CN105617944B - A kind of vertical continuous rosin dry method dissolver - Google Patents
A kind of vertical continuous rosin dry method dissolver Download PDFInfo
- Publication number
- CN105617944B CN105617944B CN201610159583.1A CN201610159583A CN105617944B CN 105617944 B CN105617944 B CN 105617944B CN 201610159583 A CN201610159583 A CN 201610159583A CN 105617944 B CN105617944 B CN 105617944B
- Authority
- CN
- China
- Prior art keywords
- autoclave body
- melting
- rosin
- dry method
- vertical continuous
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 title claims abstract description 42
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 title claims abstract description 42
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 title claims abstract description 42
- 238000000034 method Methods 0.000 title claims abstract description 31
- 238000002844 melting Methods 0.000 claims abstract description 41
- 230000008018 melting Effects 0.000 claims abstract description 41
- 239000007788 liquid Substances 0.000 claims abstract description 20
- 239000002994 raw material Substances 0.000 claims abstract description 9
- 239000002893 slag Substances 0.000 claims abstract description 4
- 239000000155 melt Substances 0.000 claims description 8
- 238000004090 dissolution Methods 0.000 abstract description 2
- 239000007921 spray Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 235000008331 Pinus X rigitaeda Nutrition 0.000 description 2
- 235000011613 Pinus brutia Nutrition 0.000 description 2
- 241000018646 Pinus brutia Species 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000001293 FEMA 3089 Substances 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 239000003818 cinder Substances 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 210000002468 fat body Anatomy 0.000 description 1
- 238000005243 fluidization Methods 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 239000003317 industrial substance Substances 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J6/00—Heat treatments such as Calcining; Fusing ; Pyrolysis
- B01J6/005—Fusing
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09F—NATURAL RESINS; FRENCH POLISH; DRYING-OILS; DRIERS (SICCATIVES); TURPENTINE
- C09F1/00—Obtaining purification, or chemical modification of natural resins, e.g. oleo-resins
- C09F1/02—Purification
Abstract
The invention discloses a kind of vertical continuous rosin dry method dissolvers, including melting autoclave body, it is equipped with slag notch in the melting autoclave body bottom, hot-oil jacket is equipped on the melting autoclave body outer wall, the hot-oil circulation pipe being connected with external jacket is equipped in the melting autoclave body；Traveling hoisting type blender and/or N are equipped in the melting autoclave body2Jet pipe；The outlet of fat liquid is set on the melting autoclave body side wall and mouth is added in rosin raw material.The vertical continuous rosin dry method dissolver of the present invention, it is simple in sturcture, ingenious in design, it is suitable for dry method continuous-dissolution rosin technique, satisfies the use demand, can effectively prepares qualified melting rosin liquid.
Description
Technical field
The present invention relates to industrial chemicals to melt (or rosin melting) equipment technical field, and in particular to a kind of vertical continuous pine
Fat dry method dissolver.
Background technology
In pine gum processing technique, the melting of rosin is very important the first procedure.It is related to rosin product
Yield and quality and subsequent machining technology are smoothed out.The purpose that rosin melts is so that rosin is liquefied completely, reduce viscosity, is made
Fluidization convenient for technique conveying, melt the distillation of fat liquid net system and net system fat liquid.
The dissolution process of rosin in traditional wet processing is boiled using Jia Shui plus decolorising agent, lively atmosphere spray, is sufficiently stirred fat
Liquid is allowed to the measures such as homogeneous heating.
But conventional wet technique is diluted with water, wash and lively atmosphere stirring spray is boiled during melting rosin, will produce a large amount of
Technique waste water, pollute environment water.Therefore, it is necessary to be reformed to traditional rosin melting equipment and technique, design is a kind of
Be not diluted with water, wash and lively atmosphere stirring spray boil melt rosin dry method rosin dissolver.
Currently, being suitble to the dissolver of dry method melting rosin not yet.
Invention content
Goal of the invention：For the deficiencies in the prior art, the object of the present invention is to provide a kind of vertical continuous rosin
Dry method dissolver is suitable for dry method and dissolves rosin technique, satisfies the use demand.
Technical solution：In order to achieve the above-mentioned object of the invention, the technical solution adopted by the present invention is：
A kind of vertical continuous rosin dry method dissolver, including autoclave body is melted, it is equipped with and slags tap in the melting autoclave body bottom
Mouthful, hot-oil jacket is equipped on the melting autoclave body outer wall, equipped with being connected with external jacket in the meltings autoclave body
Hot-oil circulation pipe；Traveling hoisting type blender and/or N are equipped in the melting autoclave body2Jet pipe；In the melting autoclave body
The outlet of fat liquid is set on side wall and mouth is added in rosin raw material.
The traveling hoisting type blender, which is located at, melts autoclave body centre position, is driven by motor.
The fat liquid outlet, which is located at, melts autoclave body side wall upper part.
The N2Jet pipe is located at melting autoclave body low inside and sets.
The rosin raw material is added mouth and is located at melting autoclave body lower sidewall.
Advantageous effect：Compared with prior art, vertical continuous rosin dry method dissolver of the invention, simple in structure, design
It is ingenious, it is suitable for continuous dry method and dissolves rosin technique, satisfy the use demand, can effectively prepares qualified melting rosin liquid.
Description of the drawings
Fig. 1 is the structural schematic diagram of vertical continuous rosin dry method dissolver.
Specific implementation mode
With reference to specific embodiment, the present invention is further illustrated.As described below is only the preferable implementation of the present invention
Example is used only for the description present invention, should not be understood as limiting the scope of the present invention.It should be pointed out that all in the present invention
Spirit and principle within all any modification, equivalent and improvement etc. done, should be included in protection scope of the present invention it
It is interior.
As shown in Figure 1, vertical continuous rosin dry method dissolver, agent structure is to melt autoclave body 2, is melting 2 bottom of autoclave body
Cinder notch 9 is set out, hot-oil jacket 4 is equipped on melting 2 outer wall of autoclave body, is melting the heat for being equipped in autoclave body 2 and being connected with external jacket
Oil circulating pipe 5, traveling hoisting type blender 6 and N2Jet pipe 8；N is installed in the lower portion melted in autoclave body 22Jet pipe 8.Melting kettle
Fat liquid outlet 3 is set on 2 side wall of body, fat liquid outlet 3, which is located at, melts 2 side wall upper part of autoclave body.Traveling hoisting type blender 6, which is located at, to be melted
2 centre position of autoclave body, is driven by motor 1.Rosin raw material being set on melting 2 side wall of autoclave body, mouth 7 being added, mouth 7 is added in rosin raw material
Positioned at 2 lower sidewall position of melting autoclave body.Wherein, traveling hoisting type blender 6 and N2Jet pipe 8 is in this dissolver to melting
Fat liquid plays stirring and promotes progradation, traveling hoisting type blender 6 can only be arranged, or N is only arranged2Jet pipe 8, can also be same
When setting traveling hoisting type blender 6 and N2Jet pipe 8.
Using the vertical continuous rosin dry method dissolver, the technique for dissolving rosin is：Before melting operation, make hot-oil jacket 4
It is full of deep fat with hot-oil circulation pipe 5, it is molten that rosin raw material is sent into vertical continuous rosin dry method after double rods or single rod mediate crusher machine
Device is solved, the turpentine oil for accounting for rosin 40-20% (wt) is added as dissolved oil, opens motor 1 and drives traveling hoisting type blender 6
(or from N2Jet pipe 8 is passed through hot N2), heating melts, and with rosin raw material and melts oily addition and travelling mechanical agitation, mixing
Feed liquid, which continuously rises to along melting wall, melts fat liquid outlet 3, according to the height of wall and adjusts blender rotating speed,
Fat liquid is set to pass through the enough melting time, fat liquid temperature at this time should reach 110-120 DEG C.The heavy seeds such as most of silt are from molten
It solves device bottom slag notch 9 to be discharged, the melting fat liquid gravity flow at most fraction contaminant filter containing light impurity filters, and enters back into high speed
It centrifuges, removes fine impurities and moisture, net system fat liquid enters gutter, and distillation is spare.
The vertical continuous rosin dry method dissolver of the present invention, it is simple in sturcture, ingenious in design, it is suitable for dry method and dissolves rosin work
Skill satisfies the use demand, and can effectively prepare qualified melting rosin liquid.
Claims (1)
1. a kind of vertical continuous rosin dry method dissolver, which is characterized in that including melting autoclave body (2), in the melting autoclave body
(2) bottom is equipped with slag notch (9), hot-oil jacket (4) is equipped on described melting autoclave body (2) outer wall, in the melting kettle
The hot-oil circulation pipe (5) being connected with external jacket is equipped in body (2)；Traveling hoisting type is equipped in the melting autoclave body (2)
Blender (6) and/or N2Jet pipe (8)；Fat liquid outlet (3) is set on described melting autoclave body (2) side wall and rosin raw material is added
Mouth (7)；The traveling hoisting type blender (6), which is located at, melts autoclave body (2) centre position, is driven by motor (1)；The fat
Liquid exports (3) and is located at melting autoclave body (2) side wall upper part；The rosin raw material is added mouth (7) and is located on melting autoclave body (2) side wall
Lower part；The N2Jet pipe (8) is located at melting autoclave body (2) low inside and sets.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610159583.1A CN105617944B (en) | 2016-03-21 | 2016-03-21 | A kind of vertical continuous rosin dry method dissolver |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610159583.1A CN105617944B (en) | 2016-03-21 | 2016-03-21 | A kind of vertical continuous rosin dry method dissolver |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105617944A CN105617944A (en) | 2016-06-01 |
| CN105617944B true CN105617944B (en) | 2018-10-16 |
Family
ID=56033521
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610159583.1A Expired - Fee Related CN105617944B (en) | 2016-03-21 | 2016-03-21 | A kind of vertical continuous rosin dry method dissolver |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105617944B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106675415B (en) * | 2016-12-22 | 2023-06-23 | 临沧方源林产品有限公司 | Rosin production system of processing |
| CN112892418B (en) * | 2021-01-14 | 2022-07-29 | 江苏维尤纳特精细化工有限公司 | M-phthalonitrile processing device |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1435745A1 (en) * | 1963-07-11 | 1969-02-13 | Vickers Zimmer Ag | Method and device for the continuous melting of solids |
| CN2034579U (en) * | 1988-05-20 | 1989-03-22 | 广东省云浮县松香厂 | Resin continuous fusion device |
| CN202006032U (en) * | 2011-02-08 | 2011-10-12 | 溧阳市利达有机硅科技有限公司 | Crude rubber dehydrating device |
| CN204582978U (en) * | 2014-12-17 | 2015-08-26 | 江西松源林产高科有限公司 | A kind of rosin high-temperature digestion device |
| CN105199607B (en) * | 2015-09-30 | 2017-08-29 | 广西大学 | Lively atmosphere tangential jet self-rotary rosin distilling apparatus and its use |
| CN205650173U (en) * | 2016-03-21 | 2016-10-19 | 南京林业大学 | Vertical continuous rosin dry process fusion ware |
-
2016
- 2016-03-21 CN CN201610159583.1A patent/CN105617944B/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN105617944A (en) | 2016-06-01 |
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| C10 | Entry into substantive examination | ||
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| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
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Granted publication date: 20181016 Termination date: 20200321 |