CN105567021B - A kind of aqueous cold pigment multifunctional thermal-insulation exterior wall true stone paint and preparation method thereof - Google Patents

A kind of aqueous cold pigment multifunctional thermal-insulation exterior wall true stone paint and preparation method thereof Download PDF

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Publication number
CN105567021B
CN105567021B CN201510179195.5A CN201510179195A CN105567021B CN 105567021 B CN105567021 B CN 105567021B CN 201510179195 A CN201510179195 A CN 201510179195A CN 105567021 B CN105567021 B CN 105567021B
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cold pigment
stone paint
true stone
aqueous
defoamer
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CN105567021A (en
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刘立新
黄利勇
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Hunan Jinhai Technology Co Ltd
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Hunan Jinhai Technology Co Ltd
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Abstract

The invention discloses a kind of aqueous cold pigment multifunctional thermal-insulation exterior wall true stone paint and preparation method thereof, is formed by water, auxiliary agent, synthetic resin emulsion, color stuffing and natural colour sand mixed preparing.Preparation method is:Water, cellulose, defoamer, ethylene glycol, coalescents, multifunctional assistant are put into dispersion tank first;It is subsequently added into styrene-acrylic emulsion;Then cold pigment, hollow glass bead, ceramic hollow microballon, rutile titanium dioxide, superfine talcum powder, infrared emission ceramic powder are sequentially added;It is slow added into quartz sand;Bactericide, defoamer, thickener are eventually adding until stirring.The present invention assigns the true mineral varnish of water-based exterior wall to block three kinds of heat-insulated, reflective insulation, radiation heat insulation effect of heat insulation by adding the color stuffings such as cold pigment, hollow glass bead;By selecting aqueous synthetic-resin emulsion and aqueous paint additive, so as to aqueous, environmental protective;Using different fineness, different colours natural quartz coloured silk sand as aggregate, make that the natural-like stone, marble, granite effect of true mineral varnish are true to nature, and paint film is rich in color, outward appearance is magnificent.

Description

A kind of aqueous cold pigment multifunctional thermal-insulation exterior wall true stone paint and preparation method thereof
Technical field
The present invention relates to technical field of coatings, in particulars relate to exterior wall true stone paint field, especially a kind of aqueous cold pigment Multifunctional thermal-insulation exterior wall true stone paint and preparation method thereof.
Background technology
True mineral varnish is that a kind of decorative effect exactly likes marble, granitic building coating.Mainly using synthetic resin emulsion, Auxiliary agent, the natural stone-powder of a variety of colors are formulated.Building after true mineral varnish finishing, has natural real natural colour, Give graceful, harmonious, serious aesthetic feeling, be suitable for the indoor and outdoor decoration of all kinds of buildings.
Exterior wall true stone paint is reaching almost identical decoration grain effect compared with granite lithotome finishing material In the case of, have that cost is low, safe, health environment-friendly, that practicality is wide, decorative effect is abundant, construction technology is simpler etc. is excellent Point.Therefore exterior wall true stone paint coating just gradually replaces exterior wall lithotome facing, turns into the main flow of external wall decorative material.
Building energy consumption has accounted for more than the 30% of mankind's total energy consumption, if these energy resource consumptions can pass through one Fixed measure is improved and saved, then effective sustainable development using with society for realizing resource will play important Effect.
With the development of economic society and the enhancing of people's energy conservation and environmental awareness, countries in the world are at energy-saving aspect Policy, regulation are more and more stricter, and consumption market is also constantly increasing the demand of environmental protection and energy saving product.Exterior wall true stone paint is excellent because of its Good performance and graceful outward appearance will be widely used in a large amount of buildings, assign exterior wall true stone paint with multi-functional heat-insulated Effect, effectively the outer heat transfer of isolating chamber and indoor energy loss can be reduced, substantially reduced caused by the operation such as air-conditioning, heating Energy consumption and the pollution to environment.
Patent CN104109439A discloses a kind of true mineral varnish of insulation and preparation method thereof.The true mineral varnish of the insulation uses silicon third The combination of emulsion, natural colour sand and hollow glass microbead three, there is excellent weatherability, resistance to station dirt, temperature variation resistant and resistance to old Change equistability and heat-insulating property and color variation.
Patent CN104356810A discloses a kind of true mineral varnish of reflection heat-insulating type.The true mineral varnish is by water, dispersant, defoaming It is agent, thickener, light ethyl cellulose, coalescents, antifreezing agent, hollow glass micropearl, aqueous polymer emulsion, bactericide, anti- Heat-insulated sand burning composition is penetrated, it is in bright gay color while there is heat preservation and insulation, it can arbitrarily allocate color, and color stability It is good.
The insulating moulding coating of Vehicles Collected from Market can be three classes according to its principle, and one kind is heat resistance type insulating moulding coating, and one kind is anti- Emitting insulating moulding coating, also one kind are Radiation Heat-insulated Paints, and this three classes insulating moulding coating has its respective advantage and feature.Such as Fruit can apply three kinds of mechanism of heat insulation in a kind of coating, realize multi-functional collaboration heat-blocking action, will greatly improve insulating moulding coating Effect of heat insulation.At present, also without a kind of multifunctional thermal-insulation exterior wall true stone paint for realizing three kinds of mechanism of heat insulation synergies.
The realization of insulation effect of true mineral varnish is simply by blocking heat-insulated, reflective insulation wherein in above-mentioned 2 patents A kind of mode, do not design and block heat-insulated, reflective insulation, the synergy of three kinds of insulating mechanisms of radiation heat insulation, can not realize Effectively insulating.
The content of the invention
For above-mentioned skill problem, the present invention provides a kind of aqueous cold pigment multifunctional thermal-insulation exterior wall true stone paint and its preparation side Method, there is multifunctional efficient effect of heat insulation, while have the following advantage of the true mineral varnish of water-based exterior wall concurrently:Odorlessness, aqueous, environmental protective, imitate True stone effect is good, antiacid alkali, weatherability are strong, performance of keeping a public place clean is good, long lifespan, construction are simple and direct.
The technical solution adopted in the present invention is:A kind of aqueous cold pigment multifunctional thermal-insulation exterior wall true stone paint, by water, is helped Agent, synthetic resin emulsion, color stuffing and natural colour sand mixed preparing form, and each component mass fraction is as follows:
Water 250 ~ 350
Cellulose 5 ~ 10
Defoamer 5 ~ 10
Ethylene glycol 20 ~ 30
Coalescents 25 ~ 35
Multifunctional assistant 2 ~ 4
Styrene-acrylic emulsion 300 ~ 400
Cold pigment 30 ~ 50
Hollow glass bead 80 ~ 100
Ceramic hollow microballon 90 ~ 120
Rutile titanium dioxide 30 ~ 40
Superfine talcum powder 40 ~ 50
Infrared emission ceramic powder 25 ~ 40
40-80 mesh quartz sand 450 ~ 500
80-120 mesh quartz sand 150 ~ 200
20-40 mesh quartz sand 100 ~ 120
Bactericide 6 ~ 9
Defoamer 5 ~ 10
Thickener 5 ~ 10.
The cellulose that the present invention uses is a kind of non-ionic water-soluble cellulose ether.
The defoamer that the present invention uses is a kind of hydrophobic gas-phase silica of mineral oil and metal soap nonionic defoamer.
The coalescents that the present invention uses are lauryl alcohol ester coalescents.
The multifunctional assistant that the present invention uses is AMP-95.
The cold pigment that the present invention uses is spinel-type composite inorganic pigment.
For the particle diameter for the hollow glass micropearl that the present invention uses for 30 ~ 120um, ceramic hollow microballon detailed catalogue is 150 ~ 300 mesh, Superfine talcum powder detailed catalogue is 1250 mesh, the mesh of infrared emission ceramic powder fineness 325.
The thickener that the present invention uses is ethoxy thickener.
Preparation method is:Water, cellulose, defoamer, ethylene glycol, coalescents, multifunctional assistant are put into first scattered It is scattered 30 minutes with 1000rpm rotating speed in tank, cellulose dissolution situation is checked, confirms transparent no bulk particle;It is subsequently added into Styrene-acrylic emulsion, it is scattered 15 minutes with 2000rpm rotating speed;Then slowly, in batches sequentially add cold pigment, hollow glass bead, Ceramic hollow microballon, rutile titanium dioxide, superfine talcum powder, infrared emission ceramic powder, are disperseed with 4000rpm rotating speed 30 minutes;40 ~ 80 mesh quartz sands, 80 ~ 120 mesh quartz sands, 20 ~ 40 mesh quartz sands are slow added into, are stirred with 5000rpm rotating speeds It is scattered 30 minutes;Bactericide, defoamer, thickener are eventually adding, it is scattered 15 minutes with 3000rpm rotating speed, until stirring is equal It is even.
A kind of aqueous cold pigment multifunctional thermal-insulation exterior wall true stone paint provided by the invention, it is empty by adding cold pigment, glass Heart microballon, ceramic hollow microballon, rutile titanium dioxide, superfine talcum powder, infrared emission ceramic powder assign water-based exterior wall True mineral varnish is to block the multifunctional efficient effect of heat insulation that three kinds of heat-insulated, reflective insulation, radiation heat insulation insulating mechanisms are had both.
The invention employs hollow glass bead, ceramic hollow microballon, superfine talcum powder, infrared emission ceramic powder proportioning Complex function filler systems, and microballon detailed catalogue in 150 mesh between 300 mesh, such system both makes full use of titanium dioxide Strong covering power, be staggered using size microballon and titanium dioxide granule, talcum particles, realize the seamless of film, improve Thermal resistance, while realize radiation heat insulation function using the infrared emission effect of infrared emission ceramic powder.
Wherein, " cold pigment " is dedicated as infrared external reflection.Why this kind of pigment is referred to as " cold pigment ", is exactly because of it There is remarkable efficacy in solar energy effect of heat insulation, have the characteristics that:1. there is spinel structure, have high covering power and The reflectivity of sunshine;2. average grain diameter is small, oil absorption is low, and swell value is low etc.;3. there is excellent chemical resistance, weatherability, Fastness to light, heat endurance, wear-resisting and non-migrating.By the compound addition of the filler of different-grain diameter to lift the reflection efficiency of coating, Filler can be made to form more fine and close reflecting layer in the coating.
By selecting aqueous synthetic-resin emulsion and aqueous paint additive, the cold pigment multifunctional thermal-insulation exterior wall prepared is true Mineral varnish aqueous, environmental protective;Using different fineness, different colours natural quartz coloured silk sand as aggregate, make true stone by reasonably matching The natural-like stone of paint, marble, granite effect are true to nature, and paint film is rich in color, outward appearance is magnificent.
Embodiment
It is further described below according to embodiment
Embodiment 1:
A kind of aqueous cold pigment multifunctional thermal-insulation exterior wall true stone paint, each component mass fraction are as follows:
Constituent mass number
Water 250
Cellulose 10
Defoamer 5
Ethylene glycol 30
Coalescents 25
Multifunctional assistant 4
Styrene-acrylic emulsion 300
Cold pigment 30
Hollow glass bead 80
Ceramic hollow microballon 90
Rutile titanium dioxide 30
Superfine talcum powder 40
Infrared emission ceramic powder 25
40 ~ 80 mesh quartz sands 450
80 ~ 120 mesh quartz sands 150
20 ~ 40 mesh quartz sands 100
Bactericide 6
Defoamer 5
Thickener 5.
Embodiment 2:
A kind of aqueous cold pigment multifunctional thermal-insulation exterior wall true stone paint, each component mass fraction are as follows:
Constituent mass number
Water 300
Cellulose 8
Defoamer 8
Ethylene glycol 25
Coalescents 30
Multifunctional assistant 3
Styrene-acrylic emulsion 350
Cold pigment 40
Hollow glass bead 90
Ceramic hollow microballon 100
Rutile titanium dioxide 35
Superfine talcum powder 45
Infrared emission ceramic powder 30
40 ~ 80 mesh quartz sands 460
80 ~ 120 mesh quartz sands 170
20 ~ 40 mesh quartz sands 110
Bactericide 8
Defoamer 8
Thickener 8.
Embodiment 3:
A kind of aqueous cold pigment multifunctional thermal-insulation exterior wall true stone paint, each component mass fraction are as follows:
Constituent mass number
Water 350
Cellulose 5
Defoamer 10
Ethylene glycol 20
Coalescents 35
Multifunctional assistant 2
Styrene-acrylic emulsion 400
Cold pigment 50
Hollow glass bead 100
Ceramic hollow microballon 120
Rutile titanium dioxide 40
Superfine talcum powder 50
Infrared emission ceramic powder 40
40 ~ 80 mesh quartz sands 500
80 ~ 120 mesh quartz sands 200
20 ~ 40 mesh quartz sands 120
Bactericide 9
Defoamer 10
Thickener 10.
The preparation method is that:According to each component mass parts numerical value in the various embodiments described above, respective quality is weighed Component, water, cellulose, defoamer, ethylene glycol, coalescents, multifunctional assistant are put into dispersion tank first, with 1000rpm Scattered 30 minutes of rotating speed, check cellulose dissolution situation, confirm transparent no bulk particle;Styrene-acrylic emulsion is subsequently added into, with 2000rpm rotating speed is scattered 15 minutes;Then slowly, sequentially add hollow glass bead, ceramic hollow microballon, rutile in batches Type titanium dioxide, superfine talcum powder, nanometer infrared emission ceramic powder, cold pigment, it is scattered 30 minutes with 4000rpm rotating speed; 40-80 mesh quartz sand, 80-120 mesh quartz sand, 20-40 mesh quartz sands are slow added into, 30 are dispersed with stirring with 5000rpm rotating speeds Minute;Bactericide, defoamer, thickener are eventually adding, it is scattered 15 minutes with 3000rpm rotating speed, until stirring.
Aqueous cold pigment multifunctional thermal-insulation exterior wall true stone paint the performance test results prepared by above-described embodiment are as follows:
Embodiment of the present invention is only the description carried out to the preferred embodiment of the present invention, not to the present invention Spirit and scope are defined, and on the premise of design philosophy of the present invention is not departed from, engineers and technicians are to this hair in this area The all variations and modifications that bright technical scheme is made, protection scope of the present invention, the claimed skill of the present invention all should be fallen into Art content, all record in detail in the claims.

Claims (9)

1. a kind of aqueous cold pigment multifunctional thermal-insulation exterior wall true stone paint, it is characterised in that by mass fraction, be made up of following component:
Constituent mass number
Water 250 ~ 350
Cellulose 5 ~ 10
Defoamer 5 ~ 10
Ethylene glycol 20 ~ 30
Coalescents 25 ~ 35
Multifunctional assistant 2 ~ 4
Styrene-acrylic emulsion 300 ~ 400
Cold pigment 30 ~ 50
Hollow glass bead 80 ~ 100
Ceramic hollow microballon 90 ~ 120
Rutile titanium dioxide 30 ~ 40
Superfine talcum powder 40 ~ 50
Infrared emission ceramic powder 25 ~ 40
40 ~ 80 mesh quartz sands 450 ~ 500
80 ~ 120 mesh quartz sands 150 ~ 200
20 ~ 40 mesh quartz sands 100 ~ 120
Bactericide 6 ~ 9
Defoamer 5 ~ 10
Thickener 5 ~ 10.
2. aqueous cold pigment multifunctional thermal-insulation exterior wall true stone paint according to claim 1, it is characterised in that:The fiber Element is a kind of non-ionic water-soluble cellulose ether.
3. aqueous cold pigment multifunctional thermal-insulation exterior wall true stone paint according to claim 1, it is characterised in that:The defoaming Agent is a kind of hydrophobic gas-phase silica of mineral oil and metal soap nonionic defoamer.
4. aqueous cold pigment multifunctional thermal-insulation exterior wall true stone paint according to claim 1, it is characterised in that:The film forming Auxiliary agent is lauryl alcohol ester coalescents.
5. aqueous cold pigment multifunctional thermal-insulation exterior wall true stone paint according to claim 1, it is characterised in that:More work( Energy auxiliary agent is AMP-95.
6. aqueous cold pigment multifunctional thermal-insulation exterior wall true stone paint according to claim 1, it is characterised in that:The cold pigment For spinel-type composite inorganic pigment.
7. aqueous cold pigment multifunctional thermal-insulation exterior wall true stone paint according to claim 1, it is characterised in that:The glass The particle diameter of cenosphere is 30 ~ 120um, and ceramic hollow microballon detailed catalogue is 150 ~ 300 mesh, and superfine talcum powder detailed catalogue is 1250 mesh, The mesh of infrared emission ceramic powder fineness 325.
8. aqueous cold pigment multifunctional thermal-insulation exterior wall true stone paint according to claim 1, it is characterised in that:The thickening Agent is ethoxy thickener.
A kind of 9. preparation method of the aqueous cold pigment multifunctional thermal-insulation exterior wall true stone paint described in claim 1, it is characterised in that: Water, cellulose, defoamer, ethylene glycol, coalescents, multifunctional assistant are put into dispersion tank first, with 1000rpm rotating speed It is scattered 30 minutes, cellulose dissolution situation is checked, confirms transparent no bulk particle;Styrene-acrylic emulsion is subsequently added into, with 2000rpm's Rotating speed is scattered 15 minutes;Then slowly, sequentially add hollow glass bead, ceramic hollow microballon, rutile-type titanium dioxide in batches Titanium, superfine talcum powder, infrared emission ceramic powder, cold pigment, it is scattered 30 minutes with 4000rpm rotating speed;It is slow added into 40- 80 mesh quartz sands, 80-120 mesh quartz sand, 20-40 mesh quartz sands, are dispersed with stirring 30 minutes with 5000rpm rotating speeds;It is eventually adding Bactericide, defoamer, thickener, it is scattered 15 minutes with 3000rpm rotating speed, until stirring.
CN201510179195.5A 2015-04-16 2015-04-16 A kind of aqueous cold pigment multifunctional thermal-insulation exterior wall true stone paint and preparation method thereof Active CN105567021B (en)

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Denomination of invention: Water-based cold-pigment multifunctional heat-insulating true stone paint for exterior wall and preparation method thereof

Effective date of registration: 20180611

Granted publication date: 20171226

Pledgee: Bank of Changsha Limited by Share Ltd science and Technology Branch

Pledgor: HUNAN JINHAI TECHNOLOGY CO., LTD.

Registration number: 2018430000036