CN105053263A - Preparation method of peony seed oil and apricot kernel oil blend edible oil - Google Patents
Preparation method of peony seed oil and apricot kernel oil blend edible oil Download PDFInfo
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- CN105053263A CN105053263A CN201510383125.1A CN201510383125A CN105053263A CN 105053263 A CN105053263 A CN 105053263A CN 201510383125 A CN201510383125 A CN 201510383125A CN 105053263 A CN105053263 A CN 105053263A
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- 235000006484 Paeonia officinalis Nutrition 0.000 title claims abstract description 73
- 235000015112 vegetable and seed oil Nutrition 0.000 title claims abstract description 48
- 239000001944 prunus armeniaca kernel oil Substances 0.000 title claims abstract description 42
- 239000000203 mixture Substances 0.000 title claims abstract description 19
- 239000008157 edible vegetable oil Substances 0.000 title claims abstract description 10
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- 244000170916 Paeonia officinalis Species 0.000 title abstract 2
- 238000000605 extraction Methods 0.000 claims abstract description 24
- 239000003921 oil Substances 0.000 claims abstract description 19
- 235000019198 oils Nutrition 0.000 claims abstract description 19
- 238000003756 stirring Methods 0.000 claims abstract description 13
- 238000000926 separation method Methods 0.000 claims abstract description 11
- 238000000034 method Methods 0.000 claims abstract description 9
- 238000001035 drying Methods 0.000 claims abstract description 5
- 241000736199 Paeonia Species 0.000 claims description 71
- 238000002156 mixing Methods 0.000 claims description 38
- 239000010779 crude oil Substances 0.000 claims description 24
- 244000144725 Amygdalus communis Species 0.000 claims description 20
- 235000011437 Amygdalus communis Nutrition 0.000 claims description 20
- 235000020224 almond Nutrition 0.000 claims description 20
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 16
- 240000005001 Paeonia suffruticosa Species 0.000 claims description 12
- 235000003889 Paeonia suffruticosa Nutrition 0.000 claims description 12
- 239000000843 powder Substances 0.000 claims description 12
- 239000006228 supernatant Substances 0.000 claims description 12
- 239000004570 mortar (masonry) Substances 0.000 claims description 8
- 239000000047 product Substances 0.000 claims description 6
- 230000015572 biosynthetic process Effects 0.000 claims description 4
- 238000005352 clarification Methods 0.000 claims description 4
- 238000004140 cleaning Methods 0.000 claims description 4
- 230000006837 decompression Effects 0.000 claims description 4
- 238000004332 deodorization Methods 0.000 claims description 4
- 239000006185 dispersion Substances 0.000 claims description 4
- 239000012530 fluid Substances 0.000 claims description 4
- 238000002309 gasification Methods 0.000 claims description 4
- 238000007689 inspection Methods 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 4
- 239000002245 particle Substances 0.000 claims description 4
- 238000000746 purification Methods 0.000 claims description 4
- 238000007789 sealing Methods 0.000 claims description 4
- 230000003068 static effect Effects 0.000 claims description 4
- 239000006200 vaporizer Substances 0.000 claims description 4
- 238000005516 engineering process Methods 0.000 abstract description 3
- 239000002253 acid Substances 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 230000003647 oxidation Effects 0.000 abstract description 2
- 238000007254 oxidation reaction Methods 0.000 abstract description 2
- 238000000199 molecular distillation Methods 0.000 abstract 2
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- 238000000194 supercritical-fluid extraction Methods 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 6
- 206010011224 Cough Diseases 0.000 description 4
- 210000004072 lung Anatomy 0.000 description 4
- 239000003205 fragrance Substances 0.000 description 3
- 235000016709 nutrition Nutrition 0.000 description 3
- 230000035764 nutrition Effects 0.000 description 3
- 206010010774 Constipation Diseases 0.000 description 2
- 206010062717 Increased upper airway secretion Diseases 0.000 description 2
- 208000006673 asthma Diseases 0.000 description 2
- 230000007812 deficiency Effects 0.000 description 2
- 235000021185 dessert Nutrition 0.000 description 2
- 201000006549 dyspepsia Diseases 0.000 description 2
- 235000008390 olive oil Nutrition 0.000 description 2
- 239000004006 olive oil Substances 0.000 description 2
- 208000026435 phlegm Diseases 0.000 description 2
- 210000000582 semen Anatomy 0.000 description 2
- 208000024891 symptom Diseases 0.000 description 2
- 244000298697 Actinidia deliciosa Species 0.000 description 1
- 235000009436 Actinidia deliciosa Nutrition 0.000 description 1
- DTOSIQBPPRVQHS-PDBXOOCHSA-N alpha-linolenic acid Chemical compound CC\C=C/C\C=C/C\C=C/CCCCCCCC(O)=O DTOSIQBPPRVQHS-PDBXOOCHSA-N 0.000 description 1
- 235000020661 alpha-linolenic acid Nutrition 0.000 description 1
- 230000036528 appetite Effects 0.000 description 1
- 235000019789 appetite Nutrition 0.000 description 1
- 238000013475 authorization Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 208000013116 chronic cough Diseases 0.000 description 1
- 230000001684 chronic effect Effects 0.000 description 1
- 235000014510 cooky Nutrition 0.000 description 1
- 210000004351 coronary vessel Anatomy 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 208000017574 dry cough Diseases 0.000 description 1
- 230000037406 food intake Effects 0.000 description 1
- 235000012631 food intake Nutrition 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 239000008141 laxative Substances 0.000 description 1
- 230000002475 laxative effect Effects 0.000 description 1
- 229960004488 linolenic acid Drugs 0.000 description 1
- KQQKGWQCNNTQJW-UHFFFAOYSA-N linolenic acid Natural products CC=CCCC=CCC=CCCCCCCCC(O)=O KQQKGWQCNNTQJW-UHFFFAOYSA-N 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000000116 mitigating effect Effects 0.000 description 1
- 235000019488 nut oil Nutrition 0.000 description 1
- 239000010466 nut oil Substances 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 239000010461 other edible oil Substances 0.000 description 1
- 235000020777 polyunsaturated fatty acids Nutrition 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
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- Fats And Perfumes (AREA)
- Edible Oils And Fats (AREA)
Abstract
A preparation method of peony seed oil and apricot kernel oil blend edible oil comprises the steps of drying, parching, supercritical extraction, molecular distillation, and mixing-heating-stirring, the operating temperature is low, and the heating time is short, so oil oxidation and rancidity induced by high temperature can be avoided; the separation degree and the product yield are high; and molecular distillation also can reduce the acid value of oil, so efficient extraction, separation, no impurities and high purity of the extraction product are realized. The method has the advantages of simple operating technology, short extraction time, cost reduction and production efficiency improvement.
Description
Technical field
The present invention relates to edible oil field, specifically the preparation method of a kind of peony seed oil and apricot kernel oil blending edible oil.
Background technology
Peony seed oil is also containing abundant polyunsaturated fatty acid, and its nutritive value is considerably beyond being called as " oil of human health " olive oil, and linolenic acid content is more than 200 times of olive oil.Many index is also all planted higher than other oil.Again not easily oxide deposition at positions such as human vas wall, heart coronary arteries.These compositions make it in medical science and nutrition, play important function and become desirable edible oil just.Say without exaggeration that, the nutrition and health care effect of peony seed oil is that other edible oil is incomparable.The peony seeds deep processing product of listing are little, this greatly reduces the economic worth of China's peony seeds.
A kind of kiwifruit nut oil and extracting method thereof disclosed in Chinese patent Authorization Notice No. CN1483795, adopt CO_2 supercritical technology, obtained essential oil of low quality, and complex process, extraction time is long, and production cost is high, and yield is low.
In view of the foregoing, the preparation method of a kind of peony seed oil and apricot kernel oil blending edible oil is now developed.
Summary of the invention
The object of the invention is to overcome deficiency of the prior art, the preparation method of a kind of peony seed oil and apricot kernel oil blending edible oil is provided, the ready-mixed oil prepared by the method not only has nutrition, the health care of peony seed oil and almond seed concurrently, and greatly improves the fragrance mouthfeel of peony seed oil.
The present invention to achieve these goals, adopts following technical scheme: the preparation method of a kind of peony seed oil and apricot kernel oil blending edible oil:
Step 1: after drying that peony seeds is shelled, formation particle diameter is that the tree peony powder of 30-50 object is for subsequent use, tree peony powder is put into pot and carries out parch, parch temperature is 120-150 DEG C, parch time 40-60 minute, almond after decortication is put into another pot and carries out parch, parch temperature is 120-145 DEG C, parch 50-60 minute, be 3: 1 mixing by the tree peony powder after parch and almond according to mass ratio, mixture is stirred 20-35 minute, stop stirring, mixture is put into airtight clutch scheming afterwards, be centrifugal 10-25 minute under the condition of 1000r/min at rotating speed, in airtight centrifuge, Stress control takes out mixture 250-400kg and is encased in extraction kettle after 0.58Mpa, start extraction, extraction temperature is 35-55 DEG C, extracting pressure is 25-28Mpa, extraction time 120-150min, close extractor, inspection guarantees that sealing is tight, use high-pressure pump that the liquid CO 2 in hold-up tank is pumped into vaporizer, gasification is input in extractor after critical fluids state, extract, pressure in setting extractor is 10-20Mpa, temperature is 30-40 DEG C, CO2 after extraction and mixture fluid-mixing input separator and carry out decompression separation, pressure in separator is 4-10Mpa, temperature is 30-40 DEG C, CO2 after separation through liquefier liquefaction directly the defeated time hold-up tank of 20-30 DEG C recycle for next round extract and separate, each takes turns extract and separate time 2-8 hour, obtained elementary peony seed oil and apricot kernel oil mixing crude oil after being separated, for subsequent use,
Step 2: the elementary peony seed oil obtained by step 1 and apricot kernel oil mixing crude oil join in molecular still, vacuum in setting molecular still is 1.0-2.0Pa, temperature is 60-70 DEG C, rotating brush film rotating speed in molecular still is 120r/min, until elementary peony seed oil and apricot kernel oil mixing crude oil are collected by heavy phase collecting tank and light phase collecting tank completely, collect in heavy phase collecting tank and obtain peony seed oil and apricot kernel oil mixing crude oil, for subsequent use;
Step 3: the peony seed oil obtained by step 2 and apricot kernel oil mixing crude oil join in molecular still again, the vacuum reset in molecular still is 1.0-2.0Pa, temperature is 60-70 DEG C, rotating brush film rotating speed in molecular still is 120r/min, until peony seed oil and apricot kernel oil mixing crude oil are collected by heavy phase collecting tank and light phase collecting tank completely, collect in heavy phase collecting tank and obtain peony seed oil and apricot kernel oil miscella;
Step 4: peony petal cleaning and chopping is put into mortar, in mortar, add quality be percent concentration is the ethanol of 90-95%, the ethanol contend that every gram of peony petal is corresponding is 45-55ml, extract supernatant, supernatant is put into the centrifugal 10-15min of centrifuge that rotating speed is 3000r/min, extract supernatant and namely obtain peony petal extract;
Step 5: take peony petal extract, and joined peony seed oil and apricot kernel oil miscella, add after stirring in dispersion machine, under 18000r/min condition, disperse 5-8 minute, static 2-3h, obtained mixed liquor is for subsequent use;
Step 6: agitator put into by mixed liquor step 5 obtained is stir under the condition of 1000r/min at rotating speed, till mixed liquor clarification, obtains ready-mixed oil, namely obtains ready-mixed oil finished product by after ready-mixed oil purification, decolouring, deodorization process.
The invention has the beneficial effects as follows: almond is divided into dessert almond and semen armeniacae amarae two kinds.The almond that south China produces belongs to dessert almond (having another name called southern almond), taste is micro-sweet, fine and smooth, is used for eating, and also can be used as raw material and adds in cake, cookies and dish, there is the effects such as moistening lung, cough-relieving, laxation, have certain mitigation to the disease such as dry cough without phlegm, chronic cough of deficiency lung; The almond that is produced from the north then belongs to semen armeniacae amarae (having another name called northern almond), bitter, does medicinal, the effect of have moistening lung, relievining asthma more, evident in efficacy for the symptom such as many phlegm, cough, asthma caused because of cold; Three large effects of almond are enumerated: moistening lung, clear having indigestion in Chinese medicine ancient books and records Compendium of Material Medica, loose stagnant.Clear having indigestion says that almond can help digest, relief of constipation symptom; " modern Practical Chinese medicinal " is recorded: " almond is for oral administration has laxative effective, and has the effect of nourishing." for old chronic constipation person, take almond effect better.
The present invention promotes fragrance and the mouthfeel of peony seed oil greatly by adding apricot kernel oil mediation in peony seed oil, in peony seed oil and apricot kernel oil ready-mixed oil, add peony petal extract simultaneously, make the delicate fragrance containing peony petal in ready-mixed oil, effectively can improve appetite, increase food-intake, promote health.
The preparation method of peony seed oil in the present invention, adopt the method that supercritical extract and molecular clock be combined with each other, not only operating temperature is low, heated time is short, the oxidation of the grease that high temperature can be avoided to cause with become sour, and the yield of separation degree and product is higher, and molecular clock can also reduce the acid value of peony seeds, do not need to carry out centrifugally operated, reduce cost.
Detailed description of the invention
Below in conjunction with embodiment and detailed description of the invention, the present invention is described in further detail:
Embodiment 1
Step 1: after drying that peony seeds is shelled, formation particle diameter is that the tree peony powder of 43 objects is for subsequent use, tree peony powder is put into pot and carries out parch, parch temperature is 145 DEG C, 46 minutes parch time, almond after decortication is put into another pot and carries out parch, parch temperature is 135 DEG C, parch 56 minutes, be 3: 1 mixing by the tree peony powder after parch and almond according to mass ratio, mixture is stirred 28 minutes, stop stirring, mixture is put into airtight clutch scheming afterwards, be under the condition of 1000r/min centrifugal 19 minutes at rotating speed, in airtight centrifuge, Stress control takes out mixture 290kg and is encased in extraction kettle after 0.58Mpa, start extraction, extraction temperature is 41 DEG C, extracting pressure is 27Mpa, extraction time 142min, close extractor, inspection guarantees that sealing is tight, use high-pressure pump that the liquid CO 2 in hold-up tank is pumped into vaporizer, gasification is input in extractor after critical fluids state, extract, pressure in setting extractor is 13Mpa, temperature is 35 DEG C, CO2 after extraction and mixture fluid-mixing input separator and carry out decompression separation, pressure in separator is 5Mpa, temperature is 34 DEG C, CO2 after separation through liquefier liquefaction directly the defeated time hold-up tank of 20-30 DEG C recycle for next round extract and separate, each takes turns 4 hours extract and separate time, obtained elementary peony seed oil and apricot kernel oil mixing crude oil after being separated, for subsequent use,
Step 2: the elementary peony seed oil obtained by step 1 and apricot kernel oil mixing crude oil join in molecular still, vacuum in setting molecular still is 1.8Pa, temperature is 66 DEG C, rotating brush film rotating speed in molecular still is 120r/min, until elementary peony seed oil and apricot kernel oil mixing crude oil are collected by heavy phase collecting tank and light phase collecting tank completely, collect in heavy phase collecting tank and obtain peony seed oil and apricot kernel oil mixing crude oil, for subsequent use;
Step 3: the peony seed oil obtained by step 2 and apricot kernel oil mixing crude oil join in molecular still again, the vacuum reset in molecular still is 1.6Pa, temperature is 66 DEG C, rotating brush film rotating speed in molecular still is 120r/min, until peony seed oil and apricot kernel oil mixing crude oil are collected by heavy phase collecting tank and light phase collecting tank completely, collect in heavy phase collecting tank and obtain peony seed oil and apricot kernel oil miscella;
Step 4: peony petal cleaning and chopping is put into mortar, in mortar, add quality be percent concentration be 94% ethanol, the ethanol contend that every gram of peony petal is corresponding is 52ml, extract supernatant, supernatant is put into the centrifugal 13min of centrifuge that rotating speed is 3000r/min, extract supernatant and namely obtain peony petal extract;
Step 5: take peony petal extract, and joined peony seed oil and apricot kernel oil miscella, add after stirring in dispersion machine, disperse 6 minutes, static 2.5h under 18000r/min condition, obtained mixed liquor is for subsequent use;
Step 6: agitator put into by mixed liquor step 5 obtained is stir under the condition of 1000r/min at rotating speed, till mixed liquor clarification, obtains ready-mixed oil, namely obtains ready-mixed oil finished product by after ready-mixed oil purification, decolouring, deodorization process.
Embodiment 2
Step 1: after drying that peony seeds is shelled, formation particle diameter is that the tree peony powder of 43 objects is for subsequent use, tree peony powder is put into pot and carries out parch, parch temperature is 128 DEG C, 49 minutes parch time, almond after decortication is put into another pot and carries out parch, parch temperature is 132 DEG C, parch 56 minutes, be 3: 1 mixing by the tree peony powder after parch and almond according to mass ratio, mixture is stirred 29 minutes, stop stirring, mixture is put into airtight clutch scheming afterwards, be under the condition of 1000r/min centrifugal 19 minutes at rotating speed, in airtight centrifuge, Stress control takes out mixture 350kg and is encased in extraction kettle after 0.58Mpa, start extraction, extraction temperature is 53 DEG C, extracting pressure is 27Mpa, extraction time 137min, close extractor, inspection guarantees that sealing is tight, use high-pressure pump that the liquid CO 2 in hold-up tank is pumped into vaporizer, gasification is input in extractor after critical fluids state, extract, pressure in setting extractor is 14Mpa, temperature is 35 DEG C, CO2 after extraction and mixture fluid-mixing input separator and carry out decompression separation, pressure in separator is 7Mpa, temperature is 35 DEG C, CO2 after separation through liquefier liquefaction directly the defeated time hold-up tank of 20-30 DEG C recycle for next round extract and separate, each takes turns 6 hours extract and separate time, obtained elementary peony seed oil and apricot kernel oil mixing crude oil after being separated, for subsequent use,
Step 2: the elementary peony seed oil obtained by step 1 and apricot kernel oil mixing crude oil join in molecular still, vacuum in setting molecular still is 1.9Pa, temperature is 66 DEG C, rotating brush film rotating speed in molecular still is 120r/min, until elementary peony seed oil and apricot kernel oil mixing crude oil are collected by heavy phase collecting tank and light phase collecting tank completely, collect in heavy phase collecting tank and obtain peony seed oil and apricot kernel oil mixing crude oil, for subsequent use;
Step 3: the peony seed oil obtained by step 2 and apricot kernel oil mixing crude oil join in molecular still again, the vacuum reset in molecular still is 1.3Pa, temperature is 66 DEG C, rotating brush film rotating speed in molecular still is 120r/min, until peony seed oil and apricot kernel oil mixing crude oil are collected by heavy phase collecting tank and light phase collecting tank completely, collect in heavy phase collecting tank and obtain peony seed oil and apricot kernel oil miscella;
Step 4: peony petal cleaning and chopping is put into mortar, in mortar, add quality be percent concentration be 92% ethanol, the ethanol contend that every gram of peony petal is corresponding is 49ml, extract supernatant, supernatant is put into the centrifugal 13min of centrifuge that rotating speed is 3000r/min, extract supernatant and namely obtain peony petal extract;
Step 5: take peony petal extract, and joined peony seed oil and apricot kernel oil miscella, add after stirring in dispersion machine, disperse 7 minutes, static 2.6h under 18000r/min condition, obtained mixed liquor is for subsequent use;
Step 6: agitator put into by mixed liquor step 5 obtained is stir under the condition of 1000r/min at rotating speed, till mixed liquor clarification, obtains ready-mixed oil, namely obtains ready-mixed oil finished product by after ready-mixed oil purification, decolouring, deodorization process.
Claims (1)
1. a preparation method for peony seed oil and apricot kernel oil blending edible oil, is characterized in that:
Step 1: after drying that peony seeds is shelled, formation particle diameter is that the tree peony powder of 30-50 object is for subsequent use, tree peony powder is put into pot and carries out parch, parch temperature is 120-150 DEG C, parch time 40-60 minute, almond after decortication is put into another pot and carries out parch, parch temperature is 120-145 DEG C, parch 50-60 minute, be 3: 1 mixing by the tree peony powder after parch and almond according to mass ratio, mixture is stirred 20-35 minute, stop stirring, mixture is put into airtight clutch scheming afterwards, be centrifugal 10-25 minute under the condition of 1000r/min at rotating speed, in airtight centrifuge, Stress control takes out mixture 250-400kg and is encased in extraction kettle after 0.58Mpa, start extraction, extraction temperature is 35-55 DEG C, extracting pressure is 25-28Mpa, extraction time 120-150min, close extractor, inspection guarantees that sealing is tight, use high-pressure pump that the liquid CO 2 in hold-up tank is pumped into vaporizer, gasification is input in extractor after critical fluids state, extract, pressure in setting extractor is 10-20Mpa, temperature is 30-40 DEG C, CO2 after extraction and mixture fluid-mixing input separator and carry out decompression separation, pressure in separator is 4-10Mpa, temperature is 30-40 DEG C, CO2 after separation through liquefier liquefaction directly the defeated time hold-up tank of 20-30 DEG C recycle for next round extract and separate, each takes turns extract and separate time 2-8 hour, obtained elementary peony seed oil and apricot kernel oil mixing crude oil after being separated, for subsequent use,
Step 2: the elementary peony seed oil obtained by step 1 and apricot kernel oil mixing crude oil join in molecular still, vacuum in setting molecular still is 1.0-2.0Pa, temperature is 60-70 DEG C, rotating brush film rotating speed in molecular still is 120r/min, until elementary peony seed oil and apricot kernel oil mixing crude oil are collected by heavy phase collecting tank and light phase collecting tank completely, collect in heavy phase collecting tank and obtain peony seed oil and apricot kernel oil mixing crude oil, for subsequent use;
Step 3: the peony seed oil obtained by step 2 and apricot kernel oil mixing crude oil join in molecular still again, the vacuum reset in molecular still is 1.0-2.0Pa, temperature is 60-70 DEG C, rotating brush film rotating speed in molecular still is 120r/min, until peony seed oil and apricot kernel oil mixing crude oil are collected by heavy phase collecting tank and light phase collecting tank completely, collect in heavy phase collecting tank and obtain peony seed oil and apricot kernel oil miscella;
Step 4: peony petal cleaning and chopping is put into mortar, in mortar, add quality be percent concentration is the ethanol of 90-95%, the ethanol contend that every gram of peony petal is corresponding is 45-55ml, extract supernatant, supernatant is put into the centrifugal 10-15min of centrifuge that rotating speed is 3000r/min, extract supernatant and namely obtain peony petal extract;
Step 5: take peony petal extract, and joined peony seed oil and apricot kernel oil miscella, add after stirring in dispersion machine, under 18000r/min condition, disperse 5-8 minute, static 2-3h, obtained mixed liquor is for subsequent use;
Step 6: agitator put into by mixed liquor step 5 obtained is stir under the condition of 1000r/min at rotating speed, till mixed liquor clarification, obtains ready-mixed oil, namely obtains ready-mixed oil finished product by after ready-mixed oil purification, decolouring, deodorization process.
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| CN107287026A (en) * | 2017-08-11 | 2017-10-24 | 洛阳泽达慧康医药科技有限公司 | A kind of peony seed oil depickling extracting method |
| CN114521655A (en) * | 2022-01-27 | 2022-05-24 | 华南理工大学 | Intestinal tract probiotic promoter containing medium-long chain triglyceride in almond oil and preparation method and application thereof |
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Application publication date: 20151118 |