CN105272150B - Tenmoku glaze procelain - Google Patents
Tenmoku glaze procelain Download PDFInfo
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- CN105272150B CN105272150B CN201510658419.0A CN201510658419A CN105272150B CN 105272150 B CN105272150 B CN 105272150B CN 201510658419 A CN201510658419 A CN 201510658419A CN 105272150 B CN105272150 B CN 105272150B
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Abstract
Disclosed tenmoku glaze porcelain comprises china clay and glaze. The glaze is composed of the following raw materials in parts by mass: 15-45 parts of potash feldspar, 10-40 parts of albite, 1-5 parts of aluminium oxide, 1-5 parts of zinc oxide, 1-5 parts of cobalt oxide, 10-50 parts of Dehua kaolin, 1-10 parts of cattle bone powder, and 1-10 parts of straw ash. The china clay is composed of the following raw materials in parts by mass: 20-55 parts of Dehua kaolin, 10-35 parts of dolomite, 5-25 parts of potash feldspar, 5-25 parts of albite, 0-5 parts of aluminium oxide, 0-5 parts of zinc oxide, 0-5 parts of cobalt oxide, 1-15 parts of Dehua mine soil, 1-10 parts of mica, and 5-15 parts of Dehua clay. The employed china clay is brown or black body, the glaze is oil-drop tenmoku glaze, and crystallized piebald points with different sizes are distributed on the glaze surface of the ceramic product prepared by using the glaze and show oil-drop-shaped pattern, and the pattern is extremely attractive.
Description
Technical field
The present invention relates to ceramic formula technical field, specifically a kind of temmoku vitreous enamel.
Background technology
Temmoku glaze is the black glazed ware device that Japanese takes back from Tianmu Mountains of Zhejiang Province, therefore named.Temmoku glaze is various in style, and famous and precious has
Oil droplet, the writing brush made of rabbit's hair, sparkling glaze, the black common name determined small cup, francolin spot, hawksbill turtle, yellow temmoku etc., be Song dynasty iron oxide black crystalline glaze.Droplet temmoku glaze
Face effect is that have silver color crystalline particle in glaze layer, has microgroove in particle in flower-shaped.Writing brush made of rabbit's hair temmoku be also known as " writing brush made of rabbit's hair temmoku flower ",
" glaze of furry appearance ", " beautiful milli glaze ", its background color is deeper dark purple black, and with foxy milli light, sericate muscle line is yellowish-brown
The coffee color of color sets off for background color.Sunlight becomes temmoku and belongs to the superfine product of temmoku glaze, the solar flare burnt till with high temperature under glaze, and solar flare is in sun
Seven glories that can glitter under the conditions of light and uniform temperature are swooned.The characteristics of yohen Tenmoku：Emerge big size naturally in black glaze
Little spot, glares around these spot surroundings colored halation such as also red, green, sky blue under the illumination of different azimuth
It is color.
Temmoku glaze is a kind of famous and precious vitreous enamel of China's Song dynasty production, and existing handed down from ancient times oneself is phoenix feathers and unicorn horns, and sunlight becomes temmoku then more
For rare rare, only three are collected respectively in the huge safety box in three museums of Japan, are just puted on display once per 7 years.
China not yet finds that so far yohen Tenmoku porcelain is handed down from ancient times, therefore since 19th century, the ceramist of countries in the world falls over each other to have put into greatly
The manpower and materials of amount, it is intended to replicate this name porcelain, but generally acknowledge that duplication is successfully not yet reported by industry.
The content of the invention
It is an object of the invention to provide a kind of temmoku vitreous enamel of the crystallization piebald point with oil droplet shape.
For achieving the above object, the present invention provides following technical scheme：
Temmoku vitreous enamel, including china clay and glaze, the glaze is made up of the raw material of following mass parts：Potassium feldspar 15-45 parts,
Albite 10-40 parts, aluminum oxide 1-5 parts, zinc oxide 1-5 parts, cobalt oxide 1-5 parts, Dehua kaolin 10-50 parts, bovine bone powder 1-
10 parts, rice-straw ash 1-10 parts；The china clay is made up of the raw material of following mass parts：Dehua kaolin 20-55 parts, white clouds soil 10-
35 parts, potassium feldspar 5-25 parts, albite 5-25 parts, aluminum oxide 0-5 parts, zinc oxide 0-5 parts, cobalt oxide 0-5 parts, Dehua mine soil
1-15 parts, mica 1-10 parts, Dehua clay 5-15 parts.
As further scheme of the invention：The glaze is made up of the raw material of following mass parts：30 parts of potassium feldspar, sodium are long
25 parts of stone, 3 parts of aluminum oxide, 3 parts of zinc oxide, 3 parts of cobalt oxide, 30 parts of Dehua kaolin, 5.5 parts of bovine bone powder, 5.5 parts of rice-straw ash；
The china clay is made up of the raw material of following mass parts：38 parts of Dehua kaolin, 22 parts of white clouds soil, 15 parts of potassium feldspar, albite 15
Part, 2.5 parts of aluminum oxide, 2.5 parts of zinc oxide, 2.5 parts of cobalt oxide, 8 parts of Dehua mine soil, 5.5 parts of mica, 10 parts of Dehua clay.
As further scheme of the invention：Glazing thickness of the glaze on china clay is 0.6-1.5mm.
The preparation method of described temmoku vitreous enamel, comprises the following steps：
（1）China clay and glaze raw material are processed, are comprised the following steps：
1）China clay raw material is processed：By above-mentioned china clay needed raw material, ground screening, proportioning, dehydration, old, hand
Work is molded, and repaired biscuit and is dried to obtain porcelain base；
2）Glaze raw material is processed：Above-mentioned glaze needed raw material is weighed in proportion, enters mill, according to glaze compound：
Mass ratio=1 of water：The ratio of 0.25-0.34, add water grinding 18-20h, and fineness control tails over≤0.1%, obtains in 250 mesh sieves
Glaze water；
（2）Glazing：By the way of leaching glaze or glaze spraying, glaze water adhesion is made in porcelain base surface, and glaze water thickness is reached
To 0.6-1.5mm；
（3）Burn till：Porcelain base after glazing is placed in into humidity for 0.5-1h in the environment of 80%, reenter klining into, first with
The ramp of 60-80 DEG C/h to 1050 DEG C, then with the ramp of 40-60 DEG C/h to 1190 DEG C, then with 60-80 DEG C/h
Ramp to 1280-1330 DEG C, be incubated 4-6h；Again 900 DEG C are cooled to the speed of 120-180 DEG C/h, it is last naturally cold
But to room temperature, temmoku vitreous enamel is obtained.
Compared with prior art, the invention has the beneficial effects as follows：The china clay that adopts of the present invention for brown or the carcass of black,
Glaze is droplet temmoku glaze, and crystallization piebald point not of uniform size is distributed with the ceramic product glaze made with the glaze, this
A little crystallization piebald points present the pattern of oil droplet shape, abnormal exquisite.
Specific embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described,
Obviously, described embodiment is only a part of embodiment of the invention, rather than the embodiment of whole.Based in the present invention
Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made, all
Belong to the scope of protection of the invention.
Embodiment 1
In the embodiment of the present invention, temmoku vitreous enamel, including china clay and glaze, the glaze by following mass parts raw material group
Into：15 parts of potassium feldspar, 40 parts of albite, 1 part of aluminum oxide, 5 parts of zinc oxide, 1 part of cobalt oxide, 50 parts of Dehua kaolin, bovine bone powder 1
Part, 10 parts of rice-straw ash；The china clay is made up of the raw material of following mass parts：20 parts of Dehua kaolin, white clouds soil 35 parts, potassium feldspar
5 parts, 25 parts of albite, 5 parts of zinc oxide, Dehua mine soil 15 parts, 1 part of mica, 15 parts of Dehua clay.
The preparation method of described temmoku vitreous enamel, comprises the following steps：
（1）China clay and glaze raw material are processed, are comprised the following steps：
1）China clay raw material is processed：By above-mentioned china clay needed raw material, ground screening, proportioning, dehydration, old, hand
Work is molded, and repaired biscuit and is dried to obtain porcelain base；
2）Glaze raw material is processed：Above-mentioned glaze needed raw material is weighed in proportion, enters mill, according to glaze compound：
Mass ratio=1 of water：0.25 ratio, add water grinding 20h, and fineness control tails over≤0.1%, obtains glaze water in 250 mesh sieves；
（2）Glazing：By the way of leaching glaze or glaze spraying, glaze water adhesion is made in porcelain base surface, and glaze water thickness is reached
To 0.6mm；
（3）Burn till：Porcelain base after glazing is placed in into humidity for 0.5h in the environment of 80%, klining is reentered into first with 80
DEG C/ramp of h to 1050 DEG C, then with the ramp of 60 DEG C/h to 1190 DEG C, then with the ramp of 80 DEG C/h
To 1330 DEG C, 6h is incubated；Again 900 DEG C are cooled to the speed of 180 DEG C/h, finally naturally cool to room temperature, obtain temmoku vitreous enamel.
Embodiment 2
In the embodiment of the present invention, temmoku vitreous enamel, including china clay and glaze, the glaze by following mass parts raw material group
Into：30 parts of potassium feldspar, 25 parts of albite, 3 parts of aluminum oxide, 3 parts of zinc oxide, 3 parts of cobalt oxide, 30 parts of Dehua kaolin, bovine bone powder
5.5 parts, 5.5 parts of rice-straw ash；The china clay is made up of the raw material of following mass parts：38 parts of Dehua kaolin, white clouds soil 22 parts, potassium
15 parts of feldspar, 15 parts of albite, 2.5 parts of aluminum oxide, 2.5 parts of zinc oxide, 2.5 parts of cobalt oxide, Dehua mine soil 8 parts, mica 5.5
Part, 10 parts of Dehua clay.
The preparation method of described temmoku vitreous enamel, comprises the following steps：
（1）China clay and glaze raw material are processed, are comprised the following steps：
1）China clay raw material is processed：By above-mentioned china clay needed raw material, ground screening, proportioning, dehydration, old, hand
Work is molded, and repaired biscuit and is dried to obtain porcelain base；
2）Glaze raw material is processed：Above-mentioned glaze needed raw material is weighed in proportion, enters mill, according to glaze compound：
Mass ratio=1 of water：03 ratio, add water grinding 20h, and fineness control tails over≤0.1%, obtains glaze water in 250 mesh sieves；
（2）Glazing：By the way of leaching glaze or glaze spraying, glaze water adhesion is made in porcelain base surface, and glaze water thickness is reached
To 1.0mm；
（3）Burn till：Porcelain base after glazing is placed in into humidity for 0.8h in the environment of 80%, klining is reentered into first with 70
DEG C/ramp of h to 1050 DEG C, then with the ramp of 50 DEG C/h to 1190 DEG C, then with the ramp of 70 DEG C/h
To 1310 DEG C, 5h is incubated；Again 900 DEG C are cooled to the speed of 150 DEG C/h, finally naturally cool to room temperature, obtain temmoku vitreous enamel.
Embodiment 3
In the embodiment of the present invention, temmoku vitreous enamel, including china clay and glaze, the glaze by following mass parts raw material group
Into：45 parts of potassium feldspar, 10 parts of albite, 5 parts of aluminum oxide, 1 part of zinc oxide, 5 parts of cobalt oxide, 10 parts of Dehua kaolin, bovine bone powder
10 parts, 1 part of rice-straw ash；The china clay is made up of the raw material of following mass parts：55 parts of Dehua kaolin, 10 parts of white clouds soil, potassium are long
25 parts of stone, 5 parts of albite, 5 parts of aluminum oxide, 5 parts of cobalt oxide, 1 part of Dehua mine soil, 10 parts of mica, 5 parts of Dehua clay.
The preparation method of described temmoku vitreous enamel, comprises the following steps：
（1）China clay and glaze raw material are processed, are comprised the following steps：
1）China clay raw material is processed：By above-mentioned china clay needed raw material, ground screening, proportioning, dehydration, old, hand
Work is molded, and repaired biscuit and is dried to obtain porcelain base；
2）Glaze raw material is processed：Above-mentioned glaze needed raw material is weighed in proportion, enters mill, according to glaze compound：
Mass ratio=1 of water：0.34 ratio, add water grinding 18h, and fineness control tails over≤0.1%, obtains glaze water in 250 mesh sieves；
（2）Glazing：By the way of leaching glaze or glaze spraying, glaze water adhesion is made in porcelain base surface, and glaze water thickness is reached
To 1.5mm；
（3）Burn till：Porcelain base after glazing is placed in into humidity for 1h in the environment of 80%, klining is reentered into first with 60 DEG C/h
Ramp to 1050 DEG C, then with the ramp of 40 DEG C/h to 1190 DEG C, then with the ramp of 60 DEG C/h extremely
1280 DEG C, it is incubated 4h；Again 900 DEG C are cooled to the speed of 120 DEG C/h, finally naturally cool to room temperature, obtain temmoku vitreous enamel.
In raw material employed in foregoing invention embodiment, Dehua kaolin, Dehua mine soil, Dehua clay are all from good fortune
Jian Sheng Dehua Counties.It is brown or black by the carcass of temmoku vitreous enamel obtained in above-mentioned technique, on the glaze of carcass surface portion
Crystallization piebald point not of uniform size is distributed with, these crystallization piebald points present the pattern of oil droplet shape, abnormal exquisite.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie
In the case of spirit or essential attributes without departing substantially from the present invention, the present invention can be in other specific forms realized.Therefore, no matter
From the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit is required rather than described above is limited, it is intended that all in the implication and scope of the equivalency of claim by falling
Change is included in the present invention.
Moreover, it will be appreciated that although this specification is been described by according to embodiment, not each embodiment is only wrapped
Containing an independent technical scheme, this narrating mode of specification is only that for clarity those skilled in the art should
Using specification as an entirety, the technical scheme in each embodiment can also Jing it is appropriately combined, form those skilled in the art
Understandable other embodiment.
Claims (3)
1. temmoku vitreous enamel, it is characterised in that including china clay and glaze, the glaze is made up of the raw material of following mass parts：Potassium is long
Stone 15-45 parts, albite 10-40 parts, aluminum oxide 1-5 parts, zinc oxide 1-5 parts, cobalt oxide 1-5 parts, Dehua kaolin 10-50
Part, bovine bone powder 1-10 parts, rice-straw ash 1-10 parts；The china clay is made up of the raw material of following mass parts：Dehua kaolin 20-55
Part, white clouds soil 10-35 parts, potassium feldspar 5-25 parts, albite 5-25 parts, aluminum oxide 0-5 parts, zinc oxide 0-5 parts, cobalt oxide 0-5
Part, Dehua mine soil 1-15 parts, mica 1-10 parts, Dehua clay 5-15 parts.
2. temmoku vitreous enamel according to claim 1, it is characterised in that the glaze is made up of the raw material of following mass parts：
30 parts of potassium feldspar, 25 parts of albite, 3 parts of aluminum oxide, 3 parts of zinc oxide, 3 parts of cobalt oxide, 30 parts of Dehua kaolin, bovine bone powder 5.5
Part, 5.5 parts of rice-straw ash；The china clay is made up of the raw material of following mass parts：38 parts of Dehua kaolin, 22 parts of white clouds soil, potassium are long
15 parts of stone, 15 parts of albite, 2.5 parts of aluminum oxide, 2.5 parts of zinc oxide, 2.5 parts of cobalt oxide, Dehua mine soil 8 parts, mica 5.5
Part, 10 parts of Dehua clay.
3. temmoku vitreous enamel according to claim 1, it is characterised in that glazing thickness of the glaze on china clay is 0.6-
1.5mm。
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105753323A (en) * | 2016-03-23 | 2016-07-13 | 杨云超 | Method for preparing jade green glaze porcelain |
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|---|---|---|---|---|
| CN106116147B (en) * | 2016-06-23 | 2019-02-22 | 德化恒瀚艺品有限公司 | A kind of oil-spot glaze and preparation method thereof containing shraff |
| CN107417250A (en) * | 2017-06-05 | 2017-12-01 | 杨合岭 | A kind of Sui's celadon formula and its manufacture craft |
| CN108840664A (en) * | 2018-08-31 | 2018-11-20 | 济源市坤彤陶瓷科技开发有限公司 | A kind of formula and its manufacture craft of colored porcelain porcelain |
| CN109052944A (en) * | 2018-09-14 | 2018-12-21 | 湖南高峰陶瓷制造有限公司 | Temmoku glaze and preparation method thereof |
| CN109369013A (en) * | 2018-10-17 | 2019-02-22 | 景德镇学院 | A kind of celeste glaze and preparation method thereof |
| CN115259667A (en) * | 2022-08-24 | 2022-11-01 | 福建省德化意达陶瓷有限公司 | Oil-drop temmoku glaze and firing method of oil-drop temmoku glaze ceramic |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102070329A (en) * | 2009-11-20 | 2011-05-25 | 路铠铭 | Raw material formula and manufacturing process for temmoku glaze porcelain |
| CN104496558A (en) * | 2014-12-04 | 2015-04-08 | 王泽彬 | Black oil-drop temmoku glaze |
| CN104649715A (en) * | 2014-12-31 | 2015-05-27 | 路今铧 | Novel temmoku glazed porcelain and firing method thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005320174A (en) * | 2002-05-10 | 2005-11-17 | Ikuyoshi Kojima | Process for producing firing-denatured tenmoku tile, firing-denatured tenmoku tile and glaze |
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2015
- 2015-10-14 CN CN201510658419.0A patent/CN105272150B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102070329A (en) * | 2009-11-20 | 2011-05-25 | 路铠铭 | Raw material formula and manufacturing process for temmoku glaze porcelain |
| CN104496558A (en) * | 2014-12-04 | 2015-04-08 | 王泽彬 | Black oil-drop temmoku glaze |
| CN104649715A (en) * | 2014-12-31 | 2015-05-27 | 路今铧 | Novel temmoku glazed porcelain and firing method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105753323A (en) * | 2016-03-23 | 2016-07-13 | 杨云超 | Method for preparing jade green glaze porcelain |
| CN105753323B (en) * | 2016-03-23 | 2018-06-01 | 杨云超 | A kind of your porcelain preparation method of emerald green glaze |
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| CN105272150A (en) | 2016-01-27 |
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