CN105815354A - Green insecticide for vegetables and preparation method of green insecticide - Google Patents
Green insecticide for vegetables and preparation method of green insecticide Download PDFInfo
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- CN105815354A CN105815354A CN201610283959.XA CN201610283959A CN105815354A CN 105815354 A CN105815354 A CN 105815354A CN 201610283959 A CN201610283959 A CN 201610283959A CN 105815354 A CN105815354 A CN 105815354A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/16—Heavy metals; Compounds thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N61/00—Biocides, pest repellants or attractants, or plant growth regulators containing substances of unknown or undetermined composition, e.g. substances characterised only by the mode of action
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/48—Zingiberaceae [Ginger family], e.g. ginger or galangal
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The invention discloses green insecticide for vegetables and a preparation method of the green insecticide. The green insecticide for the vegetables is prepared from, by weight, the root of Chinese pulsatilla, ginger, coptis chinensis, hairyvein agrimony, radix angelicae pubescentis, pinellia ternate, garden balsam stems, mint, felwort, essential balm, potassium permanganate, pepper, pogostemon cablin, gelsmium elegans, lobelia colorata baculus, black nightshade, radix phytolaccae, hindu datura flowers, wild aconite roots, radix stemonae, common threewingnut roots, pyrethrum, lithospermum, soap nuts, shaddock peel, tobacco, Chinese azalea flowers, common carpesium fruits, areca-nuts and semen torreya. The green insecticide is prepared from the pure Chinese herbal medicine raw materials, has no toxic or side effect, does not contain any chemical matter, is free of pollution after being used, does not affect the environment and can be naturally degraded, the cleanliness of the vegetables can be guaranteed, the price is low, the materials are easy to get, pests do not easily generate insecticide resistance, promotion and use are convenient, pests of leaf vegetables can be effectively prevented and treated, the yield of the leaf vegetables is increased, and the quality of the leaf vegetables is improved.
Description
Technical field
The present invention relates to preparation technique of pesticide field, specifically a kind of vegetable green pesticide and preparation method thereof.
Background technology
At present, in growing vegetables, being chemical pesticide for preventing insect pest normally used, the problem of environmental pollution caused due to a large amount of use chemical pesticides is on the rise.Meanwhile, use chemical pesticide, make various insect produce drug resistance, Drug resistance, add the difficulty of preventing and treating, even cause and prevent and treat unsuccessfully.Additionally, chemical pesticide does not have selectivity because of it, useful biology be will also result in threat.And, a lot of chemical pesticides are non-degradables or are difficult to degraded, easily pollute the enrichment of thing at animals and plants cylinder accumulation.
Along with the public is more and more higher to the requirement of " pollution-free food ", " pollution-free food ", market to pollution-free, can the ecological agricultural chemical demand of natural degradation the most gradually increase.From the point of view of the development of pesticide science, on pesticide manufacturing uses " back to nature " and " Harmless " of pesticide, being the inexorable trend of society and Development of Natural Science, therefore new bio broad spectrum pesticide has wide development prospect.
Therefore, it is necessary to design one formula is simple, prepare convenient, good disinsection effect and to person poultry harmless, pollution-free after using, also environment will not be impacted and the vegetable insecticide of energy natural degradation, to overcome the problems referred to above.
Summary of the invention
It is an object of the invention to provide a kind of simple, vegetable green pesticide of having no side effect of drawing materials and preparation method thereof, with the problem solving to propose in above-mentioned background technology.
For achieving the above object, the present invention provides following technical scheme:
nullA kind of vegetable green pesticide，Include according to the raw material of weight portion: Radix Pulsatillae 6-10 part、Rhizoma Zingiberis Recens 10-20 part、Rhizoma Coptidis 10-15 part、Radix Agrimoniae 10-20 part、Radix Angelicae Pubescentis 10-20 part、Rhizoma Pinelliae 8-12 part、Herba speranskiae tuberculatae 8-12 part、Herba Menthae 10-20 part、Radix Gentianae 10-15 part、Essential balm 8-12 part、Potassium permanganate 5-7 part、Pericarpium Zanthoxyli 10-20 part、Herba Pogostemonis 8-12 part、Herba Gelsemii Elegantis 20-25 part、Stomach mollugo 5-15 part、Herba Solani Nigri 5-10 part、Trade route 5-10 part、Flos Daturae 10-15 part、Radix Aconiti Kusnezoffii 8-12 part、Radix Stemonae 5-10 part、Radix Tripterygii Wilfordii 15-20 part、Pyrethrum 30-50 part、Radix Arnebiae (Radix Lithospermi) 5-10 part、Fructus Sapindi Mukouossi fruit 6-8 part、Pomelo peel 4-6 part、Nicotiana tabacum L. 3-5 part、Flos Rhododendri Mollis 2-4 part、Fructus Carpesii 1-3 part、Semen Arecae 1-3 part、Semen Torreyae 1-2 part.
nullAs the further scheme of the present invention: described vegetable green pesticide，Include according to the raw material of weight portion: Radix Pulsatillae 7-9 part、Rhizoma Zingiberis Recens 12-18 part、Rhizoma Coptidis 11-14 part、Radix Agrimoniae 12-18 part、Radix Angelicae Pubescentis 12-18 part、Rhizoma Pinelliae 9-11 part、Herba speranskiae tuberculatae 9-11 part、Herba Menthae 12-18 part、Radix Gentianae 11-14 part、Essential balm 9-11 part、Potassium permanganate 5.5-6.5 part、Pericarpium Zanthoxyli 12-18 part、Herba Pogostemonis 9-11 part、Herba Gelsemii Elegantis 21-24 part、Stomach mollugo 8-12 part、Herba Solani Nigri 6-9 part、Trade route 6-9 part、Flos Daturae 11-14 part、Radix Aconiti Kusnezoffii 9-11 part、Radix Stemonae 6-9 part、Radix Tripterygii Wilfordii 16-19 part、Pyrethrum 35-45 part、Radix Arnebiae (Radix Lithospermi) 6-9 part、Fructus Sapindi Mukouossi fruit 6.5-7.5 part、Pomelo peel 4.5-5.5 part、Nicotiana tabacum L. 3.5-4.5 part、Flos Rhododendri Mollis 2.5-3.5 part、Fructus Carpesii 1.5-2.5 part、Semen Arecae 1.5-2.5 part、Semen Torreyae 1.2-1.8 part.
As the present invention further scheme: described vegetable green pesticide, include according to the raw material of weight portion: the Radix Pulsatillae 8 parts, 15 parts of Rhizoma Zingiberis Recens, Rhizoma Coptidis 12 parts, Radix Agrimoniae 15 parts, Radix Angelicae Pubescentis 15 parts, the Rhizoma Pinelliae 10 parts, Herba speranskiae tuberculatae 10 parts, Herba Menthae 15 parts, Radix Gentianae 12 parts, essential balm 10 parts, 6 parts of potassium permanganate, 15 parts of Pericarpium Zanthoxyli, Herba Pogostemonis 10 parts, Herba Gelsemii Elegantis 22 parts, stomach mollugo 10 parts, Herba Solani Nigri 8 parts, 8 parts of trade route, Flos Daturae 12 parts, Radix Aconiti Kusnezoffii 10 parts, the Radix Stemonae 8 parts, Radix Tripterygii Wilfordii 18 parts, Pyrethrum 40 parts, Radix Arnebiae (Radix Lithospermi) 8 parts, Fructus Sapindi Mukouossi fruit 7 parts, pomelo peel 5 parts, Nicotiana tabacum L. 4 parts, Flos Rhododendri Mollis 3 parts, Fructus Carpesii 2 parts, Semen Arecae 2 parts, Semen Torreyae 1.5 parts.
The preparation method of described vegetable green pesticide, specifically comprises the following steps that
(1) each raw material is weighed according to weight portion；
(2) by after clean for Rhizoma Zingiberis Recens drying, it is positioned in the ethanol that volumetric concentration is 80-90% and carries out surface sterilization 8-12min, it is placed in tissue refiner for 3 times with aseptic water washing, add the sterilized water of 10-20 part, send in beater and make pasty state, then centrifugal 5-10min under conditions of temperature 3-5 DEG C, rotating speed 6000-8000r/min in centrifuge, taking supernatant, to obtain Rhizoma Zingiberis Recens extract standby；
(3) being pulverized by pomelo peel, add the water of 4-6 times amount, after being heated to boiling, slow fire is ceased fire after boiling 20-40min, takes supernatant, obtain Pericarpium Citri grandis extract standby after filtration；
(4) by the Radix Pulsatillae, Rhizoma Coptidis, Radix Agrimoniae, Radix Angelicae Pubescentis, the Rhizoma Pinelliae, Herba speranskiae tuberculatae, Herba Menthae, Radix Gentianae, Pericarpium Zanthoxyli, Herba Pogostemonis, Herba Gelsemii Elegantis, stomach mollugo, Herba Solani Nigri, trade route, Flos Daturae, Radix Aconiti Kusnezoffii, the Radix Stemonae, Radix Tripterygii Wilfordii, Pyrethrum, Radix Arnebiae (Radix Lithospermi), Fructus Sapindi Mukouossi fruit, Nicotiana tabacum L., Flos Rhododendri Mollis, Fructus Carpesii, Semen Arecae and Semen Torreyae mix homogeneously, the ethanol water of 5-10 times amount 85-95% is added at compound, 2-4h is decocted after being heated to 60-80 DEG C, filter, obtain the first filtrate, filtering residue adds the ethanol water of 5-10 times amount 85-95%, decocts 2-4h after being heated to 60-80 DEG C；Filter, obtain the second filtrate, the first filtrate and the second filtrate are merged, is concentrated to give thick paste；
(5) Rhizoma Zingiberis Recens extract and Pericarpium Citri grandis extract are all added to above-mentioned thick paste, then drip essential balm and potassium permanganate, be fed through after stirring in dehydrator, after drying pelletize, obtain insecticide finished product.
Compared with prior art, the invention has the beneficial effects as follows:
The present invention is pure Chinese herbal medicine raw material, have no side effect, without any chemical substance, pollution-free after using, also environment will not be impacted and energy natural degradation, it is possible not only to ensure the cleaning of vegetable, cheap, draw materials simple, insect is not likely to produce Drug resistance, it is simple to promotes and uses, insect pest to leafy vegetable can effectively prevent and treat, and improves yield and the quality of leafy vegetable.
Detailed description of the invention
Below in conjunction with detailed description of the invention, the technical scheme of this patent is described in more detail.
Embodiment 1
A kind of vegetable green pesticide, include according to the raw material of weight portion: the Radix Pulsatillae 6 parts, 10 parts of Rhizoma Zingiberis Recens, Rhizoma Coptidis 10 parts, Radix Agrimoniae 10 parts, Radix Angelicae Pubescentis 10 parts, the Rhizoma Pinelliae 8 parts, Herba speranskiae tuberculatae 8 parts, Herba Menthae 10 parts, Radix Gentianae 10 parts, essential balm 8 parts, 5 parts of potassium permanganate, 10 parts of Pericarpium Zanthoxyli, Herba Pogostemonis 8 parts, Herba Gelsemii Elegantis 20 parts, stomach mollugo 5 parts, Herba Solani Nigri 5 parts, 5 parts of trade route, Flos Daturae 10 parts, Radix Aconiti Kusnezoffii 8 parts, the Radix Stemonae 5 parts, Radix Tripterygii Wilfordii 15 parts, Pyrethrum 30 parts, Radix Arnebiae (Radix Lithospermi) 5 parts, Fructus Sapindi Mukouossi fruit 6 parts, pomelo peel 4 parts, Nicotiana tabacum L. 3 parts, Flos Rhododendri Mollis 2 parts, Fructus Carpesii 1 part, Semen Arecae 1 part, Semen Torreyae 1 part.
The preparation method of described vegetable green pesticide, specifically comprises the following steps that
(1) each raw material is weighed according to weight portion；
(2) by after clean for Rhizoma Zingiberis Recens drying, it is positioned in the ethanol that volumetric concentration is 80% and carries out surface sterilization 8min, it is placed in tissue refiner for 3 times with aseptic water washing, add the sterilized water of 10 parts, send in beater and make pasty state, then centrifugal 5min under conditions of temperature 3 DEG C, rotating speed 6000r/min in centrifuge, taking supernatant, to obtain Rhizoma Zingiberis Recens extract standby；
(3) being pulverized by pomelo peel, add the water of 4 times amount, after being heated to boiling, slow fire is ceased fire after boiling 20min, takes supernatant, obtain Pericarpium Citri grandis extract standby after filtration；
(4) by the Radix Pulsatillae, Rhizoma Coptidis, Radix Agrimoniae, Radix Angelicae Pubescentis, the Rhizoma Pinelliae, Herba speranskiae tuberculatae, Herba Menthae, Radix Gentianae, Pericarpium Zanthoxyli, Herba Pogostemonis, Herba Gelsemii Elegantis, stomach mollugo, Herba Solani Nigri, trade route, Flos Daturae, Radix Aconiti Kusnezoffii, the Radix Stemonae, Radix Tripterygii Wilfordii, Pyrethrum, Radix Arnebiae (Radix Lithospermi), Fructus Sapindi Mukouossi fruit, Nicotiana tabacum L., Flos Rhododendri Mollis, Fructus Carpesii, Semen Arecae and Semen Torreyae mix homogeneously, the ethanol water of 5 times amount 85% is added at compound, 2h is decocted after being heated to 60 DEG C, filter, obtain the first filtrate, filtering residue adds the ethanol water of 5 times amount 85%, decocts 2h after being heated to 60 DEG C；Filter, obtain the second filtrate, the first filtrate and the second filtrate are merged, is concentrated to give thick paste；
(5) Rhizoma Zingiberis Recens extract and Pericarpium Citri grandis extract are all added to above-mentioned thick paste, then drip essential balm and potassium permanganate, be fed through after stirring in dehydrator, after drying pelletize, obtain insecticide finished product.
Embodiment 2
A kind of vegetable green pesticide, include according to the raw material of weight portion: the Radix Pulsatillae 7 parts, 12 parts of Rhizoma Zingiberis Recens, Rhizoma Coptidis 11 parts, Radix Agrimoniae 12 parts, Radix Angelicae Pubescentis 12 parts, the Rhizoma Pinelliae 9 parts, Herba speranskiae tuberculatae 9 parts, Herba Menthae 12 parts, Radix Gentianae 11 parts, essential balm 9 parts, 5.5 parts of potassium permanganate, 12 parts of Pericarpium Zanthoxyli, Herba Pogostemonis 9 parts, Herba Gelsemii Elegantis 21 parts, stomach mollugo 8 parts, Herba Solani Nigri 6 parts, 6 parts of trade route, Flos Daturae 11 parts, Radix Aconiti Kusnezoffii 9 parts, the Radix Stemonae 6 parts, Radix Tripterygii Wilfordii 16 parts, Pyrethrum 35 parts, Radix Arnebiae (Radix Lithospermi) 6 parts, Fructus Sapindi Mukouossi fruit 6.5 parts, pomelo peel 4.5 parts, Nicotiana tabacum L. 3.5 parts, Flos Rhododendri Mollis 2.5 parts, Fructus Carpesii 1.5 parts, Semen Arecae 1.5 parts, Semen Torreyae 1.2 parts.
The preparation method of described vegetable green pesticide, specifically comprises the following steps that
(1) each raw material is weighed according to weight portion；
(2) by after clean for Rhizoma Zingiberis Recens drying, it is positioned in the ethanol that volumetric concentration is 82% and carries out surface sterilization 9min, it is placed in tissue refiner for 3 times with aseptic water washing, add the sterilized water of 12 parts, send in beater and make pasty state, then centrifugal 6min under conditions of temperature 3.5 DEG C, rotating speed 6500r/min in centrifuge, taking supernatant, to obtain Rhizoma Zingiberis Recens extract standby；
(3) being pulverized by pomelo peel, add the water of 4.5 times amount, after being heated to boiling, slow fire is ceased fire after boiling 25min, takes supernatant, obtain Pericarpium Citri grandis extract standby after filtration；
(4) by the Radix Pulsatillae, Rhizoma Coptidis, Radix Agrimoniae, Radix Angelicae Pubescentis, the Rhizoma Pinelliae, Herba speranskiae tuberculatae, Herba Menthae, Radix Gentianae, Pericarpium Zanthoxyli, Herba Pogostemonis, Herba Gelsemii Elegantis, stomach mollugo, Herba Solani Nigri, trade route, Flos Daturae, Radix Aconiti Kusnezoffii, the Radix Stemonae, Radix Tripterygii Wilfordii, Pyrethrum, Radix Arnebiae (Radix Lithospermi), Fructus Sapindi Mukouossi fruit, Nicotiana tabacum L., Flos Rhododendri Mollis, Fructus Carpesii, Semen Arecae and Semen Torreyae mix homogeneously, the ethanol water of 6 times amount 88% is added at compound, 2.5h is decocted after being heated to 65 DEG C, filter, obtain the first filtrate, filtering residue adds the ethanol water of 6 times amount 88%, decocts 2.5h after being heated to 65 DEG C；Filter, obtain the second filtrate, the first filtrate and the second filtrate are merged, is concentrated to give thick paste；
(5) Rhizoma Zingiberis Recens extract and Pericarpium Citri grandis extract are all added to above-mentioned thick paste, then drip essential balm and potassium permanganate, be fed through after stirring in dehydrator, after drying pelletize, obtain insecticide finished product.
Embodiment 3
A kind of vegetable green pesticide, include according to the raw material of weight portion: the Radix Pulsatillae 8 parts, 15 parts of Rhizoma Zingiberis Recens, Rhizoma Coptidis 12 parts, Radix Agrimoniae 15 parts, Radix Angelicae Pubescentis 15 parts, the Rhizoma Pinelliae 10 parts, Herba speranskiae tuberculatae 10 parts, Herba Menthae 15 parts, Radix Gentianae 12 parts, essential balm 10 parts, 6 parts of potassium permanganate, 15 parts of Pericarpium Zanthoxyli, Herba Pogostemonis 10 parts, Herba Gelsemii Elegantis 22 parts, stomach mollugo 10 parts, Herba Solani Nigri 8 parts, 8 parts of trade route, Flos Daturae 12 parts, Radix Aconiti Kusnezoffii 10 parts, the Radix Stemonae 8 parts, Radix Tripterygii Wilfordii 18 parts, Pyrethrum 40 parts, Radix Arnebiae (Radix Lithospermi) 8 parts, Fructus Sapindi Mukouossi fruit 7 parts, pomelo peel 5 parts, Nicotiana tabacum L. 4 parts, Flos Rhododendri Mollis 3 parts, Fructus Carpesii 2 parts, Semen Arecae 2 parts, Semen Torreyae 1.5 parts.
The preparation method of described vegetable green pesticide, specifically comprises the following steps that
(1) each raw material is weighed according to weight portion；
(2) by after clean for Rhizoma Zingiberis Recens drying, it is positioned in the ethanol that volumetric concentration is 85% and carries out surface sterilization 10min, it is placed in tissue refiner for 3 times with aseptic water washing, add the sterilized water of 15 parts, send in beater and make pasty state, then centrifugal 8min under conditions of temperature 4 DEG C, rotating speed 7000r/min in centrifuge, taking supernatant, to obtain Rhizoma Zingiberis Recens extract standby；
(3) being pulverized by pomelo peel, add the water of 5 times amount, after being heated to boiling, slow fire is ceased fire after boiling 30min, takes supernatant, obtain Pericarpium Citri grandis extract standby after filtration；
(4) by the Radix Pulsatillae, Rhizoma Coptidis, Radix Agrimoniae, Radix Angelicae Pubescentis, the Rhizoma Pinelliae, Herba speranskiae tuberculatae, Herba Menthae, Radix Gentianae, Pericarpium Zanthoxyli, Herba Pogostemonis, Herba Gelsemii Elegantis, stomach mollugo, Herba Solani Nigri, trade route, Flos Daturae, Radix Aconiti Kusnezoffii, the Radix Stemonae, Radix Tripterygii Wilfordii, Pyrethrum, Radix Arnebiae (Radix Lithospermi), Fructus Sapindi Mukouossi fruit, Nicotiana tabacum L., Flos Rhododendri Mollis, Fructus Carpesii, Semen Arecae and Semen Torreyae mix homogeneously, the ethanol water of 8 times amount 80% is added at compound, 3h is decocted after being heated to 70 DEG C, filter, obtain the first filtrate, filtering residue adds the ethanol water of 8 times amount 90%, decocts 3h after being heated to 70 DEG C；Filter, obtain the second filtrate, the first filtrate and the second filtrate are merged, is concentrated to give thick paste；
(5) Rhizoma Zingiberis Recens extract and Pericarpium Citri grandis extract are all added to above-mentioned thick paste, then drip essential balm and potassium permanganate, be fed through after stirring in dehydrator, after drying pelletize, obtain insecticide finished product.
Embodiment 4
A kind of vegetable green pesticide, include according to the raw material of weight portion: the Radix Pulsatillae 9 parts, 18 parts of Rhizoma Zingiberis Recens, Rhizoma Coptidis 14 parts, Radix Agrimoniae 18 parts, Radix Angelicae Pubescentis 18 parts, the Rhizoma Pinelliae 11 parts, Herba speranskiae tuberculatae 11 parts, Herba Menthae 18 parts, Radix Gentianae 14 parts, essential balm 11 parts, 6.5 parts of potassium permanganate, 18 parts of Pericarpium Zanthoxyli, Herba Pogostemonis 11 parts, Herba Gelsemii Elegantis 24 parts, stomach mollugo 12 parts, Herba Solani Nigri 9 parts, 9 parts of trade route, Flos Daturae 14 parts, Radix Aconiti Kusnezoffii 11 parts, the Radix Stemonae 9 parts, Radix Tripterygii Wilfordii 19 parts, Pyrethrum 45 parts, Radix Arnebiae (Radix Lithospermi) 9 parts, Fructus Sapindi Mukouossi fruit 7.5 parts, pomelo peel 5.5 parts, Nicotiana tabacum L. 4.5 parts, Flos Rhododendri Mollis 3.5 parts, Fructus Carpesii 2.5 parts, Semen Arecae 2.5 parts, Semen Torreyae 1.8 parts.
The preparation method of described vegetable green pesticide, specifically comprises the following steps that
(1) each raw material is weighed according to weight portion；
(2) by after clean for Rhizoma Zingiberis Recens drying, it is positioned in the ethanol that volumetric concentration is 88% and carries out surface sterilization 11min, it is placed in tissue refiner for 3 times with aseptic water washing, add the sterilized water of 18 parts, send in beater and make pasty state, then centrifugal 9min under conditions of temperature 4.5 DEG C, rotating speed 7500r/min in centrifuge, taking supernatant, to obtain Rhizoma Zingiberis Recens extract standby；
(3) being pulverized by pomelo peel, add the water of 5.5 times amount, after being heated to boiling, slow fire is ceased fire after boiling 35min, takes supernatant, obtain Pericarpium Citri grandis extract standby after filtration；
(4) by the Radix Pulsatillae, Rhizoma Coptidis, Radix Agrimoniae, Radix Angelicae Pubescentis, the Rhizoma Pinelliae, Herba speranskiae tuberculatae, Herba Menthae, Radix Gentianae, Pericarpium Zanthoxyli, Herba Pogostemonis, Herba Gelsemii Elegantis, stomach mollugo, Herba Solani Nigri, trade route, Flos Daturae, Radix Aconiti Kusnezoffii, the Radix Stemonae, Radix Tripterygii Wilfordii, Pyrethrum, Radix Arnebiae (Radix Lithospermi), Fructus Sapindi Mukouossi fruit, Nicotiana tabacum L., Flos Rhododendri Mollis, Fructus Carpesii, Semen Arecae and Semen Torreyae mix homogeneously, the ethanol water of 9 times amount 92% is added at compound, 3.5h is decocted after being heated to 75 DEG C, filter, obtain the first filtrate, filtering residue adds the ethanol water of 9 times amount 92%, decocts 3.5h after being heated to 75 DEG C；Filter, obtain the second filtrate, the first filtrate and the second filtrate are merged, is concentrated to give thick paste；
(5) Rhizoma Zingiberis Recens extract and Pericarpium Citri grandis extract are all added to above-mentioned thick paste, then drip essential balm and potassium permanganate, be fed through after stirring in dehydrator, after drying pelletize, obtain insecticide finished product.
Embodiment 5
A kind of vegetable green pesticide, include according to the raw material of weight portion: the Radix Pulsatillae 10 parts, 20 parts of Rhizoma Zingiberis Recens, Rhizoma Coptidis 15 parts, Radix Agrimoniae 20 parts, Radix Angelicae Pubescentis 20 parts, the Rhizoma Pinelliae 12 parts, Herba speranskiae tuberculatae 12 parts, Herba Menthae 20 parts, Radix Gentianae 15 parts, essential balm 12 parts, 7 parts of potassium permanganate, 20 parts of Pericarpium Zanthoxyli, Herba Pogostemonis 12 parts, Herba Gelsemii Elegantis 25 parts, stomach mollugo 15 parts, Herba Solani Nigri 10 parts, 10 parts of trade route, Flos Daturae 15 parts, Radix Aconiti Kusnezoffii 12 parts, the Radix Stemonae 10 parts, Radix Tripterygii Wilfordii 20 parts, Pyrethrum 50 parts, Radix Arnebiae (Radix Lithospermi) 10 parts, Fructus Sapindi Mukouossi fruit 8 parts, pomelo peel 6 parts, Nicotiana tabacum L. 5 parts, Flos Rhododendri Mollis 4 parts, Fructus Carpesii 3 parts, Semen Arecae 3 parts, Semen Torreyae 2 parts.
The preparation method of described vegetable green pesticide, specifically comprises the following steps that
(1) each raw material is weighed according to weight portion；
(2) by after clean for Rhizoma Zingiberis Recens drying, it is positioned in the ethanol that volumetric concentration is 90% and carries out surface sterilization 12min, it is placed in tissue refiner for 3 times with aseptic water washing, add the sterilized water of 20 parts, send in beater and make pasty state, then centrifugal 10min under conditions of temperature 5 DEG C, rotating speed 8000r/min in centrifuge, taking supernatant, to obtain Rhizoma Zingiberis Recens extract standby；
(3) being pulverized by pomelo peel, add the water of 6 times amount, after being heated to boiling, slow fire is ceased fire after boiling 40min, takes supernatant, obtain Pericarpium Citri grandis extract standby after filtration；
(4) by the Radix Pulsatillae, Rhizoma Coptidis, Radix Agrimoniae, Radix Angelicae Pubescentis, the Rhizoma Pinelliae, Herba speranskiae tuberculatae, Herba Menthae, Radix Gentianae, Pericarpium Zanthoxyli, Herba Pogostemonis, Herba Gelsemii Elegantis, stomach mollugo, Herba Solani Nigri, trade route, Flos Daturae, Radix Aconiti Kusnezoffii, the Radix Stemonae, Radix Tripterygii Wilfordii, Pyrethrum, Radix Arnebiae (Radix Lithospermi), Fructus Sapindi Mukouossi fruit, Nicotiana tabacum L., Flos Rhododendri Mollis, Fructus Carpesii, Semen Arecae and Semen Torreyae mix homogeneously, the ethanol water of 10 times amount 95% is added at compound, 4h is decocted after being heated to 80 DEG C, filter, obtain the first filtrate, filtering residue adds the ethanol water of 10 times amount 95%, decocts 4h after being heated to 80 DEG C；Filter, obtain the second filtrate, the first filtrate and the second filtrate are merged, is concentrated to give thick paste；
(5) Rhizoma Zingiberis Recens extract and Pericarpium Citri grandis extract are all added to above-mentioned thick paste, then drip essential balm and potassium permanganate, be fed through after stirring in dehydrator, after drying pelletize, obtain insecticide finished product.
The present invention is pure Chinese herbal medicine raw material, have no side effect, without any chemical substance, pollution-free after using, also environment will not be impacted and energy natural degradation, it is possible not only to ensure the cleaning of vegetable, cheap, draw materials simple, insect is not likely to produce Drug resistance, it is simple to promotes and uses, insect pest to leafy vegetable can effectively prevent and treat, and improves yield and the quality of leafy vegetable.
Above the better embodiment of this patent is explained in detail, but this patent is not limited to above-mentioned embodiment, in the ken that one skilled in the relevant art is possessed, it is also possible to various changes can be made on the premise of without departing from this patent objective.
Claims (4)
- null1. a vegetable green pesticide，It is characterized in that，Include according to the raw material of weight portion: Radix Pulsatillae 6-10 part、Rhizoma Zingiberis Recens 10-20 part、Rhizoma Coptidis 10-15 part、Radix Agrimoniae 10-20 part、Radix Angelicae Pubescentis 10-20 part、Rhizoma Pinelliae 8-12 part、Herba speranskiae tuberculatae 8-12 part、Herba Menthae 10-20 part、Radix Gentianae 10-15 part、Essential balm 8-12 part、Potassium permanganate 5-7 part、Pericarpium Zanthoxyli 10-20 part、Herba Pogostemonis 8-12 part、Herba Gelsemii Elegantis 20-25 part、Stomach mollugo 5-15 part、Herba Solani Nigri 5-10 part、Trade route 5-10 part、Flos Daturae 10-15 part、Radix Aconiti Kusnezoffii 8-12 part、Radix Stemonae 5-10 part、Radix Tripterygii Wilfordii 15-20 part、Pyrethrum 30-50 part、Radix Arnebiae (Radix Lithospermi) 5-10 part、Fructus Sapindi Mukouossi fruit 6-8 part、Pomelo peel 4-6 part、Nicotiana tabacum L. 3-5 part、Flos Rhododendri Mollis 2-4 part、Fructus Carpesii 1-3 part、Semen Arecae 1-3 part、Semen Torreyae 1-2 part.
- nullVegetable green pesticide the most according to claim 1，It is characterized in that，Include according to the raw material of weight portion: Radix Pulsatillae 7-9 part、Rhizoma Zingiberis Recens 12-18 part、Rhizoma Coptidis 11-14 part、Radix Agrimoniae 12-18 part、Radix Angelicae Pubescentis 12-18 part、Rhizoma Pinelliae 9-11 part、Herba speranskiae tuberculatae 9-11 part、Herba Menthae 12-18 part、Radix Gentianae 11-14 part、Essential balm 9-11 part、Potassium permanganate 5.5-6.5 part、Pericarpium Zanthoxyli 12-18 part、Herba Pogostemonis 9-11 part、Herba Gelsemii Elegantis 21-24 part、Stomach mollugo 8-12 part、Herba Solani Nigri 6-9 part、Trade route 6-9 part、Flos Daturae 11-14 part、Radix Aconiti Kusnezoffii 9-11 part、Radix Stemonae 6-9 part、Radix Tripterygii Wilfordii 16-19 part、Pyrethrum 35-45 part、Radix Arnebiae (Radix Lithospermi) 6-9 part、Fructus Sapindi Mukouossi fruit 6.5-7.5 part、Pomelo peel 4.5-5.5 part、Nicotiana tabacum L. 3.5-4.5 part、Flos Rhododendri Mollis 2.5-3.5 part、Fructus Carpesii 1.5-2.5 part、Semen Arecae 1.5-2.5 part、Semen Torreyae 1.2-1.8 part.
- Vegetable green pesticide the most according to claim 1, it is characterized in that, include according to the raw material of weight portion: the Radix Pulsatillae 8 parts, 15 parts of Rhizoma Zingiberis Recens, Rhizoma Coptidis 12 parts, Radix Agrimoniae 15 parts, Radix Angelicae Pubescentis 15 parts, the Rhizoma Pinelliae 10 parts, Herba speranskiae tuberculatae 10 parts, Herba Menthae 15 parts, Radix Gentianae 12 parts, essential balm 10 parts, 6 parts of potassium permanganate, 15 parts of Pericarpium Zanthoxyli, Herba Pogostemonis 10 parts, Herba Gelsemii Elegantis 22 parts, stomach mollugo 10 parts, Herba Solani Nigri 8 parts, 8 parts of trade route, Flos Daturae 12 parts, Radix Aconiti Kusnezoffii 10 parts, the Radix Stemonae 8 parts, Radix Tripterygii Wilfordii 18 parts, Pyrethrum 40 parts, Radix Arnebiae (Radix Lithospermi) 8 parts, Fructus Sapindi Mukouossi fruit 7 parts, pomelo peel 5 parts, Nicotiana tabacum L. 4 parts, Flos Rhododendri Mollis 3 parts, Fructus Carpesii 2 parts, Semen Arecae 2 parts, Semen Torreyae 1.5 parts.
- 4. the preparation method of the vegetable green pesticide as described in claim 1-3 is arbitrary, it is characterised in that specifically comprise the following steps that(1) each raw material is weighed according to weight portion；(2) by after clean for Rhizoma Zingiberis Recens drying, it is positioned in the ethanol that volumetric concentration is 80-90% and carries out surface sterilization 8-12min, it is placed in tissue refiner for 3 times with aseptic water washing, add the sterilized water of 10-20 part, send in beater and make pasty state, then centrifugal 5-10min under conditions of temperature 3-5 DEG C, rotating speed 6000-8000r/min in centrifuge, taking supernatant, to obtain Rhizoma Zingiberis Recens extract standby；(3) being pulverized by pomelo peel, add the water of 4-6 times amount, after being heated to boiling, slow fire is ceased fire after boiling 20-40min, takes supernatant, obtain Pericarpium Citri grandis extract standby after filtration；(4) by the Radix Pulsatillae, Rhizoma Coptidis, Radix Agrimoniae, Radix Angelicae Pubescentis, the Rhizoma Pinelliae, Herba speranskiae tuberculatae, Herba Menthae, Radix Gentianae, Pericarpium Zanthoxyli, Herba Pogostemonis, Herba Gelsemii Elegantis, stomach mollugo, Herba Solani Nigri, trade route, Flos Daturae, Radix Aconiti Kusnezoffii, the Radix Stemonae, Radix Tripterygii Wilfordii, Pyrethrum, Radix Arnebiae (Radix Lithospermi), Fructus Sapindi Mukouossi fruit, Nicotiana tabacum L., Flos Rhododendri Mollis, Fructus Carpesii, Semen Arecae and Semen Torreyae mix homogeneously, the ethanol water of 5-10 times amount 85-95% is added at compound, 2-4h is decocted after being heated to 60-80 DEG C, filter, obtain the first filtrate, filtering residue adds the ethanol water of 5-10 times amount 85-95%, decocts 2-4h after being heated to 60-80 DEG C；Filter, obtain the second filtrate, the first filtrate and the second filtrate are merged, is concentrated to give thick paste；(5) Rhizoma Zingiberis Recens extract and Pericarpium Citri grandis extract are all added to above-mentioned thick paste, then drip essential balm and potassium permanganate, be fed through after stirring in dehydrator, after drying pelletize, obtain insecticide finished product.
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