CN104987795A - Flame-retardant thermal insulation paint used for curtain walls and preparation method of flame-retardant thermal insulation paint - Google Patents
Flame-retardant thermal insulation paint used for curtain walls and preparation method of flame-retardant thermal insulation paint Download PDFInfo
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- CN104987795A CN104987795A CN201510387986.7A CN201510387986A CN104987795A CN 104987795 A CN104987795 A CN 104987795A CN 201510387986 A CN201510387986 A CN 201510387986A CN 104987795 A CN104987795 A CN 104987795A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/02—Homopolymers or copolymers of acids; Metal or ammonium salts thereof
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
Abstract
The invention discloses flame-retardant thermal insulation paint used for curtain walls and a preparation method of the flame-retardant thermal insulation paint. The flame-retardant thermal insulation paint is composed of, by weight, 100 parts to 115 parts of modified acrylic resin, 1 part to 1.6 parts of flatting agents, 3 parts to 4 parts of (1S,3S,5S)-3-(amino-carbonyl)-2-azabicyalo[3.1.0]hexane-2-tert-butyl formate, 0.8 part to 1.6 parts of guanidine carbonate, 1 part to 1.5 parts of zinc molybdate and 10 parts to 15 parts of bi(3,4-dimethyl benzylidene)sorbitol. The flame-retardant thermal insulation paint has the advantages that the flame-retardant effect and the thermal insulating effect of the paint are good; environmental protection is achieved, pollution is little, the machining process is simple, and operation is convenient; glass beads can not be separated out when the flame-retardant thermal insulation paint is used for a long time; the weather resistance of the paint is high, and paint components can not be separated out.
Description
Technical field
The present invention relates to technical field of coatings, particularly a kind of curtain wall flame-retardant insulating paint and preparation method thereof.
Background technology
Curtain wall spraying function coating is an important means of building energy conservation, and its cost is low, easy construction.Although the performance index that existing thermal insulating coating is single have reached higher level, the overall target such as comprehensive heatproof, fire-retardant, heat insulation, waterproof, sticking power has also been difficult to meet the demands.The fire retardant addition of existing coating causes greatly heat-insulating efficiency to reduce, and have impact on the over-all properties of coating.Some paint coating thickness is large, applies uneconomical.The coating also had contains a large amount of organic solvents, and VOC volatilization is high, is unfavorable for using in environment-friendly type building material.Conventional thermal insulating coating in time prolong insulation effect declines.Development curtain wall flame retarding efficiency is high, heat-insulating efficiency is high, cost is lower, and polluting little coating is a great problem of pendulum in face of people.
Summary of the invention
In order to meet the demand of current curtain wall coating, embodiments provide a kind of curtain wall flame-retardant insulating paint and preparation method thereof.
In order to realize foregoing invention object, the invention provides a kind of curtain wall flame-retardant insulating paint, be made up of the raw material of following weight part: acrylic resin modified 100-115 part, flow agent 1-1.6 part, (1S, 3S, 5S)-3-(aminocarboxyl)-2-azabicyclo [3.1.0] hexane-2-t-butyl formate 3-4 part, Guanidinium carbonate 0.8-1.6 part, zinc molybdate 1-1.5 part and two (3,4-dimethylbenzylidene) sorbyl alcohol 10-15 part.
Described acrylic resin modified preparation method comprises the following steps:
Be the nano oxidized boron, 1 of 8-9:1-2:60-70:200-220 by mass ratio; 1; after the mixing of 1-TriMethylolPropane(TMP), Tai-Ace S 150 and deionized water; stir, stirring velocity 120-160r/min, adjusted to ph is 8.2-8.5; stir after 2-3 hour; reduction stirring velocity is 20-50r/min, continues to stir after 1-2 hour, 60-80 DEG C of dry meal A;
Be that the vinylformic acid of 3-5:0.5-1:2-3:0.04-0.09:18-27, dimethyl diethylsilane, Epoxysuccinic acid, meal A and deionized water and stirring mix by mass ratio, stirring velocity 90-110r/min, under agitation drips ammoniacal liquor and regulates pH value to be that 8-8.5 obtains mixture one;
Be that the di-isopropylbenzene hydroperoxide of 6:3:5:100, N,N methylene bis acrylamide, sodium bisulfite and deionization mix to obtain mixture two by mass ratio;
Mixture two is added in mixture one mixture three continuing to stir 8-10 minute, temperature is controlled at 60-65 DEG C, insulation 20-30 minute, add hollow glass micropearl stirring velocity to be adjusted to 180-240r/min and in whipping device, to be filled with nitrogen replacement to fall oxygen in whipping device, stir after 5-8 minute, stirring velocity is reduced to 60-70r/min; Described mixture one: the mass ratio of mixture two is 1000:1-2; Described hollow glass micropearl accounts for the 2-5% of mixture three quality;
Then rapidly the bicarbonate of ammonia and 4 of mixture three quality 2-3% will be accounted for, the mixture of 4'-OBSH adds, then the Potassium Persulphate accounting for mixture three quality 0.08-0.12% is added at once, continue to stir 0.5-1min, stop stirring, place after 60-120 minute, be cooled to 20-25 DEG C, obtain acrylic resin modified;
The mass ratio of described bicarbonate of ammonia and described 4,4'-OBSH is 28:5.
Described hollow glass micropearl particle diameter is 10-30 μm.
Described flow agent is PV88.
The preparation method of described coating comprises the following steps: get described raw material in proportion and mix.
The beneficial effect that the technical scheme that the embodiment of the present invention provides is brought is:
1, the flame retardant effect of coating and good in insulation effect;
2, environmental pollution is little, and complete processing is simple, convenient operation.
3, the long-time glass microballon that uses can not be separated out.
4, coating good weatherability, and coating composition can not be separated out.
Embodiment
For the problem of curtain wall coating over-all properties difference, the invention provides a kind of curtain wall flame-retardant insulating paint and preparation method thereof.
Below adopt embodiment to describe embodiments of the present invention in detail, to the present invention, how utilisation technology means solve technical problem whereby, and the implementation procedure reaching technique effect can fully understand and implement according to this.
(1S, 3S, 5S)-3-(aminocarboxyl)-2-azabicyclo [3.1.0] hexane-2-t-butyl formate: No. CAS: 361440-67-7;
4,4'-OBSH: CAS 80-51-3;
Two (3,4-dimethylbenzylidene) sorbyl alcohol: CAS 135861-56-2;
1,1,1-TriMethylolPropane(TMP): CAS 77-99-6;
Dimethyl diethylsilane: CAS 756-81-0;
Epoxysuccinic acid: CAS 16533-72-5;
Di-isopropylbenzene hydroperoxide: CAS 26762-93-6;
N,N methylene bis acrylamide: CAS 110-26-9;
Guanidinium carbonate CAS 593-85-1.
Embodiment 1
Step 1. is acrylic resin modified preparation method comprise the following steps:
Nano oxidized boron: 1,1,1-TriMethylolPropane(TMP): Tai-Ace S 150 (i.e. Al
2(SO
4)
3): deionized water quality, than for after 8.5:1:60:200 mixing, stirs, stirring velocity 120r/min, and adjusted to ph is 8.5, stirs after 3 hours, and reduction stirring velocity is 50r/min, continuation stirring after 1 hour, 80 DEG C dry must meal A;
Be vinylformic acid, dimethyl diethylsilane, the Epoxysuccinic acid of 5:1:3:0.06:27 by mass ratio: meal A: deionized water and stirring mixes, stirring velocity 110r/min, under agitation drip ammoniacal liquor regulate pH value be 8.5 mixture one;
By di-isopropylbenzene hydroperoxide: N,N methylene bis acrylamide: sodium bisulfite: deionized water quality mixes to obtain mixture two than 6:3:5:100;
Mixture two is added in mixture one and continue the stirring mixture of 9 minutes three, temperature is controlled at 65 DEG C, be incubated 25 minutes, add hollow glass micropearl stirring velocity to be adjusted to 240r/min and in whipping device, to be filled with nitrogen replacement to fall oxygen in whipping device, stir after 5 minutes, stirring velocity is reduced to 70r/min; Described mixture one: mixture two mass ratio is 1000:1; Described hollow glass micropearl accounts for 2% of mixture three quality; Described hollow glass micropearl particle diameter is 10 μm.
Then the rapid mixture by the bicarbonate of ammonia and 4,4'-OBSH that account for mixture three quality 2% adds, and then adds the Potassium Persulphate accounting for mixture three quality 0.1% at once, continue to stir 1min, stop stirring, place after 100 minutes, be cooled to 25 DEG C, obtain acrylic resin modified;
The mass ratio of described bicarbonate of ammonia and 4,4'-OBSH is 28:5.
Step 2: the preparation of curtain wall flame-retardant insulating paint gets acrylic resin modified 100 parts, flow agent PV88 1.2 parts, (1S, 3S, 5S)-3-(aminocarboxyl)-2-azabicyclo [3.1.0] hexane-2-t-butyl formate 3 parts, Guanidinium carbonate 1 part, zinc molybdate 1.5 parts, two (3,4-dimethylbenzylidene) sorbyl alcohol 12 parts mix.
The thermal conductivity 0.0104W/ (mK) of coating; Visible reflectance 94%, near infrared light rejection rate is 90%, uv absorption rate 99.5%.
Curtain wall coating film on a glass, obtains the thick film of about 2mm, is taken off by film from sheet glass, carry out limiting oxygen index determination according to standard GB/T/T2406 after drying, oxygen index is 34.4%
Embodiment 2
Step 1. is acrylic resin modified preparation method comprise the following steps:
Nano oxidized boron: 1,1,1-TriMethylolPropane(TMP): Tai-Ace S 150 (i.e. Al
2(SO
4)
3): deionized water quality, than for after 8:1:70:220 mixing, stirs, stirring velocity 160r/min, and adjusted to ph is 8.2, stirs after 2 hours, and reduction stirring velocity is 20r/min, continuation stirring after 2 hours, 60 DEG C dry must meal A;
Be vinylformic acid, dimethyl diethylsilane, the Epoxysuccinic acid of 3:0.5:2:0.04:18 by mass ratio: meal A: deionized water and stirring mixes, stirring velocity 100r/min, under agitation drip ammoniacal liquor regulate pH value be 8 mixture one;
By di-isopropylbenzene hydroperoxide: N,N methylene bis acrylamide: sodium bisulfite: deionization mass ratio 6:3:5:100 mixes to obtain mixture two;
Mixture two is added in mixture one and continue the stirring mixture of 8 minutes three, temperature is controlled at 60 DEG C, be incubated 20 minutes, add hollow glass micropearl stirring velocity to be adjusted to 180r/min and in whipping device, to be filled with nitrogen replacement to fall oxygen in whipping device, stir after 6 minutes, stirring velocity is reduced to 60r/min; Described mixture one: mixture two mass ratio is 1000:2; Described glass microballon accounts for 3% of mixture three quality; Described hollow glass micropearl particle diameter is 30 μm.
Then rapidly the bicarbonate of ammonia and 4 of mixture three quality 3% will be accounted for, the mixture of 4'-OBSH adds, then the Potassium Persulphate accounting for mixture three quality 0.12% is added at once, continue to stir 0.5min, stop stirring, place after 60 minutes, be cooled to 20 DEG C, obtain acrylic resin modified;
The mass ratio of described bicarbonate of ammonia and 4,4'-OBSH is 28:5.
Step 2: the preparation of curtain wall flame-retardant insulating paint gets acrylic resin modified 105 parts, flow agent PV88 1.6 parts, (1S, 3S, 5S)-3-(aminocarboxyl)-2-azabicyclo [3.1.0] hexane-2-t-butyl formate 4 parts, Guanidinium carbonate 0.8 part, zinc molybdate 1 part, two (3,4-dimethylbenzylidene) sorbyl alcohol 10 parts mix.
The thermal conductivity 0.0126W/ (mK) of coating; Visible reflectance 95%, near infrared light rejection rate 92%, uv absorption rate 99.1%.
Curtain wall coating film on a glass, obtains the thick film of about 2mm, is taken off by film from sheet glass, carry out limiting oxygen index determination according to standard GB/T/T2406 after drying, oxygen index is 36.4%
Embodiment 3
Step 1. is acrylic resin modified preparation method comprise the following steps:
Nano oxidized boron: 1,1,1-TriMethylolPropane(TMP): Tai-Ace S 150 (i.e. Al
2(SO
4)
3): deionized water quality, than for after 9:2:65:210 mixing, stirs, stirring velocity 140r/min, and adjusted to ph is 8.5, stirs after 3 hours, and reduction stirring velocity is 30r/min, continuation stirring after 1 hour, 70 DEG C dry must meal A;
Be vinylformic acid, dimethyl diethylsilane, the Epoxysuccinic acid of 4:0.8:3:0.09:24 by mass ratio: meal A: deionized water and stirring mixes, stirring velocity 90r/min, under agitation drip ammoniacal liquor regulate pH value be 8.5 mixture one;
By di-isopropylbenzene hydroperoxide: N,N methylene bis acrylamide: sodium bisulfite: deionization mass ratio 6:3:5:100 mixes to obtain mixture two;
Mixture two is added in mixture one and continue the stirring mixture of 10 minutes three, temperature is controlled at 65 DEG C, be incubated 30 minutes, add hollow glass micropearl stirring velocity to be adjusted to 200r/min and in whipping device, to be filled with nitrogen replacement to fall oxygen in whipping device, stir after 8 minutes, stirring velocity is reduced to 70r/min; Described mixture one: mixture two mass ratio is 1000:1; Described glass microballon accounts for 5% of mixture three quality; Described hollow glass micropearl particle diameter is 20 μm.
Then rapidly the bicarbonate of ammonia and 4 of mixture three quality 2% will be accounted for, the mixture of 4'-OBSH adds, then the Potassium Persulphate accounting for mixture three quality 0.08% is added at once, continue to stir 1min, stop stirring, place after 120 minutes, be cooled to 25 DEG C, obtain acrylic resin modified;
The mass ratio of described bicarbonate of ammonia and 4,4'-OBSH is 28:5.
Step 2: the preparation of curtain wall flame-retardant insulating paint gets acrylic resin modified 115 parts, flow agent PV88 1 part, (1S, 3S, 5S)-3-(aminocarboxyl)-2-azabicyclo [3.1.0] hexane-2-t-butyl formate 3 parts, Guanidinium carbonate 1.6 parts, zinc molybdate 1.2 parts, two (3,4-dimethylbenzylidene) sorbyl alcohol 15 parts mix.
The thermal conductivity 0.0113W/ (mK) of coating; Visible reflectance 96%, near infrared light rejection rate is 92%, uv absorption rate 99.2%.
Curtain wall coating film on a glass, obtains the thick film of about 2mm, is taken off by film from sheet glass, carry out limiting oxygen index determination according to standard GB/T/T2406 after drying, oxygen index is 40.4%
In sum, the coating excellent combination property of embodiment of the present invention 1-3, not only has good heat-proof quality, and to visible reflectance, near infrared light rejection rate and all very high to uv absorption rate, and have good flame retardant properties.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, within the spirit and principles in the present invention all, any amendment done, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (5)
1. a curtain wall flame-retardant insulating paint, it is characterized in that, be made up of the raw material of following weight part: acrylic resin modified 100-115 part, flow agent 1-1.6 part, (1S, 3S, 5S)-3-(aminocarboxyl)-2-azabicyclo [3.1.0] hexane-2-t-butyl formate 3-4 part, Guanidinium carbonate 0.8-1.6 part, zinc molybdate 1-1.5 part and two (3,4-dimethylbenzylidene) sorbyl alcohol 10-15 part.
2. curtain wall flame-retardant insulating paint according to claim 1, is characterized in that, described acrylic resin modified preparation method comprises the following steps:
Be the nano oxidized boron, 1 of 8-9:1-2:60-70:200-220 by mass ratio; 1; after the mixing of 1-TriMethylolPropane(TMP), Tai-Ace S 150 and deionized water; stir, stirring velocity 120-160r/min, adjusted to ph is 8.2-8.5; stir after 2-3 hour; reduction stirring velocity is 20-50r/min, continues to stir after 1-2 hour, 60-80 DEG C of dry meal A;
Be that the vinylformic acid of 3-5:0.5-1:2-3:0.04-0.09:18-27, dimethyl diethylsilane, Epoxysuccinic acid, meal A and deionized water and stirring mix by mass ratio, stirring velocity 90-110r/min, under agitation drips ammoniacal liquor and regulates pH value to be that 8-8.5 obtains mixture one;
Be that the di-isopropylbenzene hydroperoxide of 6:3:5:100, N,N methylene bis acrylamide, sodium bisulfite and deionization mix to obtain mixture two by mass ratio;
Mixture two is added in mixture one mixture three continuing to stir 8-10 minute, temperature is controlled at 60-65 DEG C, insulation 20-30 minute, add hollow glass micropearl stirring velocity to be adjusted to 180-240r/min and in whipping device, to be filled with nitrogen replacement to fall oxygen in whipping device, stir after 5-8 minute, stirring velocity is reduced to 60-70r/min; Described mixture one: the mass ratio of mixture two is 1000:1-2; Described hollow glass micropearl accounts for the 2-5% of mixture three quality;
Then rapidly the bicarbonate of ammonia and 4 of mixture three quality 2-3% will be accounted for, the mixture of 4'-OBSH adds, then the Potassium Persulphate accounting for mixture three quality 0.08-0.12% is added at once, continue to stir 0.5-1min, stop stirring, place after 60-120 minute, be cooled to 20-25 DEG C, obtain acrylic resin modified;
The mass ratio of described bicarbonate of ammonia and described 4,4'-OBSH is 28:5.
3. curtain wall flame-retardant insulating paint according to claim 1, is characterized in that, described hollow glass micropearl particle diameter is 10-30 μm.
4. curtain wall flame-retardant insulating paint according to claim 1, is characterized in that, described flow agent is PV88.
5., according to the arbitrary described curtain wall flame-retardant insulating paint of claim 1-4, it is characterized in that, the preparation method of described coating comprises the following steps: get described raw material in proportion and mix.
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CN201510387986.7A CN104987795A (en) | 2015-07-06 | 2015-07-06 | Flame-retardant thermal insulation paint used for curtain walls and preparation method of flame-retardant thermal insulation paint |
PCT/CN2016/084897 WO2017005072A1 (en) | 2015-07-06 | 2016-06-06 | Flame-retardant heat-insulated coating for curtain wall and preparation method therefor |
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CN201510387986.7A CN104987795A (en) | 2015-07-06 | 2015-07-06 | Flame-retardant thermal insulation paint used for curtain walls and preparation method of flame-retardant thermal insulation paint |
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Cited By (3)
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WO2017005072A1 (en) * | 2015-07-06 | 2017-01-12 | 梁怡芃 | Flame-retardant heat-insulated coating for curtain wall and preparation method therefor |
CN106366846A (en) * | 2016-08-29 | 2017-02-01 | 岳西县日胜商贸有限公司 | Heat insulation coating special for surface of stainless steel tea cup |
CN107325651A (en) * | 2017-07-15 | 2017-11-07 | 合肥皖水信息科技有限公司 | A kind of fire-proof glass curtain wall |
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CN112521792A (en) * | 2020-12-02 | 2021-03-19 | 太仓德纳森机电工程有限公司 | Composite material for electrical control cabinet and preparation method thereof |
CN113755063A (en) * | 2021-09-15 | 2021-12-07 | 孙志远 | Exterior wall heat insulation coating and preparation method thereof |
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Application publication date: 20151021 |