CN105778577A - Energy-storage and luminous ceramic coating and preparation method thereof - Google Patents

Energy-storage and luminous ceramic coating and preparation method thereof Download PDF

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Publication number
CN105778577A
CN105778577A CN201610149378.7A CN201610149378A CN105778577A CN 105778577 A CN105778577 A CN 105778577A CN 201610149378 A CN201610149378 A CN 201610149378A CN 105778577 A CN105778577 A CN 105778577A
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China
Prior art keywords
parts
energy storage
storage luminescent
component
luminescent ceramics
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Application number
CN201610149378.7A
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Chinese (zh)
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CN105778577B (en
Inventor
冯守中
梁军锋
李亮
张胜利
朱进萍
高巍
王军
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Anhui Zhongyi New Material Technology Co.,Ltd.
China Merchants Chongqing Communications Research and Design Institute Co Ltd
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ANHUI ZHONGYI NEW MATERIAL SCIENCE & TECHNOLOGY Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D1/00Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/22Luminous paints
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/60Additives non-macromolecular
    • C09D7/61Additives non-macromolecular inorganic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/65Additives macromolecular

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Paints Or Removers (AREA)

Abstract

The invention relates to an energy-storage and luminous ceramic coating. The ceramic coating is prepared from three components including raw materials in parts by weight as follows: an component A, including 30-90 parts of nano-silica sol, 10-30 parts of nano-alumina sol, 0-20 parts of filler, 0.2-5 parts of a catalyst and 1-60 parts of water; a component B, including 30-70 parts of organic silicon resin, 10-30 parts of an organic solvent, 5-20 parts of a binder and 2-10 parts of an additive; a component C, including 50-90 parts of energy-storage luminous powder and 0-50 parts of a solvent. The coating disclosed by the invention has an autonomous luminescence characteristic besides functions of high-temperature resistance, environment protection, self-cleaning and the like of ceramic coatings, has a very broad application field such as road safety facilities and stations, and particularly has significant applications in subway stations. Meanwhile, a preparation method is mature in process and applicable to mass production; the ceramic coating has a plurality of advantages, is a novel energy-saving and environment-friendly material and has significant economic value.

Description

A kind of energy storage luminescent ceramics coating and preparation method thereof
Technical field
The present invention is belonging to field of new, relates to the preparation of a kind of energy storage luminescent ceramics coating, is particularly applicable in traffic Safety devices field, such as bus platform, station, subway station etc..
Background technology
Along with the development of China Transportation Industry, traffic safety facilities is also required that stricter.Environment-friendly and energy-efficient product Become the important need of social development.
In recent years, the development of ceramic coating is applied in multiple fields, and it is wear-resisting, high temperature resistant, high intensity, super thin The advantages such as water can to a certain degree replace traditional enamel product.The autonomous characteristics of luminescence of energy-accumulating luminous powder is transported in traffic the most Defeated field many aspects are applied, and it has obtained fully agreeing of all circles from main light emission, environmental protection and energy saving, the performance such as pollution-free Fixed.The most do not occur that the plurality of advantages with ceramic coating simultaneously can also be from the product of main light emission, literary composition Offering and also have no report in patent, this characteristic can play a significant role in the underground installations such as subway station, has city widely Field prospect.
Summary of the invention
It is an object of the invention to: a kind of energy storage luminescent ceramics coating of exploitation so that it is there is the characteristic of ceramic coating simultaneously, There is again the autonomous illumination effect of energy-conserving and environment-protective.And it is simple with manufacture craft to meet production, it is suitable for the need of large-scale production Will be with the requirement of client.
To achieve these goals, the present invention provides following technical scheme:
A kind of energy storage luminescent ceramics coating, is formed, including the raw material of following weight portion by three component configurations:
Component A:
B component:
Component C
Energy-accumulating luminous powder 50-90 part
Solvent 0-50 part.
Preferably, described colloidal silica is 1-30% with the concentration of nano alumina sol, and particle diameter is 20- 60nm。
Preferably, described filler is one or more combinations in quartz, mica powder, talcum powder, kaolin, titanium dioxide Form.
Preferably, described catalyst is acid-base modifier, in glacial acetic acid, formic acid, acetic acid, stearic acid, oleic acid Plant or multiple combination.
Preferably, described organic siliconresin is in methoxyl group trichlorosilane, dimethyldichlorosilane, phenyl trichlorosilane One or more through modified resin.
Preferably, described binding agent is methyl methacrylate, butyl acrylate, acrylonitrile emulsion, organosilicone elastic One or more in body, vinegar the third adhesive mix.
Preferably, described auxiliary agent include in dispersant, levelling agent, wetting agent, defoamer one or more combination and Becoming, described organic solvent is that one or more in ethanol, methyl alcohol, acetone, ethyl acetate, ethylene glycol mix, described Solvent be that one or more in running water, deionized water, ethanol, acetone mix.
Preferably, described energy-accumulating luminous powder is long afterglow class luminescent powder, in aluminate serial, silicate series Kind or multiple be composited.
Preferably, the preparation method of described energy storage luminescent ceramics coating, when specifically comprising the following steps that preparation the most respectively by A, B, component C configure, and are then uniformly dispersed by A:B=1:0.5-1:3 weight ratio, finally by (A+B): C=1:0.1-1:0.8 weight Amount ratio adds C, cures 4-6h with 20-150r/min speed scroll on twin-roll machine, forms product.
Preferably, the construction method of described energy storage luminescent ceramics coating, specifically comprise the following steps that
A. paint is joined
It is uniformly dispersed by A:B=1:0.5-1:3 weight ratio, finally by (A+B): C=1:0.1-1:0.8 weight ratio adds C, On twin-roll machine, the speed scroll with 20~150r/m cures 4~6h;
B. the surface of workpiece processes
Workpiece, after oil removing, carries out blasting treatment, removes the rusty stain on surface, spot;The workpiece of blasting treatment is before applying 5~10min are preheated at the environment of 50~60 DEG C;
C. construct
Take gas or airless spraying, or electrostatic spraying mode is by energy storage luminescent ceramics spray painting to workpiece;
D. solidify
Under the conditions of 150~220 DEG C, solidify 10~30min.
The profitable effect of the present invention is:
1, the energy storage luminescent ceramics coating of preparation has high temperature resistant, wear-resisting, super-hydrophobic, high intensity, noninflammability, is suitable for many necks Territory is applied;
2, the energy storage luminescent ceramics coating of preparation can be from main light emission, energy-conserving and environment-protective.
3, production technology is simple, without complicated procedures of forming, produces constant product quality, has a good application prospect.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further described:
Embodiment 1
A kind of energy storage luminescent ceramics coating, it is characterised in that formed by three components configurations, former including following weight portion Material:
Component A:
B component:
Component C
50 parts of energy-accumulating luminous powder
Solvent 1 part.
Embodiment 2
A kind of energy storage luminescent ceramics coating, it is characterised in that formed by three components configurations, former including following weight portion Material:
Component A:
B component:
Component C
70 parts of energy-accumulating luminous powder
Solvent 20 parts.
Embodiment 3
A kind of energy storage luminescent ceramics coating, it is characterised in that formed by three components configurations, former including following weight portion Material:
Component A:
B component:
Component C
90 parts of energy-accumulating luminous powder
Solvent 50 parts.
Wherein, in embodiment 1-3:
Described colloidal silica is 1-30% with the concentration of nano alumina sol, and particle diameter is 20-60nm.
Described filler is that one or more in quartz, mica powder, talcum powder, kaolin, titanium dioxide combine.
Described catalyst is acid-base modifier, for one or more in glacial acetic acid, formic acid, acetic acid, stearic acid, oleic acid Combination.
Described organic siliconresin is the one in methoxyl group trichlorosilane, dimethyldichlorosilane, phenyl trichlorosilane Or it is multiple through modified resin.
Described binding agent is methyl methacrylate, butyl acrylate, acrylonitrile emulsion, elastomer silicone, vinegar third One or more in adhesive mix.
Described auxiliary agent includes that one or more in dispersant, levelling agent, wetting agent, defoamer combine, described Organic solvent be that one or more in ethanol, methyl alcohol, acetone, ethyl acetate, ethylene glycol mix, described solvent is One or more in running water, deionized water, ethanol, acetone mix.
Described energy-accumulating luminous powder is long afterglow class luminescent powder, for the one in aluminate serial, silicate series or many Plant and be composited.
Embodiment 4
The preparation method of the energy storage luminescent ceramics coating in embodiment 1-3, when specifically comprising the following steps that preparation the most respectively by A, B, component C configure, and are then uniformly dispersed by A:B=1:0.5-1:3 weight ratio, finally by (A+B): C=1:0.1-1:0.8 weight Amount ratio adds C, cures 4-6h with 20-150r/min speed scroll on twin-roll machine, forms product.
Embodiment 5
The construction method of the energy storage luminescent ceramics coating in embodiment 1-3, specifically comprises the following steps that
A. paint is joined
It is uniformly dispersed by A:B=1:0.5-1:3 weight ratio, finally by (A+B): C=1:0.1-1:0.8 weight ratio adds C, On twin-roll machine, the speed scroll with 20~150r/m cures 4~6h;
B. the surface of workpiece processes
Workpiece, after oil removing, carries out blasting treatment, removes the rusty stain on surface, spot;The workpiece of blasting treatment is before applying 5~10min are preheated at the environment of 50~60 DEG C;
C. construct
Take gas or airless spraying, or electrostatic spraying mode is by energy storage luminescent ceramics spray painting to workpiece;
D. solidify
Under the conditions of 150~220 DEG C, solidify 10~30min.
Embodiment 6
There is the luminescent properties of excellence in order to better illustrate this energy storage luminescent ceramics coating, by the energy-accumulating luminous pottery of preparation Porcelain coating is coated on steel plate and tests, and test result is as shown in table 1.
The twilight sunset test of table 1 reflex reflection energy-accumulating luminous paint

Claims (10)

1. an energy storage luminescent ceramics coating, it is characterised in that formed, including the raw material of following weight portion by three component configurations:
Component A:
B component:
Component C
Energy-accumulating luminous powder 50-90 part
Solvent 0-50 part.
Energy storage luminescent ceramics coating the most according to claim 1, it is characterised in that described colloidal silica with receive The concentration of rice alumina sol is 1-30%, and particle diameter is 20-60nm.
Energy storage luminescent ceramics coating the most according to claim 1, it is characterised in that described filler be quartz, mica powder, One or more in talcum powder, kaolin, titanium dioxide combine.
Energy storage luminescent ceramics coating the most according to claim 1, it is characterised in that described catalyst is acid-base accommodation Agent, for one or more combinations in glacial acetic acid, formic acid, acetic acid, stearic acid, oleic acid.
Energy storage luminescent ceramics coating the most according to claim 1, it is characterised in that described organic siliconresin is methoxyl group One or more in trichlorosilane, dimethyldichlorosilane, phenyl trichlorosilane are through modified resin.
Energy storage luminescent ceramics coating the most according to claim 1, it is characterised in that described binding agent is methacrylic acid One or more in methyl esters, butyl acrylate, acrylonitrile emulsion, elastomer silicone, vinegar the third adhesive mix.
Energy storage luminescent ceramics coating the most according to claim 1, it is characterised in that described auxiliary agent includes dispersant, stream One or more in flat agent, wetting agent, defoamer combine, and described organic solvent is ethanol, methyl alcohol, acetone, acetic acid One or more in ethyl ester, ethylene glycol mix, and described solvent is in running water, deionized water, ethanol, acetone Kind or multiple mix.
Energy storage luminescent ceramics coating the most according to claim 1, it is characterised in that described energy-accumulating luminous powder is long afterglow Class luminescent powder, is composited for one or more in aluminate serial, silicate series.
9. the preparation method of the energy storage luminescent ceramics coating as described in claim 1-8 any one, it is characterised in that tool Body step is as follows: A, B, component C are configured the most respectively during preparation, is then uniformly dispersed by A:B=1:0.5-1:3 weight ratio, Finally by (A+B): C=1:0.1-1:0.8 weight ratio adds C, twin-roll machine cures 4-with 20-150r/min speed scroll 6h, forms product.
10. the construction method of the energy storage luminescent ceramics coating as described in claim 1-8 any one, it is characterised in that Specifically comprise the following steps that
A. paint is joined
It is uniformly dispersed by A:B=1:0.5-1:3 weight ratio, finally by (A+B): C=1:0.1-1:0.8 weight ratio adds C, double On roller machine, the speed scroll with 20~150r/m cures 4~6h;
B. the surface of workpiece processes
Workpiece, after oil removing, carries out blasting treatment, removes the rusty stain on surface, spot;The workpiece of blasting treatment will be before applying The environment preheating 5~10min of 50~60 DEG C;
C. construct
Take gas or airless spraying, or electrostatic spraying mode is by energy storage luminescent ceramics spray painting to workpiece;
D. solidify
Under the conditions of 150~220 DEG C, solidify 10~30min.
CN201610149378.7A 2016-03-16 2016-03-16 A kind of preparation method of energy storage luminescent ceramics coating Active CN105778577B (en)

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108084752A (en) * 2017-12-27 2018-05-29 河北省交通规划设计院 A kind of tunnel inorganic aqueous energy-accumulating luminous paint and preparation method
CN110643358A (en) * 2019-09-29 2020-01-03 五行科技股份有限公司 Novel cross-linking modified energy-storage luminescent powder for coating and preparation method thereof
CN111019517A (en) * 2019-12-26 2020-04-17 江门市安诺特炊具制造有限公司 Water-based ceramic coating and preparation method thereof
CN111484354A (en) * 2020-06-05 2020-08-04 嘉应学院 High-hardness long-afterglow luminescent coating for enamel ceramic product and preparation method thereof
CN111995949A (en) * 2020-07-14 2020-11-27 陈子辉 High-temperature-resistant coating and preparation method thereof
CN113527920A (en) * 2021-07-06 2021-10-22 浙江大学杭州国际科创中心 Inorganic lithium ion battery diaphragm coating and preparation method thereof
CN114806252A (en) * 2021-01-19 2022-07-29 杭州路丽新材料有限公司 Road coating material and spraying process

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TW201323580A (en) * 2011-12-01 2013-06-16 Arthur Shiao Photo-luminance coating, glass and applications thereof
CN104804480A (en) * 2014-01-28 2015-07-29 上海复先材料科技有限公司 Three dimensional ceramic coating, and preparation method and application thereof

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Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108084752A (en) * 2017-12-27 2018-05-29 河北省交通规划设计院 A kind of tunnel inorganic aqueous energy-accumulating luminous paint and preparation method
CN110643358A (en) * 2019-09-29 2020-01-03 五行科技股份有限公司 Novel cross-linking modified energy-storage luminescent powder for coating and preparation method thereof
CN111019517A (en) * 2019-12-26 2020-04-17 江门市安诺特炊具制造有限公司 Water-based ceramic coating and preparation method thereof
CN111019517B (en) * 2019-12-26 2021-09-10 江门市安诺特炊具制造有限公司 Water-based ceramic coating and preparation method thereof
CN111484354A (en) * 2020-06-05 2020-08-04 嘉应学院 High-hardness long-afterglow luminescent coating for enamel ceramic product and preparation method thereof
CN111995949A (en) * 2020-07-14 2020-11-27 陈子辉 High-temperature-resistant coating and preparation method thereof
CN114806252A (en) * 2021-01-19 2022-07-29 杭州路丽新材料有限公司 Road coating material and spraying process
CN113527920A (en) * 2021-07-06 2021-10-22 浙江大学杭州国际科创中心 Inorganic lithium ion battery diaphragm coating and preparation method thereof
CN113527920B (en) * 2021-07-06 2022-06-21 浙江大学杭州国际科创中心 Inorganic lithium ion battery diaphragm coating and preparation method thereof

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