CN105854778A - Brownification reagent production reaction kettle with cooling device - Google Patents
Brownification reagent production reaction kettle with cooling device Download PDFInfo
- Publication number
- CN105854778A CN105854778A CN201610462738.9A CN201610462738A CN105854778A CN 105854778 A CN105854778 A CN 105854778A CN 201610462738 A CN201610462738 A CN 201610462738A CN 105854778 A CN105854778 A CN 105854778A
- Authority
- CN
- China
- Prior art keywords
- kettle
- brownification
- chiller
- reaction
- reactor
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000001816 cooling Methods 0.000 title claims abstract description 14
- 238000006243 chemical reaction Methods 0.000 title abstract description 16
- 238000004519 manufacturing process Methods 0.000 title abstract description 9
- 239000003153 chemical reaction reagent Substances 0.000 title abstract description 5
- 238000007599 discharging Methods 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000003795 chemical substances by application Substances 0.000 claims description 15
- 238000003756 stirring Methods 0.000 claims description 15
- 239000007788 liquid Substances 0.000 claims description 12
- 239000010865 sewage Substances 0.000 claims description 5
- 239000000843 powder Substances 0.000 abstract description 9
- 238000004140 cleaning Methods 0.000 abstract description 3
- 239000000428 dust Substances 0.000 abstract description 3
- 239000000463 material Substances 0.000 abstract description 3
- 238000000034 method Methods 0.000 description 5
- 238000010276 construction Methods 0.000 description 2
- 230000005611 electricity Effects 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 230000005587 bubbling Effects 0.000 description 1
- 239000012295 chemical reaction liquid Substances 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000012495 reaction gas Substances 0.000 description 1
- 238000005316 response function Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
- B01J2219/00081—Tubes
Abstract
The invention relates to a reaction kettle, belongs to the field of chemical reaction equipment and particularly relates to a brownification reagent production reaction with a cooling device. The brownification reagent production reaction kettle comprises a kettle body, wherein a feeding hole is formed in the top of the kettle body; a discharging hole is formed in the bottom; a condenser pipe is wounded on the inner wall of the kettle body, and is connected with a circulating water cooling system. The brownification reagent production reaction kettle provided by the invention has the advantages that (1) the design is simple and the structure is simple; (2) the powder tube in kettle is short, the residual materials in the powder tube can be reduced and the powder tube can be conveniently cleaned; (3) the dust scattering amount can be effectively reduced and the personal safety of staff can be ensured; (4) the cooling treatment can be carried out and the reaction and production efficiencies are improved.
Description
Technical field
The present invention relates to a kind of reactor, belong to chemical reaction equipment field, be specifically related to cooling dress
The brown agent put produces reactor.
Background technology
Brown agent is the place improving printed circuit board multilayer printed circuit internal layer copper face with polymeric material cohesive force
Reason liquid.The production process of this reagent needs use reactor and need middle product are added hot and cold
But operate.
The broad understanding of reactor i.e. has the container physically or chemically reacted, by designing the structure of container
With parameter configuration, it is achieved the mixing of technological requirement, heating, response function.Reaction liquid and gas reaction
Thing sufficiently mixes in reactor, reacts.Generally in reactor, gas liquid reaction uses bubbling method
Carrying out, gas-to-liquid contact is insufficient, and reaction rate is the highest, and utilization rate of equipment and installations is the lowest.
In Conventional process, powder feeding mode also can produce powder wall built-up, liquid backflow, clean difficulty
Greatly, powder body pollute the factors such as working environment is severe cause powder in production process consume big, production efficiency is low
And produce respirable dust pollution to problems such as health damage.
Additionally, traditional reactor is operationally, owing to chemical heat release can cause the internal temperature of reactor
Degree raises, and affects reaction efficiency and there is potential safety hazard, and in some techniques, after needing reaction
Product carry out cooling process.
Summary of the invention
The present invention mainly solves the above-mentioned technical problem existing for prior art；Provide with cooling
The brown agent of device produces reactor.This mixer design is reasonable, simple in construction, powder body length of tube in still
Short, not only can reduce the residual material in powdered pipe, be also convenient for cleaning；Can effectively reduce dust to fly away,
Ensure safety of employees；And by chiller, reactor can be lowered the temperature, it is ensured that temperature of reaction kettle
Constant, the most also ensure equipment safety.
The above-mentioned technical problem of the present invention is mainly addressed by following technical proposals:
Brown agent with chiller produces reactor, and including kettle, the top of described kettle is provided with
Charging aperture, bottom is provided with discharging opening；It is wound around on the inwall of described kettle and is provided with condensing tube, described cold
Solidifying pipe is connected with circulating water cooling system.
Optimizing, the above-mentioned brown agent with chiller produces reactor, and described kettle is provided with
Two position alarm, described two position alarm respectively with the low liquid level buoy being arranged within kettle
It is connected with high level buoy.
Optimizing, the above-mentioned brown agent with chiller produces reactor, and described kettle is provided with
Agitating device, described agitating device includes: be installed on the stirring motor at described kettle top, with stirring electricity
The shaft that machine is connected, is installed on the stirring vane on described shaft.
Optimizing, the above-mentioned brown agent with chiller produces reactor, and described stirring vane is ripple
Shape wave.
Optimizing, the above-mentioned brown agent with chiller produces reactor, and the bottom of described kettle sets
It is equipped with sewage draining exit.
Therefore, present invention have the advantage that 1. is reasonable in design, simple in construction；2, powder can effectively be reduced
Dirt flies away, and ensures safety of employees；3. cooling process be can carry out, reaction and production efficiency improved.
Accompanying drawing explanation
Fig. 1 is the structural representation of the present invention.
Detailed description of the invention
Below by embodiment, and combine accompanying drawing, technical scheme is made more specifically
Bright.
In figure, kettle 1, charging aperture 2, discharging opening 3, condensing tube 4, circulating water cooling system 5, just
Liquid level alarm 6, low liquid level buoy 7, high level buoy 8, stirring motor 9, shaft 10, stirring
Blade 11, sewage draining exit 12.
Embodiment:
As it is shown in figure 1, the brown agent with chiller produces reactor, including kettle 1, kettle 1
Top is provided with charging aperture 2, and bottom is provided with discharging opening 3；It is wound around on the inwall of kettle 1 and is provided with condensation
Pipe 4, described condensing tube 4 is connected with circulating water cooling system 5.The bottom of kettle 1 is provided with sewage draining exit
12。
Be provided with two position alarm 6 on kettle 1, two position alarm 6 respectively be arranged at kettle
Low liquid level buoy 7 within 1 is connected with high level buoy 8.
Being provided with agitating device on kettle 1, agitating device includes: be installed on the stirring electricity at kettle 1 top
Machine 9, the shaft 10 being connected with stirring motor 9, the stirring vane 11 being installed on shaft 10, stirs
Mix blade 11 for waveform.
Use after said structure, low liquid level buoy 7 and high level buoy 8 can measure respectively minimum liquid level and
High level, and by two position alarm 6 display and warning.In course of reaction or reaction knot
Shu Hou, can carry out cooling process by chiller to reactor or product.
Specific embodiment described herein is only to present invention spirit explanation for example.Institute of the present invention
Belong to those skilled in the art described specific embodiment to make various amendment or supplement
Or use similar mode to substitute, but without departing from the spirit of the present invention or surmount claims
Scope defined in book.
Although the most more employing in figure, kettle 1, charging aperture 2, discharging opening 3, condensing tube 4,
Circulating water cooling system 5, two position alarm 6, low liquid level buoy 7, high level buoy 8, stirring
Motor 9, shaft 10, stirring vane 11, sewage draining exit 12 term such as grade, but be not precluded from using other art
The probability of language.Use these terms to be only used to more easily to describe and explain the essence of the present invention；
It is all contrary with spirit of the present invention for being construed as any additional restriction.
Claims (5)
1. the brown agent with chiller produces reactor, including kettle (1), it is characterised in that described
The top of kettle (1) is provided with charging aperture (2), and bottom is provided with discharging opening (3)；Described kettle (1) interior
Being wound around on wall and be provided with condensing tube (4), described condensing tube (4) is connected with circulating water cooling system (5).
Brown agent with chiller the most according to claim 1 produces reactor, and its feature exists
In, described kettle (1) is provided with two position alarm (6), described two position alarm (6) is respectively
The low liquid level buoy (7) internal with being arranged at kettle (1) and high level buoy (8) are connected.
Brown agent with chiller the most according to claim 1 produces reactor, and its feature exists
In, described kettle (1) is provided with agitating device, described agitating device includes: be installed on described kettle (1)
The stirring motor (9) at top, the shaft (10) being connected with stirring motor (9), it is installed on described shaft
(10) stirring vane (11) on.
Brown agent with chiller the most according to claim 3 produces reactor, and its feature exists
In, described stirring vane (11) is waveform.
Brown agent with chiller the most according to claim 1 produces reactor, and its feature exists
In, the bottom of described kettle (1) is provided with sewage draining exit (12).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610462738.9A CN105854778A (en) | 2016-06-22 | 2016-06-22 | Brownification reagent production reaction kettle with cooling device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610462738.9A CN105854778A (en) | 2016-06-22 | 2016-06-22 | Brownification reagent production reaction kettle with cooling device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105854778A true CN105854778A (en) | 2016-08-17 |
Family
ID=56655010
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610462738.9A Pending CN105854778A (en) | 2016-06-22 | 2016-06-22 | Brownification reagent production reaction kettle with cooling device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105854778A (en) |
-
2016
- 2016-06-22 CN CN201610462738.9A patent/CN105854778A/en active Pending
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20160817 |
|
| WD01 | Invention patent application deemed withdrawn after publication |