CN105268516A - Superfine powder preparing method - Google Patents

Superfine powder preparing method Download PDF

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Publication number
CN105268516A
CN105268516A CN201510808988.9A CN201510808988A CN105268516A CN 105268516 A CN105268516 A CN 105268516A CN 201510808988 A CN201510808988 A CN 201510808988A CN 105268516 A CN105268516 A CN 105268516A
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CN
China
Prior art keywords
grinding
mill
mill tube
peat soil
arm
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201510808988.9A
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Chinese (zh)
Inventor
辛衷瑜
周鑫
李楠
李智
张敏
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Individual
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Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Individual filed Critical Individual
Priority to CN201510808988.9A priority Critical patent/CN105268516A/en
Publication of CN105268516A publication Critical patent/CN105268516A/en
Priority to PCT/CN2016/106958 priority patent/WO2017088767A1/en
Priority to CN202310180213.6A priority patent/CN116218537A/en
Priority to CN201611037409.6A priority patent/CN106701092A/en
Pending legal-status Critical Current

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Abstract

The invention belongs to the technical field of superfine solid powder grinding, and particularly relates to a superfine powder preparing method. The method for processing peat soil plant remains to be of the particle size below 5 micrometers at normal temperature and normal pressure includes the steps that the peat soil plant remains with the organic matter content above 50% are pretreated to be of the particle size below 1 mm, wherein the water content is 5%-15%; the remains are placed into a three-stage controllable orbital-transfer ball mill, wherein a grinding barrel is divided into three grinding bins through three screening fences of different hole diameters, and three kinds of grinding balls of different sizes and quantities are placed into the three grinding bins; and the grinding barrel is driven by a variable frequency motor to vibrate in the horizontal and vertical directions with variable amplitudes and frequencies. Accordingly, the superfine powder grinding effect of step-by-step refining, adjustable impulse and controllable particle sizes is achieved.

Description

A kind of superfines prepare method
Technical field
The invention belongs to solid superfines grinding technology field, particularly peat soil plant remains superfines preparation method.
Background technology
Usual peat soil plant remains, also known as brown coal, sapropel, particle size is comparatively large, and physical and chemical performance is stablized, water insoluble.But when its particle diameter reaches several microns, just can show some special physical and chemical performances, such as: solubility several times increase, and be conducive to plant absorption nutrient, crop growth power and immunity obviously strengthen; To hardening, soil can play loose effect, improves rapidly soil organism state, accelerate growth of microorganism, is of great significance Improvement of Ecological Environment.
Traditional content of organic matter is greater than 50% peat soil plant remains fine-powder preparation process, temperature generally will more than 85 DEG C, some special macromolecule functional groups in organic matter are destroyed, and cause effect of its most worthy to be lost, and can only play common organic fertile effect.And traditional peat soil plant remains powder is generally about 200 orders, and 2000 object peat soil plant remains powder effects are than 200 height of eye decades of times.But at normal temperatures and pressures, current preparation method is difficult to peat soil plant remains to be ground to 2000 orders, needs to break through existing techniques in realizing.
The present invention is on the basis of existing ball mill, proposing the preparation method of three grades of controlled change rail ball mills, increasing momentum by changing track, increase is simultaneously ground cabin and is changed abrading-ball size and realizes powder granular step by step, then, powder delivery particle size is controlled by screen.Combinationally using these methods, solves the problem of solids powder mull to particle diameter 5 microns (2680 order).
Summary of the invention
The present invention proposes the peat soil plant remains superfines preparation method of three grades of controlled change rail ball mills.Comprise following part:
1), by the pretreatment of natural peat soil plant remains to particle diameter less than 1 millimeter, water content 5% ~ 15%, is transported to three grades of controlled change rail ball mills;
2), ball mill mill tube comprises the screen fence that three are respectively 100-500um, 30-80um, 5-20um different pore size, mill tube is divided into three mill cabins by three screen fence, places the abrading-ball that three kinds of diameters are the different size of 15-30mm, 10-15mm, 3-10mm respectively in three mill cabins;
3), mill tube two ends are fixed in the track of two equidirectionals and size, and be fixed in the middle of mill tube on the arm of force flexible up and down, the track at mill tube two ends is fixed on the arm of force of horizontal motion, the arm of force of both direction is driven by variable-frequency motor, forms controllable variable track vibromill;
4), two identical controlled change rail vibromills, utilize a central point to connect the arm of force of horizontal direction, make two mill tube horizontal direction symmetrical operations, balance is positioned over support.
5), the vibration frequency of the arm of force of level and upper and lower two vertical direction is 10-60Hz, and amplitude is 5-38cm, by variable-frequency motor power adjusting.
6), from material inlet to outlet, the magic ball of descending different-diameter and the screen of different meshes are placed in three mill cabins; Material outlet screen is at 1340-3000 order, and material grinding finished product grain size is less than 10 microns.
7), mill tube and grinding ball material have stronger heat conduction, corrosion-resistant, impact resistance, as strengthening steel.
Essential characteristic of the present invention is:
One, controllable variations track increases the momentum of spheroid, makes grinding charge receive more strike;
Two, vibration frequency, amplitude and variation track are adjustable controlled, and momentum is changeable;
Three, the size of ball radius and the change of number make powder attenuate step by step;
Four, the screen pore size control particle diameter of powder reaches corresponding grinding effect with the corresponding relation of the size and number of abrading-ball;
Five, mill tube inwall and abrading-ball select shock-resistant, corrosion-resistant, that heat conduction is fast material can reach temperature control effect and service life.
Example one
By natural peat soil in drum through rotary-cut, the wind of less than 65 DEG C is blown in rotary-cut process, water content is made to reach 10-12%, through normal temperature Cemented filling to feed bin, the alkali (NaOH) of even blending 6%, by a downward Cemented filling to three grades of controlled change rail ball mill entrances, three grades of controlled change rail ball mill frequency 50Hz, amplitude 30cm in the horizontal direction, under the vibro-grinding of vertical direction frequency 20Hz, amplitude 10cm, powder delivery 500kg per hour.
Example two
By natural peat soil in drum through rotary-cut, the wind of less than 55 DEG C is blown in rotary-cut process, water content is made to reach 5-15%, through normal temperature Cemented filling to feed bin, the alkali (each half of CaO and NaOH) of evenly blending 10%, by a downward pipeline, naturally fall, be transported to three grades of controlled change rail ball mill entrances, three grades of controlled change rail ball mills under the vibro-grinding of frequency 40Hz, amplitude 20cm, powder delivery 400kg per hour.

Claims (6)

1. the preparation method of a peat soil plant remains superfines, concrete steps: first, by natural peat soil in drum through rotary-cut, the wind of 30-85 DEG C is blown in rotary-cut process, the pretreatment of natural peat soil plant remains is to particle diameter less than 1 millimeter, water content 5% ~ 15%, is transported to three grades of controlled change rail ball mills, prepares the superfine powder of particle diameter below 10 microns.
2. according to claim 1, ball mill mill tube comprises the screen fence that three are respectively 100-500um, 30-80um, 5-12um different pore size, mill tube is divided into three mill cabins by three screen fence, places the abrading-ball that three kinds of diameters are the different size of 15-30mm, 10-15mm, 3-10mm respectively in three mill cabins.
3. according to claim 2, mill tube two ends are fixed in the track of two equidirectionals and size, be fixed on the arm of force flexible up and down in the middle of mill tube, the track at mill tube two ends is fixed on the arm of force of horizontal motion, the arm of force of both direction is driven by variable-frequency motor, forms controllable variable track vibromill.
4. according to claim 3, two identical controlled change rail vibromills, utilize a central point to connect the arm of force of horizontal direction, make two mill tube horizontal direction symmetrical operations, balance is positioned over support.
5. according to claim 3, the vibration frequency of both direction is 10-60Hz, and amplitude is 5-38cm, by variable-frequency motor power adjusting.
6. according to claim 2, mill tube and grinding ball material adopt stronger heat conduction, corrosion-resistant, impact resistance, as strengthening steel.
CN201510808988.9A 2015-11-23 2015-11-23 Superfine powder preparing method Pending CN105268516A (en)

Priority Applications (4)

Application Number Priority Date Filing Date Title
CN201510808988.9A CN105268516A (en) 2015-11-23 2015-11-23 Superfine powder preparing method
PCT/CN2016/106958 WO2017088767A1 (en) 2015-11-23 2016-11-23 Soil conditioner, preparation method therefor, and application thereof
CN202310180213.6A CN116218537A (en) 2015-11-23 2016-11-23 A kind of soil conditioner and its preparation method and application, method of soil conditioning
CN201611037409.6A CN106701092A (en) 2015-11-23 2016-11-23 Soil conditioner, and preparation method and application thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510808988.9A CN105268516A (en) 2015-11-23 2015-11-23 Superfine powder preparing method

Publications (1)

Publication Number Publication Date
CN105268516A true CN105268516A (en) 2016-01-27

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510808988.9A Pending CN105268516A (en) 2015-11-23 2015-11-23 Superfine powder preparing method

Country Status (1)

Country Link
CN (1) CN105268516A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105521856A (en) * 2016-02-19 2016-04-27 湖南升华科技股份有限公司 Sanding device and method using zirconium balls in different sizes
CN106701092A (en) * 2015-11-23 2017-05-24 辛衷瑜 Soil conditioner, and preparation method and application thereof
CN114985747A (en) * 2022-06-14 2022-09-02 山东泰山钢铁集团有限公司 Method for quickly adjusting bulk density of primary powder
CN120094692A (en) * 2025-04-15 2025-06-06 深圳市臻金新瓷电子材料科技有限公司 Device and method for preparing black alumina ceramic substrate with high mechanical strength and breakdown strength

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106701092A (en) * 2015-11-23 2017-05-24 辛衷瑜 Soil conditioner, and preparation method and application thereof
WO2017088767A1 (en) * 2015-11-23 2017-06-01 辛衷瑜 Soil conditioner, preparation method therefor, and application thereof
CN105521856A (en) * 2016-02-19 2016-04-27 湖南升华科技股份有限公司 Sanding device and method using zirconium balls in different sizes
CN114985747A (en) * 2022-06-14 2022-09-02 山东泰山钢铁集团有限公司 Method for quickly adjusting bulk density of primary powder
CN120094692A (en) * 2025-04-15 2025-06-06 深圳市臻金新瓷电子材料科技有限公司 Device and method for preparing black alumina ceramic substrate with high mechanical strength and breakdown strength
CN120094692B (en) * 2025-04-15 2025-11-25 深圳市臻金新瓷电子材料科技有限公司 Preparation device and method of black alumina ceramic substrate with high mechanical and breakdown strength

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Application publication date: 20160127