CN105854768B - A kind of integrated form reaction kettle - Google Patents

A kind of integrated form reaction kettle Download PDF

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Publication number
CN105854768B
CN105854768B CN201610364500.2A CN201610364500A CN105854768B CN 105854768 B CN105854768 B CN 105854768B CN 201610364500 A CN201610364500 A CN 201610364500A CN 105854768 B CN105854768 B CN 105854768B
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China
Prior art keywords
tank body
pipe
head cover
wall
solution
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Application number
CN201610364500.2A
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Chinese (zh)
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CN105854768A (en
Inventor
王晓元
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SUZHOU CITY JINXIANG PRESSURE CONTAINER MANUFACTURE CO Ltd
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SUZHOU CITY JINXIANG PRESSURE CONTAINER MANUFACTURE CO Ltd
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Priority to CN201610364500.2A priority Critical patent/CN105854768B/en
Publication of CN105854768A publication Critical patent/CN105854768A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D29/00Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/50Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition
    • B01D29/56Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition in series connection
    • B01D29/58Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition in series connection arranged concentrically or coaxially
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D35/00Filtering devices having features not specifically covered by groups B01D24/00 - B01D33/00, or for applications not specifically covered by groups B01D24/00 - B01D33/00; Auxiliary devices for filtration; Filter housing constructions
    • B01D35/02Filters adapted for location in special places, e.g. pipe-lines, pumps, stop-cocks
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00054Controlling or regulating the heat exchange system
    • B01J2219/00056Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00058Temperature measurement
    • B01J2219/00063Temperature measurement of the reactants
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00076Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
    • B01J2219/00081Tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The invention discloses a kind of integrated form reaction kettle, including tank body, deflector, head cover, feed pipe, electric machine assembly, shaft, impeller, inner cylinder, coil pipe, casing, filter assemblies, grid, thermocouple, discharge nozzle, catalyst is placed on grid upper end in advance and coats filter assemblies, solution is pumped into tank body through feed pipe, due to the guide functions of inclined tube and deflector, solution flows into coil pipe along inner tank wall, come into full contact with after the filtering of the filtered component of solution with catalyst, until solution fills tank body, deep fat is injected into coil pipe to heat solution, electric machine assembly is rotated by shaft impeller, so as to be stirred to solution, thermocouple monitors solution temperature in real time, so that reaction carries out at a constant temperature.The apparatus structure is simple, and the functions such as automatic stirring, automatic fitration, automatic heating are integrated in one so that and solution comes into full contact with catalyst, meanwhile, homogeneous heating, improves reaction uniformity and stability.

Description

A kind of integrated form reaction kettle
Technical field
The present invention relates to a kind of reaction kettle, more particularly to a kind of integrated form reaction kettle.
Background technology
Reaction kettle is comprehensive reaction vessel, and it is raw to be widely used in oil, chemical industry, rubber, pesticide, dyestuff, medicine, food etc. Production type user and the research of various scientific experiment projects, for completing to hydrolyze, neutralizing, crystallizing, the technical process such as isothermal reaction Container.Existing reaction kettle function is more single, does not such as have automatic fitration function, causes solution surface gentle with a large amount of impurity Bubble, meanwhile, more to use heated by electrodes, heating uniformity is poor.In view of disadvantages described above, it is really necessary to design a kind of integrated form reaction Kettle.
The content of the invention
The technical problems to be solved by the invention are:A kind of integrated form reaction kettle is provided, to solve existing reaction kettle work( Can single and heating uniformity it is poor the problem of.
In order to solve the above technical problems, the technical scheme is that:A kind of integrated form reaction kettle, including tank body, water conservancy diversion Plate, head cover, feed pipe, electric machine assembly, shaft, impeller, inner cylinder, coil pipe, casing, filter assemblies, grid, thermocouple, discharge nozzle, The deflector is located on the right side of inner tank wall upper end, and the deflector is connected with tank body screw thread, and the head cover is located at tank At the top of body, the head cover is connected with tank body screw thread, and the feed pipe runs through head cover, and the feed pipe welds phase with head cover Even, the electric machine assembly is located at head cover top center, and the electric machine assembly is connected with head cover screw thread, and the shaft is passed through Wear head cover and be located at electric machine assembly lower end, the shaft is rotatedly connected with head cover and is connected with electric machine assembly close-fitting, described Impeller is located at shaft outer wall, and the impeller is connected with shaft close-fitting, and the inner cylinder is located at inner tank wall center, described Inner cylinder is connected with tank body welding, and the coil pipe is located at inner cylinder inner wall, and the coil pipe is weldingly connected with inner cylinder, the casing On the right side of inner tank wall lower end, the casing is connected with tank body welding, and the filter assemblies are through tank body and positioned at set Inside pipe wall, the filter assemblies are connected with tank body screw thread and are connected with shell clearance, and the grid is located at inner tank wall bottom Portion, the grid are connected with tank body welding, and the thermocouple runs through head cover, and the thermocouple is connected with head cover screw thread, The discharge nozzle is located at tank wall bottom, and the discharge nozzle is connected with tank body welding.
Further improvement of the invention is as follows:
Further, the tank body is additionally provided with probe tube, and the probe tube is located at tank wall bottom, and described takes Sample pipe is connected with tank body welding.
Further, the tank body is additionally provided with air inlet pipe, and the air inlet pipe is located at tank wall bottom, it is described into Tracheae is connected with tank body welding.
Further, the tank body is additionally provided with ear mount, and the ear mount is located at tank wall upper end, the ear mount with Tank body welding is connected.
Further, the feed pipe is additionally provided with inclined tube, and the inclined tube is located at feed pipe lower end, the inclined tube with Feed pipe is integrally connected.
Further, the angle between the feed pipe axis and inclined tube axis is 135 °.
Further, the inclined tube is additionally provided with pull rod, and the pull rod is located at inclined tube outer wall and is located at head cover lower end, institute The pull rod stated is weldingly connected with inclined tube and is weldingly connected with head cover.
Further, the inner cylinder is additionally provided with connecting plate, and the connecting plate is located at inner tank theca and in tank body Wall, the connecting plate are weldingly connected with inner cylinder and are connected with tank body welding.
Further, the filter assemblies further include screen pipe, filter screen, and the screen pipe is through tank body and is located at Internal surface of sleeve pipe, the screen pipe are connected with tank body screw thread and are connected with shell clearance, and the filter screen is located at outside screen pipe At the top of wall, the filter screen is weldingly connected with screen pipe.
Further, the screen pipe also seeks to orchid, and the flange is on the left of filtering pipe outer wall, the flange It is weldingly connected with screen pipe.
Compared with prior art, catalyst, during work, is placed on grid upper end and incited somebody to action by the integrated form reaction kettle in advance Component cladding is filtered, solution is pumped into tank body through feed pipe, and due to the guide functions of inclined tube and deflector, solution is along inner tank wall Coil pipe is flowed into, is come into full contact with after the filtering of the filtered component of solution with catalyst, until solution fills tank body, is injected into coil pipe Deep fat heats solution, and electric machine assembly is rotated by shaft impeller, so as to be stirred to solution, thermocouple is real-time Solution temperature is monitored, so that reaction carries out at a constant temperature.The apparatus structure is simple, by automatic stirring, automatic fitration, The functions such as automatic heating are integrated in one so that and solution comes into full contact with catalyst, meanwhile, homogeneous heating, it is uniform to improve reaction Property and stability.
Brief description of the drawings
Fig. 1 shows front view of the present invention
Fig. 2 shows feed pipe front view of the present invention
Fig. 3 shows filter assemblies front view of the present invention
1 deflector 2 of tank body
3 feed pipe 4 of head cover
5 shaft 6 of electric machine assembly
7 inner cylinder 8 of impeller
9 casing 10 of coil pipe
11 grid 12 of filter assemblies
13 discharge nozzle 14 of thermocouple
101 air inlet pipe 102 of probe tube
103 inclined tube 401 of ear mount
402 connecting plate 801 of pull rod
1101 filter screen 1102 of screen pipe
Flange 1103
Embodiment
As shown in Figure 1, Figure 2, Figure 3 shows, a kind of integrated form reaction kettle, including tank body 1, deflector 2, head cover 3, feed pipe 4, electricity Thermomechanical components 5, shaft 6, impeller 7, inner cylinder 8, coil pipe 9, casing 10, filter assemblies 11, grid 12, thermocouple 13, discharge nozzle 14, institute The deflector 2 stated is located on the right side of 1 inner wall upper end of tank body, and the deflector 2 is connected with 1 screw thread of tank body, and the head cover 3 is located at The top of tank body 1, the head cover 3 are connected with 1 screw thread of tank body, and the feed pipe 4 runs through head cover 3, the feed pipe 4 and top Lid 3 is weldingly connected, and the electric machine assembly 5 is located at 3 top center of head cover, the electric machine assembly 5 and 3 screw thread phase of head cover Even, the shaft 6 through head cover 3 and is located at 5 lower end of electric machine assembly, and the shaft 6 is rotatedly connected with head cover 3 and and motor 5 close-fitting of component is connected, and the impeller 7 is located at 6 outer wall of shaft, and the impeller 7 is connected with 6 close-fitting of shaft, the inner cylinder 8 At 1 inner wall center of tank body, the inner cylinder 8 is weldingly connected with tank body 1, and the coil pipe 9 is located at 8 inner wall of inner cylinder, described Coil pipe 9 be weldingly connected with inner cylinder 8, the casing 10 is located on the right side of 1 inner wall lower end of tank body, the casing 10 and tank body 1 It is weldingly connected, the filter assemblies 11 are through tank body 1 and are located at 10 inner wall of casing, the filter assemblies 11 and 1 spiral shell of tank body Line is connected and is connected with 10 gap of casing, and the grid 12 is located at 1 inner wall bottom of tank body, and the grid 12 is welded with tank body 1 Connect connected, described thermocouple 13 and run through head cover 3, the thermocouple 13 is connected with 3 screw thread of head cover, the discharge nozzle 14 In 1 outer wall bottom of tank body, the discharge nozzle 14 is weldingly connected with tank body 1, and the tank body 1 is additionally provided with probe tube 101, described Probe tube 101 be located at 1 outer wall bottom of tank body, the probe tube 101 is weldingly connected with tank body 1, and the tank body 1 is additionally provided with Air inlet pipe 102, the air inlet pipe 102 are located at 1 outer wall bottom of tank body, and the air inlet pipe 102 is weldingly connected with tank body 1, into The air pressure that tracheae 102 is used for tank body 1 detects, and the tank body 1 is additionally provided with ear mount 103, and the ear mount 103 is located at outside tank body 1 Wall upper end, the ear mount 103 are weldingly connected with tank body 1, and the feed pipe 4 is additionally provided with inclined tube 401, the inclined tube 401 Positioned at 4 lower end of feed pipe, the inclined tube 401 is connected with the one of feed pipe 4,4 axis of feed pipe and 401 axis of inclined tube Between angle be 135 °, the inclined tube 401 is additionally provided with pull rod 402, and the pull rod 402 is located at 401 outer wall of inclined tube and position In 3 lower end of head cover, the pull rod 402 is weldingly connected with inclined tube 401 and is weldingly connected with head cover 3, and the inner cylinder 8 is additionally provided with Connecting plate 801, the connecting plate 801 are located at 8 outer wall of inner cylinder and are located at 1 inner wall of tank body, the connecting plate 801 and inner cylinder 8 It is weldingly connected and is weldingly connected with tank body 1, the filter assemblies 11 further includes screen pipe 1101, filter screen 1102, described Screen pipe 1101 is through tank body 1 and is located at 10 inner wall of casing, the screen pipe 1101 be connected with 1 screw thread of tank body and with casing 10 Gap is connected, and the filter screen 1102 is located at the top of 1101 outer wall of screen pipe, the filter screen 1102 and screen pipe 1101 It is weldingly connected, the screen pipe 1101 also seeks to orchid 1103, and the flange 1103 is located on the left of 1101 outer wall of screen pipe, institute The flange 1103 stated is weldingly connected with screen pipe 1101, the integrated form reaction kettle, and during work, catalyst is placed on grid in advance 12 upper ends simultaneously coat filter assemblies, and solution is pumped into tank body 1 through feed pipe 4, since the water conservancy diversion of inclined tube 401 and deflector 2 is made With solution flows into coil pipe 9 along 1 inner wall of tank body, is come into full contact with after the filtering of the filtered component 11 of solution with catalyst, Zhi Daorong Liquid fills tank body, deep fat is injected into coil pipe 9 solution is heated, and electric machine assembly 5 is rotated by 6 impeller 7 of shaft, from And solution is stirred, thermocouple 13 monitors solution temperature in real time, so that reaction carries out at a constant temperature.The device It is simple in structure, the functions such as automatic stirring, automatic fitration, automatic heating are integrated in one so that solution fully connects with catalyst Touch, meanwhile, homogeneous heating, improves reaction uniformity and stability.
The present invention is not limited to above-mentioned specific embodiment, those of ordinary skill in the art from above-mentioned design, Without performing creative labour, a variety of conversion made, are within the scope of the present invention.

Claims (7)

1. a kind of integrated form reaction kettle, it is characterised in that including tank body, deflector, head cover, feed pipe, electric machine assembly, shaft, leaf Wheel, inner cylinder, coil pipe, casing, filter assemblies, grid, thermocouple, discharge nozzle, the deflector are located at the inner tank wall upper end right side Side, the deflector are connected with tank body screw thread, and the head cover is located at the top of tank body, the head cover and tank body screw thread phase Even, the feed pipe runs through head cover, and the feed pipe is weldingly connected with head cover, and the electric machine assembly is located at the top of head cover At center, the electric machine assembly is connected with head cover screw thread, and the shaft is through head cover and is located at electric machine assembly lower end, described Shaft be rotatedly connected with head cover and be connected with electric machine assembly close-fitting, the impeller is located at shaft outer wall, the impeller with Shaft close-fitting is connected, and the inner cylinder is located at inner tank wall center, and the inner cylinder is connected with tank body welding, the coil pipe Positioned at inner cylinder inner wall, the coil pipe is weldingly connected with inner cylinder, and the casing is located on the right side of inner tank wall lower end, the set Pipe is connected with tank body welding, and the filter assemblies are through tank body and are located at internal surface of sleeve pipe, the filter assemblies and tank body spiral shell Line is connected and is connected with shell clearance, and the grid is located at inner tank wall bottom, and the grid is connected with tank body welding, institute The thermocouple stated runs through head cover, and the thermocouple is connected with head cover screw thread, and the discharge nozzle is located at tank wall bottom, institute The discharge nozzle stated is connected with tank body welding;The feed pipe is additionally provided with inclined tube, and the inclined tube is located at feed pipe lower end, described Inclined tube and feed pipe be integrally connected;The inclined tube is additionally provided with pull rod, and the pull rod is located at inclined tube outer wall and is located at head cover Lower end, the pull rod are weldingly connected with inclined tube and are weldingly connected with head cover;The tank body is additionally provided with probe tube, and described takes Sample pipe is located at tank wall bottom, and the probe tube is connected with tank body welding.
2. integrated form reaction kettle as claimed in claim 1, it is characterised in that the tank body is additionally provided with air inlet pipe, it is described into Tracheae is located at tank wall bottom, and the air inlet pipe is connected with tank body welding.
3. integrated form reaction kettle as claimed in claim 1, it is characterised in that the tank body is additionally provided with ear mount, the ear mount Positioned at tank wall upper end, the ear mount is connected with tank body welding.
4. integrated form reaction kettle as claimed in claim 1, it is characterised in that between the feed pipe axis and inclined tube axis Angle be 135 °.
5. integrated form reaction kettle as claimed in claim 1, it is characterised in that the inner cylinder is additionally provided with connecting plate, the company Fishplate bar is located at inner tank theca and is located at inner tank wall, and the connecting plate is weldingly connected with inner cylinder and is connected with tank body welding.
6. integrated form reaction kettle as claimed in claim 1, it is characterised in that the filter assemblies further include screen pipe, filtering Net, the screen pipe is through tank body and is located at internal surface of sleeve pipe, and the screen pipe is connected with tank body screw thread and and shell clearance It is connected, at the top of filtering pipe outer wall, the filter screen is weldingly connected the filter screen with screen pipe.
7. integrated form reaction kettle as claimed in claim 6, it is characterised in that the screen pipe also seeks to orchid, the flange On the left of filtering pipe outer wall, the flange is weldingly connected with screen pipe.
CN201610364500.2A 2016-05-30 2016-05-30 A kind of integrated form reaction kettle Active CN105854768B (en)

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Application Number Priority Date Filing Date Title
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Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610364500.2A CN105854768B (en) 2016-05-30 2016-05-30 A kind of integrated form reaction kettle

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CN105854768A CN105854768A (en) 2016-08-17
CN105854768B true CN105854768B (en) 2018-05-04

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CN106823878B (en) * 2017-02-13 2024-09-06 安徽翠鸟生物技术有限公司 Solution extraction premixing device
CN106621457B (en) * 2017-02-13 2024-08-30 安徽翠鸟生物技术有限公司 Premixing stirring extraction device
CN107961742B (en) * 2017-12-08 2020-12-22 江苏旭阳化工设备有限公司 Chemical catalytic reaction cauldron
CN110449108A (en) * 2019-09-10 2019-11-15 浙江伟博化工科技有限公司 Esterification device is used in a kind of preparation of trioctyl trimellitate (TOTM)
CN112439378B (en) * 2020-10-21 2022-10-21 贵州凯襄新材料有限公司 Concrete water reducing agent preparation facilities

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU1155288A1 (en) * 1982-06-07 1985-05-15 Пензенский филиал Всесоюзного научно-исследовательского института антибиотиков Reactor
CN203725153U (en) * 2014-03-21 2014-07-23 连云港市三联化工有限公司 Reaction kettle capable of carrying out desalinating operation
CN204134607U (en) * 2014-08-29 2015-02-04 江苏弘盛新材料股份有限公司 A kind of caprolactam molten-bath
CN204619967U (en) * 2015-02-25 2015-09-09 无锡嘉加纳米科技有限公司 A kind of double-deck chemical industry reagent reacting still
CN204911507U (en) * 2015-09-10 2015-12-30 浙江亚迪纳新材料科技股份有限公司 Melamine resin reation kettle
CN205761148U (en) * 2016-05-30 2016-12-07 苏州市锦翔压力容器制造有限公司 A kind of integrated form reactor

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU1155288A1 (en) * 1982-06-07 1985-05-15 Пензенский филиал Всесоюзного научно-исследовательского института антибиотиков Reactor
CN203725153U (en) * 2014-03-21 2014-07-23 连云港市三联化工有限公司 Reaction kettle capable of carrying out desalinating operation
CN204134607U (en) * 2014-08-29 2015-02-04 江苏弘盛新材料股份有限公司 A kind of caprolactam molten-bath
CN204619967U (en) * 2015-02-25 2015-09-09 无锡嘉加纳米科技有限公司 A kind of double-deck chemical industry reagent reacting still
CN204911507U (en) * 2015-09-10 2015-12-30 浙江亚迪纳新材料科技股份有限公司 Melamine resin reation kettle
CN205761148U (en) * 2016-05-30 2016-12-07 苏州市锦翔压力容器制造有限公司 A kind of integrated form reactor

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