CN105434311A - Active egg white essence facial mask and preparation method thereof - Google Patents
Active egg white essence facial mask and preparation method thereof Download PDFInfo
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- CN105434311A CN105434311A CN201510999558.XA CN201510999558A CN105434311A CN 105434311 A CN105434311 A CN 105434311A CN 201510999558 A CN201510999558 A CN 201510999558A CN 105434311 A CN105434311 A CN 105434311A
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- Prior art keywords
- gallus domesticus
- ovum gallus
- domesticus album
- active
- elite
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- 102000002322 Egg Proteins Human genes 0.000 title claims abstract description 93
- 108010000912 Egg Proteins Proteins 0.000 title claims abstract description 93
- 230000001815 facial effect Effects 0.000 title claims abstract description 33
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- QCVGEOXPDFCNHA-UHFFFAOYSA-N 5,5-dimethyl-2,4-dioxo-1,3-oxazolidine-3-carboxamide Chemical compound CC1(C)OC(=O)N(C(N)=O)C1=O QCVGEOXPDFCNHA-UHFFFAOYSA-N 0.000 title abstract 7
- 235000014103 egg white Nutrition 0.000 title abstract 7
- 210000000969 egg white Anatomy 0.000 title abstract 7
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 40
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 33
- 239000000463 material Substances 0.000 claims abstract description 29
- 239000007788 liquid Substances 0.000 claims abstract description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000002202 Polyethylene glycol Substances 0.000 claims abstract description 12
- 229920001223 polyethylene glycol Polymers 0.000 claims abstract description 12
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims abstract description 11
- 229960005323 phenoxyethanol Drugs 0.000 claims abstract description 11
- 239000001509 sodium citrate Substances 0.000 claims abstract description 11
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 claims abstract description 11
- SZXQTJUDPRGNJN-UHFFFAOYSA-N dipropylene glycol Chemical compound OCCCOCCCO SZXQTJUDPRGNJN-UHFFFAOYSA-N 0.000 claims abstract description 8
- 210000004681 ovum Anatomy 0.000 claims description 86
- 241000287828 Gallus gallus Species 0.000 claims description 84
- 239000000758 substrate Substances 0.000 claims description 28
- 230000000975 bioactive effect Effects 0.000 claims description 21
- 239000004615 ingredient Substances 0.000 claims description 20
- 238000000034 method Methods 0.000 claims description 19
- VGEREEWJJVICBM-UHFFFAOYSA-N phloretin Chemical compound C1=CC(O)=CC=C1CCC(=O)C1=C(O)C=C(O)C=C1O VGEREEWJJVICBM-UHFFFAOYSA-N 0.000 claims description 17
- BJRNKVDFDLYUGJ-RMPHRYRLSA-N hydroquinone O-beta-D-glucopyranoside Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC1=CC=C(O)C=C1 BJRNKVDFDLYUGJ-RMPHRYRLSA-N 0.000 claims description 15
- 239000004745 nonwoven fabric Substances 0.000 claims description 15
- 230000002087 whitening effect Effects 0.000 claims description 14
- 239000000835 fiber Substances 0.000 claims description 13
- 102000004169 proteins and genes Human genes 0.000 claims description 11
- 108090000623 proteins and genes Proteins 0.000 claims description 11
- 239000012535 impurity Substances 0.000 claims description 10
- 229920002101 Chitin Polymers 0.000 claims description 9
- 239000003795 chemical substances by application Substances 0.000 claims description 9
- 239000011347 resin Substances 0.000 claims description 9
- 229920005989 resin Polymers 0.000 claims description 9
- ZWTDXYUDJYDHJR-UHFFFAOYSA-N (E)-1-(2,4-dihydroxyphenyl)-3-(2,4-dihydroxyphenyl)-2-propen-1-one Natural products OC1=CC(O)=CC=C1C=CC(=O)C1=CC=C(O)C=C1O ZWTDXYUDJYDHJR-UHFFFAOYSA-N 0.000 claims description 8
- YQHMWTPYORBCMF-UHFFFAOYSA-N Naringenin chalcone Natural products C1=CC(O)=CC=C1C=CC(=O)C1=C(O)C=C(O)C=C1O YQHMWTPYORBCMF-UHFFFAOYSA-N 0.000 claims description 8
- 238000003756 stirring Methods 0.000 claims description 8
- QGZKDVFQNNGYKY-UHFFFAOYSA-O ammonium group Chemical class [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 7
- 229960000271 arbutin Drugs 0.000 claims description 7
- 239000000284 extract Substances 0.000 claims description 7
- 239000012528 membrane Substances 0.000 claims description 7
- BJRNKVDFDLYUGJ-UHFFFAOYSA-N p-hydroxyphenyl beta-D-alloside Natural products OC1C(O)C(O)C(CO)OC1OC1=CC=C(O)C=C1 BJRNKVDFDLYUGJ-UHFFFAOYSA-N 0.000 claims description 7
- KIUKXJAPPMFGSW-DNGZLQJQSA-N (2S,3S,4S,5R,6R)-6-[(2S,3R,4R,5S,6R)-3-Acetamido-2-[(2S,3S,4R,5R,6R)-6-[(2R,3R,4R,5S,6R)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylic acid Chemical compound CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 KIUKXJAPPMFGSW-DNGZLQJQSA-N 0.000 claims description 6
- 150000001450 anions Chemical class 0.000 claims description 6
- 239000000287 crude extract Substances 0.000 claims description 6
- 229920002674 hyaluronan Polymers 0.000 claims description 6
- 229960003160 hyaluronic acid Drugs 0.000 claims description 6
- 230000007935 neutral effect Effects 0.000 claims description 6
- 229920000297 Rayon Polymers 0.000 claims description 5
- 238000010521 absorption reaction Methods 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 5
- DUFKCOQISQKSAV-UHFFFAOYSA-N Polypropylene glycol (m w 1,200-3,000) Chemical class CC(O)COC(C)CO DUFKCOQISQKSAV-UHFFFAOYSA-N 0.000 claims description 4
- 150000003863 ammonium salts Chemical group 0.000 claims description 4
- 238000000746 purification Methods 0.000 claims description 4
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims description 3
- 230000033228 biological regulation Effects 0.000 claims description 3
- 239000003729 cation exchange resin Substances 0.000 claims description 3
- 230000008030 elimination Effects 0.000 claims description 3
- 238000003379 elimination reaction Methods 0.000 claims description 3
- 238000010828 elution Methods 0.000 claims description 3
- 238000005325 percolation Methods 0.000 claims description 3
- 239000002537 cosmetic Substances 0.000 abstract description 7
- -1 hydroxyphenyl ester Chemical class 0.000 abstract description 3
- 239000003755 preservative agent Substances 0.000 abstract 1
- 230000037307 sensitive skin Effects 0.000 abstract 1
- XUMBMVFBXHLACL-UHFFFAOYSA-N Melanin Chemical compound O=C1C(=O)C(C2=CNC3=C(C(C(=O)C4=C32)=O)C)=C2C4=CNC2=C1C XUMBMVFBXHLACL-UHFFFAOYSA-N 0.000 description 12
- 229960004106 citric acid Drugs 0.000 description 9
- 235000015165 citric acid Nutrition 0.000 description 9
- 230000036564 melanin content Effects 0.000 description 6
- 230000003750 conditioning effect Effects 0.000 description 4
- 230000003020 moisturizing effect Effects 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 229960001790 sodium citrate Drugs 0.000 description 3
- 241000272522 Anas Species 0.000 description 2
- 241000272814 Anser sp. Species 0.000 description 2
- 241001465754 Metazoa Species 0.000 description 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Natural products OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 230000002421 anti-septic effect Effects 0.000 description 2
- GPLRAVKSCUXZTP-UHFFFAOYSA-N diglycerol Chemical compound OCC(O)COCC(O)CO GPLRAVKSCUXZTP-UHFFFAOYSA-N 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000000049 pigment Substances 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 230000037303 wrinkles Effects 0.000 description 2
- 206010061218 Inflammation Diseases 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000036592 analgesia Effects 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000006065 biodegradation reaction Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000002500 effect on skin Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 230000003203 everyday effect Effects 0.000 description 1
- 230000035876 healing Effects 0.000 description 1
- 230000023597 hemostasis Effects 0.000 description 1
- 230000002209 hydrophobic effect Effects 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 238000005286 illumination Methods 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- 230000011514 reflex Effects 0.000 description 1
- 239000000523 sample Substances 0.000 description 1
- 230000003595 spectral effect Effects 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 230000029663 wound healing Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/817—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Compositions or derivatives of such polymers, e.g. vinylimidazol, vinylcaprolactame, allylamines (Polyquaternium 6)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
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- A—HUMAN NECESSITIES
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/981—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of mammals or bird
- A61K8/982—Reproductive organs; Embryos, Eggs
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- Health & Medical Sciences (AREA)
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- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Dermatology (AREA)
- Emergency Medicine (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Developmental Biology & Embryology (AREA)
- Reproductive Health (AREA)
- Zoology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a facial mask and in particular relates to an active egg white essence facial mask and a preparation method thereof. The active egg white essence facial mask consists of active egg white essence liquid and a facial mask base material, and is characterized in that the active egg white essence liquid comprises the following components in parts by weight: 0.01-0.05 part of poly-quaternary salt-51, 0.01-0.05 part of phenoxyethanol, 0.1 part of citric acid, 0.1 part of sodium citrate, 2 parts of polyethylene glycol, 4-6 parts of glycerol, 5 parts of dipropylene glycol, 5-10 parts of an active egg white essence, and 100 parts of water. The active egg white essence facial mask disclosed by the invention, differing from most cosmetics on the market, while keeping components of a cosmetic fresh, can protect skin from being hurt by hydroxyphenyl ester type preservatives, thereby being extremely suitable for people with sensitive skins.
Description
technical field:
The present invention relates to a kind of facial film, refer to a kind of active Ovum Gallus domesticus album elite facial film and preparation method thereof especially.
background technology:
Along with the raising day by day of living standard, people are also more and more high to the requirement of cosmetics.Particularly women for cosmetics understanding and select also more diversified.Natural class cosmetics also because healthy from however be subject to the attention of consumer and like.Ovum Gallus domesticus album has nourishes rough skin, conditioning whitening, wrinkle removing speckle dispelling, the curative effects such as convergence pore, but traditional Ovum Gallus domesticus album flush coat is not advocated, and one is because effective active composition in Ovum Gallus domesticus album is low, the excessive absorption being unfavorable for skin of molecule; Two is also be unfavorable for active ingredient exerts effect containing partial impurities in Ovum Gallus domesticus album.For improving above-mentioned shortcoming, promote the absorption of Ovum Gallus domesticus album elite, conditioning skin water oil balance, moisturizing moisturizing, the active essence of Ovum Gallus domesticus album combines with the woven non-woven fabrics face mask substrate material of chitin fiber by the present invention, be made into a kind of antibacterial, the degradable facial mask that are rich in active Ovum Gallus domesticus album elite, the care for responsive skin is very applicable.
summary of the invention:
A first aspect of the present invention is to provide a kind of active Ovum Gallus domesticus album elite facial film being suitable for responsive skin.
The present invention is achieved by the following technical solutions:
A kind of active Ovum Gallus domesticus album elite facial film, be made up of active Ovum Gallus domesticus album essence and face mask substrate material, it is characterized in that: described active Ovum Gallus domesticus album essence, comprises the component of following weight parts: 0.01-0.05 part polyquaternary ammonium salt-51,0.01-0.05 part phenoxyethanol, 0.1 part of citric acid, 0.1 part of sodium citrate, 2 parts of Polyethylene Glycol, 4-6 part glycerol, 5 parts of dipropylene glycols, the active Ovum Gallus domesticus album elite of 5-10 part, 100 parts of water.
Preferably, described active Ovum Gallus domesticus album essence, comprises the component of following weight parts: 0.01-0.05 part polyquaternary ammonium salt-51,0.01-0.05 part phenoxyethanol, 0.1 part of citric acid, 0.1 part of sodium citrate, 2 parts of Polyethylene Glycol, 4-6 part glycerol, 5 parts of dipropylene glycols, the active Ovum Gallus domesticus album elite of 5-10 part, the agent of 0.05-0.2 part whitening skin and preserving moisture, 100 parts of water.
Described whitening skin and preserving moisture agent be selected from phloretin, arbutin, hyaluronic at least two kinds, be particularly preferably made up of by weight following component: 10-30 part phloretin, 10-30 part arbutin, 50-100 part hyaluronic acid.
Described active Ovum Gallus domesticus album elite, extracting method step is as follows:
get Ovum Gallus domesticus album, regulate PH to 4-6, filter out insoluble Ovum Gallus domesticus album impurity, extract Ovum Gallus domesticus album crude extract;
Described Ovum Gallus domesticus album obtains from animal egg as extracted egg, Ovum Anas domestica, goose egg etc.;
ovum Gallus domesticus album crude extract PH is adjusted to 6-8, crosses elimination insoluble protein impurity, through the process of resin anion (R.A.) exchange column, collect the percolation component containing bioactive ingredients;
by the composition regulation PH to 4-8 after the process of resin anion (R.A.) exchange column, cross and filter insoluble impurity, again through cation exchange resin column process, bioactive ingredients is made to be adsorbed on resin, with the neutral buffered liquid containing different salinity, foreign protein is washed out again, then with containing the neutral buffered liquid of 0.3-1mol salinity by Ovum Gallus domesticus album bioactive ingredients eluting, collecting the elution fraction containing bioactive ingredients, obtaining active Ovum Gallus domesticus album elite.
further, in order to purification Ovum Gallus domesticus album bioactive ingredients:
By step
the Ovum Gallus domesticus album bioactive ingredients obtained, crosses and filters insoluble foreign protein, extracts clear liquid, is separated by the filter membrane of this clear liquid 100KDcutoff, collects the active component of filtered solution acquisition containing below 100KD molecular weight;
5. further, in order to purification Ovum Gallus domesticus album bioactive ingredients:
By step
the active component containing below 100KD molecular weight obtained; Cross and filter insoluble foreign protein, extract clear liquid, the filter membrane of this clear liquid 50KDcutoff is separated, collect the active component of more than 50KD molecular weight.
Be further purified, the Ovum Gallus domesticus album bioactive ingredients of more than 50KD below the 100KD molecular weight of acquisition, have better bioactive while, the care for responsive skin is very applicable.
The preparation method of active Ovum Gallus domesticus album essence of the present invention is not particularly limited, industry universal method can be adopted to be prepared from, such as: Polyethylene Glycol is dissolved in the water, add dipropylene glycol and glycerol, stir, then add active Ovum Gallus domesticus album elite and whitening agent, be uniformly mixed, add citric acid, sodium citrate, phenoxyethanol, polyquaternary ammonium salt again, stir, this active Ovum Gallus domesticus album essence can be obtained.
Second aspect present invention object is to provide a kind of preparation method of active Ovum Gallus domesticus album elite facial film, comprise the following steps: face mask substrate material of the present invention is cut into the suitable size of face, again active Ovum Gallus domesticus album essence is adsorbed on face mask substrate material, make patch formula facial film to use, preferably, often open on face mask substrate material that grammes per square metre is 20-80g, active Ovum Gallus domesticus album essence absorption 20-50g.
Face mask substrate material of the present invention can select existing face mask substrate material, the present invention provides a kind of non-woven fabrics face mask substrate material especially, there is better effect, this non-woven fabrics face mask substrate material is made up of viscose rayon non-woven fabrics and chitin fiber non-woven fabrics, wherein: face mask substrate material top fibre layer is the woven viscose rayon non-woven fabrics of water jet process, bottom fiber layer is the woven chitin fiber non-woven fabrics of water jet process.
Described non-woven fabrics face mask substrate material can adopt industry universal method to weave and form.
Non-woven fabrics face mask substrate material of the present invention has good hydrophilic and very high hygroscopicity, and because of the chitin fiber that it adopts, macromolecular chain exists the hydrophilic radical such as a large amount of hydroxyls (-OH) and amino (-NH2), and its water retention value is all about 130%; Viscose rayon non-woven fabrics hydrophobic force is strong compared with chitin fiber, can prevent the evaporation of essence.Chitin fiber woven non-woven fabrics face mask substrate material also has the functions such as antibacterial, antiinflammatory, hemostasis, analgesia, promotion wound healing, is applicable to the crowd of responsive skin.Again because of chitin fiber very easily biodegradation, also there is certain power-assisted to environmental protection.
The component that the present invention relates to and No. CAS as follows:
Polyquaternary ammonium salt-51, English name: POLYQUATERNIUM-51, No. CAS: 125275-25-4.
Citric acid, English name: Citricacid, No. CAS: 77-92-9.
Polyethylene Glycol, English name: Polyethyleneglycoladipateforglc, No. CAS: 24938-37-2.
Dipropylene glycol, English name: oxybis-Propanediol, No. CAS: 59113-36-9.
Hyaluronic acid, Hyaluronicacid, No. CAS: 9004-61-9.
Phloretin, English name: Phloretin, CAS accession number: 60-82-2.
Arbutin, English name: Arbutin, CAS accession number: 497-76-7.
Beneficial effect of the present invention is as follows:
A kind of active Ovum Gallus domesticus album elite facial film effectively can prevent skin ageing, wrinkle removing speckle dispelling, convergence pore, level and smooth skin, moisturizing moisturizing, and face mask substrate material carries anti-inflammation, calm Healing, and not containing oxybenzene lipid antiseptic in component.Be different from most of cosmetics on the market, the present invention can while maintenance cosmetic composition be fresh, and protection skin is not by the injury of oxybenzene lipid antiseptic.Component can eliminate the melanin on skin, skin whitening, efficient moisture-retention after adding whitening skin and preserving moisture agent, and conditioning skin water oil balance, is very applicable to responsive skin crowd.
detailed description of the invention:
Following examples further illustrate of the present invention, instead of limit the scope of the invention, the active Ovum Gallus domesticus album elite in embodiment, adopts following methods preparation:
get Ovum Gallus domesticus album, regulate PH to 4-6, filter out insoluble Ovum Gallus domesticus album impurity, extract Ovum Gallus domesticus album crude extract;
Described Ovum Gallus domesticus album obtains from animal egg as extracted egg, Ovum Anas domestica, goose egg etc.;
ovum Gallus domesticus album crude extract PH is adjusted to 6-8, crosses elimination insoluble protein impurity, through the process of resin anion (R.A.) exchange column, collect the percolation component containing bioactive ingredients;
by the composition regulation PH to 4-8 after the process of resin anion (R.A.) exchange column, cross and filter insoluble impurity, again through cation exchange resin column process, bioactive ingredients is made to be adsorbed on resin, with the neutral buffered liquid containing different salinity, foreign protein is washed out again, then with containing the neutral buffered liquid of 0.3-1mol salinity by Ovum Gallus domesticus album bioactive ingredients eluting, the elution fraction containing bioactive ingredients is collected;
by step
the Ovum Gallus domesticus album bioactive ingredients collected, crosses and filters insoluble foreign protein, extracts clear liquid, is separated by the filter membrane of this clear liquid 100KDcutoff, collects the active component of filtered solution acquisition containing below 100KD molecular weight;
5. by step
the active component containing below 100KD molecular weight of collecting, crosses and filters insoluble foreign protein, extract clear liquid, be separated by the filter membrane of this clear liquid 50KDcutoff, collect the active component of more than 50KD molecular weight.
Embodiment 1:
Take: 0.05mL polyquaternary ammonium salt-51,0.05mL phenoxyethanol, 0.5mL citric acid, 0.5mL sodium citrate, the active Ovum Gallus domesticus album elite of 50mL, 10mL part Polyethylene Glycol, 20mL glycerol, 25mL dipropylene glycol, 500mL water.Polyethylene Glycol is dissolved in the water, adds dipropylene glycol and glycerol, stir, then add active Ovum Gallus domesticus album elite, be uniformly mixed, then add citric acid, sodium citrate, phenoxyethanol, polyquaternary ammonium salt, stir, this active Ovum Gallus domesticus album essence can be obtained.
The face mask substrate material that the present invention adopts is cut into the suitable size of face, then is adsorbed on face mask substrate material by active Ovum Gallus domesticus album essence, make patch formula facial film and use, and often open on face mask substrate material that grammes per square metre is 20-80g, the adsorbance of facial mask liquid is 20-50g.
Embodiment 2-5:
Each raw material is taken respectively by the embodiment 2-5 data of table 1 correspondence.Each raw material is at room temperature uniformly mixed, Polyethylene Glycol is dissolved in the water, add dipropylene glycol and glycerol, stir, add active Ovum Gallus domesticus album elite and whitening agent again, be uniformly mixed, then add citric acid, sodium citrate, phenoxyethanol, polyquaternary ammonium salt, stir, this active Ovum Gallus domesticus album essence can be obtained.Face mask substrate material is cut into the size that face is suitable, then be adsorbed on face mask substrate material by active Ovum Gallus domesticus album essence, make patch formula facial film and use, and often open on face mask substrate material that grammes per square metre is 20-80g, the adsorbance of facial mask liquid is 20-50g.
Table 1: active Ovum Gallus domesticus album essence formula table (unit: mL)
| Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | |
| Polyquaternary ammonium salt-51 | 0.05 | 0.05 | 0.05 | 0.05 |
| Phenoxyethanol | 0.05 | 0.05 | 0.05 | 0.05 |
| Citric acid | 0.5 | 0.5 | 0.5 | 0.5 |
| Sodium citrate | 0.5 | 0.5 | 0.5 | 0.5 |
| Active Ovum Gallus domesticus album elite | 50 | 50 | 50 | 50 |
| Polyethylene Glycol | 10 | 10 | 10 | 10 |
| Glycerol | 20 | 20 | 20 | 20 |
| Dipropylene glycol | 25 | 25 | 25 | 25 |
| Phloretin | 0.02 | / | 0.04 | 0.04 |
| Arbutin | 0.02 | 0.04 | / | 0.04 |
| Hyaluronic acid | 0.04 | 0.04 | 0.04 | / |
| Water | 500 | 500 | 500 | 500 |
test case:
Experiment selects 25 responsive flesh female volunteers altogether, measures melanin content in human body skin, evaluates the white-skinned face function of astringent product.
The often group each selection of test 5 healthy womens, age is in 20-40 year, sign Informed Consent Form with study subject, adopt the MEXAMETERMX18 skin pigment instrument of German Courage+Khazaka company using first 1 day of astringent and using astringent within 14 days, to measure the melanin content of its skin of face afterwards continuously.Measure environment: test environment temperature (22 scholar 1) DEG C, humidity (50 scholar 5) %, averages.Study subject uses an astringent product every day, and using method is: after clean facial skin, dry, patted on facial skin by astringent with hands.Study subject does not use other whitening products at test period.
This instrument of MEXAMETERMX18 skin pigment instrument is the principle (RGB) based on spectral absorption, by measure the illumination of specific wavelength on human body skin after volume reflection determine melanic content in skin.The emitter of instrument probe sends the light that wavelength is respectively 568nm, 660nm and 880nm tri-kinds of wavelength and is radiated at skin surface, and accepter records the light of skin reflex.Because radiative amount is certain, therefore just can measure the amount of the light be absorbed by the skin, measure the content of dermal melanin.The measuring range of instrument is 0-999, measures numerical value higher, illustrates that in skin, melanin content is higher.
Melanin reduction rate=(using the astringent melanin content of first 1 day to use astringent melanin content after 14 days continuously) uses astringent melanin content of first 1 day again 100%.Melanin reduction rate is higher, illustrates that whitening effect is more obvious.
Table 2: test data table.
| Sequence number | Melanin reduction rate, % |
| Embodiment 1 | 1.6 |
| Embodiment 2 | 9.5 |
| Embodiment 3 | 8.1 |
| Embodiment 4 | 8.9 |
| Embodiment 5 | 9.3 |
The test data of experiment of associative list 2, can find out significantly:
1, one of the present invention active Ovum Gallus domesticus album elite facial film, can eliminate the melanin on skin, skin whitening, efficient moisture-retention, and conditioning skin water oil balance, is very applicable to responsive skin crowd;
2, by by phloretin, Folium Vaccinii vitis-idaeae former times and the composite use of hyaluronic acid, for white-skinned face function, obvious synergistic function is served.
Claims (10)
1. an active Ovum Gallus domesticus album elite facial film, be made up of active Ovum Gallus domesticus album essence and face mask substrate material, it is characterized in that: described active Ovum Gallus domesticus album essence, comprises the component of following weight parts: 0.01-0.05 part polyquaternary ammonium salt-51,0.01-0.05 part phenoxyethanol, 0.1 part of citric acid, 0.1 part of sodium citrate, 2 parts of Polyethylene Glycol, 4-6 part glycerol, 5 parts of dipropylene glycols, the active Ovum Gallus domesticus album elite of 5-10 part, 100 parts of water.
2. an active Ovum Gallus domesticus album elite facial film, is made up of active Ovum Gallus domesticus album essence and face mask substrate material, it is characterized in that: described active Ovum Gallus domesticus album essence, comprise the component of following weight parts: 0.01-0.05 part polyquaternary ammonium salt-51,0.01-0.05 part phenoxyethanol, 0.1 part of citric acid, 0.1 part of sodium citrate, 2 parts of Polyethylene Glycol, 4-6 part glycerol, 5 parts of dipropylene glycols, the active Ovum Gallus domesticus album elite of 5-10 part, the agent of 0.05-0.2 part whitening skin and preserving moisture, 100 parts of water.
3. one according to claim 2 active Ovum Gallus domesticus album elite facial film, is characterized in that: described whitening skin and preserving moisture agent be selected from phloretin, arbutin, hyaluronic at least two kinds.
4. one according to claim 3 active Ovum Gallus domesticus album elite facial film, is characterized in that: described whitening skin and preserving moisture agent is made up of by weight following component: 10-30 part phloretin, 10-30 part arbutin, 50-100 part hyaluronic acid.
5. one according to claim 1 and 2 active Ovum Gallus domesticus album elite facial film, is characterized in that: described active Ovum Gallus domesticus album elite, and extracting method step is as follows:
get Ovum Gallus domesticus album, regulate PH to 4-6, filter out insoluble Ovum Gallus domesticus album impurity, extract Ovum Gallus domesticus album crude extract;
ovum Gallus domesticus album crude extract PH is adjusted to 6-8, crosses elimination insoluble protein impurity, through the process of resin anion (R.A.) exchange column, collect the percolation component containing bioactive ingredients;
by the composition regulation PH to 4-8 after the process of resin anion (R.A.) exchange column, cross and filter insoluble impurity, again through cation exchange resin column process, bioactive ingredients is made to be adsorbed on resin, again foreign protein is washed out, then by Ovum Gallus domesticus album bioactive ingredients eluting, collect the elution fraction containing bioactive ingredients, obtain active Ovum Gallus domesticus album elite.
6. one according to claim 5 active Ovum Gallus domesticus album elite facial film, is characterized in that: step
in, adopt the neutral buffered liquid containing different salinity to be washed out by foreign protein, then with containing the neutral buffered liquid of 0.3-1mol salinity by Ovum Gallus domesticus album bioactive ingredients eluting.
7. one according to claim 5 active Ovum Gallus domesticus album elite facial film, is characterized in that: by step
the Ovum Gallus domesticus album bioactive ingredients obtained carries out further purification: be separated with the filter membrane of 100KDcutoff, collects filtered solution and obtains the active component containing below 100KD molecular weight.
8. one according to claim 5 active Ovum Gallus domesticus album elite facial film, is characterized in that: by step
the Ovum Gallus domesticus album bioactive ingredients obtained carries out further purification: be first separated with the filter membrane of 100KDcutoff, collects filtered solution and obtains the active component containing below 100KD molecular weight; Then be separated with the filter membrane of 50KDcutoff, collect the active component of more than 50KD molecular weight.
9. one according to claim 2 active Ovum Gallus domesticus album elite facial film, it is characterized in that: the preparation method of said active Ovum Gallus domesticus album essence is as follows: be dissolved in the water by Polyethylene Glycol, add dipropylene glycol and glycerol, stir, add active Ovum Gallus domesticus album elite and whitening agent again, be uniformly mixed, then add citric acid, sodium citrate, phenoxyethanol, polyquaternary ammonium salt, stir, this active Ovum Gallus domesticus album essence can be obtained.
10. the preparation method of the described active Ovum Gallus domesticus album elite facial film of one of claim 1-9, it is characterized in that: face mask substrate material is cut into the size that face is suitable, again active Ovum Gallus domesticus album essence is adsorbed on face mask substrate material, make patch formula facial film, often open on face mask substrate material that grammes per square metre is 20-80g, active Ovum Gallus domesticus album essence absorption 20-50g; Described face mask substrate material is made up of viscose rayon non-woven fabrics and chitin fiber non-woven fabrics, wherein: the top fibre layer of face mask substrate material is the woven viscose rayon non-woven fabrics of water jet process, the bottom fiber layer of face mask substrate material is the woven chitin fiber non-woven fabrics of water jet process.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2728488Y (en) * | 2003-12-31 | 2005-09-28 | 上海中大科技发展有限公司 | Chitin pack |
| CN103315935A (en) * | 2013-07-05 | 2013-09-25 | 上海珍馨化工科技有限公司 | Mint toning lotion |
| CN103536505A (en) * | 2013-09-26 | 2014-01-29 | 江阴康奈尔生物科技有限公司 | Extraction method of active egg white essence and egg white essence skincare product |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2728488Y (en) * | 2003-12-31 | 2005-09-28 | 上海中大科技发展有限公司 | Chitin pack |
| CN103315935A (en) * | 2013-07-05 | 2013-09-25 | 上海珍馨化工科技有限公司 | Mint toning lotion |
| CN103536505A (en) * | 2013-09-26 | 2014-01-29 | 江阴康奈尔生物科技有限公司 | Extraction method of active egg white essence and egg white essence skincare product |
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