CN105801175A - Antibacterial ceramic tiles and production method thereof - Google Patents

Antibacterial ceramic tiles and production method thereof Download PDF

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Publication number
CN105801175A
CN105801175A CN201610124189.4A CN201610124189A CN105801175A CN 105801175 A CN105801175 A CN 105801175A CN 201610124189 A CN201610124189 A CN 201610124189A CN 105801175 A CN105801175 A CN 105801175A
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CN
China
Prior art keywords
layer
pore
glaze
antibacterial
transparent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610124189.4A
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Chinese (zh)
Inventor
王培青
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zhejiang Gengen Ceramic Co Ltd
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Zhejiang Gengen Ceramic Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zhejiang Gengen Ceramic Co Ltd filed Critical Zhejiang Gengen Ceramic Co Ltd
Priority to CN201610124189.4A priority Critical patent/CN105801175A/en
Publication of CN105801175A publication Critical patent/CN105801175A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/52Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/53After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone involving the removal of at least part of the materials of the treated article, e.g. etching, drying of hardened concrete
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
    • C04B41/81Coating or impregnation
    • C04B41/89Coating or impregnation for obtaining at least two superposed coatings having different compositions
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
    • C04B41/91After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics involving the removal of part of the materials of the treated articles, e.g. etching

Abstract

The invention discloses antibacterial ceramic tiles and a production method thereof. The antibacterial ceramic tile comprises a base blank layer, a ground glaze layer, a cover glaze layer, a printing decoration layer and a transparent or semitransparent glaze layer from bottom to top. The topmost layer of the antibacterial ceramic tile is full of pores; and each pore is filled with an antibacterial antifouling material to form an antibacterial antifouling layer. In the invention, the pores formed by the ceramic tile polishing and grinding are filled with the antibacterial antifouling material to form the antibacterial antifouling layer. Since the pores are filled by the antibacterial antifouling layer, the antibacterial antifouling layer does not disappear easily by wear, and the antibacterial property is more stale and lasting.

Description

A kind of antibiotic ceramic tile and manufacture method thereof
Technical field
The present invention relates to Ceramic Tiles field, be specifically related to a kind of antibiotic ceramic tile and manufacture method thereof.
Background technology
Along with improving constantly of people's living standard, environment protection health life is pursued and is increasingly paid attention to by people, more and more stronger for antibacterial antifouling demand, particularly between kitchen, the antibacterial such as communal bathroom easily grows district, the ceramic tile therefore with antibacterial anti-pollution function has great practicality, but this function ceramic tile also compares shortage in the market.
Summary of the invention
For the deficiencies in the prior art, it is desirable to provide a kind of antibiotic ceramic tile and manufacture method thereof, it is achieved the antibacterial effect of antibiotic ceramic tile is stable, extends antibacterial effect duration, and simplifies the manufacturing process of antibiotic ceramic tile so that it is can realize large-scale production.
A kind of antibiotic ceramic tile, includes end base layer, ground glaze layer, cover coat, printed decor and transparent or semitransparent glaze layer from the bottom up successively;The top of described antibiotic ceramic tile is abound with pore, is all filled with antibacterial anti-fouling material in pore, thus forming antibacterial stain-proofing layer.
Further, base layer thickness in the end is 3mm-12mm;The thickness of described ground glaze layer and cover coat respectively 0.01mm-0.6mm, described printing ornament layer thickness is 0.01mm-0.8mm;Described transparent or semitransparent glazed thickness is 0.3mm-1.3mm;The described pore degree of depth is between 0.01 μm of-0.3mm, and the thickness of described antibacterial stain-proofing layer keeps consistent with the pore degree of depth.
A kind of method manufacturing above-mentioned antibiotic ceramic tile, comprises the steps:
Ceramic powder compacting is formed adobe and burns till biscuit by S1, forms end base layer;On end base layer, spoon ground glaze layer, cover coat and printed decor from lower to upper respectively;
S2 drenches bright or translucent glaze layer on printed decor;
S3 glaze firing;
Also include:
S4 is in the semi-finished product glaze paint baked, use buffing machine that glaze paint is carried out throwing and cut rubbing down, owing in buffing machine, abrading block contains corundum, hardness is higher than transparent or semitransparent glaze layer, so after transparent or semitransparent glaze layer surface-pressure high speed rubbing down, being abound with on transparent or semitransparent glaze layer surface with the visible pore not of uniform size of magnifier;
S5 uses super clean bright machine to fill the mixed liquor of super clean brilliant polish antifouling wax liquid and inorganic antiseptic in pore, or uses super clean bright machine to be taken up in order of priority the super clean brilliant polish antifouling wax liquid of filling and inorganic antiseptic in pore, and pressurization simultaneously throw flat throw bright.
Further, described printed decor is one or more combinations in screen printing, roller printing, inkjet printing stamp.
Further, the manufacture method of the transparent or semitransparent glaze layer in described step S2 is that transparent or semitransparent frit, methylcellulose and Kaolin add water and is processed to form liquid glaze through little ball milling.
Further, in described step S4, the described pore degree of depth is between 0.01 μm of-0.3mm.
Further, in step S5, described inorganic antiseptic be silver ion series, copper, zinc, titanium system individually or the inorganic antiseptic being mixed to form.
The beneficial effects of the present invention is: by the pore of formation being filled antibacterial anti-fouling material and formed antibacterial stain-proofing layer after ceramic tile rubbing down.Owing to antibacterial stain-proofing layer is in pore, making antibacterial stain-proofing layer not easily wears, anti-microbial property is more stable persistently.
Accompanying drawing explanation
Fig. 1 is the cross section structure schematic diagram of antibiotic ceramic tile of the present invention.
Detailed description of the invention
Below with reference to accompanying drawing, the invention will be further described, it is necessary to explanation, and the present embodiment, premised on the technical program, gives detailed embodiment and concrete operating process, but protection scope of the present invention is not limited to the present embodiment.
As it is shown in figure 1, a kind of antibiotic ceramic tile, including including end base layer 1, ground glaze layer 2, cover coat 3, printed decor 4 and transparent or semitransparent glaze layer 5 from the bottom up successively;The top of described antibiotic ceramic tile is abound with pore, is all filled with antibacterial anti-fouling material in each pore, thus forming antibacterial stain-proofing layer 6.
Further, base layer thickness in the end is 3mm-12mm;The thickness of described ground glaze layer and cover coat respectively 0.01mm-0.6mm, described printing ornament layer thickness is 0.01mm-0.8mm;Described transparent or semitransparent glazed thickness is 0.3mm-1.3mm;The described pore degree of depth is at 0.01 μm of-0.3mm, and the thickness of described antibacterial stain-proofing layer keeps consistent with the pore degree of depth.
A kind of method manufacturing above-mentioned antibiotic ceramic tile comprises the steps:
Ceramic powder compacting is formed adobe and burns till biscuit by S1, forms end base layer;On end base layer, spoon ground glaze layer, cover coat and printed decor from lower to upper respectively;
S2 drenches bright or translucent glaze layer on printed decor;
S3 glaze firing;
Also include:
S4 is in the semi-finished product glaze paint baked, use buffing machine that glaze paint is carried out throwing and cut rubbing down, owing in buffing machine, abrading block contains corundum, hardness is higher than transparent or semitransparent glaze layer, so after transparent or semitransparent glaze layer surface-pressure high speed rubbing down, being abound with on transparent or semitransparent glaze layer surface with the visible pore not of uniform size of magnifier;
S5 uses super clean bright machine to fill the mixed liquor of super clean brilliant polish antifouling wax liquid and inorganic antiseptic in pore, or uses super clean bright machine to be taken up in order of priority the super clean brilliant polish antifouling wax liquid of filling and inorganic antiseptic in pore, and pressurization simultaneously throw flat throw bright.
Further, described printed decor is one or more combinations in screen printing, roller printing, inkjet printing stamp.
Further, the manufacture method of the transparent or semitransparent glaze layer in described step S2 is that transparent or semitransparent frit, methylcellulose and Kaolin add water and is processed to form liquid glaze through little ball milling.
Further, in described step S4, the described pore degree of depth is between 0.01 μm of-0.3mm.
Further, in step S5, described inorganic antiseptic be silver ion series, copper, zinc, titanium system individually or the inorganic antiseptic being mixed to form.
Embodiment 1
Selecting to manufacture specification is the antibiotic ceramic tile of 300 × 600mm, and its blank raw material (ceramic powder) is primary raw material for the known Kaolin of prior art, clay, sand etc., then is aided with other auxiliary materials such as magnesium soil;
The manufacture method of antibiotic ceramic tile comprises the steps
Ceramic powder compacting is formed adobe and burns till 300 × 600mm biscuit by S1, forms end base layer;On end base layer, from bottom to top spoon ground glaze layer, cover coat and printed decor respectively;
S2 drenches clear frit layer on printed decor;
S3 glaze burns till: under oxidizing atmosphere, burns till with 850~1150 DEG C in roller kilns, and firing period is 40 minutes;
S4 uses the buffing machine that Guangdong Kodak Jie Neng limited company produces that clear frit layer 5 is carried out mechanical polishing.After rubbing down, clear frit surface layer is frosted shape, is abound with pore under magnifier as seen, the pore degree of depth and size is controlled between 0.01 μm of-0.2mm by the size of corundum granule in the pressure of adjustment buffing machine and abrading block;
S5 uses the super clean bright wax-polishing machine of Guangdong Kodak Jie Neng limited company production to instil in pore and fills the mixed liquor of the super clean brilliant polish antifouling wax liquid (accounting 97%) of pottery and inorganic antiseptic (accounting 3%), and pressurization simultaneously is thrown to put down and thrown the antibacterial stain-proofing layer of bright formation;
Packaging warehouse-in after drying, edging.
Base layer thickness at the bottom of the antibiotic ceramic tile of the present embodiment is 3mm;Ground glaze layer thickness is 0.01mm;Cover coat thickness 0.01mm;Printing ornament layer thickness is 0.01mm;Clear frit layer thickness is 0.3mm, and after rubbing down, clear frit layer thickness is 0.2mm;Antibacterial stain-proofing layer is filled according to the pore degree of depth, and this example thickness is between 0.01 μm of-0.2mm.Data above industry professional can suitably adjust as required.
Producing antibiotic ceramic tile by the method, antibacterial bacteriostatic average effect is more than 97%.
Embodiment 2
Selecting to manufacture specification is the antibiotic ceramic tile of 300 × 600mm, and its blank raw material (ceramic powder) is primary raw material for the known Kaolin of prior art, clay, sand etc., then is aided with other auxiliary materials such as magnesium soil;
The manufacture method of antibiotic ceramic tile comprises the steps
Ceramic powder compacting is formed adobe and burns till 300 × 600mm biscuit by S1, forms end base layer;On end base layer, from bottom to top spoon ground glaze layer, cover coat and printed decor respectively;
S2 drenches clear frit layer on printed decor;
S3 glaze burns till: under oxidizing atmosphere, burns till with 850~1150 DEG C in roller kilns, and firing period is 45 minutes.
S4 uses the buffing machine that Guangdong Kodak Jie Neng limited company produces that clear frit layer 5 is carried out mechanical polishing.After rubbing down, clear frit surface layer is frosted shape, is abound with pore under magnifier as seen, the pore degree of depth and size is controlled between 0.01 μm of-0.3mm by the big I of corundum granule in the pressure of adjustment buffing machine and abrading block;
S5 uses the super clean bright wax-polishing machine of Guangdong Kodak Jie Neng limited company production to instil in pore and fills the mixed liquor of the super clean brilliant polish antifouling wax liquid (accounting 97%) of pottery and inorganic antiseptic (accounting 3%), and pressurization simultaneously is thrown to put down and thrown the antibacterial stain-proofing layer of bright formation;
Packaging warehouse-in after drying, edging.
Base layer thickness at the bottom of the antibiotic ceramic tile of the present embodiment is 9mm;Ground glaze layer thickness is 0.25mm;Cover coat thickness 0.3mm;Printing ornament layer thickness is 0.1mm;Clear frit layer thickness is 0.5mm, and after rubbing down, clear frit layer thickness is 0.3mm;Antibacterial stain-proofing layer is filled according to the pore degree of depth, and this example thickness is between 0.01 μm of-0.3mm.Data above industry professional can suitably adjust as required.
Producing antibiotic ceramic tile by the method, antibacterial bacteriostatic average effect is more than 97%.
Embodiment 3
Selecting to manufacture specification is the antibiotic ceramic tile of 800 × 800mm, and its blank raw material is the known Kaolin of prior art, clay, sand etc. is primary raw material, then is aided with other auxiliary materials such as magnesium soil;
The manufacture method of antibiotic ceramic tile comprises the steps:
Ceramic powder is suppressed base at the bottom of formation 800 × 800mm and dries by S1, forms end base layer;On end base layer, from bottom to top drench ground glaze layer, cover coat and printed decor respectively;
S2 drenches clear frit layer on printed decor;
S3 glaze burns till: under oxidizing atmosphere, burns till with 850~1250 DEG C in roller kilns, and firing period is 80 minutes;
S4 uses the buffing machine that Guangdong Kodak Jie Neng limited company produces that clear frit layer is carried out mechanical polishing, after rubbing down, clear frit surface layer is abound with pinhole, the pore degree of depth and size is controlled between 0.01 μm of-0.3mm by adjusting the size of corundum granule in buffing machine pressure and abrading block;
S5 uses the super clean bright wax-polishing machine that Guangdong Kodak Jie Neng limited company produces to instil in pore and fills the mixed liquor of the super clean brilliant polish antifouling wax liquid (accounting 97%) of pottery and inorganic antiseptic (accounting 3%), the antibacterial stain-proofing layer of flat formation is thrown in pressurization simultaneously, and original pore is filled and led up.
Packaging warehouse-in after edging.
Base layer thickness at the bottom of the antibiotic ceramic tile of the present embodiment is 12mm;Ground glaze layer thickness is 0.6mm;Cover coat thickness 0.6mm;Printing ornament layer thickness is 0.8mm;Clear frit layer thickness is 1.3mm, and after rubbing down, clear frit layer thickness is 1mm;Antibacterial stain-proofing layer is filled by the pressurization of super clean bright wax-polishing machine according to the pore degree of depth, and this example thickness is between 0.01 μm of-0.3mm.Data above industry professional can suitably adjust as required.
Producing antibiotic ceramic tile by the method, antibacterial bacteriostatic average effect is more than 97%.
In above 3 embodiments, the inorganic antiseptic (accounting 3%) used adopts the silver-based inorganic antibacterial agent that Shanghai Xingya Glass Material Co., Ltd. provides, brand is U.S. spirit health and happiness MILLIONKILLER, and model is SHPG-601S1, and mean diameter is the white powder of 3 nanometers.It is blended into the super clean brilliant polish antifouling wax liquid (accounting 97%) produced by Foshan rich AudioCodes skill Materials Co., Ltd to stir use.Needing exist for illustrating, the similar products that other company produces on the market can be suitable for.
For a person skilled in the art, it is possible to according to above technical scheme and design, make various corresponding change and deformation, and all these changes and deforms within the protection domain that should be construed as being included in the claims in the present invention.

Claims (7)

1. an antibiotic ceramic tile, includes end base layer, ground glaze layer, cover coat, printed decor and transparent or semitransparent glaze layer from the bottom up successively;It is characterized in that, the top of described antibiotic ceramic tile is abound with pore, is all filled with antibacterial anti-fouling material in pore, thus forming antibacterial stain-proofing layer.
2. antibiotic ceramic tile according to claim 1, it is characterised in that end base layer thickness is 3mm-12mm;The thickness of described ground glaze layer and cover coat respectively 0.01mm-0.6mm, described printing ornament layer thickness is 0.01mm-0.8mm;Described transparent or semitransparent glazed thickness is 0.3mm-1.3mm;The described pore degree of depth is between 0.01 μm of 0.3mm, and the thickness of described antibacterial stain-proofing layer keeps consistent with the pore degree of depth.
3. a method for the arbitrary described antibiotic ceramic tile of manufacturing claims 1-2, comprises the steps:
Ceramic powder compacting is formed adobe and burns till biscuit by S1, forms end base layer;On end base layer, spoon ground glaze layer, cover coat and printed decor from lower to upper respectively;
S2 drenches bright or translucent glaze layer on printed decor;
S3 glaze firing;
It is characterized in that: also include:
S4 is in the semi-finished product glaze paint baked, use buffing machine that glaze paint is carried out throwing and cut rubbing down, owing in buffing machine, abrading block contains corundum, hardness is higher than transparent or semitransparent glaze layer, so after transparent or semitransparent glaze layer surface-pressure high speed rubbing down, being abound with on transparent or semitransparent glaze layer surface with the visible pore not of uniform size of magnifier;
S5 uses super clean bright machine to fill the mixed liquor of super clean brilliant polish antifouling wax liquid and inorganic antiseptic in pore, or uses super clean bright machine to be taken up in order of priority the super clean brilliant polish antifouling wax liquid of filling and inorganic antiseptic in pore, and pressurization simultaneously throw flat throw bright.
4. method according to claim 3, it is characterised in that described printed decor is one or more combinations in screen printing, roller printing, inkjet printing stamp.
5. method according to claim 3, it is characterised in that the manufacture method of the transparent or semitransparent glaze layer in described step S2 is that transparent or semitransparent frit, methylcellulose and Kaolin add water and is processed to form liquid glaze through little ball milling.
6. method according to claim 3, it is characterised in that in described step S4, the described pore degree of depth is between 0.01 μm of 0.3mm.
7. method according to claim 3, it is characterised in that in step S5, described inorganic antiseptic be silver ion series, copper, zinc, titanium system individually or the inorganic antiseptic being mixed to form.
CN201610124189.4A 2016-03-04 2016-03-04 Antibacterial ceramic tiles and production method thereof Pending CN105801175A (en)

Priority Applications (1)

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Application Number Priority Date Filing Date Title
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107814587A (en) * 2017-09-22 2018-03-20 山东狮子王陶瓷科技有限公司 The preparation method of seven bright cloud ink stones
CN109016098A (en) * 2018-06-27 2018-12-18 清远市简陶瓷有限公司 A kind of antibiotic ceramic tile and preparation method thereof
CN111056862A (en) * 2019-12-13 2020-04-24 佛山欧神诺陶瓷有限公司 Production process of antibacterial ceramic tile
WO2021114539A1 (en) * 2019-12-13 2021-06-17 佛山欧神诺陶瓷有限公司 Antibacterial ceramic tile and preparation method therefor

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101082249A (en) * 2007-07-06 2007-12-05 广东博华陶瓷有限公司 Polishing brick and method for making same
CN201635275U (en) * 2010-01-07 2010-11-17 泉州荣达陶瓷有限公司 Novel antibacterial ceramic tile
CN103104080A (en) * 2011-11-15 2013-05-15 常州诺瑞格纳米科技有限公司 Antifouling nanometer brick
CN104876586A (en) * 2015-04-20 2015-09-02 福罗尼陶瓷有限公司 Production method of novel ceramic tile
CN104909828A (en) * 2015-06-19 2015-09-16 浙江根根陶瓷有限公司 Inner wall crystal-polishing mirror surface ceramic chip and manufacturing method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101082249A (en) * 2007-07-06 2007-12-05 广东博华陶瓷有限公司 Polishing brick and method for making same
CN201635275U (en) * 2010-01-07 2010-11-17 泉州荣达陶瓷有限公司 Novel antibacterial ceramic tile
CN103104080A (en) * 2011-11-15 2013-05-15 常州诺瑞格纳米科技有限公司 Antifouling nanometer brick
CN104876586A (en) * 2015-04-20 2015-09-02 福罗尼陶瓷有限公司 Production method of novel ceramic tile
CN104909828A (en) * 2015-06-19 2015-09-16 浙江根根陶瓷有限公司 Inner wall crystal-polishing mirror surface ceramic chip and manufacturing method thereof

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107814587A (en) * 2017-09-22 2018-03-20 山东狮子王陶瓷科技有限公司 The preparation method of seven bright cloud ink stones
CN109016098A (en) * 2018-06-27 2018-12-18 清远市简陶瓷有限公司 A kind of antibiotic ceramic tile and preparation method thereof
CN111056862A (en) * 2019-12-13 2020-04-24 佛山欧神诺陶瓷有限公司 Production process of antibacterial ceramic tile
WO2021114539A1 (en) * 2019-12-13 2021-06-17 佛山欧神诺陶瓷有限公司 Antibacterial ceramic tile and preparation method therefor

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Application publication date: 20160727