CN105248449A - Toothbrush cleaning tablets and preparation method and usage method thereof - Google Patents
Toothbrush cleaning tablets and preparation method and usage method thereof Download PDFInfo
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- CN105248449A CN105248449A CN201510660614.7A CN201510660614A CN105248449A CN 105248449 A CN105248449 A CN 105248449A CN 201510660614 A CN201510660614 A CN 201510660614A CN 105248449 A CN105248449 A CN 105248449A
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Abstract
The invention discloses toothbrush cleaning tablets and a preparation method and usage method thereof. The toothbrush cleaning tablets are prepared from oxygen releasing agents, alkali carbonate raw materials, acid raw materials, tablet auxiliary materials, mint or lemon essence and food coloring, wherein povidone-hydrogen peroxide complex compounds are adopted as the oxygen releasing agents. The preparation method of the toothbrush cleaning tablets comprises the technological steps that 1, the acid raw materials and lubricating agents are added into a mixing machine to be mixed and ground; 2, carbonate and/or bicarbonate are continuously added into the mixing machine to serve as the alkali carbonate raw materials, and the materials are continuously mixed and ground; 3, the oxygen releasing agents, the lubricating agents, the mint or lemon essence and the food coloring are added into the mixing machine, and the materials are evenly stirred to obtain powder materials; 4, the powder materials are pressed into tablets through a rotation tablet press, and then the toothbrush disinfection effervescent tablets are obtained. When the effervescent tablets are used, the effervescent tablets are melted into an aqueous solution, and a toothbrush is soaked in the aqueous solution and taken out to be washed and air-dried 10 minutes later. The toothbrush cleaning tablets can perform sterilization and disinfection on the toothbrush and have the very important practical significance on ensuring physical health of people.
Description
Technical field
The present invention relates to toothbrush and gargle the disinfection technical field of washing apparatus and shallow contact daily necessities, particularly a kind of toothbrush cleaning foil and preparation method thereof, using method with other.
Background technology
Not yet to have in conventional detergents and be specifically designed to toothbrush and clean use.The formation of conventional cleaning agent comprises the components such as surfactant, sodium carbonate, bleaching powder.The bactericidal action of this cleaning agent is very weak and sterilization flora is single, is not suitable as the direct substitute to toothbrush cleaning-sterilizing.Especially the killing action for the various protozoons retained on toothbrush of being everlasting (amoeba meleagridis, the own trichomonad of ox, balantidium coli, flagellate etc.) and various bacterium (downright bad grey oxygen screw mandrel bacterium, Clostridium, staphylococcus anaerobius, intestines vibrios, treponema bacterium etc.)/(coccus, Bacillus acidi lactici, bacillus and conveyor screw, wherein Bacillus acidi lactici occupies very large ratio (about 30 ~ 40%)) is poor.
Medicine clinical research demonstrates the number of bacteria that the use toothbrush of 1 ~ 2 week retains can up to hundreds of thousands, and wherein a lot of bacterium has damaging effect to human body.Such as Bacillus acidi lactici can make the swill fermentation and acid remained in dental surface and teeth space, the enamel acid corrosion of dental surface and deliquescing, flavescence, so that defect and form carious tooth;
Dentist detects the used toothbrush of people, find that new toothbrush only uses 3 ~ 4 weeks and just have a large amount of white to read the various pathogens breedings such as coccus, Streptococcus mutans, hemolytic streptococcus, pneumobacillus, staphylococcus, these bacteriums directly can invade mucous membrane of mouth.
The process toothbrush of brushing teeth is easy to be polluted, comprising the microorganism in source, oral cavity, as sick in dental caries pathogenic bacteria ~ Streptococcus mutans, Periodontal Pathogens, Candida albicans, also comprise some non-oral microorganisms, as some intestinal bacteria, from used toothbrush, isolate pseudomonas in addition.Research shows, cariogenic bacteria and Periodontal Pathogens can propagate into another position by reusing the toothbrush of pollution from a position in oral cavity.And after patient changes contaminated toothbrush, mouth disease such as lichen planus, mouth syndrome of burning all can be eased.This illustrates that controlling toothbrush pollutes and can effectively reduce the probability infected again in oral cavity.Therefore toothbrush can regard a potential source of infection as, likely causes oral cavity and whole body system to infect when collective's resistance declines.And some are had to the crowd of systemic disease, as diabetic and cardiac valves patient and immune deficiency person, use the serious toothbrush of microbial contamination to further increase it and infect probability.The sterilization of toothbrush as can be seen here, stops microorganism to multiply breeding on toothbrush, for ensureing that the health of human oral cavity and health other system is very meaningful and very necessary.
Bacterium on toothbrush is mainly derived from oral cavity and air.Human oral cavity is the environment that a various bacteria exists on the one hand, and rear section bacterium of brushing teeth is not washed away and remain on toothbrush, on the other hand, generally exposes in atmosphere, make toothbrush have with the bacterium in air the chance contacted after toothbrush uses.And toothbrush is often placed in the dark moist place of washing room, germ more easily grows breeding.Unclean toothbrush may be the source of infection of various diseases, because these bacteriums can remain in when brushing teeth in the gap, every nook and cranny in tooth and oral cavity, can by directly to swallow or the mucous membrane of mouth of breakage and cavity invade human body and give rise to diseases, the sterilization of visible toothbrush, the sanitation and hygiene keeping toothbrush are very important, therefore must take measures to reduce or eliminate these noxious bacterias.
Summary of the invention
The object of the invention is the defect for above-mentioned prior art, there is provided a kind of toothbrush cleaning foil and preparation method thereof, using method, use polyvidone/hydrogen peroxide complex compound to do oxygen evolution agent, be equipped with basic carbonate raw material, additive of tablet, peppermint or lemon extract, food coloring makes stable performance, the sterilized disinfection tablet of toothbrush easy to use.Sterilization being carried out to toothbrush, having very major and immediate significance for ensureing that people are healthy.Except can be used for toothbrush clean except, can also be used for other and gargle the sterilization washing utensil.
To achieve these goals, technical scheme of the present invention is:
A kind of toothbrush cleaning foil, described toothbrush cleaning foil makes the effervescent tablet made by oxygen evolution agent by polyvidone/hydrogen peroxide complex compound.
Preferably, described toothbrush cleaning foil is used for the sterilization of toothbrush.
Preferably, described toothbrush cleaning foil is for gargling the sterilization washing apparatus.
Preferably, described toothbrush cleaning foil is used for the sterilization of the shallow contact daily necessities of toothbrush.
Preferably, described effervescent tablet comprises oxygen evolution agent, basic carbonate raw material, acid material, additive of tablet, peppermint or lemon extract and food coloring, and described oxygen evolution agent is polyvidone/hydrogen peroxide complex compound.
Preferably, the mass fraction of described polyvidone/hydrogen peroxide complex compound is 0.1 ~ 10.
Preferably, described toothbrush cleaning foil also comprises basic carbonate raw material, and described basic carbonate raw material is carbonate and/or bicarbonate.
Preferably, the mass fraction of described carbonate and/or bicarbonate is 0.5 ~ 30.
Preferably, described acid material is selected from one or more the mixture in citric acid, malic acid, tartaric acid, fumaric acid, and the mass fraction of described acid material is 1.0 ~ 20.
Preferably, the mass fraction of described additive of tablet is 1 ~ 20; Described additive of tablet comprises adhesive and lubricant, and described adhesive is polyvinylpyrrolidone, and described lubricant is superfine silica gel powder or talcum powder.
Preferably, the mass fraction of described Mint Essence is 0.01 ~ 1.0.
Preferably, described food coloring is light blue, ciba blue 2b, indigo carmine, indigo blue potassium, indigo, indigo two sulfuric acid sylvite, thioindigo, indigo naturalis look food coloring, and the mass fraction of described food coloring is 0.01 ~ 1.0.
The present invention also provides the preparation method of above-mentioned toothbrush cleaning foil, and the processing step of this preparation method is:
(A) lubricant in acid material, additive of tablet is added mixing in mixer to grind;
(B) continue to add carbonate and/or bicarbonate makes basic carbonate raw material, continue mixing and grind;
(C) then add oxygen evolution agent, the lubricant of additive of tablet, peppermint or lemon extract, food coloring, stir, the powder mixed obtained;
(D) powder mixed step (C) obtained, through rotary pelleting machine compressing tablet, obtains described toothbrush sanitizing effervescent tablet.
Invention additionally provides the using method that above-mentioned toothbrush cleaning foil is applied as disinfectant detergent, the using method of this toothbrush cleaning foil is:
(A) a slice toothbrush cleaning foil is got, toothbrush cleaning foil is put into water and puts into about 100ml water, under acid material and the acting in conjunction of basic carbonate raw material, produce a large amount of bubble (carbonic acid gas), make the rapid disintegration of toothbrush cleaning foil and thawing, form the effervesce aqueous solution;
(B) toothbrush or other are gargled wash utensil and shallow contact daily necessities is immersed in 5-10 minute in the effervesce aqueous solution;
(C) take out, naturally dry with after tap water.
Dimension ketone is that universal love is newly increased income the product of production of company in vain, and it is polyvinylpyrrolidone and H
2o
2complex compound; Outward appearance is white powder, the H existed in solid form
2o
2content is the hydrogen peroxide w/w that 16-20%(comprises more than 20%), can stablize in the dry state and preserve the several years, can water-soluble and other organic solvents, and sustained release can be stablized when water, saliva contacts go out H
2o
2, namely within the regular hour, keep H certain in solution
2o
2concentration, thus obviously can increase H
2o
2the effect of sterilizing.Be safe, stable and be H
2o
2.These products meet water then can discharge H rapidly
2o
2.
Dimension ketone is based on NVP (NVP) and H in vain
2o
2hydrogen bonding compound.Pyrrolidones is the five membered lactams rings having amidocarbonylation, and amidocarbonylation is a strong hydrogen bond acceptor, and H
2o
2be a strong hydrogen bond supplier, so it forms a stable complex compound by with pyrrolidones.Detect through nuclear magnetic resonnance (NMR) and show, there is a kind of bottom offset of key in solid carbon 13, demonstrate H in carbonyl carbon
2o
2and between PVP, there is network and effect.When complex compound contacts with excessive water in aqueous, the H of hydrogen bond one end on complex compound
2o
2just be replaced by water, therefore H
2o
2just be released.
With simple compound H
2o
2the H of release during solution is white unlike, complex compound dimension ketone
2o
2concentration time limited, only have when 1) complex solution dilutes further, 2) consume part H because of sterilization, discoloration
2o
2, free H in complex solution
2o
2concentration lower time, just can discharge the free H made new advances in complex compound
2o
2; And as free H out
2o
2when concentration arrives certain limit, will stop and continue release.Most of H in complex solution
2o
2with PVP-H
2o
2/ PVPP-H
2o
2the form of polymer exists.This feature is to minimizing H
2o
2shortcoming (higher toxicity and excitant) have the effect of highly significant, reduce the stimulation of calcination to skin or wound, use as mild as a dove.Therefore, dimension ketone is very safe in vain, can not form a kind of hydrogen peroxide product of injury to human body.
Have due to dimension ketone white product and sustained release can be stablized when water, saliva contacts go out H
2o
2, the characteristic of active oxygen is provided, thus ties up the white PVP-H of ketone
2o
2complex compound as oxygen evolution agent, can be applicable to oral cavity whitening care product, disinfection nursing product, can have sterilizing, characteristic effect that decontamination is brightened as the effective calculus removal agent/bleaching agent in toothwash tablet.
The most outstanding feature of product is exactly H
2o
2be complex pattern with polyvinylpyrrolidone, by the complex protection effect of polyvinylpyrrolidone under dry powder, effectively can keep H
2o
2complexing stablize, extend H
2o
2stable period; And when running into water, saliva, by the hydrophilic dissolubility that polyvinylpyrrolidone is good, the H of complexing
2o
2be discharged in solution continuously, if the H in solution
2o
2concentration increases, H
2o
2the speed of complexing release can slow down, thus reaches the object of Stable Release in certain hour, maintains H
2o
2solution concentration, extend H
2o
2the action time of sterilizing, increase H
2o
2the action effect of sterilizing.
And simple H
2o
2, poor stability, H under long-time storage
2o
2concentration can reduce; H during use
2o
2concentration just becomes very large quickly, and reduces rapidly, H
2o
2the continuous action time is very short, and not only the effect of sterilizing can reduce very soon, and high concentration H
2o
2also can cause some human body side effects.
Other sterilizing objects, many employing peroxide salts substances, as SODIUM PERCARBONATE, sodium peroxydisulfate, sodium perborate etc., discharge H rapidly when these materials are all and dissolve
2o
2, the H in a period of time cannot be kept
2o
2concentration stabilize, thus for meeting the needs of sterilizing, needs the proportion scale increasing peroxide, H in solution when making to use beginning
2o
2dense, easily cause human body side effect.
Mechanism of the present invention is: after effervescent tablet puts into water, effervescent tablet is met water and is reacted, under acid material and the acting in conjunction of basic carbonate raw material, produce a large amount of bubble (carbonic acid gas), make the rapid disintegration of tablet and thawing, be effervesce shape when tablet collapses loose, the bubble that disintegration produces can make tablet roll up and down in water, accelerates its disintegration and thawing.Oxygen evolution agent polyvidone/hydrogen peroxide complex compound (dimension ketone is white), it can in the effervescent tablet aqueous solution sustained release oxonium ion, there is the function of Continuous sterilization sterilization, strong suppression and killing action is had for various protozoon and bacterium, continue broad-spectrum sterilization, and free from extraneous odour, without carcinogenic, without problems such as teratogenesis, revolutionize that existing all purpose cleaner bactericidal effect is poor, sterilization flora is single, be not suitable for for the clean present situation of toothbrush.
Getting this product during use to put into about 100ml water and form the effervesce aqueous solution, toothbrush being immersed in 5-10 minute in the effervesce aqueous solution, with naturally drying the effect that can reach toothbrush sanitizing sterilizing after tap water.Preparation technology of the present invention is simple and easy to do, easy to use, have that sterilizing is strong, safety non-toxic, steady performance, toothbrush remaining bacteria is killed and can be reached 100%, the toothbrush sanitizing sterilizing be applicable to very much in daily life uses, and also can be used for other and gargles the disinfection washing apparatus and shallow contact daily necessities.By adding oxygen evolution agent polyvidone/hydrogen peroxide complex compound (dimension ketone is white) that conventional detergents never uses in formula, this cleaning agent is made to have better toothbrush cleaning effect.
This disinfectant also can be used for the disinfection of other shallow contact daily necessitiess.
It is below sterilizing experimental data table of the present invention
Embodiment
Below in conjunction with specific embodiment, the present invention is further described.
Embodiment 1
(A) select one or more the mixture in citric acid, malic acid, tartaric acid, fumaric acid to make acid material, the mass fraction of described acid material is 1.0; Select polyvinylpyrrolidone to make adhesive, select superfine silica gel powder or talcum powder to make lubricant, adhesive and lubricant are as additive of tablet, and the mass fraction of additive of tablet is 1;
Lubricant in acid material, additive of tablet is added mixing in mixer to grind;
(B) continue to add carbonate or bicarbonate makes basic carbonate raw material, the mass fraction of basic carbonate raw material is that 0.5 continuation mixing grinds;
(C) then add oxygen evolution agent polyvidone/hydrogen peroxide complex compound, mass fraction be 0.1, the lubricant of additive of tablet, peppermint or lemon extract, food coloring, stir, mixing is sieved 100 orders, the powder mixed obtained;
Food coloring is light blue, ciba blue 2b, indigo carmine, indigo blue potassium, indigo, indigo two sulfuric acid sylvite, thioindigo, indigo naturalis look food coloring, and the mass fraction of described food coloring is 0.01;
(D) powder mixed step (C) obtained is through rotary pelleting machine compressing tablet, and compression force 15-20KN, sheet diameter is 22mm, hardness 60-80N, obtains described toothbrush sanitizing effervescent tablet.
The using method that this toothbrush cleaning foil is applied as disinfectant detergent is:
(A) a slice toothbrush cleaning foil is got, toothbrush cleaning foil is put into water and puts into about 100ml water, under acid material and the acting in conjunction of basic carbonate raw material, produce a large amount of bubble (carbonic acid gas), make the rapid disintegration of toothbrush cleaning foil and thawing, form the effervesce aqueous solution;
(B) toothbrush or other are gargled wash utensil and shallow contact daily necessities is immersed in 5-10 minute in the effervesce aqueous solution;
(C) take out, naturally dry with after tap water.
Embodiment 2
(A) select one or more the mixture in citric acid, malic acid, tartaric acid, fumaric acid to make acid material, the mass fraction of described acid material is 20; Select polyvinylpyrrolidone to make adhesive, select superfine silica gel powder or talcum powder to make lubricant, adhesive and lubricant are as additive of tablet, and the mass fraction of additive of tablet is 20;
Lubricant in acid material, additive of tablet is added mixing in mixer to grind;
(B) continue to add carbonate and bicarbonate makes basic carbonate raw material, the mass fraction of basic carbonate raw material is that 30 continuation mixing grind;
(C) then add oxygen evolution agent polyvidone/hydrogen peroxide complex compound, mass fraction be 10, the lubricant of additive of tablet, peppermint or lemon extract, food coloring, stir, mixing is sieved 100 orders, the powder mixed obtained;
Food coloring is light blue, ciba blue 2b, indigo carmine, indigo blue potassium, indigo, indigo two sulfuric acid sylvite, thioindigo, indigo naturalis look food coloring, and the mass fraction of described food coloring is 1.0;
(D) powder mixed step (C) obtained is through rotary pelleting machine compressing tablet, and compression force 18-20KN, sheet diameter is 22mm, hardness 60-90N, obtains described toothbrush sanitizing effervescent tablet.
Embodiment 3
(A) select one or more the mixture in citric acid, malic acid, tartaric acid, fumaric acid to make acid material, the mass fraction of described acid material is 10; Select polyvinylpyrrolidone to make adhesive, select superfine silica gel powder or talcum powder to make lubricant, adhesive and lubricant are as additive of tablet, and the mass fraction of additive of tablet is 10;
Lubricant in acid material, additive of tablet is added mixing in mixer to grind;
(B) continue to add carbonate and/or bicarbonate makes basic carbonate raw material, the mass fraction of basic carbonate raw material is that 15 continuation mixing grind;
(C) then add oxygen evolution agent polyvidone/hydrogen peroxide complex compound, mass fraction be 5, the lubricant of additive of tablet, peppermint or lemon extract, food coloring, stir, mixing is sieved 100 orders, the powder mixed obtained;
Food coloring is light blue, ciba blue 2b, indigo carmine, indigo blue potassium, indigo, indigo two sulfuric acid sylvite, thioindigo, indigo naturalis look food coloring, and the mass fraction of described food coloring is 0.5;
(D) powder mixed step (C) obtained is through rotary pelleting machine compressing tablet, and compression force 18-20KN, sheet diameter is 22mm, hardness 60-80N, obtains described toothbrush sanitizing effervescent tablet.
The using method that this toothbrush cleaning foil is applied as disinfectant detergent is:
(A) a slice toothbrush cleaning foil is got, toothbrush cleaning foil is put into water and puts into about 100ml water, under acid material and the acting in conjunction of basic carbonate raw material, produce a large amount of bubble (carbonic acid gas), make the rapid disintegration of toothbrush cleaning foil and thawing, form the effervesce aqueous solution;
(B) toothbrush or other are gargled wash utensil and shallow contact daily necessities is immersed in 5-10 minute in the effervesce aqueous solution;
(C) take out, naturally dry with after tap water.
The above is only one embodiment of the present invention, it should be pointed out that for those skilled in the art, under the prerequisite not departing from the technology of the present invention principle, can also make some improvement, and these improvement also should be considered as protection scope of the present invention.
Claims (9)
1. a toothbrush cleaning foil, is characterized in that: described toothbrush cleaning foil is used for the sterilization of toothbrush; Or for gargling the sterilization washing apparatus; Or for the sterilization of the shallow contact daily necessities of toothbrush.
2. toothbrush cleaning foil according to claim 1, described toothbrush cleaning foil makes the effervescent tablet made by oxygen evolution agent by polyvidone/hydrogen peroxide complex compound, and its mass fraction is 0.1 ~ 10.
3. toothbrush cleaning foil according to claim 1 and 2, is characterized in that: described toothbrush cleaning foil also comprises basic carbonate raw material, and described basic carbonate raw material is carbonate and/or bicarbonate; The mass fraction of described carbonate and/or bicarbonate is 0.5 ~ 30.
4. toothbrush cleaning foil according to claim 1 and 2, is characterized in that: described toothbrush cleaning foil also includes acid material, and described acid material is selected from one or more the mixture in citric acid, malic acid, tartaric acid, fumaric acid; The mass fraction of described acid material is 1.0 ~ 20.
5. toothbrush cleaning foil according to claim 1 and 2, it is characterized in that: described toothbrush cleaning foil also includes additive of tablet, described additive of tablet comprises adhesive and lubricant, and described adhesive is polyvinylpyrrolidone, and described lubricant is superfine silica gel powder or talcum powder; The mass fraction of described additive of tablet is 1 ~ 20.
6. toothbrush cleaning foil according to claim 1 and 2, is characterized in that: described toothbrush cleaning foil also includes peppermint or lemon extract; The mass fraction of described peppermint or lemon extract is 0.01 ~ 1.0.
7. toothbrush cleaning foil according to claim 1 and 2, is characterized in that: described toothbrush cleaning foil also includes food coloring; Described food coloring is light blue, ciba blue 2b, indigo carmine, indigo blue potassium, indigo, indigo two sulfuric acid sylvite, thioindigo, indigo naturalis look food coloring; The mass fraction of described food coloring is 0.01 ~ 1.0.
8. prepare a preparation method for toothbrush cleaning foil according to claim 1, it is characterized in that: the processing step of this preparation method is:
(A) lubricant in acid material, additive of tablet is added mixing in mixer to grind;
(B) continue to add carbonate and/or bicarbonate makes basic carbonate raw material, continue mixing and grind;
(C) then add oxygen evolution agent, the lubricant of additive of tablet, peppermint or lemon extract, food coloring, stir, the powder mixed obtained;
(D) powder mixed step (C) obtained, through rotary pelleting machine compressing tablet, obtains described toothbrush sanitizing effervescent tablet.
9. the using method applied as disinfectant detergent of toothbrush cleaning foil according to claim 1, is characterized in that: the using method of this toothbrush cleaning foil is:
(A) a slice toothbrush cleaning foil is got, toothbrush cleaning foil is put into water and puts into about 100ml water, under acid material and the acting in conjunction of basic carbonate raw material, produce a large amount of bubble (carbonic acid gas), make the rapid disintegration of toothbrush cleaning foil and thawing, form the effervesce aqueous solution;
(B) toothbrush or other are gargled wash utensil and shallow contact daily necessities is immersed in 5-10 minute in the effervesce aqueous solution;
(C) take out, naturally dry with after tap water.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510660614.7A CN105248449B (en) | 2015-10-15 | 2015-10-15 | A kind of toothbrush cleansing tablet and preparation method thereof, application method |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510660614.7A CN105248449B (en) | 2015-10-15 | 2015-10-15 | A kind of toothbrush cleansing tablet and preparation method thereof, application method |
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| CN105248449A true CN105248449A (en) | 2016-01-20 |
| CN105248449B CN105248449B (en) | 2018-04-24 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111257408A (en) * | 2020-02-18 | 2020-06-09 | 广东省特种设备检测研究院珠海检测院 | A kind of effervescent tablet containing nanometer magnetic powder and its application |
| CN111307931A (en) * | 2020-02-18 | 2020-06-19 | 广东省特种设备检测研究院珠海检测院 | Effervescent tablet containing magnetic powder and preparation method thereof |
| CN111690480A (en) * | 2020-06-23 | 2020-09-22 | 刘晓彤 | Anti-inflammation and sterilization traditional Chinese medicine toothbrush cleaning sheet |
| CN111748415A (en) * | 2020-07-24 | 2020-10-09 | 广州立白企业集团有限公司 | Toothbrush sterilizing and cleaning effervescent tablet and preparation method thereof |
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| CN202654429U (en) * | 2011-12-16 | 2013-01-09 | 上海高丰医疗电器有限公司 | Disinfecting tablet for false tooth brush |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111257408A (en) * | 2020-02-18 | 2020-06-09 | 广东省特种设备检测研究院珠海检测院 | A kind of effervescent tablet containing nanometer magnetic powder and its application |
| CN111307931A (en) * | 2020-02-18 | 2020-06-19 | 广东省特种设备检测研究院珠海检测院 | Effervescent tablet containing magnetic powder and preparation method thereof |
| CN111690480A (en) * | 2020-06-23 | 2020-09-22 | 刘晓彤 | Anti-inflammation and sterilization traditional Chinese medicine toothbrush cleaning sheet |
| CN111748415A (en) * | 2020-07-24 | 2020-10-09 | 广州立白企业集团有限公司 | Toothbrush sterilizing and cleaning effervescent tablet and preparation method thereof |
| CN111748415B (en) * | 2020-07-24 | 2022-02-25 | 广州立白企业集团有限公司 | Toothbrush sterilizing and cleaning effervescent tablet and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN105248449B (en) | 2018-04-24 |
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