CN105949833B - Solution of surface treatment for Longquan sword highly effective antirust and preparation method thereof - Google Patents
Solution of surface treatment for Longquan sword highly effective antirust and preparation method thereof Download PDFInfo
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- CN105949833B CN105949833B CN201610551585.5A CN201610551585A CN105949833B CN 105949833 B CN105949833 B CN 105949833B CN 201610551585 A CN201610551585 A CN 201610551585A CN 105949833 B CN105949833 B CN 105949833B
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- longquan sword
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- 238000004381 surface treatment Methods 0.000 title claims abstract description 8
- 238000002360 preparation method Methods 0.000 title claims description 7
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 claims abstract description 4
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 claims abstract description 4
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000000203 mixture Substances 0.000 claims abstract description 3
- 239000002994 raw material Substances 0.000 claims description 11
- 239000012530 fluid Substances 0.000 claims description 7
- 239000012153 distilled water Substances 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 229920004890 Triton X-100 Polymers 0.000 claims description 4
- 239000013504 Triton X-100 Substances 0.000 claims description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 3
- NWGKJDSIEKMTRX-AAZCQSIUSA-N Sorbitan monooleate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O NWGKJDSIEKMTRX-AAZCQSIUSA-N 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 3
- 238000002604 ultrasonography Methods 0.000 claims description 3
- ORVGYTXFUWTWDM-UHFFFAOYSA-N silicic acid;sodium Chemical compound [Na].O[Si](O)(O)O ORVGYTXFUWTWDM-UHFFFAOYSA-N 0.000 claims 1
- 238000005260 corrosion Methods 0.000 abstract description 8
- 230000007797 corrosion Effects 0.000 abstract description 8
- 239000002932 luster Substances 0.000 abstract description 5
- 239000004115 Sodium Silicate Substances 0.000 abstract description 4
- 235000019795 sodium metasilicate Nutrition 0.000 abstract description 4
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 abstract description 4
- 229910052911 sodium silicate Inorganic materials 0.000 abstract description 4
- QRUDEWIWKLJBPS-UHFFFAOYSA-N benzotriazole Chemical compound C1=CC=C2N[N][N]C2=C1 QRUDEWIWKLJBPS-UHFFFAOYSA-N 0.000 abstract 1
- 239000012964 benzotriazole Substances 0.000 abstract 1
- 238000003672 processing method Methods 0.000 abstract 1
- GPRLSGONYQIRFK-MNYXATJNSA-N triton Chemical compound [3H+] GPRLSGONYQIRFK-MNYXATJNSA-N 0.000 abstract 1
- 238000000034 method Methods 0.000 description 12
- 150000003839 salts Chemical class 0.000 description 9
- 238000002474 experimental method Methods 0.000 description 6
- 239000003595 mist Substances 0.000 description 6
- 239000007921 spray Substances 0.000 description 3
- JMTMSDXUXJISAY-UHFFFAOYSA-N 2H-benzotriazol-4-ol Chemical compound OC1=CC=CC2=C1N=NN2 JMTMSDXUXJISAY-UHFFFAOYSA-N 0.000 description 2
- -1 5- hexyl Chemical group 0.000 description 2
- PZBQVZFITSVHAW-UHFFFAOYSA-N 5-chloro-2h-benzotriazole Chemical class C1=C(Cl)C=CC2=NNN=C21 PZBQVZFITSVHAW-UHFFFAOYSA-N 0.000 description 2
- 150000001565 benzotriazoles Chemical class 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- NPZTUJOABDZTLV-UHFFFAOYSA-N hydroxybenzotriazole Substances O=C1C=CC=C2NNN=C12 NPZTUJOABDZTLV-UHFFFAOYSA-N 0.000 description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 2
- 235000008331 Pinus X rigitaeda Nutrition 0.000 description 1
- 235000011613 Pinus brutia Nutrition 0.000 description 1
- 241000018646 Pinus brutia Species 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D1/00—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
- C09D1/02—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances alkali metal silicates
- C09D1/04—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances alkali metal silicates with organic additives
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
Abstract
The solution and processing method of a kind of surface treatment for Longquan sword highly effective antirust, the solution is by following proportioning solution composition：0.50~7.0g/L of sodium metasilicate, 0.0001~0.005g/L of benzotriazole and its derivative, 0.5~6g/L of sorbester p17,0.1~3.0g/L of rosin；0.2~6.0g/L of Triton X-100,0.10~4.0g/L of PPI, treatment temperature are normal temperature, realize Longquan sword surface antirust treatment, and the sword face after handling keeps the intrinsic metallic luster of Longquan sword bright, and there are good stability and corrosion resistance.
Description
Technical field
The invention belongs to Longquan sword highly effective antirust treatment technology, and in particular to one kind is efficiently prevented for Longquan sword
The solution of the surface treatment of rust.
Background technology
Longquan sword with its advanced cultural deposits, complicated technological process and composition, sharp blade and it is famous, but dragon
Spring double-edged sword complex manufacturing technology, cause its protection and maintenance method troublesome, such as periodically apply antirust oil, sword body can not be touched.
It is an object of the invention to provide the surface treatment method that a kind of step of Longquan sword highly effective antirust one is completed, this method
After handling Longquan sword antirust workpiece, keep the intrinsic metallic luster of Longquan sword bright, and have good stabilization
Property and corrosion resistance.
The content of the invention
The technical problems to be solved by the invention are to provide at the surface that a kind of step of Longquan sword highly effective antirust one is completed
The solution of reason, after this method is handled Longquan sword antirust workpiece, keep the intrinsic metallic luster of Longquan sword bright, and
And there are good stability and corrosion resistance.
Technical scheme is that the 1L solution is made up of the raw material of following quality proportionings used by solving above-mentioned technical problem：
Limited as further, 1L Longquan swords antirust treatment liquid of the present invention is most preferably by the raw material group of following quality proportionings
Into：
The present invention be used for Longquan sword treatment fluid preparation method be：700mL distilled water is measured to add in beaker, according to
The quality proportioning of above-mentioned raw materials, by sodium metasilicate, Arlacel-80, rosin, Triton X-100, PPI adds should
In beaker, ultrasound to solid is completely dissolved；50ml alcohol separately is taken, by BTA or derivatives thereof dissolving wherein, then by 2
Kind solution is well mixed, and is settled to 1L with distilled water, is configured to treatment fluid.
The present invention realizes Longquan sword antirusting treating method by adding corrosion inhibiter and surface filming agent in the solution,
Treatment fluid has the stability of height simultaneously, after this method is handled Longquan sword antirust workpiece, keeps Longquan sword to consolidate
Some metallic luster is bright, and has good stability and corrosion resistance.
Brief description of the drawings
Fig. 1 is the photo before Longquan sword salt mist experiment；
Fig. 2 is that Longquan sword does not use the antirusting treating method salt mist experiment photo of 12 hours of the present invention；
Fig. 3 is that Longquan sword uses the antirusting treating method salt mist experiment photo of 12 hours of the present invention；
Fig. 4 is that Longquan sword does not use the antirusting treating method salt mist experiment photo of 60 hours of the present invention；
Fig. 5 is that Longquan sword uses one of 60 hours photo of antirusting treating method salt mist experiment of the present invention；
Fig. 6 is that Longquan sword uses the two of the antirusting treating method salt mist experiment photo of 60 hours of the present invention.
Embodiment
With reference to example, the present invention is described in more detail, but the invention is not restricted to these embodiments.
1L solution of the present invention is made up of the raw material of following quality proportionings：
Wherein Benzotriazole Derivative include methyl benzotriazazole, hydroxy benzo triazole, 5- Chloro-Benzotriazoles,
5- nitros BTA, 5- hexyl BTAs.
Embodiment 1
Exemplified by preparing Longquan sword surface antirust solution 1L of the present invention, raw materials used and its quality proportioning is：
Its preparation method is as follows：
Measure 700mL distilled water to add in beaker, according to the quality proportioning of above-mentioned raw materials, by sodium metasilicate, Arlacel-80, pine
Perfume (or spice), Triton X-100, PPI are added in the beaker, and ultrasound to solid is completely dissolved；50ml alcohol separately is taken,
By BTA or derivatives thereof dissolving wherein, then 2 kinds of solution are well mixed, 1L is settled to distilled water, is configured to
Treatment fluid.
Longquan sword result such as Fig. 3 is handled using the embodiment, salt spray test keeps gloss in 12 hours.
Embodiment 2
Exemplified by preparing Longquan sword surface antirust solution 1L of the present invention, raw materials used and its quality proportioning is：
Corrosion inhibiter and surface filming agent are added in solution, Longquan sword antirust treatment is realized, result such as Fig. 6, makes
After Longquan sword salt spray test 60 hours, intrinsic metallic luster light is kept, and has good stability and corrosion resistance,
The solution has not stratified, the excellent performance of non-setting high stability.Corrosion inhibiter：BTA or derivatives thereof, into
Film：Sodium metasilicate, Triton X-100, PPI and rosin.
Wherein Benzotriazole Derivative include methyl benzotriazazole, hydroxy benzo triazole, 5- Chloro-Benzotriazoles,
5- nitros BTA, 5- hexyl BTAs.
Its preparation method is same as Example 1.
Embodiment 3
Exemplified by preparing Longquan sword surface antirust solution 1L of the present invention, raw materials used and its quality proportioning is：
Its preparation method is same as Example 1.
Longquan sword result such as Fig. 5 is handled using the embodiment, salt spray test also keeps certain gloss in 60 hours.
Claims (3)
1. the solution of a kind of surface treatment for Longquan sword highly effective antirust, it is characterised in that the 1L treatment fluids are by following quality
The raw material composition of proportioning：
2. the solution of the surface treatment according to claim 1 for Longquan sword highly effective antirust, it is characterised in that 1 L should
Treatment fluid is made up of the raw material of following quality proportionings：
3. the solution of the surface treatment according to claim 1 or 2 for Longquan sword highly effective antirust, it is characterised in that
The preparation method of the solution is：Measure 700mL distilled water to add in beaker, according to the quality proportioning of above-mentioned raw materials, by silicic acid
Sodium, Arlacel-80, rosin, Triton X-100, PPI are added in the beaker, and ultrasound to solid is completely dissolved；
50ml alcohol separately is taken, by BTA or derivatives thereof dissolving wherein, then 2 kinds of solution is well mixed, determined with distilled water
Hold to 1L, be configured to treatment fluid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610551585.5A CN105949833B (en) | 2016-07-11 | 2016-07-11 | Solution of surface treatment for Longquan sword highly effective antirust and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610551585.5A CN105949833B (en) | 2016-07-11 | 2016-07-11 | Solution of surface treatment for Longquan sword highly effective antirust and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105949833A CN105949833A (en) | 2016-09-21 |
| CN105949833B true CN105949833B (en) | 2017-12-26 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610551585.5A Active CN105949833B (en) | 2016-07-11 | 2016-07-11 | Solution of surface treatment for Longquan sword highly effective antirust and preparation method thereof |
Country Status (1)
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| CN (1) | CN105949833B (en) |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| BE825180A (en) * | 1974-02-12 | 1975-08-04 | RELATIVELY LOW TEMPERATURE CURING COATING COMPOSITION | |
| CN1140768A (en) * | 1995-07-15 | 1997-01-22 | 武汉水利电力大学 | Copper corrosion inhibitor and its using method |
| CN102618374A (en) * | 2012-03-07 | 2012-08-01 | 东莞市安美润滑科技有限公司 | Water-based cutting fluid used in slice machining of hard brittle crystal material and preparation method of water-based cutting fluid |
| CN102936732B (en) * | 2012-11-30 | 2014-07-02 | 山东大学 | Aluminum alloy die-cast surface cleaning agent and preparation method thereof |
| CN103074174A (en) * | 2012-12-29 | 2013-05-01 | 江苏飞拓界面工程科技有限公司 | Cleaning agent for heavy oil dirt |
| CN104017636B (en) * | 2014-06-06 | 2016-07-13 | 清华大学 | A kind of complete synthesis metal grinding fluid of water solublity |
| CN105695996B (en) * | 2016-02-01 | 2017-12-29 | 重庆大学 | A kind of pH sensitive intelligence corrosion inhibiter and preparation method thereof |
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| TR01 | Transfer of patent right |
Effective date of registration: 20190429 Address after: 313105 Lushan Township Industrial Concentration Zone, Changxing County, Huzhou City, Zhejiang Province Patentee after: Zhejiang Zhanxin New Energy Technology Co.,Ltd. Address before: 323000 Xueyuan Road 1, Lishui, Zhejiang Patentee before: Lishui University |
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| TR01 | Transfer of patent right |
Effective date of registration: 20231017 Address after: No. 19-3 Baoqiao Road, Huaxi Street, Changxing County, Huzhou City, Zhejiang Province, 313114 Patentee after: Zhejiang Zhixin Technology Co.,Ltd. Address before: 313105 Lushan Township Industrial Concentration Zone, Changxing County, Huzhou City, Zhejiang Province Patentee before: Zhejiang Zhanxin New Energy Technology Co.,Ltd. |
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