CN105036814B - A kind of production method of natural cavity stone imitation glazed tile and its unfired brick structure of acquisition - Google Patents

A kind of production method of natural cavity stone imitation glazed tile and its unfired brick structure of acquisition Download PDF

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Publication number
CN105036814B
CN105036814B CN201510354863.3A CN201510354863A CN105036814B CN 105036814 B CN105036814 B CN 105036814B CN 201510354863 A CN201510354863 A CN 201510354863A CN 105036814 B CN105036814 B CN 105036814B
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low temperature
glaze
charity
adobe
production
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CN201510354863.3A
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CN105036814A (en
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丘云灵
金国庭
周燕
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佛山市东鹏陶瓷有限公司
广东东鹏控股股份有限公司
清远纳福娜陶瓷有限公司
丰城市东鹏陶瓷有限公司
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Abstract

A kind of production method of natural cavity stone imitation glazed tile and its unfired brick structure of acquisition, comprise the following steps:A, the adobe surface charity ground-coat enamel after shaping and drying;B, charity low temperature glaze:Charity low temperature glaze in adobe after step A stamps;C, stamp is handled:Stamp is carried out in the adobe that step B is obtained;D, charity clear frit:The adobe charity clear frit obtained to step C;E, polishing is fired, obtains finished product.The present invention proposes a kind of production method of the high imitative hole stone glazed tile of emulator, and its color and luster is rich and changeful, and hole stone effect controllability is high.

Description

A kind of production method of natural cavity stone imitation glazed tile and its unfired brick structure of acquisition
Technical field
The present invention relates to building material technical field, more particularly to a kind of production method of natural cavity stone imitation glazed tile and its The unfired brick structure of acquisition.
Background technology
Hole stone, scientific name are called calcareous tufa, English name:(Travertine) it is a kind of porous rock, so usual people Also it is its hole stone.Hole stone belongs to continental deposit rock, and it is a kind of deposit of calcium carbonate.Hole stone is mostly formed at rich in calcium carbonate Lime stone landform, formed by calcium calcium carbonate soluble in water and other mineral depositions in riverbed, lakebed and other places.Due to It sometimes appear that hole, simultaneously because the main component of its own is calcium carbonate again, itself just holds very much during accumulate again Corrosion easily is dissolved in water, so many natural random holes occur in these deposits.Natural cavity stone clean mark, Gently abundant texture, from natural, but surmount natural.Finished product out, reasonable organization, concavo-convex harmony, seemingly just from mud Come back to life in soil, in lines tendency, the texture of texture, hide prehistory civilized vestige deeply, but its total figure modelling again can be with Described with " modern trend ", show a kind of big divisional design demeanour especially, rank and honour, elegance, top product speciality are showed Incisively and vividly, because deep doted on by numerous architects.
In natural travertine stone-imitated tile, two kinds can be divided into, a kind of to have true hole, ceramic tile is carved in process of production Meaning generation hole, such as application number 200610167363.X natural cavity stone imitation ceramic tiles, using polishing residue material as fabric A part, material is heated when firing produces gas, and gas distributes the hole so as to surface from fabric.It is this imitative Natural cavity stone ceramic tile and natural cavity stone are relatively.Another natural travertine stone-imitated tile, then it is on the basis of the first, incites somebody to action Caused hole is filled using transparency material, and hole is appeared to have so as to form one kind, but touches up what no hole was felt Ceramic tile, the benefit of this ceramic tile are can be used as ground tile paving, and because hole is filled, will not be sheltered evil people and countenance evil practices, convenient clear It is clean, while the natural aesthetic feeling of hole stone is remained again.But existing natural travertine stone-imitated tile is generally polished bricks, its color and luster texture With low uncertainty, the design of brick face can not be rich and changeful, has certain limitation, and pattern true not as good as glazed tile texture is abundant thin The characteristics of greasy.
The content of the invention
It is an object of the invention to propose a kind of production method of the high imitative hole stone glazed tile of emulator, its color and luster enriches Changeable, hole stone effect controllability is high.
It is another object of the present invention to the brick for proposing that a kind of production method using above-mentioned imitative hole stone glazed tile obtains Blank structure.
To use following technical scheme up to this purpose, the present invention:
A kind of production method of natural cavity stone imitation glazed tile, comprises the following steps:
A, the adobe surface charity ground-coat enamel after shaping and drying;
B, charity low temperature glaze:Charity low temperature glaze in adobe after step A stamps;
C, stamp is handled:Stamp is carried out in the adobe that step B is obtained;
D, charity clear frit:The adobe charity clear frit obtained to step C;
E, polishing is fired, obtains finished product.
Preferably, the softening point of the low temperature glaze is less than 850 DEG C.
Preferably, the cloth applying method of the low temperature glaze is one or more combinations in silk screen printing or ink-jet glaze spraying.
Preferably, printed the position that the printed design that low temperature glaze is set surely according to brick face in step B corresponds to its stamp.
Preferably, the glaze of low temperature glaze described in step B includes following components:30-40%SiO2, 55-65%PbO, 3- 8%Al2O3, 1-3% (Na2O, K2) and 0.2-1%MgO O.
Preferably, step C carries out stamp by way of one or more combinations in locating ink-jet or silk-screen printing.
Preferably, step C decalcomania is designed by the spelling group of two or more pattern.
Preferably, the printed design that low temperature glaze is set surely according to brick face in step B, the position of corresponding one or more of which pattern Put and printed.
Preferably, in step B low temperature glaze stochastic print on step A ground glaze layers.
Preferably, the unfired brick structure that step E is obtained includes initial bed, ground glaze layer, printed layer and transparent glaze layer from bottom to top, Low temperature glaze layer is also set up between the ground glaze layer and the printed layer.
Preferably, the low temperature glaze layer presses the design of the printed layer, and the position for being not provided with decalcomania is designed in brick face Put and be also not provided with the low temperature glaze layer.
Beneficial effects of the present invention:1st, gas confinement is in melting layer caused by base substrate is burnt till after being melted using low temperature glaze In, hole stone effect is obtained, fires polishing after forming hole stone effect on brick face, can obtain hole stone bottom has decorative pattern or texture maps The glazed tile of case;2nd, its color and luster can change according to people's different demands to the technologic change such as bed material or clear frit, than Polished bricks color and luster is more abundant, and emulator is higher;3rd, by imitating interval or the Random Design of hole stone, the stereopsis in enhancing brick face Feel effect.
Brief description of the drawings
Fig. 1 is the preparation flow schematic diagram of the blank structure of one embodiment of the present of invention;
Fig. 2 is the preparation flow schematic diagram of the blank structure of an alternative embodiment of the invention;
Fig. 3 is the brick face schematic diagram of the imitative hole stone glazed tile burnt till of one embodiment of the present of invention.
Wherein:Initial bed 1, ground glaze layer 2, low temperature glaze layer 3, printed layer 4, transparent glaze layer 5.
Embodiment
Further illustrate technical scheme below in conjunction with the accompanying drawings and by embodiment.
A kind of production method of natural cavity stone imitation glazed tile, comprises the following steps:
A, the adobe surface charity ground-coat enamel after shaping and drying;
B, charity low temperature glaze:Charity low temperature glaze in adobe after step A stamps;
C, stamp is handled:Stamp is carried out in the adobe that step B is obtained;
D, charity clear frit:The adobe charity clear frit obtained to step C;
E, polishing is fired, obtains finished product.
The present invention obtains hole stone effect using low temperature glaze, fires polishing after forming hole stone effect on brick face, can obtain Hole stone bottom has the glazed tile of decorative pattern or textured pattern, and low temperature glaze refers to that firing temperature is less than 1120 DEG C of glaze, and its color and luster can The technologic change such as bed material or glazing stamp is changed according to people's different demands, it is more abundanter than polished bricks color and luster, Emulator is higher.Sintering procedure is that the base substrate for drenching glaze completion is sent into kiln kiln roasting, firing temperature 1100- in step E 1250℃.The spray of ground-coat enamel in step A, every square metre of 200-300g.The spray of clear frit in step D, every square metre of 150- 1200g.It is polished in step E using soft rubbing down tool, the soft rubbing down tool of resin can be selected and be polished, cavitation after polishing.
Preferably, the softening point of the low temperature glaze is less than 850 DEG C.
Preferably, the cloth applying method of the low temperature glaze is one or more combinations in silk screen printing or ink-jet glaze spraying.
The present invention obtains hole stone effect using low temperature glaze, and can pass through the mesh number size of silk screen or the thickness of ink-jet glaze spraying And the viscosity of low temperature glaze is printed on the quantity of billet surface to determine low temperature glaze, the quantity that low temperature glaze cloth imposes on billet surface determines The quantity and size of cavitation, cavitation effect controllability is high, and low temperature glaze can be according to the design of stamp, in printed surface or stamp Spaced design printed, printing can be spaced and fire cavitation, be randomly distributed in existing hole stone imitative natural on brick face Hole stone polished brick is compared, and effect is more diversified, has bigger market.
Preferably, printed the position that the printed design that low temperature glaze is set surely according to brick face in step B corresponds to its stamp.It is logical Cross positioning and will appear from the local corresponding with the position of stamp of hole stone, low temperature glaze layer is corresponded to positioned at the lower section of printed layer, burn Appeared pit hole face situation by the change observable of stamp on the stone of hole after into polishing, and the structure of hole stone make stamp in hole to The three-dimensional visual effect of people.
Preferably, the glaze of low temperature glaze described in step B includes following components:30-40%SiO2, 55-65%PbO, 3- 8%Al2O3, 1-3% (Na2O, K2) and 0.2-1%MgO O.Under 900 DEG C or so, lead oxide watery fusion, base substrate can be discharged Gas be completely or partially enclosed in melting layer, form bubble, and part bubble can rise brokenly transparent glaze layer, form exposed hole Hole, brick face is printed on the position of low temperature glaze and leave hole, part or closed air bubbles are also exposed on brick face after polishing, are formed fine Hole stone effect.The range of viscosities value of low temperature glaze is 6000-11000mpa.s, and specific gravity range value is 1.5-1.8.
Contain a certain amount of water of constitution and organic matter and decomposable carbonate in blank raw material, these components all can be Gas is produced when burning till and is discharged.Because it is relatively low to produce gas temperature, about 800-1000 DEG C, warm herein for traditional glaze Do not melted under degree, gas is easy to discharge, and low temperature flux is contained in low temperature glaze provided by the invention, can be produced in base substrate gas Melted at raw temperature, by gas caused by base substrate, completely or partially closing wherein, forms bubble.
Preferably, step C carries out stamp by way of one or more combinations in locating ink-jet or silk-screen printing.Institute Silk screen that step B is used is stated as 60-160 mesh.Using the low temperature glaze of same viscosity, its meshcount is smaller, is printed under low temperature glaze The quantity of base substrate is more.
Preferably, step C decalcomania is designed by the spelling group of two or more pattern.Charity ground-coat enamel is laggard Row stamp, its decalcomania are formed by the spelling group of two or more pattern, and design is unrestricted, and range of choice is wide.
Preferably, the printed design that low temperature glaze is set surely according to brick face in step B, the position of corresponding one or more of which pattern Put and printed.
Preferably, in step B low temperature glaze stochastic print on step A ground glaze layers.Low temperature glaze is set surely according to brick face in step B Printed design, the position of corresponding one or more of which pattern is printed or stochastic print is on step A ground glaze layers, makes brick The part with hole stone is provided with decalcomania at random on face, and stamp can be located at hole stone surface or on smooth ground glaze layer, rich The decorative effect in rich brick face, and by imitating interval or the Random Design of hole stone, the stereoscopic visual effect in enhancing brick face.
Preferably, the unfired brick structure that step E is obtained includes initial bed, ground glaze layer, printed layer and transparent glaze layer from bottom to top, Low temperature glaze layer is also set up between the ground glaze layer and the printed layer.
Preferably, the low temperature glaze layer presses the design of the printed layer, and the position for being not provided with decalcomania is designed in brick face Put and be also not provided with the low temperature glaze layer.
Embodiment 1
The unfired brick structure used in Examples below, the powder chemical constituent (wt%) of its green body layer are:SiO2:70%, Al2O3:21%, CaO:1%, MgO:2%, K2O:2%, Na2O:3%, Fe2O3:0.5%, TiO2:0.5%, by said ratio system Standby powder, by the powder pressing prepared into drying for standby after adobe;
The powder chemical constituent (wt%) of its ground glaze layer is:SiO2:68.4%, Al2O3:17.9%, Fe2O3:0.8%, CaO:5.4%, MgO:2.7%, K2O:2.3%, Na2O:0.9%, B2O3:1.6%.
The chemical constituent of its low temperature glaze:SiO2:38%th, PbO:55%th, Al2O3:3%th, (Na2O, K2O):3%, MgO:1%, The low temperature glaze viscosity prepared by mixing and ball milling is 7000mpa.s, proportion 1.65, and the softening point of the low temperature glaze is 850℃。
The chemical constituent (wt%) of its clear frit is:NaO:1.5%;KO:2%;AlO:11%;CaO:8%;MgO:5%; ZnO:2%;ZrO:4%;High temperature frit:15%;Loss on ignition:6%;SiO is 45.5%.Flow velocity is 40s, proportion 1.75.
A kind of production method of natural cavity stone imitation glazed tile, comprises the following steps (flow can be) as shown in Figure 2:
A, the adobe surface charity ground-coat enamel after shaping and drying;
B, charity low temperature glaze:The charity low temperature glaze in the adobe of step A charity ground-coat enamels, wherein being determined using silk screen according to brick face If printed design correspond to its stamp position printing low temperature glaze, meshcount is 120 mesh.
C, stamp is carried out using locating ink-jet, wherein decalcomania is spliced by two kinds of pattern spacings;
D, charity clear frit:The adobe charity clear frit obtained to step C;
E, fire polishing, obtain finished product, brick face effect as shown in figure 3, hole face is provided with textured pattern, make textured pattern to People 3D visual effect, hole stone emulator are high, and the visibility of hole stone is 5-6m, and the hole length of hole stone is 5-15mm, width For 2-8mm, depth 3-6mm.
Embodiment 2
Use adobe same as Example 1, ground-coat enamel and clear frit.
The chemical constituent of its low temperature glaze:SiO2:30%th, PbO:65%th, Al2O3:3%th, (Na2O, K2O):1%, MgO: 1%, the low temperature glaze viscosity prepared by mixing and ball milling is 7500mpa.s, proportion 1.75, the softening point of the low temperature glaze For 800 DEG C.
A kind of production method of natural cavity stone imitation glazed tile, comprises the following steps (flow can be) as shown in Figure 2:
A, the adobe surface charity ground-coat enamel after shaping and drying;
B, charity low temperature glaze:The charity low temperature glaze in the adobe of step A charity ground-coat enamels, wherein using ink-jet printer according to The printed design that brick face is set surely corresponds to the position sprayed coating low temperature glaze of its stamp, thickness 5mm.
C, stamp is carried out using locating ink-jet, stamp is the texture of imitating natural marble crackle;
D, charity clear frit:The adobe charity clear frit obtained to step C;
E, fire polishing, obtain finished product, hole face be provided with imitating natural marble crackle textured pattern, make textured pattern to People 3D visual effect, image-stone face is to caused crackle under the Nature corrosion function, fine true to nature, hole stone emulator Height, the visibility of hole stone is 6-7m, and the hole length of hole stone is 10-30mm, width 3-8mm, depth 3-8mm.
Embodiment 3
Use adobe same as Example 1, ground-coat enamel and clear frit.
The chemical constituent of its low temperature glaze:SiO2:40%th, PbO:55%th, Al2O3:3.8%th, (Na2O, K2O):1%, MgO: 0.2%, the low temperature glaze viscosity prepared by mixing and ball milling is 9500mpa.s, proportion 1.67, the softening of the low temperature glaze Point is 780 DEG C.
A kind of production method of natural cavity stone imitation glazed tile, comprises the following steps (flow can be) as shown in Figure 2:
A, the adobe surface charity ground-coat enamel after shaping and drying;
B, charity low temperature glaze:The charity low temperature glaze in the adobe of step A charity ground-coat enamels, wherein being determined using silk screen according to brick face If printed design correspond to its stamp position printing low temperature glaze, meshcount is 160 mesh.
C, stamp is carried out using locating ink-jet, stamp is the texture of imitating natural marble crackle;
D, charity clear frit:The adobe charity clear frit obtained to step C;
E, fire polishing, obtain finished product, hole face be provided with imitating natural marble crackle textured pattern, make textured pattern to People 3D visual effect, image-stone face is to caused crackle under the Nature corrosion function, fine true to nature, hole stone emulator Height, the visibility of hole stone is 3-5m, and the hole length of hole stone is 10-20mm, width 3-5mm, depth 2-4mm.
Embodiment 4
Use adobe same as Example 1, ground-coat enamel and clear frit.
The chemical constituent of its low temperature glaze:SiO2:30.8%th, PbO:60%th, Al2O3:8%th, (Na2O, K2O):1%, MgO: 0.2%, the low temperature glaze viscosity prepared by mixing and ball milling is 6500mpa.s, proportion 1.73, the softening of the low temperature glaze Point is 820 DEG C.
A kind of production method of natural cavity stone imitation glazed tile, comprises the following steps (flow can be) as shown in Figure 2:
A, the adobe surface charity ground-coat enamel after shaping and drying;
B, charity low temperature glaze:The charity low temperature glaze in the adobe of step A charity ground-coat enamels, wherein being determined using silk screen according to brick face If printed design correspond to its stamp position printing low temperature glaze, meshcount is 100 mesh.
C, stamp is carried out using locating ink-jet, stamp is the texture of natural-like stone;
D, charity clear frit:The adobe charity clear frit obtained to step C;
E, polishing is fired, obtains finished product, hole face is provided with the pattern of imitating natural stone texture, textured pattern is given people 3D's Visual effect, fine true to nature as flowing the stone structure that is formed of accumulation naturally by magma, hole stone emulator height, hole stone can Degree of opinion is 4-5m, and the hole length of hole stone is 10-15mm, width 3-5mm, depth 2-5mm.
Embodiment 5
Use adobe same as Example 1 and clear frit;
The chemical constituent of its low temperature glaze:SiO2:40%th, PbO:50%th, Al2O3:7.5%th, (Na2O, K2O):2%, MgO: 0.5%, the low temperature glaze viscosity prepared by mixing and ball milling is 8470mpa.s, proportion 1.60, the softening of the low temperature glaze Point is 900 DEG C.
A kind of production method of natural cavity stone imitation glazed tile, comprises the following steps:
A, the adobe surface charity ground-coat enamel after shaping and drying;
B, charity low temperature glaze:The charity low temperature glaze on the throwing base that step A is obtained, low temperature glaze correspond to the pattern on adobe surface Texture carries out charity, meshcount 120 using silk screen;
C, stamp is carried out:Stamp is carried out using silk-screen printing, wherein stamp position is consistent with the position of low temperature glaze charity, Decalcomania is the stamp of imitating natural stone texture;
D, charity clear frit:Clear frit is applied to the step C throwing fabrics obtained;
E, polishing is fired, obtains finished product, hole is provided with imitating natural stone texture, imitating natural stone texture is given people regarding for 3D Feel effect, finely true to nature as flow the stone structure that is formed of accumulation naturally by magma, hole stone emulator height, hole stone it is visible Spend for 5-6m, the hole length of hole stone is 5-10mm, width 3-4mm, depth 2-3mm.The softening point of the low temperature glaze is 900 DEG C, because generation gas temperature is relatively low, about 800-1000 DEG C, if at 900 DEG C, low temperature glaze just forms melting layer, The gas of a part can be run away before 900 DEG C, the formation of hole is diminished, is unfavorable for controlling the formation of hole.
The technical principle of the present invention is described above in association with specific embodiment.These descriptions are intended merely to explain the present invention's Principle, and limiting the scope of the invention can not be construed in any way.Based on explanation herein, the technology of this area Personnel would not require any inventive effort the other embodiments that can associate the present invention, and these modes are fallen within Within protection scope of the present invention.

Claims (6)

  1. A kind of 1. production method of natural cavity stone imitation glazed tile, it is characterised in that:Comprise the following steps:
    A, the adobe surface charity ground-coat enamel after shaping and drying;
    B, charity low temperature glaze:Charity low temperature glaze in adobe after step A stamps;
    C, stamp is handled:Stamp is carried out in the adobe that step B is obtained;
    D, charity clear frit:The adobe charity clear frit obtained to step C;
    E, polishing is fired, obtains finished product;
    Wherein, the glaze of low temperature glaze described in step B includes following components:30-40%SiO2, 55-65%PbO, 3-8% Al2O3, 1-3% (Na2O, K2) and 0.2-1%MgO O;The softening point of the low temperature glaze is less than 850 DEG C;
    The position that the printed design that low temperature glaze is set surely according to brick face in step B corresponds to its stamp is printed, or low temperature in step B Glaze stochastic print is on step A ground glaze layers.
  2. A kind of 2. production method of natural cavity stone imitation glazed tile according to claim 1, it is characterised in that:The low temperature glaze Cloth applying method be one or more combinations in silk screen printing or ink-jet glaze spraying.
  3. A kind of 3. production method of natural cavity stone imitation glazed tile according to claim 1, it is characterised in that:Step C passes through The mode of one or more combinations in locating ink-jet or silk-screen printing carries out stamp.
  4. A kind of 4. production method of natural cavity stone imitation glazed tile according to claim 1, it is characterised in that:Step C print Floral pattern is designed by the spelling group of two or more pattern.
  5. A kind of 5. production method of natural cavity stone imitation glazed tile according to claim 4, it is characterised in that:It is low in step B The printed design that warm glaze is set surely according to brick face, the position of corresponding one or more of which pattern are printed.
  6. 6. usage right requires the adobe knot that a kind of production method of natural cavity stone imitation glazed tile described in 1-5 any one obtains Structure, it is characterised in that:The unfired brick structure includes initial bed, ground glaze layer, printed layer and transparent glaze layer, the ground-coat enamel from bottom to top Low temperature glaze layer is also set up between layer and the printed layer.
CN201510354863.3A 2015-06-24 2015-06-24 A kind of production method of natural cavity stone imitation glazed tile and its unfired brick structure of acquisition CN105036814B (en)

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CN106187324B (en) * 2015-05-04 2019-03-29 杭州诺贝尔陶瓷有限公司 A kind of Imitation Rock Porcelain Tiles and preparation method thereof with three-dimensional decorative effect
CN105461358B (en) * 2015-11-19 2019-04-19 杭州诺贝尔陶瓷有限公司 A kind of Imitation Rock Porcelain Tiles and its production method of imitative stone pattern three-dimensional decorative effect
CN105481478B (en) * 2015-12-18 2019-02-05 广东家美陶瓷有限公司 A kind of preparation method of pattern permeating tile
CN106242527A (en) * 2016-08-09 2016-12-21 佛山欧神诺陶瓷股份有限公司 A kind of high emulation entire body throws glaze marble ceramic tile and production method thereof entirely
CN107344814B (en) * 2017-07-11 2020-02-07 佛山市华力达材料科技有限公司 Soft light brick surface glaze and soft light brick
CN107651971A (en) * 2017-09-30 2018-02-02 唐硕度 A kind of anti-bacteria ceramic thin plate and preparation method thereof
CN107759090B (en) * 2017-11-21 2020-12-01 广东道氏技术股份有限公司 Glaze material with effect of imitating black gold sand marble and application thereof
CN108101365A (en) * 2017-12-05 2018-06-01 湖南陶润会文化传播有限公司 Double-deck reaction glaze of solution cavity and preparation method thereof
CN108545999B (en) * 2018-04-13 2020-12-01 佛山东华盛昌新材料有限公司 Preparation method of hole material, marble-imitated hole brick and preparation method thereof

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CN104130032A (en) * 2014-08-01 2014-11-05 佛山市东鹏陶瓷有限公司 Glazed brick manufacturing method and product

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CN201754821U (en) * 2010-05-20 2011-03-09 郑菁菁 Stimulated porcelain flower
CN103524147A (en) * 2013-10-25 2014-01-22 广东金牌陶瓷有限公司 Glazed brick production process
CN104130032A (en) * 2014-08-01 2014-11-05 佛山市东鹏陶瓷有限公司 Glazed brick manufacturing method and product

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