CN104947239A - Down feather composite fiber having good skin smoothing and skin-friendly effects - Google Patents
Down feather composite fiber having good skin smoothing and skin-friendly effects Download PDFInfo
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- CN104947239A CN104947239A CN201510368720.8A CN201510368720A CN104947239A CN 104947239 A CN104947239 A CN 104947239A CN 201510368720 A CN201510368720 A CN 201510368720A CN 104947239 A CN104947239 A CN 104947239A
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Abstract
The invention discloses a down feather composite fiber having good skin smoothing and skin-friendly effects. The down feather composite fiber is characterized by being prepared from the following raw materials in parts by weight: 70-100 parts of poultry feather, 13-15 parts of goose down, 30-50 parts of ramine fiber, 7-10 parts of silane coupling agent kh590, 5-7 parts of urea, 0.2-0.4 part of potassium metabisulphate, 0.1-0.3 part of sodium dodecyl sulfate, 1-3 part of betaine, 0.4-0.7 part of tea saponin, 0.2-0.5 part of wax ester, 2-4 parts of collagen fiber and an appropriate amount of water; according to the down feather composite fiber, the treatment mixed solution of the tea saponin, the wax ester and the collagen fiber are added, and consequently, the lubricity of fabrics can be enhanced and the skin comfort can be improved; the feather is effectively utilized, the added value of the down feather fiber is increased and the application of the feather in other fields is developed; besides, the down feather composite fiber is simple in preparation process, relatively low in cost and free from pollution on the ecological environment, and has great application prospect.
Description
Technical field
The present invention relates to textile material technical field, be specifically related to effective eider down composite fibre of a kind of soft skin pro-skin and preparation method thereof.
Background technology
along with to the attention of environmental protection and the raising of consumer demand, the research and development of the tencel of environmental beneficial are more and more received publicity, some discarded textile raw materials are as wool, eider down, silk etc. belong to high-quality natural protein material, there is health, environmental friendliness, reproducible feature, China is bird big producing country, a large amount of filoplumes is difficult to direct utilization because of the restriction of itself structure, warming packing material is used as or as except reinforcing material except a small amount of, mostly just simply be processed into feed even directly to abandon, the lower occurring in nature keratin of value-added content of product extensively exists, only China discards poultry feather year just more than 70 ten thousand tons, therefore the regenerated protein obtained in discarded object or byproduct should give consideration.Protein content in feather can reach 85-89%, and present keratin is widely used in biological medicine industry, textile industry and animal feed industries etc.For the characteristic of spun protein, keratin as natural polymer meets completely, but because keratin is the protein being rich in disulfide bond, show again the characteristic different from other protein, wherein the degree of cross linking is large, be not easy dissolve, so utilization rate is low, can not be good given play to due characteristic.By feather, to make keratin solution and other material copolymerization be means through modified in the present invention, by wet spinning processing method, the shortcomings such as when solving keratin independent spinning, bad mechanical property, firmness are strong, tensile strength is low, and feather stem is also utilized, greatly strengthen utilization ratio.Keratin, as the broad-spectrum biomaterial of one, contains infinite commercial opportunities and fine development prospect, promotes the development and utilization of new resources, is worthy to be popularized.
Summary of the invention
The object of this invention is to provide effective eider down composite fibre of a kind of soft skin pro-skin and preparation method thereof, to overcome the deficiencies in the prior art.
The object of the invention is to be realized by following technological means:
The eider down composite fibre that a kind of soft skin pro-skin is effective, it is characterized in that, be made up of the raw material of following weight portion: poultry feather 70-100, goose down 13-15, ramee 30-50, silane coupler kh5907-10, urea 5-7, potassium metabisulfite 0.2-0.4, lauryl sodium sulfate 0.1-0.3, betaine 1-3, Tea Saponin 0.4-0.7, wax ester 0.2-0.5, collagen fabric 2-4, water are appropriate;
The eider down composite fibre that a kind of soft skin pro-skin of the present invention is effective, be made up of following concrete steps:
(1) poultry feather and feather stem are separated, use clear water rinsed clean respectively, dry, carry out processed, feather extruding is separated, and feather stem carries out torsion extruding, sterilizing and deodorization under 100-200 ° of C in high-pressure sterilizing pot is added to goose down mixing after again feather and feather stem being cut into mean size, after spontaneous combustion cooling, mixing feather material is placed in alcohol and soaks 4-6 hour, then be neutral post-drying with clear water washing surface, be ground into powder for subsequent use;
(2) dissolved by the silane coupler kh590 acetone soln of 10-15 times amount, then add Powdered feather meal, mixed at high speed is even, and raised temperature to 80 ° C constant temperature keeps 1h, then heating is back to except desolventizing, and crushed after being dried obtains modified fish oil powder;
(3) urea, Sodium Metabisulfite and lauryl sodium sulfate are mixed, be dissolved in water and make the concentration of urea be 0.1mol/l, the modified fish oil powder that step (2) obtains is added in lysate, seal bottleneck and be placed in 95 ° of C water-bath concussion pots with the rotating speed of 100r/min concussion 20-25min, residue filter is removed by rapid gauze, obtains feather keratin solution for standby;
(4) water betaine being added 30 times amount makes solution, add Tea Saponin, wax ester, collagen fabric mixing and stirring again, ramee is processed into cellulose sulfonate solution through yellow again after dipping by lye, add betaine mixed solution again to stir, then the keratin solution obtained with step (3) is mixed to get feather protein viscose glue, carries out wet spinning and obtains feather protein viscose;
(5) the feather protein viscose that step (4) obtained successively carries out coagulating bath process, pickling, washing are dried and obtained albumen feather fiber.
Advantage of the present invention is: the present invention is by feather and feather stem sterilizing, deodorizing, by silane coupler modified after ungrease treatment, mixing feather powder is had excellent hydrophobic, the performance of moisture absorption, the protein degradation liquid that recycling suitable proportion obtains makes feather powder dissolution obtain viscosity, the good keratin solution of rheological characteristic, by keratin solution with mix through the ramee lysate of modification and carry out spinning, enhance the toughness of feather fiber greatly, tensile strength, fragility, ABRASION RESISTANCE, the characteristics such as spinnability, improve productive value and social benefit, the present invention adds Tea Saponin, wax ester, collagen fabric process mixed solution, enhance the lubricity of fabric, good to skin comfort level, the present invention effectively make use of feather, add the added value of down fiber, open the application at other field, and preparation technology of the present invention is simple, cost is lower, pollution-free to ecological environment, have great application prospect.
Detailed description of the invention
The eider down composite fibre that a kind of soft skin pro-skin is effective, it is characterized in that, be made up of the raw material of following weight portion (kilogram): poultry feather 95, goose down 15, ramee 48, silane coupler kh5909, urea 6, potassium metabisulfite 0.3, lauryl sodium sulfate 0.3, betaine 3, Tea Saponin 0.6, wax ester 0.3, collagen fabric 3, water are appropriate;
The eider down composite fibre that a kind of soft skin pro-skin of the present invention is effective, be made up of following concrete steps:
(1) poultry feather and feather stem are separated, use clear water rinsed clean respectively, dry, carry out processed, feather extruding is separated, and feather stem carries out torsion extruding, sterilizing and deodorization under 150 ° of C in high-pressure sterilizing pot is added to goose down mixing after again feather and feather stem being cut into mean size, after spontaneous combustion cooling, mixing feather material is placed in alcohol to soak 6 hours, then is neutral post-drying with clear water washing surface, be ground into powder for subsequent use;
(2) dissolved by the silane coupler kh590 acetone soln of 13 times amount, then add Powdered feather meal, mixed at high speed is even, and raised temperature to 80 ° C constant temperature keeps 1h, then heating is back to except desolventizing, and crushed after being dried obtains modified fish oil powder;
(3) urea, Sodium Metabisulfite and lauryl sodium sulfate are mixed, be dissolved in water and make the concentration of urea be 0.1mol/l, the modified fish oil powder that step (2) obtains is added in lysate, seal bottleneck and be placed in 95 ° of C water-bath concussion pots with the rotating speed of 100r/min concussion 20min, residue filter is removed by rapid gauze, obtains feather keratin solution for standby;
(4) water betaine being added 30 times amount makes solution, add Tea Saponin, wax ester, collagen fabric mixing and stirring again, ramee is processed into cellulose sulfonate solution through yellow again after dipping by lye, add betaine mixed solution again to stir, then the keratin solution obtained with step (3) is mixed to get feather protein viscose glue, carries out wet spinning and obtains feather protein viscose;
(5) the feather protein viscose that step (4) obtained successively carries out coagulating bath process, pickling, washing are dried and obtained albumen feather fiber.
The eider down composite fibre performance indications parameter using the present invention to prepare is as follows:
Hydroscopicity (%): 11.5;
Regain (%): 5.1;
Extensibility (%): 28.3;
Tensile break strength (N): 5.1.
Claims (2)
1. the eider down composite fibre that a soft skin pro-skin is effective, it is characterized in that, be made up of the raw material of following weight portion: poultry feather 70-100, goose down 13-15, ramee 30-50, silane coupler kh5907-10, urea 5-7, potassium metabisulfite 0.2-0.4, lauryl sodium sulfate 0.1-0.3, betaine 1-3, Tea Saponin 0.4-0.7, wax ester 0.2-0.5, collagen fabric 2-4, water are appropriate.
2. the eider down composite fibre that a kind of soft skin pro-skin is effective according to claim 1, is characterized in that, be made up of following concrete steps:
(1) poultry feather and feather stem are separated, use clear water rinsed clean respectively, dry, carry out processed, feather extruding is separated, and feather stem carries out torsion extruding, sterilizing and deodorization at 100-200 DEG C in high-pressure sterilizing pot is added to goose down mixing after again feather and feather stem being cut into mean size, after spontaneous combustion cooling, mixing feather material is placed in alcohol and soaks 4-6 hour, then be neutral post-drying with clear water washing surface, be ground into powder for subsequent use;
(2) the silane coupler kh590 acetone soln of 10-15 times amount is dissolved, then add Powdered feather meal, mixed at high speed is even, and raised temperature to 80 DEG C constant temperature keeps 1h, heating is back to except desolventizing again, and crushed after being dried obtains modified fish oil powder;
(3) urea, Sodium Metabisulfite and lauryl sodium sulfate are mixed, be dissolved in water and make the concentration of urea be 0.1mol/l, the modified fish oil powder that step (2) obtains is added in lysate, seal bottleneck and be placed in 95 ° of C water-bath concussion pots with the rotating speed of 100r/min concussion 20-25min, residue filter is removed by rapid gauze, obtains feather keratin solution for standby;
(4) water betaine being added 30 times amount makes solution, add Tea Saponin, wax ester, collagen fabric mixing and stirring again, ramee is processed into cellulose sulfonate solution through yellow again after dipping by lye, add betaine mixed solution again to stir, then the keratin solution obtained with step (3) is mixed to get feather protein viscose glue, carries out wet spinning and obtains feather protein viscose;
(5) the feather protein viscose that step (4) obtained successively carries out coagulating bath process, pickling, washing are dried and obtained albumen feather fiber.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510368720.8A CN104947239A (en) | 2015-06-26 | 2015-06-26 | Down feather composite fiber having good skin smoothing and skin-friendly effects |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510368720.8A CN104947239A (en) | 2015-06-26 | 2015-06-26 | Down feather composite fiber having good skin smoothing and skin-friendly effects |
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| CN104947239A true CN104947239A (en) | 2015-09-30 |
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| CN201510368720.8A Pending CN104947239A (en) | 2015-06-26 | 2015-06-26 | Down feather composite fiber having good skin smoothing and skin-friendly effects |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1435516A (en) * | 2002-12-12 | 2003-08-13 | 内蒙古鄂尔多斯羊绒集团有限责任公司 | Technique for processing regenerated keratin functional fibre |
| CN102733001A (en) * | 2012-07-11 | 2012-10-17 | 成都起点投资有限公司 | Feather protein fiber and method for preparing same |
| CN102899741A (en) * | 2012-04-28 | 2013-01-30 | 四川省宜宾惠美线业有限责任公司 | Viscose filament yarns prepared from feather protein and wood fibers and preparation method thereof |
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2015
- 2015-06-26 CN CN201510368720.8A patent/CN104947239A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1435516A (en) * | 2002-12-12 | 2003-08-13 | 内蒙古鄂尔多斯羊绒集团有限责任公司 | Technique for processing regenerated keratin functional fibre |
| CN102899741A (en) * | 2012-04-28 | 2013-01-30 | 四川省宜宾惠美线业有限责任公司 | Viscose filament yarns prepared from feather protein and wood fibers and preparation method thereof |
| CN102733001A (en) * | 2012-07-11 | 2012-10-17 | 成都起点投资有限公司 | Feather protein fiber and method for preparing same |
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Application publication date: 20150930 |