CN105158237A - Sulfur detector with room temperature cooling function - Google Patents

Sulfur detector with room temperature cooling function Download PDF

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Publication number
CN105158237A
CN105158237A CN201510527247.3A CN201510527247A CN105158237A CN 105158237 A CN105158237 A CN 105158237A CN 201510527247 A CN201510527247 A CN 201510527247A CN 105158237 A CN105158237 A CN 105158237A
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CN
China
Prior art keywords
room temperature
tray
temperature cooling
crucible
ice tray
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Pending
Application number
CN201510527247.3A
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Chinese (zh)
Inventor
班书昊
柳铭
李晓艳
华同曙
蒋学东
徐然
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Changzhou University
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Changzhou University
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Publication date
Application filed by Changzhou University filed Critical Changzhou University
Priority to CN201510527247.3A priority Critical patent/CN105158237A/en
Publication of CN105158237A publication Critical patent/CN105158237A/en
Pending legal-status Critical Current

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  • Investigating Or Analyzing Materials Using Thermal Means (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)

Abstract

The invention discloses an aldrin sulfur detector with a room temperature cooling function, and belongs to the field of automatic measuring equipment of sulfur contents in coal. The sulfur detector comprises an aldrin sample manufacturing device, a combustion furnace, a room temperature cooling device, a solution stirring and filtering device, a methyl orange indicating device, a second filtering device, a room temperature weighing device and a control system which are fixed on a bottom plate; the room temperature cooling device is arranged between the combustion furnace and the solution stirring and filtering device and comprises a tray support, a tray, a fan, a main container and an ice block container; the tray support is assembled on the bottom plate; the tray is assembled on the tray support; and the fan, the main container and the ice block container are assembled right above the tray. By the aldrin sulfur detector with the room temperature cooling function, a high-temperature crucible can be quickly cooled down at room temperature, and improvement of sulfur detection efficiency is guaranteed.

Description

There is the sulphur meter of room temperature refrigerating function
Technical field
The present invention relates generally to the automatic measuring equipment field of sulfur content in coal amount, refers in particular to a kind of Emhorn sulphur meter with room temperature refrigerating function.
Background technology
Sulphur is one of important indicator evaluating ature of coal.In prior art, in order to measure the sulfur content in combustible accurately and rapidly, the general constant sulphur appliance that adopts is as conventional measuring equipment.In various measuring equipment, coulomb is all adopted to survey sulphur method.Coulomb surveys sulphur method to be needed with pump as power source, and the mode of employing continuous air extraction, continuous coverage measures.Due in gas containing sulphur concentration time to time change, therefore sulfur content is difficult to Accurate Determining, and the pump life-span also shortens because of laod unbalance simultaneously.
Germany Chinese mugwort scholar is stuck in and within 1874, has formulated a classical Chinese mugwort scholar and survey sulphur method, is the standard method of the general mensuration full content of Sulphur in coal content in various countries at present, has that accuracy is high, the advantage such as mensuration in batch.Emhorn is surveyed in sulphur process, and need crucible to take out from muffle furnace, cool to room temperature, is configured to solution afterwards again.Temperature due to crucible is about 800 DEG C, and rely on nature cooling to need the longer time, this obviously have impact on conventional efficient.
Summary of the invention
The technical matters that the present invention need solve is: the technical matters existed for prior art, the invention provides a kind of Emhorn sulphur meter with room temperature refrigerating function, it can realize cooling the room temperature of high-temperature crucibles fast, for instrument full automation and the raising of surveying sulphur efficiency provide favourable guarantee.
In order to solve the problem, the solution that the present invention proposes is: a kind of Emhorn sulphur meter with room temperature refrigerating function, it comprises the Emhorn sample making device be fixed on base plate, combustion furnace, room temperature cooling device, solution agitation and filtration device, methyl orange indicating device, second filtration unit, room temperature meausring apparatus and control system, described room temperature cooling device is arranged at described combustion furnace, between described solution agitation and filtration device, it is characterized in that: described room temperature cooling device comprises the tray supporter be installed on described base plate, be installed in the pallet on described tray supporter, be installed in the fan directly over described pallet, primary tank and ice tray, described pallet is provided with multiple crucible hole, and the center of circle of described crucible hole is circumferentially same, described primary tank is the hollow cylinder container of bottom opening, and its internal diameter equals the external diameter of described ice tray, described crucible to be cooled is positioned in described ice tray, and described ice tray is positioned in described primary tank, and described primary tank is installed in the crucible hole of pallet.
The material of ice tray of the present invention is solid water, and its shape is that an its center cuts out a round platform, and the size of described round platform equals the base profile size of crucible.
Compared with prior art, the invention has the advantages that: the present invention have the Emhorn sulphur meter structure of room temperature refrigerating function simple, by the ice tray be positioned in primary tank, high-temperature crucibles the latter half is cooled fast, solid ice absorbs heat and is heated and becomes water from crucible, and the water of generation flows out from the base apertures of primary tank; The present invention is also provided with fan simultaneously above pallet, cools the first half of crucible.It can thus be appreciated that the crucible taken out from combustion furnace only needs the very short time just can be quickly cooled to room temperature, significantly improve complete machine and survey sulphur efficiency.
Accompanying drawing explanation
Fig. 1 is the plan structure schematic diagram with the Emhorn sulphur meter of room temperature refrigerating function of the present invention.
Fig. 2 is the structural principle schematic diagram of room temperature cooling device of the present invention.
In figure, 1-Emhorn sample making device; 2-combustion furnace; 3-room temperature cooling device; 4-solution agitation and filtration device; 5-methyl orange indicating device; 6-the second filtration unit; 7-room temperature meausring apparatus; 8-control system; 9-base plate; 31-fan; 32-crucible; 33-ice tray; 34-primary tank; 35-pallet; 36-crucible hole; 37-tray supporter.
Embodiment
Below with reference to the drawings and specific embodiments, the present invention is described in further detail.
Shown in Figure 1, the Emhorn sulphur meter with room temperature refrigerating function of the present invention, it comprises the Emhorn sample making device 1 be fixed on base plate 9, combustion furnace 2, room temperature cooling device 3, solution agitation and filtration device 4, methyl orange indicating device 5, second filtration unit 6, room temperature meausring apparatus 7 and control system 8, room temperature cooling device 3 is arranged between combustion furnace 2 and solution agitation and filtration device 4, it is characterized in that: room temperature cooling device 3 comprises the tray supporter 37 be installed on base plate 9, be installed in the pallet 35 on tray supporter 37, be installed in the fan 31 directly over pallet 35, primary tank 34 and ice tray 33, pallet 35 is provided with multiple crucible hole 36, and the center of circle of crucible hole 36 is circumferentially same, primary tank 34 is the hollow cylinder container of bottom opening, and its internal diameter equals the external diameter of ice tray 33, crucible 32 to be cooled is positioned in ice tray 33, and ice tray 33 is positioned in primary tank 34, and primary tank 34 is installed in the crucible hole 36 of pallet 35.
Shown in Fig. 1 and Fig. 2, the material of ice tray 33 is solid water, and its shape is that an its center cuts out a round platform, and the size of round platform equals the base profile size of crucible 32.
Cooling principle: the high-temperature crucibles 32 of taking out from combustion furnace 2 is positioned in ice tray 33, solid ice, by the latter half of contact crucible 32, absorbs heat liquefy water, and flows out from the hole of primary tank 34 base plate; Simultaneously, start the fan 31 above pallet 35, be positioned at the first half crucible 32 of ice tray 33 outside by air flowing cooling; High-temperature crucibles 32, under the acting in conjunction of fan 31 and ice tray 33, can be quickly cooled to room temperature.
These are only one of some embodiments of the present invention, but be not limited to the textural association form of above-described embodiment.

Claims (2)

1. one kind has the Emhorn sulphur meter of room temperature refrigerating function, it comprises the Emhorn sample making device (1) be fixed on base plate (9), combustion furnace (2), room temperature cooling device (3), solution agitation and filtration device (4), methyl orange indicating device (5), second filtration unit (6), room temperature meausring apparatus (7) and control system (8), described room temperature cooling device (3) is arranged between described combustion furnace (2) and described solution agitation and filtration device (4), it is characterized in that: described room temperature cooling device (3) comprises the tray supporter (37) be installed on described base plate (9), be installed in the pallet (35) on described tray supporter (37), be installed in the fan (31) directly over described pallet (35), primary tank (34) and ice tray (33), described pallet (35) is provided with multiple crucible hole (36), and the center of circle of described crucible hole (36) is circumferentially same, the hollow cylinder container that described primary tank (34) is bottom opening, its internal diameter equals the external diameter of described ice tray (33), described crucible (32) to be cooled is positioned in described ice tray (33), described ice tray (33) is positioned in described primary tank (34), and described primary tank (34) is installed in the crucible hole (36) of pallet (35).
2. the Emhorn sulphur meter with room temperature refrigerating function according to claim 1, it is characterized in that: the material of described ice tray (33) is solid water, its shape is that an its center cuts out a round platform, and the size of described round platform equals the base profile size of crucible (32).
CN201510527247.3A 2015-08-25 2015-08-25 Sulfur detector with room temperature cooling function Pending CN105158237A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510527247.3A CN105158237A (en) 2015-08-25 2015-08-25 Sulfur detector with room temperature cooling function

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Application Number Priority Date Filing Date Title
CN201510527247.3A CN105158237A (en) 2015-08-25 2015-08-25 Sulfur detector with room temperature cooling function

Publications (1)

Publication Number Publication Date
CN105158237A true CN105158237A (en) 2015-12-16

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CN201510527247.3A Pending CN105158237A (en) 2015-08-25 2015-08-25 Sulfur detector with room temperature cooling function

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Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2003029501A1 (en) * 2001-10-03 2003-04-10 Daniel Davitz High percentage zinc alloy for use with silver or gold
CN1865466A (en) * 2006-06-22 2006-11-22 曹大力 Method for preparing aluminum-titanium-carbon intermediate alloy
CN101264871A (en) * 2008-03-27 2008-09-17 上海交通大学 Method for preparing tetracalcium phosphate from natural bone powder
US20090142669A1 (en) * 2007-12-03 2009-06-04 Seiko Epson Corporation Sulfide-based lithium-ion-conducting solid electrolyte glass, all-solid lithium secondary battery, and method for manufacturing all-solid lithium secondary battery
CN201628433U (en) * 2010-03-19 2010-11-10 深圳市艾阿尔电气有限公司 Molten chemical rapid cooling device
CN201666861U (en) * 2010-03-05 2010-12-08 攀钢集团钢铁钒钛股份有限公司 Device for testing weight loss on heating of solid object
CN102344997A (en) * 2011-10-02 2012-02-08 北京科技大学 High-calcium high-aluminum fluorine-free refining slags for producing high purity steel and refining method
CN102967494A (en) * 2012-10-30 2013-03-13 中国科学院上海应用物理研究所 Molten salt sample preparation device, prepared molten salt sample and preparation and crystallization method thereof
CN203591869U (en) * 2013-11-07 2014-05-14 山西农业大学 Auxiliary device for ice mortars
CN204550691U (en) * 2015-04-20 2015-08-12 山东海源光电科技有限公司 Cooling crucible device

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2003029501A1 (en) * 2001-10-03 2003-04-10 Daniel Davitz High percentage zinc alloy for use with silver or gold
CN1865466A (en) * 2006-06-22 2006-11-22 曹大力 Method for preparing aluminum-titanium-carbon intermediate alloy
US20090142669A1 (en) * 2007-12-03 2009-06-04 Seiko Epson Corporation Sulfide-based lithium-ion-conducting solid electrolyte glass, all-solid lithium secondary battery, and method for manufacturing all-solid lithium secondary battery
CN101264871A (en) * 2008-03-27 2008-09-17 上海交通大学 Method for preparing tetracalcium phosphate from natural bone powder
CN201666861U (en) * 2010-03-05 2010-12-08 攀钢集团钢铁钒钛股份有限公司 Device for testing weight loss on heating of solid object
CN201628433U (en) * 2010-03-19 2010-11-10 深圳市艾阿尔电气有限公司 Molten chemical rapid cooling device
CN102344997A (en) * 2011-10-02 2012-02-08 北京科技大学 High-calcium high-aluminum fluorine-free refining slags for producing high purity steel and refining method
CN102967494A (en) * 2012-10-30 2013-03-13 中国科学院上海应用物理研究所 Molten salt sample preparation device, prepared molten salt sample and preparation and crystallization method thereof
CN203591869U (en) * 2013-11-07 2014-05-14 山西农业大学 Auxiliary device for ice mortars
CN204550691U (en) * 2015-04-20 2015-08-12 山东海源光电科技有限公司 Cooling crucible device

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
唐军等: "《煤炭试验仪器设备、采样制样、试验方法及标准使用手册 第3卷》", 30 April 2005 *
张福捐: "《无机化学实验》", 31 August 2009 *

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Application publication date: 20151216