module top is when being embedded into the intermediate throughholes of graphite hydrogen guide, and the height of chlorine pilot hole is higher than the upper surface of graphite hydrogen guide.
Further, if described chlorine pilot hole is distributed as dried layer on graphite chlorine guide, and the chlorine pilot hole shape ringwise of each layer is distributed on graphite chlorine guide.
It is an advantage of the current invention that: by being respectively arranged with several hydrogen pilot holes and chlorine pilot hole in hydrogen module and chlorine module, make hydrogen and chlorine when mixing after hydrogen module and chlorine module, hydrogen and chlorine rotate rising the most in the shape of a spiral, hydrogen is contacted in synthetic furnace more abundant with chlorine, hydrogenation during synthesis is more abundant.
Accompanying drawing explanation
The present invention is further detailed explanation with detailed description of the invention below in conjunction with the accompanying drawings.
Fig. 1 is that hydrochloric acid synthetic furnace gas is distributed graphite components hydrogen module top view.
Fig. 2 is that hydrochloric acid synthetic furnace gas is distributed graphite components hydrogen module front view.
Fig. 3 is that hydrochloric acid synthetic furnace gas is distributed graphite components chlorine module front view.
Fig. 4 is that hydrochloric acid synthetic furnace gas is distributed graphite components chlorine module top view.
Fig. 5 is that hydrochloric acid synthetic furnace gas is distributed graphite components top view.
Detailed description of the invention
The following examples can make professional and technical personnel that the present invention is more fully understood, but the most therefore limits the present invention among described scope of embodiments.
A kind of hydrochloric acid synthetic furnace gas distribution graphite components as shown in Figures 1 to 5, this is that graphite components includes: hydrogen module 1 and chlorine module 2;
Hydrogen module 1 includes module bodies 11 and graphite hydrogen guide 12;Described module bodies 11 is in ring type, and outward flange is the hypotenuse from the most outward-dipping extension of extreme direction on earth of module bodies 11 top, and inwall is the circular contour limit of vertical direction;Described graphite hydrogen guide 12 is cylindric, and the outer wall of graphite hydrogen guide 12 and the inwall of module bodies 11 are connected by resin glue and graphite hydrogen guide 12 uses interference fit with module bodies 11.
The centre of graphite hydrogen guide 12 has through hole 13, inwall at graphite hydrogen guide 12 has some groups of equally spaced hydrogen pilot holes 14, described hydrogen pilot hole 14 is obliquely installed on graphite hydrogen guide 12, and the axis direction of hydrogen pilot hole 14 and horizontal direction are 30 ° of angles;Described hydrogen pilot hole 14 connects with the inwall of graphite hydrogen guide 12.
Chlorine module 2 top closure bottom end opening, chlorine module 2 top is embedded in the through hole 13 arranged in the middle of graphite hydrogen guide 12, and chlorine module 2 includes chlorine conduit 21 and graphite chlorine guide 22;Described graphite chlorine guide 22 is arranged on the top of chlorine conduit 21 and forms the top closed, graphite chlorine guide 22 and chlorine conduit 21 integral die-cast molding;The outline of described graphite chlorine guide 22 is parabolic shape, offers several chlorine pilot holes 23 on graphite chlorine guide 22;Described chlorine pilot hole 23 22 is obliquely installed on graphite chlorine guide, and the axis of chlorine pilot hole 23 and chlorine conduit 21 axis direction are 30 ° of angles.
The graphite chlorine guide 22 on chlorine module 2 top is when being embedded into the intermediate throughholes 13 of graphite hydrogen guide 12, and the height of chlorine pilot hole 23 is higher than the upper surface of graphite hydrogen guide 12.
If chlorine pilot hole 23 is distributed as dried layer on graphite chlorine guide 22, and chlorine pilot hole 23 shape ringwise of each layer is distributed on graphite chlorine guide 22.
Skilled person will appreciate that of the industry; the present invention is not restricted to the described embodiments; the principle that the present invention is simply described described in above-described embodiment and description; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements both fall within scope of the claimed invention.Claimed scope is defined by appending claims and equivalent thereof.

Claims (3)

1. a hydrochloric acid synthetic furnace gas distribution graphite components, it is characterised in that: this is that graphite components includes: hydrogen module and chlorine module;
Described hydrogen module includes module bodies and graphite hydrogen guide;Described module bodies is ring type, and outward flange is the hypotenuse from the most outward-dipping extension of extreme direction on earth of module bodies top, and inwall is the circular contour limit of vertical direction;Described graphite hydrogen guide is cylindric, and the outer wall of graphite hydrogen guide and the inwall of module bodies are connected by resin glue and graphite hydrogen guide uses interference fit with module bodies;
The centre of described graphite hydrogen guide has through hole, inwall at graphite hydrogen guide has some groups of equally spaced hydrogen pilot holes, described hydrogen pilot hole is obliquely installed on graphite hydrogen guide, and the axis direction of hydrogen pilot hole and horizontal direction are 30 ° of angles;Described hydrogen pilot hole connects with the inwall of graphite hydrogen guide;
Described chlorine module top closure bottom end opening, chlorine module top is embedded in the through hole arranged in the middle of graphite hydrogen guide, and chlorine module includes chlorine conduit and graphite chlorine guide;Described graphite chlorine guide is arranged on the top of chlorine conduit and forms the top closed, graphite chlorine guide and chlorine conduit integral die-cast molding;The outline of described graphite chlorine guide is parabolic shape, offers several chlorine pilot holes on graphite chlorine guide;Described chlorine pilot hole is obliquely installed on graphite chlorine guide, and the axis of chlorine pilot hole and chlorine conduit axis direction are 30 ° of angles.
A kind of hydrochloric acid synthetic furnace gas distribution graphite components the most according to claim 1, it is characterized in that: the graphite chlorine guide on described chlorine module top is when being embedded into the intermediate throughholes of graphite hydrogen guide, and the height of chlorine pilot hole is higher than the upper surface of graphite hydrogen guide.
A kind of hydrochloric acid synthetic furnace gas distribution graphite components the most according to claim 1, it is characterized in that: if described chlorine pilot hole is distributed as dried layer on graphite chlorine guide, and the chlorine pilot hole shape ringwise of each layer is distributed on graphite chlorine guide.
CN201610537837.9A 2016-07-11 2016-07-11 Gas distribution graphite component for hydrochloric acid synthesis furnace CN105967146A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610537837.9A CN105967146A (en) 2016-07-11 2016-07-11 Gas distribution graphite component for hydrochloric acid synthesis furnace

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610537837.9A CN105967146A (en) 2016-07-11 2016-07-11 Gas distribution graphite component for hydrochloric acid synthesis furnace

Publications (1)

Publication Number Publication Date
CN105967146A true CN105967146A (en) 2016-09-28

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CN (1) CN105967146A (en)

Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20080233043A1 (en) * 2003-12-23 2008-09-25 Basf Akiengesellschaft Method For the Production of Chlorine By Means of Gas Phase Oxidation of Hydrogen Chloride
CN201632200U (en) * 2010-04-11 2010-11-17 豆林涛 Straight-pipe-type cyclone mixer
CN203215674U (en) * 2013-04-10 2013-09-25 郑州宏瑞耐火材料有限公司 Combustor with built-in hot air pipe and combustion in nozzle orthogonal jet mixed heat accumulator
CN203212320U (en) * 2013-04-02 2013-09-25 南通华耐特石墨设备有限公司 Hydrogen chloride synthetic furnace lamp head with guiding structure
CN103591586A (en) * 2013-05-20 2014-02-19 洛阳疋姆泰可精密零件制造有限公司 Fuel gas mixer
CN204127954U (en) * 2014-07-21 2015-01-28 宝鸡市晋旺达机械设备有限公司 Gas ignition jet pipe and mineral hot furnace
CN104373939A (en) * 2013-08-14 2015-02-25 赵广庆 Oxygen/hydrogen mixture fired diffusion nozzle
CN204320187U (en) * 2014-12-09 2015-05-13 淄博中旭医疗科技有限公司 Vortex generator and air flow stirring apparatus
CN204503037U (en) * 2015-01-13 2015-07-29 刘英聚 A kind of three-dimensional mixed distribution device
CN105090980A (en) * 2015-08-19 2015-11-25 河南科技大学 Spiral-flow type fluidized bed incinerator
CN205055840U (en) * 2015-09-02 2016-03-02 中冶华天南京工程技术有限公司 Gaseous swirler and whirl blender
CN205907027U (en) * 2016-07-11 2017-01-25 南通星球石墨设备有限公司 Hydrochloric acid synthetic furnace gas distribution graphite subassembly

Patent Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20080233043A1 (en) * 2003-12-23 2008-09-25 Basf Akiengesellschaft Method For the Production of Chlorine By Means of Gas Phase Oxidation of Hydrogen Chloride
CN201632200U (en) * 2010-04-11 2010-11-17 豆林涛 Straight-pipe-type cyclone mixer
CN203212320U (en) * 2013-04-02 2013-09-25 南通华耐特石墨设备有限公司 Hydrogen chloride synthetic furnace lamp head with guiding structure
CN203215674U (en) * 2013-04-10 2013-09-25 郑州宏瑞耐火材料有限公司 Combustor with built-in hot air pipe and combustion in nozzle orthogonal jet mixed heat accumulator
CN103591586A (en) * 2013-05-20 2014-02-19 洛阳疋姆泰可精密零件制造有限公司 Fuel gas mixer
CN104373939A (en) * 2013-08-14 2015-02-25 赵广庆 Oxygen/hydrogen mixture fired diffusion nozzle
CN204127954U (en) * 2014-07-21 2015-01-28 宝鸡市晋旺达机械设备有限公司 Gas ignition jet pipe and mineral hot furnace
CN204320187U (en) * 2014-12-09 2015-05-13 淄博中旭医疗科技有限公司 Vortex generator and air flow stirring apparatus
CN204503037U (en) * 2015-01-13 2015-07-29 刘英聚 A kind of three-dimensional mixed distribution device
CN105090980A (en) * 2015-08-19 2015-11-25 河南科技大学 Spiral-flow type fluidized bed incinerator
CN205055840U (en) * 2015-09-02 2016-03-02 中冶华天南京工程技术有限公司 Gaseous swirler and whirl blender
CN205907027U (en) * 2016-07-11 2017-01-25 南通星球石墨设备有限公司 Hydrochloric acid synthetic furnace gas distribution graphite subassembly

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Application publication date: 20160928