CN105819692B - A kind of brown opaque glaze and the method with glaze making vase - Google Patents

A kind of brown opaque glaze and the method with glaze making vase Download PDF

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Publication number
CN105819692B
CN105819692B CN201610130850.2A CN201610130850A CN105819692B CN 105819692 B CN105819692 B CN 105819692B CN 201610130850 A CN201610130850 A CN 201610130850A CN 105819692 B CN105819692 B CN 105819692B
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parts
glaze
component
weight proportion
frit
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CN201610130850.2A
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CN105819692A (en
Inventor
王必炉
张月群
王天
王天一
王文云
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Jingdezhen Royal Kiln Ceramic Co., Ltd.
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Ninghai Gallop Metal Products Co Ltd
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Priority to CN2015110241901 priority
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    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • C03C8/14Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/50Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
    • C04B41/5022Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
    • C04B41/81Coating or impregnation
    • C04B41/85Coating or impregnation with inorganic materials
    • C04B41/86Glazes; Cold glazes

Abstract

The invention discloses a kind of brown opaque glazes, including following component and weight proportion number:Frit:49 parts, feldspar:7~9 parts, quartz:13~14 parts, kaolin:8~9 parts, calcite:3.5~4.5 parts, dolomite:2~3 parts, burn talcum:8~10 parts, burn tin oxide:3~4 parts, black pigment:0.5~1 part, bronzing colorant:1~2 part;The glaze colours power is slightly strong, uniform color glaze is fine and smooth, and hardness is good, and durability against pollution is good, and acidproof alkali ability is good.A kind of method that brown opaque glaze good, simple for process makes vase that the invention also discloses environment-friendly types.

Description

A kind of brown opaque glaze and the method with glaze making vase
Technical field
The present invention relates to ceramic technology fields, are especially a kind of brown opaque glaze and the side with glaze making vase Method.
Background technology
Glaze is the glassy thin layer for the colorless or colored for being covered in ceramic surface.Glaze is outer in ceramic vase is exactly without glaze The inner wall for referring to this vase is that have glassy thin layer, does not have glassy thin layer on the bottle of outside.The inner wall of vase can be shown in this way Obtain smooth, scintillation glass gloss;Foreign body surface can generate dumb light with the texture of frosted, be during a kind of porcelain makes, frequently with Manufacture technique, embody a kind of unique smell being different from common porcelain, but tinting strength, tinting power is slightly lower, is especially making ceramics modelled after an antique When product, uneven color is even, and simple and unsophisticated effect is not achieved, at the same glaze is not fine and smooth enough, hardness is poor, durability against pollution is poor and Acidproof alkali ability is poor.
Invention content
The technical problem to be solved by the present invention is to provide that a kind of color power is slightly strong, uniform color glaze is fine and smooth, hardness is good, resistance to Dirty ability is good, the good brown opaque glaze of acidproof alkali ability and the method for making vase with the glaze.
To achieve the object of the present invention, following technical scheme is provided:
A kind of brown opaque glaze, including following component and weight proportion number:Frit:49 parts, feldspar:7~9 parts, stone English:13~14 parts, kaolin:8~9 parts, calcite:3.5~4.5 parts, dolomite:2~3 parts, burn talcum:8~10 parts, burn oxygen Change tin:3~4 parts, black pigment:0.5~1 part, bronzing colorant:1~2 part;
Wherein frit includes following component and weight proportion number:Red lead:33~35.5 parts, quartz:23~25.5, boron Sand:16~19 parts, calcite:6~10 parts, feldspar:11~14 parts, kaolin:4.5~6 parts;
Wherein black pigment includes following component and weight proportion number:Cobalt oxide:3~4 parts, iron oxide:26~30 parts, Chromium oxide:26~29 parts, pyrolusite:6~7 parts, quartz:15.5~17 parts, kaolin:15.5~17 parts;
Wherein bronzing colorant includes following component and weight proportion number:Iron oxide:15~18.5 parts, chromium oxide: 15.5~17 parts, zinc white:48~52 parts, aluminium hydroxide:15~17.5 parts.
A method of making vase with brown opaque glaze described in claim 1, it is characterised in that:It includes following Step:
(1) raw material in the frit formula is stirred evenly, is melted at a temperature of 1160-11180 DEG C;
(2) raw material in the frit obtained in step (1) and the glaze formula is entered into mill, matched after being crushed to certain particle size Expect fine grinding, 325 mesh of fineness, oversize returns to fine grinding after fine grinding, crosses 200-250 mesh sieve, meets the minus mesh of granularity requirements The ceramic powder particle of water content 10%~12% is granulated into through humidifying prilling machine humidification, then after drying and vibrosieve, sieve Feeding through it is micro- it is broken after be again introduced into vibrating screen, minus mesh send to feed bin it is aging after to get with ceramic powder;
(3) by the glaze obtained in step (2), glaze spraying is dried in bique, and the bique is machined vertical by vertical engraving Body pattern, glazed thickness are 5 grams/100cm2, enter kiln oxidation and fire, firing condition is:Room temperature heats, with 3~5 DEG C/min's Rate is warming up to 360 DEG C, is then warming up to 900 DEG C with the rate of 2~4 DEG C/min, then be warming up to the rate of 1~2 DEG C/min 1150~1180 DEG C, 20~30min is kept the temperature, room temperature is naturally cooled to.
Compared with prior art, the present invention has the following advantages:Tinting strength, tinting power is slightly strong, is especially making ceramic modelled after an antique When, uniform color, and achieve the effect that it is simple and unsophisticated, while glaze is fine and smooth, hardness is preferable, the good and acidproof alkali ability of durability against pollution compared with It is good.The dry method pulverized coal preparation system of the present invention is closed-circuit system, to powder is all out in closed ring since raw material enters system It is carried out in border, which reduces the discharge of dust, environment-friendly type is good;Powder particles made from dry method due to being full particle so Dry-pressing compression ratio is small, and the green body pressed out through press can be high compared with wet method powder consistency, simple for process.
Specific implementation mode
The invention will be further described below.
Embodiment 1:A kind of brown opaque glaze of the present invention, including following component and weight proportion number:Frit:49 Part, feldspar:8.2 parts, quartz:13.6 parts, kaolin:8.5 parts, calcite:4 parts, dolomite:2.2 parts, burn talcum:8.5 parts, Burn tin oxide:3.5 parts, black pigment:0.8 part, bronzing colorant:1.5 part;
Wherein frit includes following component and weight proportion number:Red lead:34 parts, quartz:24.5 borax:16.5 parts, side Xie Shi:7 parts, feldspar:12 parts, kaolin:5 parts;
Wherein black pigment includes following component and weight proportion number:Cobalt oxide:3.5 parts, iron oxide:27 parts, oxidation Chromium:28 parts, pyrolusite:6.5 parts, quartz:15 parts, kaolin:16 parts;
Wherein bronzing colorant includes following component and weight proportion number:Iron oxide:16 parts, chromium oxide:17 parts, zinc In vain:49 parts, aluminium hydroxide:16.6 parts.
The method that the brown opaque glaze of the present invention makes vase, it includes the following steps:
(1) raw material in the frit formula is stirred evenly, is melted at a temperature of 1160 DEG C;
(2) raw material in the frit obtained in step (1) and the glaze formula is entered into mill, matched after being crushed to certain particle size Expect fine grinding, 325 mesh of fineness, oversize returns to fine grinding after fine grinding, crosses 200 mesh sieve, meets the minus mesh of granularity requirements through increasing Wet comminutor humidification is granulated into the ceramic powder particle of water content 10%, then after drying and vibrosieve, and oversize is through micro- broken Be again introduced into vibrating screen after broken, minus mesh send to feed bin it is aging after to get with ceramic powder;
(3) by the glaze obtained in step (2), glaze spraying is dried in bique, and the bique is machined vertical by vertical engraving Body pattern, glazed thickness are 5 grams/100cm2, enter kiln oxidation and fire, firing condition is:Room temperature heats, with the speed of 3 DEG C/min Rate is warming up to 360 DEG C, is then warming up to 900 DEG C with the rate of 2 DEG C/min, then be warming up to 1150 DEG C with the rate of 1 DEG C/min, protects Warm 20min, naturally cools to room temperature.
Embodiment 2
A kind of brown opaque glaze of the present invention, including following component and weight proportion number:Frit:49 parts, feldspar: 8.5 parts, quartz:14 parts, kaolin:8.7 parts, calcite:4.5 parts, dolomite:2.5 parts, burn talcum:9 parts, burn tin oxide:4 Part, black pigment:1 part, bronzing colorant:1.7 part;
Wherein frit includes following component and weight proportion number:Red lead:35 parts, quartz:25, borax:16.7 parts, Fang Xie Stone:7.2 parts, feldspar:12.2 parts, kaolin:5.5 part;
Wherein black pigment includes following component and weight proportion number:Cobalt oxide:3.8 parts, iron oxide:27.5 parts, oxygen Change chromium:28.5 parts, pyrolusite:6.8 parts, quartz:15.2 parts, kaolin:16.2 parts;
Wherein bronzing colorant includes following component and weight proportion number:Iron oxide:16.2 parts, chromium oxide:17.3 part, Zinc white:49.5 parts, aluminium hydroxide:17 parts.
The method that the brown opaque glaze of the present invention makes vase, it includes the following steps:
(1) raw material in the frit formula is stirred evenly, is melted at a temperature of 1170 DEG C;
(2) raw material in the frit obtained in step (1) and the glaze formula is entered into mill, matched after being crushed to certain particle size Expect fine grinding, 325 mesh of fineness, oversize returns to fine grinding after fine grinding, crosses 220 mesh sieve, meets the minus mesh of granularity requirements through increasing Wet comminutor humidification is granulated into the ceramic powder particle of water content 10%, then after drying and vibrosieve, and oversize is through micro- broken Be again introduced into vibrating screen after broken, minus mesh send to feed bin it is aging after to get with ceramic powder;
(3) by the glaze obtained in step (2), glaze spraying is dried in bique, and the bique is machined vertical by vertical engraving Body pattern, glazed thickness are 5 grams/100cm2, enter kiln oxidation and fire, firing condition is:Room temperature heats, with the speed of 4 DEG C/min Rate is warming up to 360 DEG C, is then warming up to 900 DEG C with the rate of 3 DEG C/min, then be warming up to 1150 DEG C with the rate of 1 DEG C/min, protects Warm 25min, naturally cools to room temperature.
Embodiment 3
The brown opaque glaze of the present invention, it is characterised in that:Including following component and weight proportion number:Frit:49 parts, Feldspar:9 parts, quartz:13.5 parts, kaolin:8.6 parts, calcite:4.2 parts, dolomite:2.2 parts, burn talcum:8.7 parts, burn oxygen Change tin:3.6 parts, black pigment:0.6 part, bronzing colorant:2 parts;
Wherein frit includes following component and weight proportion number:Red lead:34.5 parts, quartz:24, borax:18 parts, Fang Xie Stone:8 parts, feldspar:13 parts, kaolin:5.2 part;
Wherein black pigment includes following component and weight proportion number:Cobalt oxide:4 parts, iron oxide:26 parts, chromium oxide: 26 parts, pyrolusite:6.67 parts, quartz:16 parts, kaolin:16 parts;
Wherein bronzing colorant includes following component and weight proportion number:Iron oxide:18.5 parts, chromium oxide:17 parts, zinc In vain:49 parts, aluminium hydroxide:17 parts.
The method that the brown opaque glaze of the present invention makes vase, it includes the following steps:
(1) raw material in the frit formula is stirred evenly, is melted at a temperature of 1180 DEG C;
(2) raw material in the frit obtained in step (1) and the glaze formula is entered into mill, matched after being crushed to certain particle size Expect fine grinding, 325 mesh of fineness, oversize returns to fine grinding after fine grinding, crosses 250 mesh sieve, meets the minus mesh of granularity requirements through increasing Wet comminutor humidification is granulated into the ceramic powder particle of water content 12%, then after drying and vibrosieve, and oversize is through micro- broken Be again introduced into vibrating screen after broken, minus mesh send to feed bin it is aging after to get with ceramic powder;
(3) by the glaze obtained in step (2), glaze spraying is dried in bique, and the bique is machined vertical by vertical engraving Body pattern, glazed thickness are 5 grams/100cm2, enter kiln oxidation and fire, firing condition is:Room temperature heats, with the speed of 5 DEG C/min Rate is warming up to 360 DEG C, is then warming up to 900 DEG C with the rate of 4 DEG C/min, then be warming up to 1180 DEG C with the rate of 2 DEG C/min, protects Warm 30min, naturally cools to room temperature.

Claims (3)

1. a kind of brown opaque glaze, it is characterised in that:Including following component and weight proportion number:Frit:49 parts, feldspar:7 ~9 parts, quartz:13~14 parts, kaolin:8~9 parts, calcite:3.5~4.5 parts, dolomite:2~3 parts, burn talcum:8~ 10 parts, burn tin oxide:3~4 parts, black pigment:0.5~1 part, bronzing colorant:1~2 part;
Wherein frit includes following component and weight proportion number:Red lead:33~35.5 parts, quartz:23~25.5, borax:16 ~19 parts, calcite:6~10 parts, feldspar:11~14 parts, kaolin:4.5~6 parts;Wherein black pigment includes following component With weight proportion number:Cobalt oxide:3~4 parts, iron oxide:26~30 parts, chromium oxide:26~29 parts, pyrolusite:6~7 parts, stone English:15.5~17 parts, kaolin:15.5~17 parts;
Wherein bronzing colorant includes following component and weight proportion number:Iron oxide:15~18.5 parts, chromium oxide:15.5~ 17 parts, zinc white:48~52 parts, aluminium hydroxide:15~17.5 parts.
2. brown opaque glaze according to claim 1, it is characterised in that:Including following component and weight proportion number: Frit:49 parts, feldspar:9 parts, quartz:13.5 parts, kaolin:8.6 parts, calcite:4.2 part, dolomite:2.2 parts, burn talcum: 8.7 parts, burn tin oxide:3.6 parts, black pigment:0.6 part, bronzing colorant:2 parts;
Wherein frit includes following component and weight proportion number:Red lead:34.5 parts, quartz:24, borax:18 parts, calcite:8 Part, feldspar:13 parts, kaolin:5.2 part;
Wherein black pigment includes following component and weight proportion number:Cobalt oxide:4 parts, iron oxide:26 parts, chromium oxide:26 Part, pyrolusite:6. 67 parts, quartz:16 parts, kaolin:16 parts;
Wherein bronzing colorant includes following component and weight proportion number:Iron oxide:18.5 parts, chromium oxide:17 parts, zinc white: 49 parts, aluminium hydroxide:17 parts.
3. a kind of method making vase with brown opaque glaze described in claim 1, it is characterised in that:It includes following step Suddenly:
(1) raw material in the frit formula is stirred evenly, is melted at a temperature of 1160~1180 DEG C;
(2) raw material in the frit and glaze formula that are obtained in step (1) is entered into mill, is crushed to dispensing fine grinding after certain particle size, 325 mesh of fineness, oversize returns to fine grinding after fine grinding, crosses 200~250 mesh sieve, meets the minus mesh of granularity requirements through humidification Comminutor, which is humidified, is granulated into the ceramic powder particle of water content 10%~12%, then after drying and vibrosieve, oversize warp It is micro- it is broken after be again introduced into vibrating screen, minus mesh send to feed bin it is aging after to get with ceramic powder;
(3) by the ceramic powder obtained in step (2), glaze spraying is dried in bique, and the bique is machined vertical by vertical engraving Body pattern, glazed thickness are 5 grams/100cm2, enter kiln oxidation and fire, firing condition is:Room temperature heats, with 3~5 DEG C/min's Rate is warming up to 360 DEG C, is then warming up to 900 DEG C with the rate of 2~4 DEG C/min, then be warming up to the rate of 1~2 DEG C/min 1150~1180 DEG C, 20~30min is kept the temperature, room temperature is naturally cooled to.
CN201610130850.2A 2015-12-31 2016-03-08 A kind of brown opaque glaze and the method with glaze making vase Active CN105819692B (en)

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Families Citing this family (6)

* Cited by examiner, † Cited by third party
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CN106517783A (en) * 2016-11-30 2017-03-22 伟业陶瓷有限公司 Wear-resisting black bubble glaze and preparation method thereof
CN106986539A (en) * 2017-05-18 2017-07-28 东北大学 A kind of brown has Ceramic glaze material of snakeskin texture and preparation method thereof
CN107973529A (en) * 2017-12-31 2018-05-01 湖南省明丰达陶瓷琉璃瓦业有限公司 A kind of golden transparent glaze
CN109439020A (en) * 2018-10-27 2019-03-08 景德镇陶瓷大学 The preparation method of brown color color material on a kind of glaze
CN111517652B (en) * 2020-01-17 2021-06-15 齐鲁工业大学 Yellow ground glaze for marigold and method for manufacturing marigold by adopting yellow ground glaze
CN111517650B (en) * 2020-01-17 2021-03-23 齐鲁工业大学 Blue ground glaze for marigold and method for manufacturing marigold by adopting blue ground glaze for marigold

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN86103510A (en) * 1986-05-16 1987-12-02 核工业部东北地质勘探局二四○研究所 With the natural stone is feedstock production dark color (crystallization) glaze and method
CN1070629A (en) * 1991-09-18 1993-04-07 唐山市开平区栗园瓷厂 The ceramic glaze single firing process of prizing
CN104150962A (en) * 2014-07-28 2014-11-19 安徽青花坊瓷业股份有限公司 Bone china glazing technique

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN86103510A (en) * 1986-05-16 1987-12-02 核工业部东北地质勘探局二四○研究所 With the natural stone is feedstock production dark color (crystallization) glaze and method
CN1070629A (en) * 1991-09-18 1993-04-07 唐山市开平区栗园瓷厂 The ceramic glaze single firing process of prizing
CN104150962A (en) * 2014-07-28 2014-11-19 安徽青花坊瓷业股份有限公司 Bone china glazing technique

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