CN105613709A - Pork fresh-keeping agent with excellent fresh-keeping performance and preparation method thereof - Google Patents
Pork fresh-keeping agent with excellent fresh-keeping performance and preparation method thereof Download PDFInfo
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- CN105613709A CN105613709A CN201610200302.2A CN201610200302A CN105613709A CN 105613709 A CN105613709 A CN 105613709A CN 201610200302 A CN201610200302 A CN 201610200302A CN 105613709 A CN105613709 A CN 105613709A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B4/00—General methods for preserving meat, sausages, fish or fish products
- A23B4/14—Preserving with chemicals not covered by groups A23B4/02 or A23B4/12
- A23B4/18—Preserving with chemicals not covered by groups A23B4/02 or A23B4/12 in the form of liquids or solids
- A23B4/20—Organic compounds; Microorganisms; Enzymes
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B4/00—General methods for preserving meat, sausages, fish or fish products
- A23B4/14—Preserving with chemicals not covered by groups A23B4/02 or A23B4/12
- A23B4/18—Preserving with chemicals not covered by groups A23B4/02 or A23B4/12 in the form of liquids or solids
- A23B4/20—Organic compounds; Microorganisms; Enzymes
- A23B4/22—Microorganisms; Enzymes; Antibiotics
Abstract
The invention discloses a pork fresh-keeping agent with an excellent fresh-keeping performance. The pork fresh-keeping agent is characterized by comprising the following materials in parts by weight: 20-40 parts of clove and cinnamon compound extracting solution, 5-15 parts of pomegranate extracting solution, 2-5 parts of chitosan, 3-6 parts of trehalose, 2-6 parts of propolis, 3-8 parts of lysozyme, 1-4 parts of tea polyphenol, 2-5 parts of Epsilon-polylysine, 1-4 parts of acetic acid, 1-3 parts of sodium lactate, 1-3 parts of grape-seed essential oil, 1-3 parts of orange essential oil and 2-4 parts of bacillus natto. The invention also discloses a preparation method of the pork fresh-keeping agent with the excellent fresh-keeping performance. The pork fresh-keeping agent disclosed by the invention has excellent preservative and fresh-keeping performances.
Description
Technical field
The present invention relates to Food Engineering Development field, particularly relate to a kind of pork preservative and its preparation method with excellent fresh keeping property.
Background technology
Along with the raising of living standards of the people, people more pay attention to the safety and sanitation quality of meat product, with consumption form, the process systems of meat are had higher requirement simultaneously. Form sold by the fresh meat that Chilled Meats is widespread use at present both at home and abroad. Chilled Meats is being produced with in the process of circulation, although under being in low temperature control always, the retentiveness of Chilled Meats, tenderness and fresh taste etc. are all farthest improved, but meat still pollutes and has some psychrophilic bacterias, such as monocyte Liszt hyperplasia bacterium and Rhodopseudomonas etc., they under refrigerated conditions still can raised growth and breeding, finally cause Chilled Meats occur putrid and deteriorated. The surperficial brown stain of Chilled Meats is another class problem that Chilled Meats often occurs in sales process, shelf-lives planted agent at Chilled Meats makes putrid and deteriorated and surperficial brown stain control to minimum level, the problem of current these two aspects is the key point that restriction Chilled Meats is widelyd popularize and popularized always, therefore, the research of the preservation technique of Chilled Meats has very important significance.
Pork is the meat of porcine animals man pig, its nature and flavor are sweet salty flat, containing compositions such as abundant protein and fat, carbohydrate, calcium, iron, phosphorus, it it is the main nonstaple food of daily life, there is qi-restoratives keep fit, the effect of flesh nourshing Yin and drynsessmoistening prescription, rich pool skin, is one of animal food important on people's dining table, is also the important research content of Chilled Meats preservation technique.
Pork preservation technique is a systems engineering, and comprising the bacterium phase change in the control of raw meat initial bacterium number, storage process and fresh-keeping liquid process and different packaging means etc., the applied research of bio-preservative is a wherein extremely important link. At present, although it is both at home and abroad that pork preservative research aspect report is more, but focusing mostly in the application of Chemical Preservative or the research of single creature sanitas, after multiple bio-preservative is composite, research to the comprehensive preservation effect that the fresh-keeping effect of pork and preservation agent and irradiation technique, modified atmosphere packaging technology combine is still not deep enough. Along with the mankind are to improving constantly that own health and environmental issue recognize, people find that many chemosynthesis antiseptic-germicides have potential " three cause " effect gradually, and the exploitation of new chemical synthetic antimicrobial sanitas is more and more difficult so that biogenic pork preservative is subject to the favor of people.
The more biogenic pork preservative of research can be divided into plant-sourced pork preservative, animal source pork preservative and microbial source pork preservative by its source at present. Every class comprises again multiple, so widely using the development trend that composite mode is pork preservative, adopt composite mode, the sphere of action of former single sanitas can be expanded, can also reducing the Dosages of single sanitas, the pork preservative of different sources is composite simultaneously, moreover it is possible to produce synergistic effect, improve fresh keeping property, decrease the consumption of preservation agent.
Summary of the invention
The technical problem existed for solving in background technology, the present invention proposes a kind of pork preservative and its preparation method with excellent fresh keeping property, the composite pork preservative good refreshing effect obtained, health environment-friendly.
A kind of pork preservative with excellent fresh keeping property that the present invention proposes, its raw material comprises by weight: cloves cassia bark compound extracted solution 20-40 part, pomegranate rind extracting solution 5-15 part, chitosan 2-5 part, trehalose 3-6 part, propolis 2-6 part, N,O-Diacetylmuramidase 3-8 part, tea-polyphenol 1-4 part, epsilon-polylysine 2-5 part, acetic acid 1-4 part, Sodium.alpha.-hydroxypropionate 1-3 part, Semen Vitis viniferae essence oil 1-3 part, tangerine oil 1-3 part, bacillus natto 2-4 part;
The raw material of described Chinese medicine composite additive comprises by weight: Elettaria cardamomum (L.) Maton 5-6 part, jamaica pepper 2-8 part, Thymus vulgaris 1-4 part, ginger 2-6 part, Persea cubeba 1-4 part, mustard seed 2-6 part, Salvia japonica Thunb. 1-4 part, dried orange peel 2-6 part;
Described cloves cassia bark compound extracted solution is prepared by following technique: take Ground Cloves and Cortex cinnamomi japonici powder, join in 80-120ml distilled water, 70-90 DEG C of water bath with thermostatic control heating 7-9h, it is cooled to normal temperature, the process of cooling does not stop jolting, then turn/centrifugal the 10-30min of min in 2500-3000, get supernatant liquor, namely obtain the cloves cassia bark compound extracted solution containing effective constituent 5-8%.
Preferably, in the preparation technology of described cloves cassia bark compound extracted solution, the weight ratio of Ground Cloves and Cortex cinnamomi japonici powder is 2-5:1-3.
Preferably, described pomegranate rind extracting solution is prepared by following technique: crosses 30-50 order sieve after being pulverized by pomegranate pericarp, take water as solvent, solid-liquid ratio 2-4:17, extracts 1-3h in 60-80 DEG C, obtain pomegranate rind extracting solution after filtration.
Preferably, described Chinese medicine composite additive is prepared by following technique: by Elettaria cardamomum (L.) Maton, jamaica pepper, Thymus vulgaris, ginger, Persea cubeba, mustard seed, Salvia japonica Thunb. and dried orange peel co-grinding, mix and obtain material a, then material a is added in ethanolic soln, carry out frozen dried after stirring evenly and obtain material b; Then material b and water are mixed, decoct for 65-85 DEG C and boil 2-4h, be cooled to room temperature and obtain filtrate, then filtrate is carried out concentrating under reduced pressure and obtain concentrated solution, then it is cooled to normal temperature by after concentrated solution 65-85 DEG C of drying, then it is ground to the Chinese medicine composite additive of 20-40 order granular material.
Preferably, the weight ratio of cloves cassia bark compound extracted solution, pomegranate rind extracting solution, chitosan, trehalose and propolis is 25-35:8-12:3-4:4-5:3-5.
Preferably, the weight ratio of cloves cassia bark compound extracted solution, pomegranate rind extracting solution, Semen Vitis viniferae essence oil and tangerine oil is 25-35:8-12:1.5-2.5:1.5-2.5.
Preferably, the weight ratio of cloves cassia bark compound extracted solution, N,O-Diacetylmuramidase, tea-polyphenol, epsilon-polylysine, acetic acid, Sodium.alpha.-hydroxypropionate and bacillus natto is 25-35:4-7:2-3:3-4:2-3:1.5-2.5:2.5-3.5.
Preferably, its raw material comprises by weight: cloves cassia bark compound extracted solution 25-35 part, pomegranate rind extracting solution 8-12 part, chitosan 3-4 part, trehalose 4-5 part, propolis 3-5 part, N,O-Diacetylmuramidase 4-7 part, tea-polyphenol 2-3 part, epsilon-polylysine 3-4 part, acetic acid 2-3 part, Sodium.alpha.-hydroxypropionate 1.5-2.5 part, Semen Vitis viniferae essence oil 1.5-2.5 part, tangerine oil 1.5-2.5 part, bacillus natto 2.5-3.5 part.
Preferably, its raw material comprises by weight: cloves cassia bark compound extracted solution 30 parts, pomegranate rind extracting solution 10 parts, chitosan 3.5 parts, trehalose 4.5 parts, propolis 4 parts, N,O-Diacetylmuramidase 5.5 parts, tea-polyphenol 2.5 parts, epsilon-polylysine 3.5 parts, acetic acid 2.5 parts, Sodium.alpha.-hydroxypropionate 2 parts, Semen Vitis viniferae essence oil 2 parts, tangerine oil 2 parts, bacillus natto 3 parts.
The preparation method of a kind of pork preservative with excellent fresh keeping property that the present invention proposes, comprises the steps:
S1, chitosan, acetic acid and Sodium.alpha.-hydroxypropionate are mixed, in 50-60 DEG C of water bath with thermostatic control heating 5-15min, then add trehalose and propolis mixes, be cooled to room temperature and obtain material a;
S2, in material a, add cloves cassia bark compound extracted solution, pomegranate rind extracting solution, tea-polyphenol, epsilon-polylysine, Semen Vitis viniferae essence oil and tangerine oil mix, in 50-70 DEG C of water bath with thermostatic control 30-50min, be cooled to room temperature and obtain material b;
S3, in material b, add N,O-Diacetylmuramidase and bacillus natto mixes the pork preservative obtaining having excellent fresh keeping property.
Chitosan is a kind of high molecular polymer with high-efficiency antimicrobial effect and good filming, is obtained by de-acetyl by chitin, is widely used in food fresh keeping. Epsilon-polylysine (��-PL) is many polyamino acid that a class is formed by peptide linkage by the epsilon-amino of 1B and ��-carboxyl, has the features such as safety, efficient, nutrition, Heat stability is good. Gram-negative bacteria, gram-positive microorganism, yeast and mould are had good restraining effect by ��-PL. In some developed countries, ��-PL has been widely used in food industry-by-industry, such as bread dessert, milk preparation and refrigerated food etc.; ��-PL is applied to milk, fresh cut vegetables aspect, and is almost in blank in the application of chilled pork. Tea-polyphenol is the general name of polyphenols in tealeaves, comprises flavanol compound, flavonoid and phenolic acids etc., has anti-oxidant and bacteriostatic action, also have good result in food fresh keeping. Acetic acid, also known as acetic acid, is a kind of organic compound being extensively present in nature, usually used as a kind of acidity regulator; It also has certain bacteriostatic action. Plants essential oil be generally acknowledge at present a kind of safely, there is the chemical substance of broad-spectrum antibacterial, food officina of the U.S. has ratified it and can be applicable to field of food. Tangerine oil is mainly present in orange peel, and bacterium and some product poison bacteriums of Penicillium fungi and product spore are had certain restraining effect by tangerine oil. Bacillus natto has stronger anti-microbial effect, and the features such as it is nontoxic, efficient, suitability wide, stable performance are a kind of natural bio-preservatives well. Bacillus natto antibacterial protein has significant preservative effect in the preservation of fresh thin pork and sterilized milk. Sodium.alpha.-hydroxypropionate is not only a kind of nontoxic biological preservative, the simultaneously interpolation of Sodium.alpha.-hydroxypropionate can improve the tenderness of SDS in broiler chickens, local flavor, color, matter structure etc., and lot of documents shows that Sodium.alpha.-hydroxypropionate and other sanitass or extraneous physical action coupling are better to SDS in broiler chickens corrosion-resistanting fresh-keeping effect. Reason is as follows: one is that Gram-negative bacteria is only had restraining effect by Sodium.alpha.-hydroxypropionate, gram-positive microorganism is invalid, gram-positive microorganism is had by Sodium.alpha.-hydroxypropionate and other sanitas coupling of relatively high inhibition effect, play the complementary synergism of multiple sanitas, the antimicrobial spectrum of sanitas can be expanded, obtain very good corrosion-resistanting fresh-keeping effect; Two be Sodium.alpha.-hydroxypropionate when being used alone desired concn higher, but the Sodium.alpha.-hydroxypropionate of high density can affect protein expression and stability in pork, Sodium.alpha.-hydroxypropionate and other are had the sanitas of synergy, extraneous physical action coupling, both the consumption of single sanitas can have been reduced, prevent protein denaturation, can also there be wider antimicrobial spectrum and antibacterial intensity, it is possible to extend its shelf-lives longlyer; In addition, Sodium.alpha.-hydroxypropionate is incorporated in preeictive microbiology model as environmental factor, under the prerequisite not carrying out microorganism detection, the growth rhythm of prediction spoilage microorganisms, its degree of spoilage of monitor in real time in the process of circulation is preserved at SDS in broiler chickens, quality and safety to SDS in broiler chickens make reasonable judgement, considerably increase the confidence level of product forecasting shelf life. Semen Vitis viniferae essence oil has the ability of strong oxidation and removing free radicals owing to being rich in pycnogenols.
A kind of pork preservative with excellent fresh keeping property of the present invention, its raw material comprises cloves cassia bark compound extracted solution, pomegranate rind extracting solution, chitosan, trehalose, propolis, N,O-Diacetylmuramidase, tea-polyphenol, epsilon-polylysine, acetic acid, Sodium.alpha.-hydroxypropionate, Semen Vitis viniferae essence oil, tangerine oil and bacillus natto. Wherein with cloves cassia bark compound extracted solution, composite by cloves and cassia bark, and carry out its juice of mixed extraction, effectively play the antiseptic property of cloves and cassia bark, and then effectively enhance the fresh keeping property of the pork preservative of the present invention; The pomegranate rind extracting solution, chitosan, trehalose, propolis, N,O-Diacetylmuramidase, tea-polyphenol, epsilon-polylysine, acetic acid, Sodium.alpha.-hydroxypropionate, Semen Vitis viniferae essence oil, tangerine oil and the bacillus natto that add cooperatively interact, and conservative control proportioning, play extremely good preservative effect, synergy fresh keeping property. The Chinese medicine composite additive wherein added is taking Elettaria cardamomum (L.) Maton, jamaica pepper, Thymus vulgaris, ginger, Persea cubeba, mustard seed, Salvia japonica Thunb. and dried orange peel as raw material, and boil by decocting, extract, concentrated, the Chinese medicine composite additive that grinding flour obtains has excellent anti-corrosive fresh-keeping performance, and then effectively facilitates the corrosion-resistanting fresh-keeping effect of the pork preservative of the present invention.
Embodiment
Below in conjunction with specific embodiment, the present invention is described in detail; should understand; embodiment only for illustration of the present invention, instead of for the present invention is limited, any make on basis of the present invention amendment, equivalent replacement etc. is all in protection scope of the present invention.
Embodiment 1
A kind of pork preservative with excellent fresh keeping property that the present invention proposes, its raw material comprises by weight: cloves cassia bark compound extracted solution 30 parts, pomegranate rind extracting solution 10 parts, chitosan 3.5 parts, trehalose 4.5 parts, propolis 4 parts, N,O-Diacetylmuramidase 5.5 parts, tea-polyphenol 2.5 parts, epsilon-polylysine 3.5 parts, acetic acid 2.5 parts, Sodium.alpha.-hydroxypropionate 2 parts, Semen Vitis viniferae essence oil 2 parts, tangerine oil 2 parts, bacillus natto 3 parts.
Cloves cassia bark compound extracted solution is prepared by following technique: take 3.5 parts of Ground Cloves and 2 parts of Cortex cinnamomi japonici powderes by weight, join in 100ml distilled water, 80 DEG C of water bath with thermostatic control heating 8h, it is cooled to normal temperature, the process of cooling does not stop jolting, then in the centrifugal 20min of 2750 turns/min, get supernatant liquor, namely obtain the cloves cassia bark compound extracted solution containing effective constituent 7.5%.
Chinese medicine composite additive is prepared by following technique: by 5.5 portions of Elettaria cardamomum (L.) Matons, 5 parts of jamaica pepper, 2.5 parts of Thymus vulgariss, 4 portions of gingers, 2.5 portions of Persea cubeba, 4 parts of mustard seeds, 2.5 parts of Salvia japonica Thunb.s and 4 parts of dried orange peel co-grindings, mix and obtain material a, then material a is added in ethanolic soln, carry out frozen dried after stirring evenly and obtain material b; Then material b and water are mixed, decoct for 75 DEG C and boil 3h, be cooled to room temperature and obtain filtrate, then filtrate is carried out concentrating under reduced pressure and obtain concentrated solution, then it is cooled to normal temperature by after concentrated solution 75 DEG C of dryings, then it is ground to the Chinese medicine composite additive of 30 order granular materials.
The preparation method of a kind of pork preservative with excellent fresh keeping property that the present invention proposes, comprises the steps:
S1, chitosan, acetic acid and Sodium.alpha.-hydroxypropionate are mixed, in 55 DEG C of waters bath with thermostatic control heating 20min, then add trehalose and propolis mixes, be cooled to room temperature and obtain material a;
S2, in material a, add cloves cassia bark compound extracted solution, pomegranate rind extracting solution, tea-polyphenol, epsilon-polylysine, Semen Vitis viniferae essence oil and tangerine oil mix, in 60 DEG C of water bath with thermostatic control 40min, be cooled to room temperature and obtain material b;
S3, in material b, add N,O-Diacetylmuramidase and bacillus natto mixes the pork preservative obtaining having excellent fresh keeping property.
Embodiment 2
A kind of pork preservative with excellent fresh keeping property that the present invention proposes, its raw material comprises by weight: cloves cassia bark compound extracted solution 20 parts, pomegranate rind extracting solution 15 parts, chitosan 2 parts, trehalose 6 parts, propolis 2 parts, N,O-Diacetylmuramidase 8 parts, tea-polyphenol 1 part, epsilon-polylysine 5 parts, acetic acid 1 part, Sodium.alpha.-hydroxypropionate 3 parts, Semen Vitis viniferae essence oil 1 part, tangerine oil 3 parts, bacillus natto 2 parts.
Wherein, pomegranate rind extracting solution is prepared by following technique: crossing 40 order sieves after being pulverized by pomegranate pericarp, take water as solvent, solid-liquid ratio 3:17, extracts 2h in 70 DEG C, obtain pomegranate rind extracting solution after filtration.
Chinese medicine composite additive is prepared by following technique: by 5 portions of Elettaria cardamomum (L.) Matons, 8 parts of jamaica pepper, 1 part of Thymus vulgaris, 6 portions of gingers, 1 portion of Persea cubeba, 6 parts of mustard seeds, 1 part of Salvia japonica Thunb. and 6 parts of dried orange peel co-grindings, mix and obtain material a, then material a is added in ethanolic soln, carry out frozen dried after stirring evenly and obtain material b; Then material b and water are mixed, decoct for 65 DEG C and boil 4h, be cooled to room temperature and obtain filtrate, then filtrate is carried out concentrating under reduced pressure and obtain concentrated solution, then it is cooled to normal temperature by after concentrated solution 65 DEG C of dryings, then it is ground to the Chinese medicine composite additive of 40 order granular materials.
The preparation method of a kind of pork preservative with excellent fresh keeping property that the present invention proposes, comprises the steps:
S1, chitosan, acetic acid and Sodium.alpha.-hydroxypropionate are mixed, in 50 DEG C of waters bath with thermostatic control heating 15min, then add trehalose and propolis mixes, be cooled to room temperature and obtain material a;
S2, in material a, add cloves cassia bark compound extracted solution, pomegranate rind extracting solution, tea-polyphenol, epsilon-polylysine, Semen Vitis viniferae essence oil and tangerine oil mix, in 50 DEG C of water bath with thermostatic control 50min, be cooled to room temperature and obtain material b;
S3, in material b, add N,O-Diacetylmuramidase and bacillus natto mixes the pork preservative obtaining having excellent fresh keeping property.
Embodiment 3
A kind of pork preservative with excellent fresh keeping property that the present invention proposes, its raw material comprises by weight: cloves cassia bark compound extracted solution 40 parts, pomegranate rind extracting solution 5 parts, chitosan 5 parts, trehalose 3 parts, propolis 6 parts, N,O-Diacetylmuramidase 3 parts, tea-polyphenol 4 parts, epsilon-polylysine 2 parts, acetic acid 4 parts, Sodium.alpha.-hydroxypropionate 1 part, Semen Vitis viniferae essence oil 3 parts, tangerine oil 1 part, bacillus natto 4 parts.
Chinese medicine composite additive is prepared by following technique: by 6 portions of Elettaria cardamomum (L.) Matons, 2 parts of jamaica pepper, 4 parts of Thymus vulgariss, 2 portions of gingers, 4 portions of Persea cubeba, 2 parts of mustard seeds, 4 parts of Salvia japonica Thunb.s and 2 parts of dried orange peel co-grindings, mix and obtain material a, then material a is added in ethanolic soln, carry out frozen dried after stirring evenly and obtain material b; Then material b and water are mixed, decoct for 85 DEG C and boil 2h, be cooled to room temperature and obtain filtrate, then filtrate is carried out concentrating under reduced pressure and obtain concentrated solution, then it is cooled to normal temperature by after concentrated solution 85 DEG C of dryings, then it is ground to the Chinese medicine composite additive of 20 order granular materials.
The preparation method of a kind of pork preservative with excellent fresh keeping property that the present invention proposes, comprises the steps:
S1, chitosan, acetic acid and Sodium.alpha.-hydroxypropionate are mixed, in 60 DEG C of waters bath with thermostatic control heating 5min, then add trehalose and propolis mixes, be cooled to room temperature and obtain material a;
S2, in material a, add cloves cassia bark compound extracted solution, pomegranate rind extracting solution, tea-polyphenol, epsilon-polylysine, Semen Vitis viniferae essence oil and tangerine oil mix, in 70 DEG C of water bath with thermostatic control 30min, be cooled to room temperature and obtain material b;
S3, in material b, add N,O-Diacetylmuramidase and bacillus natto mixes the pork preservative obtaining having excellent fresh keeping property.
Embodiment 4
A kind of pork preservative with excellent fresh keeping property that the present invention proposes, its raw material comprises by weight: cloves cassia bark compound extracted solution 25 parts, pomegranate rind extracting solution 12 parts, chitosan 3 parts, trehalose 5 parts, propolis 3 parts, N,O-Diacetylmuramidase 7 parts, tea-polyphenol 2 parts, epsilon-polylysine 4 parts, acetic acid 2 parts, Sodium.alpha.-hydroxypropionate 2.5 parts, Semen Vitis viniferae essence oil 1.5 parts, tangerine oil 2.5 parts, bacillus natto 2.5 parts.
Chinese medicine composite additive is prepared by following technique: by 5.2 portions of Elettaria cardamomum (L.) Matons, 7 parts of jamaica pepper, 2 parts of Thymus vulgariss, 5 portions of gingers, 2 portions of Persea cubeba, 5 parts of mustard seeds, 2 parts of Salvia japonica Thunb.s and 5 parts of dried orange peel co-grindings, mix and obtain material a, then material a is added in ethanolic soln, carry out frozen dried after stirring evenly and obtain material b; Then material b and water are mixed, decoct for 66 DEG C and boil 3.5h, be cooled to room temperature and obtain filtrate, then filtrate is carried out concentrating under reduced pressure and obtain concentrated solution, then it is cooled to normal temperature by after concentrated solution 68 DEG C of dryings, then it is ground to the Chinese medicine composite additive of 35 order granular materials.
The preparation method of a kind of pork preservative with excellent fresh keeping property that the present invention proposes, comprises the steps:
S1, chitosan, acetic acid and Sodium.alpha.-hydroxypropionate are mixed, in 52 DEG C of waters bath with thermostatic control heating 12min, then add trehalose and propolis mixes, be cooled to room temperature and obtain material a;
S2, in material a, add cloves cassia bark compound extracted solution, pomegranate rind extracting solution, tea-polyphenol, epsilon-polylysine, Semen Vitis viniferae essence oil and tangerine oil mix, in 55 DEG C of water bath with thermostatic control 45min, be cooled to room temperature and obtain material b;
S3, in material b, add N,O-Diacetylmuramidase and bacillus natto mixes the pork preservative obtaining having excellent fresh keeping property.
Embodiment 5
A kind of pork preservative with excellent fresh keeping property that the present invention proposes, its raw material comprises by weight: cloves cassia bark compound extracted solution 35 parts, pomegranate rind extracting solution 8 parts, chitosan 4 parts, trehalose 4 parts, propolis 5 parts, N,O-Diacetylmuramidase 4 parts, tea-polyphenol 3 parts, epsilon-polylysine 3 parts, acetic acid 3 parts, Sodium.alpha.-hydroxypropionate 1.5 parts, Semen Vitis viniferae essence oil 2.5 parts, tangerine oil 1.5 parts, bacillus natto 3.5 parts.
Chinese medicine composite additive is prepared by following technique: by 5.8 portions of Elettaria cardamomum (L.) Matons, 3 parts of jamaica pepper, 3 parts of Thymus vulgariss, 3 portions of gingers, 3 portions of Persea cubeba, 3 parts of mustard seeds, 3 parts of Salvia japonica Thunb.s and 3 parts of dried orange peel co-grindings, mix and obtain material a, then material a is added in ethanolic soln, carry out frozen dried after stirring evenly and obtain material b; Then material b and water are mixed, decoct for 84 DEG C and boil 2.5h, be cooled to room temperature and obtain filtrate, then filtrate is carried out concentrating under reduced pressure and obtain concentrated solution, then it is cooled to normal temperature by after concentrated solution 82 DEG C of dryings, then it is ground to the Chinese medicine composite additive of 25 order granular materials.
The preparation method of a kind of pork preservative with excellent fresh keeping property that the present invention proposes, comprises the steps:
S1, chitosan, acetic acid and Sodium.alpha.-hydroxypropionate are mixed, in 58 DEG C of waters bath with thermostatic control heating 8min, then add trehalose and propolis mixes, be cooled to room temperature and obtain material a;
S2, in material a, add cloves cassia bark compound extracted solution, pomegranate rind extracting solution, tea-polyphenol, epsilon-polylysine, Semen Vitis viniferae essence oil and tangerine oil mix, in 65 DEG C of water bath with thermostatic control 35min, be cooled to room temperature and obtain material b;
S3, in material b, add N,O-Diacetylmuramidase and bacillus natto mixes the pork preservative obtaining having excellent fresh keeping property.
The chopping board sterilized in cleaning by fresh pig longissimus dorsi muscle removes manadesma, sized by cutting evenly, the cube meat of quality (200g �� 10) g, then 6 cube meat are numbered, it is divided into a cube meat, No. two cube meat, No. three cube meat, No. four cube meat, No. five cube meat and No. six cube meat, the preservation agent obtained is dipped in leaching embodiment 1 on a cube meat surface, and the preservation agent obtained is dipped in leaching embodiment 2 on No. two cube meat surfaces, the preservation agent obtained is dipped in leaching embodiment 3 on No. three cube meat surfaces, and the preservation agent obtained is dipped in leaching embodiment 4 on No. four cube meat surfaces, the preservation agent obtained is dipped in leaching embodiment 5 on No. five cube meat surfaces, leaching distilled water (blank) is dipped on No. six cube meat surfaces, after leaving standstill 15min, correct amount, load vacuum packaging in sterile bag, put into (4 �� 1) DEG C freezer refrigeration, for subsequent use, the mensuration of meat surface bacteria number is carried out after 2 weeks, total plate count measures and measures according to GB/T4789.2-2008 microbiological test of food hygiene-total number of bacterial colony, beef extract-peptone nutrient agar-flat board is adopted to pour into counting process, judgement criteria: green meat < 4, secondary fresh meat 4-6, rotten meat > 7, measured data are as shown in table 1.
The above; it is only the present invention's preferably embodiment; but protection scope of the present invention is not limited thereto; any it is familiar with those skilled in the art in the technical scope that the present invention discloses; technical scheme and invention design thereof according to the present invention are equal to replacement or are changed, and all should be encompassed within protection scope of the present invention.
Claims (10)
1. one kind has the pork preservative of excellent fresh keeping property, it is characterized in that, its raw material comprises by weight: cloves cassia bark compound extracted solution 20-40 part, pomegranate rind extracting solution 5-15 part, chitosan 2-5 part, trehalose 3-6 part, propolis 2-6 part, N,O-Diacetylmuramidase 3-8 part, tea-polyphenol 1-4 part, epsilon-polylysine 2-5 part, acetic acid 1-4 part, Sodium.alpha.-hydroxypropionate 1-3 part, Semen Vitis viniferae essence oil 1-3 part, tangerine oil 1-3 part, bacillus natto 2-4 part;
The raw material of described Chinese medicine composite additive comprises by weight: Elettaria cardamomum (L.) Maton 5-6 part, jamaica pepper 2-8 part, Thymus vulgaris 1-4 part, ginger 2-6 part, Persea cubeba 1-4 part, mustard seed 2-6 part, Salvia japonica Thunb. 1-4 part, dried orange peel 2-6 part;
Described cloves cassia bark compound extracted solution is prepared by following technique: take Ground Cloves and Cortex cinnamomi japonici powder, join in 80-120ml distilled water, 70-90 DEG C of water bath with thermostatic control heating 7-9h, it is cooled to normal temperature, the process of cooling does not stop jolting, then turn/centrifugal the 10-30min of min in 2500-3000, get supernatant liquor, namely obtain the cloves cassia bark compound extracted solution containing effective constituent 5-8%.
2. the pork preservative with excellent fresh keeping property according to claim 1, it is characterised in that, in the preparation technology of described cloves cassia bark compound extracted solution, the weight ratio of Ground Cloves and Cortex cinnamomi japonici powder is 2-5:1-3.
3. the pork preservative with excellent fresh keeping property according to claim 1 and 2, it is characterized in that, described pomegranate rind extracting solution is prepared by following technique: cross 30-50 order sieve after being pulverized by pomegranate pericarp, take water as solvent, solid-liquid ratio 2-4:17, extract 1-3h in 60-80 DEG C, after filtration, obtain pomegranate rind extracting solution.
4. the pork preservative with excellent fresh keeping property according to the arbitrary item of claim 1-3, it is characterized in that, described Chinese medicine composite additive is prepared by following technique: by Elettaria cardamomum (L.) Maton, jamaica pepper, Thymus vulgaris, ginger, Persea cubeba, mustard seed, Salvia japonica Thunb. and dried orange peel co-grinding, mix and obtain material a, then material a is added in ethanolic soln, carry out frozen dried after stirring evenly and obtain material b; Then material b and water are mixed, decoct for 65-85 DEG C and boil 2-4h, be cooled to room temperature and obtain filtrate, then filtrate is carried out concentrating under reduced pressure and obtain concentrated solution, then it is cooled to normal temperature by after concentrated solution 65-85 DEG C of drying, then it is ground to the Chinese medicine composite additive of 20-40 order granular material.
5. the pork preservative with excellent fresh keeping property according to the arbitrary item of claim 1-4, it is characterized in that, the weight ratio of cloves cassia bark compound extracted solution, pomegranate rind extracting solution, chitosan, trehalose and propolis is 25-35:8-12:3-4:4-5:3-5.
6. the pork preservative with excellent fresh keeping property according to the arbitrary item of claim 1-5, it is characterized in that, the weight ratio of cloves cassia bark compound extracted solution, pomegranate rind extracting solution, Semen Vitis viniferae essence oil and tangerine oil is 25-35:8-12:1.5-2.5:1.5-2.5.
7. the pork preservative with excellent fresh keeping property according to the arbitrary item of claim 1-6, it is characterized in that, the weight ratio of cloves cassia bark compound extracted solution, N,O-Diacetylmuramidase, tea-polyphenol, epsilon-polylysine, acetic acid, Sodium.alpha.-hydroxypropionate and bacillus natto is 25-35:4-7:2-3:3-4:2-3:1.5-2.5:2.5-3.5.
8. the pork preservative with excellent fresh keeping property according to the arbitrary item of claim 1-7, it is characterized in that, its raw material comprises by weight: cloves cassia bark compound extracted solution 25-35 part, pomegranate rind extracting solution 8-12 part, chitosan 3-4 part, trehalose 4-5 part, propolis 3-5 part, N,O-Diacetylmuramidase 4-7 part, tea-polyphenol 2-3 part, epsilon-polylysine 3-4 part, acetic acid 2-3 part, Sodium.alpha.-hydroxypropionate 1.5-2.5 part, Semen Vitis viniferae essence oil 1.5-2.5 part, tangerine oil 1.5-2.5 part, bacillus natto 2.5-3.5 part.
9. the pork preservative with excellent fresh keeping property according to the arbitrary item of claim 1-8, it is characterized in that, its raw material comprises by weight: cloves cassia bark compound extracted solution 30 parts, pomegranate rind extracting solution 10 parts, chitosan 3.5 parts, trehalose 4.5 parts, propolis 4 parts, N,O-Diacetylmuramidase 5.5 parts, tea-polyphenol 2.5 parts, epsilon-polylysine 3.5 parts, acetic acid 2.5 parts, Sodium.alpha.-hydroxypropionate 2 parts, Semen Vitis viniferae essence oil 2 parts, tangerine oil 2 parts, bacillus natto 3 parts.
10. the preparation method of a pork preservative with excellent fresh keeping property according to the arbitrary item of claim 1-9, it is characterised in that, comprise the steps:
S1, chitosan, acetic acid and Sodium.alpha.-hydroxypropionate are mixed, in 50-60 DEG C of water bath with thermostatic control heating 5-15min, then add trehalose and propolis mixes, be cooled to room temperature and obtain material a;
S2, in material a, add cloves cassia bark compound extracted solution, pomegranate rind extracting solution, tea-polyphenol, epsilon-polylysine, Semen Vitis viniferae essence oil and tangerine oil mix, in 50-70 DEG C of water bath with thermostatic control 30-50min, be cooled to room temperature and obtain material b;
S3, in material b, add N,O-Diacetylmuramidase and bacillus natto mixes the pork preservative obtaining having excellent fresh keeping property.
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