CN105441189A - Method for purifying magnolia flower essential oil - Google Patents
Method for purifying magnolia flower essential oil Download PDFInfo
- Publication number
- CN105441189A CN105441189A CN201510877016.5A CN201510877016A CN105441189A CN 105441189 A CN105441189 A CN 105441189A CN 201510877016 A CN201510877016 A CN 201510877016A CN 105441189 A CN105441189 A CN 105441189A
- Authority
- CN
- China
- Prior art keywords
- essential oil
- yulan magnolia
- purification
- ultrasonic
- oil according
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
Abstract
The invention discloses a method for purifying magnolia flower essential oil. The method comprises the steps that magnolia flower washing, ultrasonic treatment, extracting, rectification and the like are carried out, and the magnolia flower essential oil with the purity higher than 99% is obtained. The high-purity safe magnolia flower essential oil is extracted from natural materials, and can be applied to the fields of cosmetics, medicine and the like, and good market prospects are achieved. The method is easy and convenient to operate, low in manufacturing cost and suitable for large-scale production.
Description
Technical field
The invention belongs to technical field of fine, relate to a kind of method of purification of Yulan Magnolia essential oil.
Background technology
Plants essential oil is the distinctive aromatoising substance of extraction plant, is taken from herbal flower, leaf, root, bark, fruit, seed, resin etc. and extract with distillation, squeezing mode.Because essential oil-fumigation volatility is high, and molecule is little, be easy to be absorbed by the body, and energy rapid permeability people intracorporeal organ, unnecessary composition is excreted, whole process only needs several minutes, and the fragrance of plant itself, the also secretion of direct Stimulation of The Brain pendant, ferment and hormone secretion etc., function in balanced body, plays the effect of beauty and skin care.But from the natural matters such as fresh flower, extract that plants essential oil cost is high, purity is low traditionally, be difficult to meet the need of market.
Summary of the invention
The object of this invention is to provide a kind of method of purification of Yulan Magnolia essential oil.
In order to realize object of the present invention, the present invention is by following scheme implementation:
A method of purification for Yulan Magnolia essential oil, comprises the following steps:
(1) clean: choose fresh Yulan Magnolia, clean with clean water, pulverize;
(2) ultrasonic: the 30-70% alcoholic solution adding 50-100 times of Yulan Magnolia weight in crushed material, ultrasonic 30-90 minute;
(3) extract: the solution after ultrasonic is added separating funnel, adds organic extractant simultaneously, vibration mixing 3-10 minute, leaves standstill and isolates organic phase after 5-15 minute;
(4) rectifying: put into precise distillation tower by extracting the organic phase that obtains, the impurity in vacuum precision distillation removing organic phase, obtain purity higher than 99% essential oil.
Preferably, described alcoholic solution is any one in ethanol, Virahol, butanols.
Preferably, described its frequency ultrasonic is 50-200KHz.
Preferably, described its power ultrasonic is 500-1000W.
Preferably, the volume of described organic extractant be ultrasonic after liquor capacity 1-3 doubly.
Preferably, described organic extractant is any one in ethyl acetate, sherwood oil, methylene dichloride, normal hexane, normal heptane.
Preferably, described precise distillation tower is filled with high efficiency separation filler.
Preferably, described high efficiency separation filler is any one in metal sheet corrugated regular filler, wire cloth structured packing, grid packing, Impulse packing.
Preferably, described vacuum precision distillation is continuous still battery.
Advantage of the present invention is:
(1) the essential oil purity extracted of the present invention is higher than 99%, best in quality;
(2) the present invention prepares highly purified essential oil is Nantural non-toxic product, and can be applied to makeup, medicine and other fields, market outlook are good;
(3) the present invention's solution reagent used can reclaim and reuse, and does not produce discarded waste liquid;
(4) easy and simple to handle, the low manufacturing cost of the present invention, is applicable to large-scale production.
Embodiment
Below in conjunction with specific embodiment, technical scheme of the present invention is described in further detail, but embodiments of the present invention are not limited thereto.
embodiment 1
A method of purification for Yulan Magnolia essential oil, comprises the following steps:
(1) clean: choose fresh Yulan Magnolia, clean with clean water, pulverize;
(2) ultrasonic: 60% aqueous isopropanol adding 80 times of Yulan Magnolia weight in crushed material, under 100KHz, 800W ultrasonic 60 minutes;
(3) extract: the solution after ultrasonic is added separating funnel, add simultaneously ultrasonic after the ethyl acetate of liquor capacity 3 times, vibration mixing 5 minutes, leaves standstill and isolates organic phase after 5 minutes; (4) rectifying: put into the precise distillation tower being filled with Impulse packing by extracting the organic phase that obtains, the impurity in vacuum continuous precision distillation removing organic phase, obtain purity higher than 99% essential oil.
embodiment 2
A method of purification for Yulan Magnolia essential oil, comprises the following steps:
(1) clean: choose fresh Yulan Magnolia, clean with clean water, pulverize;
(2) ultrasonic: 30% ethanolic soln adding 50 times of Yulan Magnolia weight in crushed material, under 50KHz, 1000W ultrasonic 90 minutes;
(3) extract: the solution after ultrasonic is added separating funnel, add simultaneously ultrasonic after the sherwood oil of liquor capacity 1 times, vibration mixing 10 minutes, leaves standstill and isolates organic phase after 15 minutes;
(4) rectifying: put into the precise distillation tower being filled with metal sheet corrugated regular filler by extracting the organic phase that obtains, the impurity in vacuum continuous precision distillation removing organic phase, obtain purity higher than 99% essential oil.
embodiment 3
A method of purification for Yulan Magnolia essential oil, comprises the following steps:
(1) clean: choose fresh Yulan Magnolia, clean with clean water, pulverize;
(2) ultrasonic: 70% butanol solution adding 100 times of Yulan Magnolia weight in crushed material, under 200KHz, 500W ultrasonic 30 minutes;
(3) extract: the solution after ultrasonic is added separating funnel, add simultaneously ultrasonic after the methylene dichloride of liquor capacity 2 times, vibration mixing 8 minutes, leaves standstill and isolates organic phase after 10 minutes;
(4) rectifying: put into the precise distillation tower being filled with wire cloth structured packing by extracting the organic phase that obtains, the impurity in vacuum continuous precision distillation removing organic phase, obtain purity higher than 99% essential oil.
embodiment 4
A method of purification for Yulan Magnolia essential oil, comprises the following steps:
(1) clean: choose fresh Yulan Magnolia, clean with clean water, pulverize;
(2) ultrasonic: 50% butanol solution adding 60 times of Yulan Magnolia weight in crushed material, under 120KHz, 600W ultrasonic 50 minutes;
(3) extract: the solution after ultrasonic is added separating funnel, add simultaneously ultrasonic after the normal hexane of liquor capacity 3 times, vibration mixing 3 minutes, leaves standstill and isolates organic phase after 8 minutes;
(4) rectifying: put into the precise distillation tower being filled with grid packing by extracting the organic phase that obtains, the impurity in vacuum continuous precision distillation removing organic phase, obtain purity higher than 99% essential oil.
embodiment 5
A method of purification for Yulan Magnolia essential oil, comprises the following steps:
(1) clean: choose fresh Yulan Magnolia, clean with clean water, pulverize;
(2) ultrasonic: 40% ethanolic soln adding 90 times of Yulan Magnolia weight in crushed material, under 150KHz, 800W ultrasonic 80 minutes;
(3) extract: the solution after ultrasonic is added separating funnel, add simultaneously ultrasonic after the normal heptane of liquor capacity 2 times, vibration mixing 6 minutes, leaves standstill and isolates organic phase after 6 minutes;
(4) rectifying: put into the precise distillation tower being filled with metal sheet corrugated regular filler by extracting the organic phase that obtains, the impurity in vacuum continuous precision distillation removing organic phase, obtain purity higher than 99% essential oil.
Claims (9)
1. a method of purification for Yulan Magnolia essential oil, is characterized in that, comprises the following steps:
(1) clean: choose fresh Yulan Magnolia, clean with clean water, pulverize;
(2) ultrasonic: the 30-70% alcoholic solution adding 50-100 times of Yulan Magnolia weight in crushed material, ultrasonic 30-90 minute;
(3) extract: the solution after ultrasonic is added separating funnel, adds organic extractant simultaneously, vibration mixing 3-10 minute, leaves standstill and isolates organic phase after 5-15 minute;
(4) rectifying: put into precise distillation tower by extracting the organic phase that obtains, the impurity in vacuum precision distillation removing organic phase, obtain purity higher than 99% essential oil.
2. the method for purification of Yulan Magnolia essential oil according to claim 1, is characterized in that, described alcoholic solution is any one in ethanol, Virahol, butanols.
3. the method for purification of Yulan Magnolia essential oil according to claim 1, is characterized in that, described its frequency ultrasonic is 50-200KHz.
4. the method for purification of Yulan Magnolia essential oil according to claim 1, is characterized in that, described its power ultrasonic is 500-1000W.
5. the method for purification of Yulan Magnolia essential oil according to claim 1, is characterized in that, the volume of described organic extractant be ultrasonic after liquor capacity 1-3 doubly.
6. the method for purification of Yulan Magnolia essential oil according to claim 5, is characterized in that, described organic extractant is any one in ethyl acetate, sherwood oil, methylene dichloride, normal hexane, normal heptane.
7. the method for purification of Yulan Magnolia essential oil according to claim 1, is characterized in that, described precise distillation tower is filled with high efficiency separation filler.
8. the method for purification of Yulan Magnolia essential oil according to claim 7, is characterized in that, described high efficiency separation filler is any one in metal sheet corrugated regular filler, wire cloth structured packing, grid packing, Impulse packing.
9. the method for purification of Yulan Magnolia essential oil according to claim 7, is characterized in that, described vacuum precision distillation is continuous still battery.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510877016.5A CN105441189A (en) | 2015-12-03 | 2015-12-03 | Method for purifying magnolia flower essential oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510877016.5A CN105441189A (en) | 2015-12-03 | 2015-12-03 | Method for purifying magnolia flower essential oil |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105441189A true CN105441189A (en) | 2016-03-30 |
Family
ID=55551838
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510877016.5A Pending CN105441189A (en) | 2015-12-03 | 2015-12-03 | Method for purifying magnolia flower essential oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105441189A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106318633A (en) * | 2016-08-26 | 2017-01-11 | 广西灏源盛世生物科技有限公司 | Extracting method of cananga odorata essential oil |
| CN107189858A (en) * | 2017-04-27 | 2017-09-22 | 陶发助 | A kind of preparation method of yulan magnolia hydrosol |
| CN115044413A (en) * | 2022-07-01 | 2022-09-13 | 扬州芬曼生物科技有限公司 | Natural plant essential oil extraction method |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102018263A (en) * | 2009-09-11 | 2011-04-20 | 天津科技大学 | Purely natural essential oil composition for keeping fresh and preparation method and using method thereof |
| CN103555425A (en) * | 2013-11-14 | 2014-02-05 | 浙江安赛生物科技有限公司 | Method for preparing jasmine concrete by using high-frequency ultrasonic cavitation technology |
| CN104120037A (en) * | 2014-08-08 | 2014-10-29 | 广西壮族自治区林业科学研究院 | Extracting method for jasmine flower essential oil |
| CN104164302A (en) * | 2014-09-04 | 2014-11-26 | 南京标科生物科技有限公司 | Extraction method of gardenia jasminoides volatile oil |
| CN104178354A (en) * | 2014-09-04 | 2014-12-03 | 南京标科生物科技有限公司 | Method for extracting stigma croci essential oil |
-
2015
- 2015-12-03 CN CN201510877016.5A patent/CN105441189A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102018263A (en) * | 2009-09-11 | 2011-04-20 | 天津科技大学 | Purely natural essential oil composition for keeping fresh and preparation method and using method thereof |
| CN103555425A (en) * | 2013-11-14 | 2014-02-05 | 浙江安赛生物科技有限公司 | Method for preparing jasmine concrete by using high-frequency ultrasonic cavitation technology |
| CN104120037A (en) * | 2014-08-08 | 2014-10-29 | 广西壮族自治区林业科学研究院 | Extracting method for jasmine flower essential oil |
| CN104164302A (en) * | 2014-09-04 | 2014-11-26 | 南京标科生物科技有限公司 | Extraction method of gardenia jasminoides volatile oil |
| CN104178354A (en) * | 2014-09-04 | 2014-12-03 | 南京标科生物科技有限公司 | Method for extracting stigma croci essential oil |
Non-Patent Citations (1)
| Title |
|---|
| 詹益兴: "《绿色精细化工—天然产品制造法（第2集）》", 31 July 2006 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106318633A (en) * | 2016-08-26 | 2017-01-11 | 广西灏源盛世生物科技有限公司 | Extracting method of cananga odorata essential oil |
| CN107189858A (en) * | 2017-04-27 | 2017-09-22 | 陶发助 | A kind of preparation method of yulan magnolia hydrosol |
| CN115044413A (en) * | 2022-07-01 | 2022-09-13 | 扬州芬曼生物科技有限公司 | Natural plant essential oil extraction method |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105441193A (en) | Method for purifying sweet osmanthus essential oil | |
| CN105441194A (en) | Purification method for jasmine essential oil | |
| CN105441191A (en) | Purification method for lavender essential oil | |
| CN102807921A (en) | Method for preparing cypress essential oil by combining water vapor distillation with supercritical CO2 extraction | |
| CN101601639A (en) | A kind of assembly of Paeonia suffruticosa moisturizing essential oil and manufacture method | |
| CN105441189A (en) | Method for purifying magnolia flower essential oil | |
| CN105273843A (en) | Extraction method of wood essential oil | |
| CN105567428A (en) | Method for purifying flos caryophylli essential oil | |
| CN105542961A (en) | Purifying method of gardenia flower essential oil | |
| CN102731587A (en) | Method for extracting salicin from white willow bark | |
| CN106543245A (en) | A kind of method that arctiin is isolated and purified from burdock | |
| CN104558066A (en) | Extraction method for arbutin | |
| CN105441188A (en) | Method for purifying tulip essential oil | |
| CN105441195A (en) | Purifying method for rose essential oil | |
| CN105441192A (en) | Purification method for greenish lily flower essential oil | |
| CN105482896A (en) | Purification method of violet essential oil | |
| CN104193711A (en) | New method for extracting apigenin from celery | |
| CN104547286A (en) | Method for preparing Chinese Eaglewood leaf extract | |
| CN103371956A (en) | Novel honey moistening liquid shampoo | |
| CN109609275A (en) | A kind of extraction process of Rosemary Oil | |
| CN104224864A (en) | Method for extracting general flavone from myrica rubra leaves | |
| CN107569622A (en) | A kind of antipruritic Anti-hair loss hair lotion | |
| CN107751863A (en) | A kind of aloes lozenge and preparation method thereof | |
| CN111973533B (en) | Plant fermentation product and moisturizing mask prepared from same | |
| KR101281060B1 (en) | Composition for accelerating hair groth and the manufacturing method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20160330 |
|
| WD01 | Invention patent application deemed withdrawn after publication |