CN104941246A - Impinging stream super-gravity liquid-liquid extractor - Google Patents
Impinging stream super-gravity liquid-liquid extractor Download PDFInfo
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Abstract
本发明涉及一种撞击流超重力液液萃取器,属于化工及冶金设备技术领域。该撞击流超重力液液萃取器,包括动力传递结构、液体收集器机构、转轴结构、液体传质结构及固定构件结构,动力传递结构为上下两套对称的动力传递机构,将萃取液体喷入液体收集器机构,萃取液体在转轴结构和液体传质结构内处于滞留并紊乱的对撞状态中,完成萃取后从该萃取器中流出。该萃取器采用双电机驱动,增加了超重力萃取反应器的可调参数,涡流挡板产生的负压及锥筒多孔板的共同作用延长了混合液体的传质过程,增大了传质面积。
The invention relates to an impinging flow supergravity liquid-liquid extractor, which belongs to the technical field of chemical and metallurgical equipment. The impinging flow supergravity liquid-liquid extractor includes a power transmission structure, a liquid collector mechanism, a rotating shaft structure, a liquid mass transfer structure and a fixed component structure. In the liquid collector mechanism, the extraction liquid is in a stagnant and turbulent collision state in the rotating shaft structure and the liquid mass transfer structure, and flows out of the extractor after the extraction is completed. The extractor is driven by dual motors, which increases the adjustable parameters of the high-gravity extraction reactor. The negative pressure generated by the vortex baffle and the multi-hole plate of the cone tube prolong the mass transfer process of the mixed liquid and increase the mass transfer area. .
Description
技术领域 technical field
本发明涉及一种撞击流超重力液液萃取器,属于化工及冶金设备技术领域。 The invention relates to an impinging flow supergravity liquid-liquid extractor, which belongs to the technical field of chemical and metallurgical equipment.
背景技术 Background technique
超重力旋转设备是上世纪80年代初兴起的一种新型设备。与传统的设备相比,具有传质效率高,设备体积小,占地面积小,液体利用率高,能耗低等优势。一般超重力场旋转设备是由机壳、转子、物料进口、物料出口、转轴和电机组成,但目前多见的转子都是同心圆槽的填料转子,并且需要的丝网填料面积大,易造成材料的浪费,检修和维护不方便。 Hypergravity rotating equipment is a new type of equipment that emerged in the early 1980s. Compared with traditional equipment, it has the advantages of high mass transfer efficiency, small equipment volume, small footprint, high liquid utilization rate and low energy consumption. Generally, the high-gravity field rotating equipment is composed of a casing, a rotor, a material inlet, a material outlet, a rotating shaft and a motor. However, the most common rotors at present are filled rotors with concentric circular grooves, and the required wire mesh packing area is large, which is easy to cause Waste of materials, inconvenient overhaul and maintenance.
中国专利数据库中已有一些属于超重力场反应方法或反应设备的专利申请件,例如91109255.2号《旋转床超重力场强化传递与反应装置》、91229204.0号《旋转床超重力场传递与反应装置》、99105437.7号《涡流式超重力场反应装置及其应用》、99200696.1号《超重力场传质、反应装置》、99208429.6号《气动涡流式超重力场反应装置》、01143459.7号《超重力场中高压旋转床气液传质与反应设备》、200310103434.6号《一种超重力场旋转床传质与反应设备》、200410073624.2号《一种在超重力场中进行催化反应的方法》、02224172.8号《旋转床超重力多相反应器》等。但目前针对液液萃取的超重力设备开发较少。 There are already some patent applications belonging to the hypergravity field reaction method or reaction equipment in the Chinese patent database, such as No. 91109255.2 "Rotating Bed Supergravity Field Enhanced Transmission and Reaction Device", No. 91229204.0 "Rotating Bed Supergravity Field Transmission and Reaction Device" , No. 99105437.7 "Vortex Type Supergravity Field Reactor and Its Application", No. 99200696.1 "Mass Transfer and Reactor in Supergravity Field", No. 99208429.6 "Aerodynamic Vortex Type Supergravity Field Reactor", No. 01143459.7 "Medium and High Pressure in Supergravity Field Rotating Bed Gas-Liquid Mass Transfer and Reaction Equipment", No. 200310103434.6 "A Mass Transfer and Reaction Equipment for a Rotating Bed in a Supergravity Field", No. 200410073624.2 "A Method for Catalytic Reaction in a Supergravity Field", No. 02224172.8 "Rotating Bed High Gravity Multiphase Reactor", etc. However, the development of high-gravity equipment for liquid-liquid extraction is less.
发明内容 Contents of the invention
针对上述现有技术存在的问题及不足,本发明提供一种撞击流超重力液液萃取器。该萃取器采用双电机驱动,增加了超重力萃取反应器的可调参数,涡流挡板产生的负压及锥筒多孔板的共同作用延长了混合液体的传质过程,增大了传质面积,本发明通过以下技术方案实现。 Aiming at the problems and deficiencies in the above-mentioned prior art, the present invention provides an impinging flow high-gravity liquid-liquid extractor. The extractor is driven by dual motors, which increases the adjustable parameters of the high-gravity extraction reactor. The negative pressure generated by the vortex baffle and the multi-hole plate of the cone tube prolong the mass transfer process of the mixed liquid and increase the mass transfer area. , the present invention is realized through the following technical solutions.
一种撞击流超重力液液萃取器,包括动力传递结构、液体收集器机构、转轴结构、液体传质结构及固定构件结构,动力传递结构为上下两套对称的动力传递机构,液体收集器机构包括水嘴2、液体收集器端盖3、液体收集器4和唇形密封圈5,液体收集器机构为上下两套对称的结构,转轴结构包括轴承6、轴承座7和转轴,转轴结构为上下两套对称的结构,转轴根据位置分为上下对称的上转轴13和下转轴19,液体传质结构包括上转轴螺旋多孔板14、锥筒多孔板15、涡流挡板16、喷淋管17、下转轴螺旋多孔板18、螺旋导流槽20和出液口22,固定构件结构包括机架8和壳体21; An impinging flow supergravity liquid-liquid extractor, including a power transmission structure, a liquid collector mechanism, a rotating shaft structure, a liquid mass transfer structure and a fixed component structure, the power transmission structure is two sets of upper and lower symmetrical power transmission mechanisms, and the liquid collector mechanism Including faucet 2, liquid collector end cover 3, liquid collector 4 and lip seal ring 5, the liquid collector mechanism is two sets of upper and lower symmetrical structures, the rotating shaft structure includes bearing 6, bearing seat 7 and rotating shaft, the rotating shaft structure is Two sets of upper and lower symmetrical structures, the rotating shaft is divided into upper and lower symmetrical upper rotating shaft 13 and lower rotating shaft 19 according to the position, the liquid mass transfer structure includes the upper rotating shaft spiral perforated plate 14, cone perforated plate 15, vortex baffle 16, spray pipe 17 , the lower rotating shaft spiral perforated plate 18, the spiral guide groove 20 and the liquid outlet 22, the fixed component structure includes a frame 8 and a housing 21;
所述固定构件结构中机架8内固定壳体21,外置电动机1通过动力传递结构的同步带轮9将动力传递给转轴; In the fixed member structure, the housing 21 is fixed inside the frame 8, and the external motor 1 transmits power to the rotating shaft through the synchronous pulley 9 of the power transmission structure;
所述转轴结构中转轴通过轴承6和轴承座7固定在机架8上,轴承座7通过螺钉联接固定在机架8上,轴承6内圈与转轴配合,外圈与轴承座7配合,转轴从中间位置垂直插入壳体21内部,转轴为空心轴; In the structure of the rotating shaft, the rotating shaft is fixed on the frame 8 through the bearing 6 and the bearing seat 7, the bearing seat 7 is fixed on the frame 8 through screw connection, the inner ring of the bearing 6 is matched with the rotating shaft, the outer ring is matched with the bearing seat 7, and the rotating shaft Vertically inserted into the housing 21 from the middle position, the rotating shaft is a hollow shaft;
所述液体收集器机构中水嘴2通过内外管螺纹配合固定在液体收集器端盖3顶部,收集器端盖3与液体收集器4间隙配合,收集器端盖3通过螺钉联接固定在液体收集器4上,液体收集器4通过唇形密封圈5与转轴连接,唇形密封圈5内圈与转轴配合,外圈与液体收集器4的内腔配合; In the liquid collector mechanism, the faucet 2 is fixed on the top of the liquid collector end cap 3 through internal and external pipe threads, the collector end cap 3 and the liquid collector 4 are in clearance fit, and the collector end cap 3 is fixed on the liquid collector through screw connection. On the device 4, the liquid collector 4 is connected to the rotating shaft through the lip seal ring 5, the inner ring of the lip seal ring 5 cooperates with the rotating shaft, and the outer ring cooperates with the inner cavity of the liquid collector 4;
所述液体传质结构中,上转轴螺旋多孔板14通过螺钉联接固定在上转轴13底端,锥筒多孔板15固定在上转轴螺旋多孔板14下端面,锥筒多孔板15表面均匀焊接涡流挡板16,转轴空心口与喷淋管17入口连接,喷淋管17通过内外螺纹配合固定在转轴上,下转轴19上端通过螺钉联接固定下转轴螺旋多孔板18,螺旋导流槽20通过螺钉联接固定在壳体21内部底部,壳体21底端设有出液口22。 In the liquid mass transfer structure, the upper rotating shaft spiral porous plate 14 is fixed on the bottom of the upper rotating shaft 13 through screw connection, the cone porous plate 15 is fixed on the lower end surface of the upper rotating shaft spiral porous plate 14, and the surface of the cone porous plate 15 is evenly welded with eddy current The baffle plate 16, the hollow opening of the rotating shaft is connected with the inlet of the spray pipe 17, the spray pipe 17 is fixed on the rotating shaft through internal and external threads, the upper end of the lower rotating shaft 19 is fixed by screw connection and the lower rotating shaft spiral perforated plate 18, and the spiral guide groove 20 is connected by screws It is connected and fixed on the inner bottom of the housing 21 , and the bottom of the housing 21 is provided with a liquid outlet 22 .
所述转轴为带法兰盘的阶梯轴,法兰盘上均布用于螺纹联接的通孔,转轴底部内孔设计为与喷淋管17相配合的内螺纹。 The rotating shaft is a stepped shaft with a flange, and through holes for threaded connection are evenly distributed on the flange, and the inner hole at the bottom of the rotating shaft is designed as an internal thread matched with the spray pipe 17 .
所述锥筒多孔板15的锥度为2o~5o,锥筒多孔板15为厚度1~2mm的不锈钢板,锥筒多孔板15表面均匀分布直径为1~2mm的微孔。 The conical perforated plate 15 has a taper of 2 o to 5 o , the perforated conical plate 15 is a stainless steel plate with a thickness of 1 to 2 mm, and micropores with a diameter of 1 to 2 mm are evenly distributed on the surface of the perforated conical plate 15.
所述涡流挡板16为3~6块,形状为直角梯形。 The vortex baffles 16 are 3-6 pieces, and the shape is a right-angled trapezoid.
所述上转轴螺旋多孔板14、下转轴螺旋多孔板18为厚度2~4mm的不锈钢板,在不锈钢板上均匀分布有直径为1~2mm的微孔,上转轴螺旋多孔板14、下转轴螺旋多孔板18的内侧和外侧都焊接有螺旋形不锈钢筋条。 The upper rotating shaft spiral porous plate 14 and the lower rotating shaft spiral porous plate 18 are stainless steel plates with a thickness of 2 to 4 mm, and micropores with a diameter of 1 to 2 mm are evenly distributed on the stainless steel plates. The upper rotating shaft spiral porous plate 14 and the lower rotating shaft spiral The inner and outer sides of the perforated plate 18 are welded with spiral stainless steel tendons.
所述螺旋导流槽20由从内到外高度依次升高的隔板组成,隔板的分布采用阿基米德螺旋线呈均匀分布。 The spiral diversion groove 20 is composed of baffles whose height increases sequentially from the inside to the outside, and the distribution of the baffles adopts the Archimedes spiral to be evenly distributed.
所述该撞击流超重力液液萃取器上部分的电机1停止转动,只调节下部分的电机1,该撞击流超重力液液萃取器转化为动静盘式折流超重力反应器。 The motor 1 on the upper part of the impinging flow supergravity liquid-liquid extractor stops rotating, and only the motor 1 on the lower part is adjusted, and the impinging flow supergravity liquid-liquid extractor is transformed into a dynamic and static disc baffle supergravity reactor.
本发明装置使用时,同时开启上、下两电机1电源,通过调频器及电源的接线方式可以分别调节上转轴13和下转轴19的转速及旋转方向。通过磁力泵及玻璃转子流量计调节两相液体的压力和流速后,将两相液体分别通过上、下的水嘴2,进入液体收集器4的腔体内,上转轴13虽然处于旋转状态,但不断向液体收集器4喷入的液体将会涌入上转轴13的中空通道,并通过喷淋管17向外喷射。两相液体分别从上、下两个喷淋管喷出后实现了逆流对撞后,将向外喷射,遇到随着上转轴13一同旋转的锥筒多孔板15及涡流挡板16,在涡流挡板16的阻挡作用下,混合液体将在锥筒多孔板15内处于滞留并紊乱的对撞状态中,锥筒的锥度有利于液体更长时间的滞留。混合液体穿过锥筒多孔板15的小孔后,在离心力的作用下喷向下转轴螺旋多孔板18,在下转轴螺旋多孔板18的不同转速及分布在其内外壁上的螺旋筋条的共同作用下,混合液体将在锥筒多孔板15和下转轴螺旋多孔板18之间处于滞留并紊乱的对撞状态。混合液体穿过下转轴螺旋多孔板18的小孔后,在离心力的作用下喷向上转轴螺旋多孔板14,在上转轴螺旋多孔板14的不同转速及分布在其内外壁上的螺旋筋条的共同作用下,混合液体将在上转轴螺旋多孔板14和下转轴螺旋多孔板18之间处于滞留并紊乱的对撞状态。混合液体穿过上转轴螺旋多孔板14的小孔后,在离心力的作用下喷固定在壳体21上静止不动的螺旋导流槽20上,经过螺旋导流槽20的折流通道之后,将沉积在壳体21的内壁底部,通过出液口22,流出到壳体21的外部。 When the device of the present invention is in use, the power supply of the upper and lower motors 1 is turned on simultaneously, and the speed and direction of rotation of the upper rotating shaft 13 and the lower rotating shaft 19 can be adjusted respectively through the frequency regulator and the wiring mode of the power supply. After adjusting the pressure and flow rate of the two-phase liquid through the magnetic pump and glass rotameter, the two-phase liquid passes through the upper and lower faucets 2 respectively and enters the cavity of the liquid collector 4. Although the upper shaft 13 is in a rotating state, The liquid continuously sprayed into the liquid collector 4 will pour into the hollow channel of the upper rotating shaft 13 and spray outwards through the spray pipe 17 . After the two-phase liquid is sprayed from the upper and lower spray pipes and realizes countercurrent collision, it will spray outwards and encounter the cone perforated plate 15 and the vortex baffle 16 that rotate with the upper shaft 13. Under the blocking effect of the vortex baffle 16, the mixed liquid will be in a stagnant and chaotic collision state in the cone perforated plate 15, and the taper of the cone is beneficial for the liquid to stay for a longer time. After the mixed liquid passes through the small hole of the cone perforated plate 15, it is sprayed down the spiral perforated plate 18 under the action of centrifugal force. Under the action, the mixed liquid will be in stagnant and chaotic collision state between the cone perforated plate 15 and the lower rotating shaft helical perforated plate 18 . After the mixed liquid passes through the small hole of the spiral porous plate 18 of the lower rotating shaft, it is sprayed on the spiral porous plate 14 of the upward rotating shaft under the action of centrifugal force. Under the combined action, the mixed liquid will be in a stagnant and chaotic collision state between the upper rotating shaft helical perforated plate 14 and the lower rotating shaft helical perforated plate 18 . After the mixed liquid passes through the small hole of the spiral perforated plate 14 on the upper shaft, it is sprayed and fixed on the stationary spiral guide groove 20 on the housing 21 under the action of centrifugal force, and after passing through the baffle channel of the spiral guide groove 20, The deposits will be deposited on the bottom of the inner wall of the housing 21 and flow out to the outside of the housing 21 through the liquid outlet 22 .
反应器内各部件的材质均为耐腐蚀的不锈钢。所有多孔板中小孔直径的大小及小孔间的间距需根据具体的液体粘度与性质决定。 All parts in the reactor are made of corrosion-resistant stainless steel. The size of the diameter of the small holes and the spacing between the small holes in all perforated plates need to be determined according to the specific viscosity and properties of the liquid.
本发明的有益效果是:1、双电机驱动,增加了超重力萃取反应器的可调参数;2、两相液体经过喷淋管喷出实现了逆流对撞效果,提高了初次混合传质效率;3、涡流挡板产生的负压及锥筒多孔板的共同作用延长了混合液体的传质过程,增大了传质面积;4、上下转轴螺旋多孔板的微孔结构及带螺旋的内外螺旋筋条改变了混合液体的运动轨迹,增大了传质面积、延长了反应时间,提高了传质效果;5、螺旋导流槽的阿基米德螺旋线结构延长了混合液体在反应器的滞留时间。6、多孔板的采用避免了传统填料可能出现的堵塞现象。 The beneficial effects of the present invention are: 1. Driven by double motors, the adjustable parameters of the hypergravity extraction reactor are increased; 2. The two-phase liquid is sprayed out through the spray pipe to realize the effect of countercurrent collision and improve the efficiency of primary mixing and mass transfer ; 3. The negative pressure generated by the vortex baffle and the combined effect of the cone porous plate prolong the mass transfer process of the mixed liquid and increase the mass transfer area; The spiral ribs change the trajectory of the mixed liquid, increase the mass transfer area, prolong the reaction time, and improve the mass transfer effect; residence time. 6. The use of porous plates avoids the possible clogging of traditional packing.
附图说明 Description of drawings
图1是本发明撞击流超重力液液萃取器结构示意图; Fig. 1 is the structure schematic diagram of impinging flow hypergravity liquid-liquid extractor of the present invention;
图2是本发明撞击流超重力液液萃取器的电机、壳体与支架结构示意图; Fig. 2 is a structural schematic diagram of the motor, housing and support of the impinging flow hypergravity liquid-liquid extractor of the present invention;
图3是本发明撞击流超重力液液萃取器的液体收集器机构结构示意图; Fig. 3 is a structural schematic diagram of the liquid collector mechanism of the impinging flow hypergravity liquid-liquid extractor of the present invention;
图4是本发明撞击流超重力液液萃取器的上转轴结构示意图; Fig. 4 is a schematic diagram of the structure of the upper shaft of the impinging flow hypergravity liquid-liquid extractor of the present invention;
图5是本发明撞击流超重力液液萃取器的上转轴俯视示意图; Fig. 5 is a top view schematic diagram of the upper rotating shaft of the impinging flow hypergravity liquid-liquid extractor of the present invention;
图6是本发明喷流撞击超重力液液萃取器的锥筒多孔板与涡流挡板示意图; Fig. 6 is a schematic diagram of the cone perforated plate and the vortex baffle of the jet impinging on the supergravity liquid-liquid extractor of the present invention;
图7是本发明喷流撞击超重力液液萃取器的锥筒多孔板与涡流挡板俯视示意图; Fig. 7 is a top view schematic diagram of the cone perforated plate and the vortex baffle of the jet impinging on the supergravity liquid-liquid extractor of the present invention;
图8是本发明喷流撞击超重力液液萃取器的下转轴螺旋多孔板示意图; Fig. 8 is a schematic diagram of the lower rotating shaft spiral porous plate of the jet impinging on the supergravity liquid-liquid extractor of the present invention;
图9是本发明喷流撞击超重力液液萃取器的上转轴螺旋多孔板示意图; Fig. 9 is a schematic diagram of the upper rotating shaft spiral porous plate of the jet impinging on the supergravity liquid-liquid extractor of the present invention;
图10是本发明喷流撞击超重力液液萃取器的阿基米德螺旋导流槽示意图A; Fig. 10 is a schematic diagram A of the Archimedes spiral diversion tank of the jet impinging on the hypergravity liquid-liquid extractor of the present invention;
图11是本发明喷流撞击超重力液液萃取器的阿基米德螺旋导流槽示意图B; Fig. 11 is a schematic diagram B of the Archimedes spiral diversion groove of the jet impinging on the hypergravity liquid-liquid extractor of the present invention;
图中:1-电机,2-水嘴,3-液体收集器端盖,4-液体收集器,5-唇形密封圈,6-轴承,7-轴承座,8-机架,9-同步带轮,10-壳体端盖,11-调心轴承,12-壳体盖板,13-上转轴,14-上转轴螺旋多孔板,15-锥筒多孔板,16-涡流挡板,17-喷淋管,18-下转轴螺旋多孔板,19-下转轴,20-螺旋导流槽,21-壳体,22-出液口。 In the figure: 1-motor, 2-faucet, 3-end cover of liquid collector, 4-liquid collector, 5-lip seal, 6-bearing, 7-bearing housing, 8-frame, 9-synchronization Pulley, 10-shell end cover, 11-aligning bearing, 12-shell cover plate, 13-upper shaft, 14-upper shaft spiral perforated plate, 15-cone tube perforated plate, 16-vortex baffle, 17 -Spray pipe, 18-lower shaft spiral perforated plate, 19-lower shaft, 20-spiral diversion groove, 21-housing, 22-liquid outlet.
具体实施方式 Detailed ways
下面结合附图和具体实施方式,对本发明作进一步说明。 The present invention will be further described below in combination with the accompanying drawings and specific embodiments.
实施例1 Example 1
如图1至11所示,该撞击流超重力液液萃取器,包括动力传递结构、液体收集器机构、转轴结构、液体传质结构及固定构件结构,动力传递结构为上下两套对称的动力传递机构,液体收集器机构包括水嘴2、液体收集器端盖3、液体收集器4和唇形密封圈5,液体收集器机构为上下两套对称的结构,转轴结构包括轴承6、轴承座7和转轴,转轴结构为上下两套对称的结构,转轴根据位置分为上下对称的上转轴13和下转轴19,液体传质结构包括上转轴螺旋多孔板14、锥筒多孔板15、涡流挡板16、喷淋管17、下转轴螺旋多孔板18、螺旋导流槽20和出液口22,固定构件结构包括机架8和壳体21; As shown in Figures 1 to 11, the impinging flow hypergravity liquid-liquid extractor includes a power transmission structure, a liquid collector mechanism, a rotating shaft structure, a liquid mass transfer structure and a fixed component structure, and the power transmission structure is two sets of upper and lower symmetrical power The transmission mechanism, the liquid collector mechanism includes the faucet 2, the liquid collector end cover 3, the liquid collector 4 and the lip seal ring 5, the liquid collector mechanism has two sets of upper and lower symmetrical structures, the rotating shaft structure includes the bearing 6, the bearing seat 7 and the rotating shaft. The rotating shaft structure is two sets of upper and lower symmetrical structures. The rotating shaft is divided into upper and lower symmetrical upper rotating shaft 13 and lower rotating shaft 19 according to the position. The liquid mass transfer structure includes the upper rotating shaft spiral perforated plate 14, cone perforated plate 15, vortex baffle Plate 16, spray pipe 17, lower rotating shaft spiral perforated plate 18, spiral guide groove 20 and liquid outlet 22, the fixed component structure includes a frame 8 and a housing 21;
所述固定构件结构中机架8内固定壳体21,外置电动机1通过动力传递结构的同步带轮9将动力传递给转轴; In the fixed member structure, the housing 21 is fixed inside the frame 8, and the external motor 1 transmits power to the rotating shaft through the synchronous pulley 9 of the power transmission structure;
所述转轴结构中转轴通过轴承6和轴承座7固定在机架8上,轴承座7通过螺钉联接固定在机架8上,轴承6内圈与转轴配合,外圈与轴承座7配合,转轴从中间位置垂直插入壳体21内部,转轴为空心轴; In the structure of the rotating shaft, the rotating shaft is fixed on the frame 8 through the bearing 6 and the bearing seat 7, the bearing seat 7 is fixed on the frame 8 through screw connection, the inner ring of the bearing 6 is matched with the rotating shaft, the outer ring is matched with the bearing seat 7, and the rotating shaft Vertically inserted into the housing 21 from the middle position, the rotating shaft is a hollow shaft;
所述液体收集器机构中水嘴2通过内外管螺纹配合固定在液体收集器端盖3顶部,收集器端盖3与液体收集器4间隙配合,收集器端盖3通过螺钉联接固定在液体收集器4上,液体收集器4通过唇形密封圈5与转轴连接,唇形密封圈5内圈与转轴配合,外圈与液体收集器4的内腔配合; In the liquid collector mechanism, the faucet 2 is fixed on the top of the liquid collector end cap 3 through internal and external pipe threads, the collector end cap 3 and the liquid collector 4 are in clearance fit, and the collector end cap 3 is fixed on the liquid collector through screw connection. On the device 4, the liquid collector 4 is connected to the rotating shaft through the lip seal ring 5, the inner ring of the lip seal ring 5 cooperates with the rotating shaft, and the outer ring cooperates with the inner cavity of the liquid collector 4;
所述液体传质结构中,上转轴螺旋多孔板14通过螺钉联接固定在上转轴13底端,锥筒多孔板15固定上转轴螺旋多孔板14下端面,锥筒多孔板15表面均匀焊接涡流挡板16,转轴空心口与喷淋管17入口连接,喷淋管17通过内外螺纹配合固定在转轴上,下转轴19上端通过螺钉联接固定下转轴螺旋多孔板18,螺旋导流槽20通过螺钉联接固定在壳体21内部底部,壳体21底端设有出液口22。 In the liquid mass transfer structure, the upper rotating shaft spiral porous plate 14 is fixed on the bottom of the upper rotating shaft 13 through screw connection, the cone porous plate 15 is fixed on the lower end surface of the upper rotating shaft spiral porous plate 14, and the surface of the cone porous plate 15 is evenly welded to the eddy current baffle The plate 16, the hollow opening of the rotating shaft is connected with the inlet of the spray pipe 17, the spray pipe 17 is fixed on the rotating shaft through internal and external threads, the upper end of the lower rotating shaft 19 is fixed by screw connection, and the lower rotating shaft spiral perforated plate 18 is fixed, and the spiral guide groove 20 is connected by screws It is fixed on the inner bottom of the housing 21 , and the bottom of the housing 21 is provided with a liquid outlet 22 .
其中转轴为带法兰盘的阶梯轴,法兰盘上均布用于螺纹联接的通孔,转轴底部内孔设计为与喷淋管17相配合的内螺纹;锥筒多孔板15的锥度为2o,锥筒多孔板15为厚度1mm的不锈钢板,锥筒多孔板15表面均匀分布直径为1mm的微孔;所述涡流挡板16为3~6块,形状为直角梯形;所述上转轴螺旋多孔板14、下转轴螺旋多孔板18为厚度2mm的不锈钢板,在不锈钢板上均匀分布有直径为1mm的微孔,上转轴螺旋多孔板14、下转轴螺旋多孔板18的内侧和外侧都焊接有螺旋形不锈钢筋条;螺旋导流槽20由从内到外高度依次升高的隔板组成,隔板的分布采用阿基米德螺旋线呈均匀分布。 Wherein the rotating shaft is a stepped shaft with a flange, and the flange is evenly distributed with through holes for threaded connection, and the inner hole at the bottom of the rotating shaft is designed as an internal thread matched with the spray pipe 17; the taper of the cone perforated plate 15 is 2 o , the cone-tube perforated plate 15 is a stainless steel plate with a thickness of 1mm, and micropores with a diameter of 1mm are evenly distributed on the surface of the cone-tube perforated plate 15; the vortex baffles 16 are 3 to 6 pieces, and the shape is a right-angled trapezoid; The rotating shaft spiral perforated plate 14 and the lower rotating shaft spiral perforated plate 18 are stainless steel plates with a thickness of 2 mm, and micropores with a diameter of 1 mm are evenly distributed on the stainless steel plates. All are welded with spiral stainless steel ribs; the spiral diversion groove 20 is composed of baffles whose heights rise sequentially from the inside to the outside, and the distribution of the baffles adopts the Archimedes spiral to form a uniform distribution.
实施例2 Example 2
如图1至11所示,该撞击流超重力液液萃取器,包括动力传递结构、液体收集器机构、转轴结构、液体传质结构及固定构件结构,动力传递结构为上下两套对称的动力传递机构,液体收集器机构包括水嘴2、液体收集器端盖3、液体收集器4和唇形密封圈5,液体收集器机构为上下两套对称的结构,转轴结构包括轴承6、轴承座7和转轴,转轴结构为上下两套对称的结构,转轴根据位置分为上下对称的上转轴13和下转轴19,液体传质结构包括上转轴螺旋多孔板14、锥筒多孔板15、涡流挡板16、喷淋管17、下转轴螺旋多孔板18、螺旋导流槽20和出液口22,固定构件结构包括机架8和壳体21; As shown in Figures 1 to 11, the impinging flow hypergravity liquid-liquid extractor includes a power transmission structure, a liquid collector mechanism, a rotating shaft structure, a liquid mass transfer structure and a fixed component structure, and the power transmission structure is two sets of upper and lower symmetrical power The transmission mechanism, the liquid collector mechanism includes the faucet 2, the liquid collector end cover 3, the liquid collector 4 and the lip seal ring 5, the liquid collector mechanism has two sets of upper and lower symmetrical structures, the rotating shaft structure includes the bearing 6, the bearing seat 7 and the rotating shaft. The rotating shaft structure is two sets of upper and lower symmetrical structures. The rotating shaft is divided into upper and lower symmetrical upper rotating shaft 13 and lower rotating shaft 19 according to the position. The liquid mass transfer structure includes the upper rotating shaft spiral perforated plate 14, cone perforated plate 15, vortex baffle Plate 16, spray pipe 17, lower rotating shaft spiral perforated plate 18, spiral guide groove 20 and liquid outlet 22, the fixed component structure includes a frame 8 and a housing 21;
所述固定构件结构中机架8内固定壳体21,外置电动机1通过动力传递结构的同步带轮9将动力传递给转轴; In the fixed member structure, the housing 21 is fixed inside the frame 8, and the external motor 1 transmits power to the rotating shaft through the synchronous pulley 9 of the power transmission structure;
所述转轴结构中转轴通过轴承6和轴承座7固定在机架8上,轴承座7通过螺钉联接固定在机架8上,轴承6内圈与转轴配合,外圈与轴承座7配合,转轴从中间位置垂直插入壳体21内部,转轴为空心轴; In the structure of the rotating shaft, the rotating shaft is fixed on the frame 8 through the bearing 6 and the bearing seat 7, the bearing seat 7 is fixed on the frame 8 through screw connection, the inner ring of the bearing 6 cooperates with the rotating shaft, the outer ring cooperates with the bearing seat 7, and the rotating shaft Vertically inserted into the housing 21 from the middle position, the rotating shaft is a hollow shaft;
所述液体收集器机构中水嘴2通过内外管螺纹配合固定在液体收集器端盖3顶部,收集器端盖3与液体收集器4间隙配合,收集器端盖3通过螺钉联接固定在液体收集器4上,液体收集器4通过唇形密封圈5与转轴连接,唇形密封圈5内圈与转轴配合,外圈与液体收集器4的内腔配合; In the liquid collector mechanism, the faucet 2 is fixed on the top of the liquid collector end cap 3 through internal and external pipe threads, the collector end cap 3 and the liquid collector 4 are in clearance fit, and the collector end cap 3 is fixed on the liquid collector through screw connection. On the device 4, the liquid collector 4 is connected to the rotating shaft through the lip seal ring 5, the inner ring of the lip seal ring 5 cooperates with the rotating shaft, and the outer ring cooperates with the inner cavity of the liquid collector 4;
所述液体传质结构中,上转轴螺旋多孔板14通过螺钉联接固定在上转轴13底端,锥筒多孔板15固定上转轴螺旋多孔板14下端面,锥筒多孔板15表面均匀焊接涡流挡板16,转轴空心口与喷淋管17入口连接,喷淋管17通过内外螺纹配合固定在转轴上,下转轴19上端通过螺钉联接固定下转轴螺旋多孔板18,螺旋导流槽20通过螺钉联接固定在壳体21内部底部,壳体21底端设有出液口22。 In the liquid mass transfer structure, the upper rotating shaft spiral porous plate 14 is fixed on the bottom of the upper rotating shaft 13 through screw connection, the cone porous plate 15 is fixed on the lower end surface of the upper rotating shaft spiral porous plate 14, and the surface of the cone porous plate 15 is evenly welded to the eddy current baffle The plate 16, the hollow opening of the rotating shaft is connected with the inlet of the spray pipe 17, the spray pipe 17 is fixed on the rotating shaft through internal and external threads, the upper end of the lower rotating shaft 19 is fixed by screw connection, and the lower rotating shaft spiral perforated plate 18 is fixed, and the spiral guide groove 20 is connected by screws It is fixed on the inner bottom of the housing 21 , and the bottom of the housing 21 is provided with a liquid outlet 22 .
其中转轴为带法兰盘的阶梯轴,法兰盘上均布用于螺纹联接的通孔,转轴底部内孔设计为与喷淋管17相配合的内螺纹;锥筒多孔板15的锥度为5o,锥筒多孔板15为厚度2mm的不锈钢板,锥筒多孔板15表面均匀分布直径为2mm的微孔;所述涡流挡板16为6~8块,形状为直角梯形;所述上转轴螺旋多孔板14、下转轴螺旋多孔板18为厚度3mm的不锈钢板,在不锈钢板上均匀分布有直径为2mm的微孔,上转轴螺旋多孔板14、下转轴螺旋多孔板18的内侧和外侧都焊接有螺旋形不锈钢筋条;螺旋导流槽20由从内到外高度依次升高的隔板组成,隔板的分布采用阿基米德螺旋线呈均匀分布。 Wherein the rotating shaft is a stepped shaft with a flange, and the flange is evenly distributed with through holes for threaded connection, and the inner hole at the bottom of the rotating shaft is designed as an internal thread matched with the spray pipe 17; the taper of the cone perforated plate 15 is 5 ° , the conical perforated plate 15 is a stainless steel plate with a thickness of 2mm, and micropores with a diameter of 2mm are evenly distributed on the surface of the conical perforated plate 15; the vortex baffles 16 are 6 to 8 pieces, and the shape is a right-angled trapezoid; The rotating shaft spiral perforated plate 14 and the lower rotating shaft spiral perforated plate 18 are stainless steel plates with a thickness of 3 mm, and micropores with a diameter of 2 mm are evenly distributed on the stainless steel plates. All are welded with spiral stainless steel ribs; the spiral diversion groove 20 is composed of baffles whose heights rise sequentially from the inside to the outside, and the distribution of the baffles adopts the Archimedes spiral to form a uniform distribution.
实施例3 Example 3
如图1至11所示,该撞击流超重力液液萃取器,包括动力传递结构、液体收集器机构、转轴结构、液体传质结构及固定构件结构,动力传递结构为上下两套对称的动力传递机构,液体收集器机构包括水嘴2、液体收集器端盖3、液体收集器4和唇形密封圈5,液体收集器机构为上下两套对称的结构,转轴结构包括轴承6、轴承座7和转轴,转轴结构为上下两套对称的结构,转轴根据位置分为上下对称的上转轴13和下转轴19,液体传质结构包括上转轴螺旋多孔板14、锥筒多孔板15、涡流挡板16、喷淋管17、下转轴螺旋多孔板18、螺旋导流槽20和出液口22,固定构件结构包括机架8和壳体21; As shown in Figures 1 to 11, the impinging flow hypergravity liquid-liquid extractor includes a power transmission structure, a liquid collector mechanism, a rotating shaft structure, a liquid mass transfer structure and a fixed component structure, and the power transmission structure is two sets of upper and lower symmetrical power The transmission mechanism, the liquid collector mechanism includes the faucet 2, the liquid collector end cover 3, the liquid collector 4 and the lip seal ring 5, the liquid collector mechanism has two sets of upper and lower symmetrical structures, the rotating shaft structure includes the bearing 6, the bearing seat 7 and the rotating shaft. The rotating shaft structure is two sets of upper and lower symmetrical structures. The rotating shaft is divided into upper and lower symmetrical upper rotating shaft 13 and lower rotating shaft 19 according to the position. The liquid mass transfer structure includes the upper rotating shaft spiral perforated plate 14, cone perforated plate 15, vortex baffle Plate 16, spray pipe 17, lower rotating shaft spiral perforated plate 18, spiral guide groove 20 and liquid outlet 22, the fixed component structure includes a frame 8 and a housing 21;
所述固定构件结构中机架8内固定壳体21,外置电动机1通过动力传递结构的同步带轮9将动力传递给转轴; In the fixed member structure, the housing 21 is fixed inside the frame 8, and the external motor 1 transmits power to the rotating shaft through the synchronous pulley 9 of the power transmission structure;
所述转轴结构中转轴通过轴承6和轴承座7固定在机架8上,轴承座7通过螺钉联接固定在机架8上,轴承6内圈与转轴配合,外圈与轴承座7配合,转轴从中间位置垂直插入壳体21内部,转轴为空心轴; In the structure of the rotating shaft, the rotating shaft is fixed on the frame 8 through the bearing 6 and the bearing seat 7, the bearing seat 7 is fixed on the frame 8 through screw connection, the inner ring of the bearing 6 is matched with the rotating shaft, the outer ring is matched with the bearing seat 7, and the rotating shaft Vertically inserted into the housing 21 from the middle position, the rotating shaft is a hollow shaft;
所述液体收集器机构中水嘴2通过内外管螺纹配合固定在液体收集器端盖3顶部,收集器端盖3与液体收集器4间隙配合,收集器端盖3通过螺钉联接固定在液体收集器4上,液体收集器4通过唇形密封圈5与转轴连接,唇形密封圈5内圈与转轴配合,外圈与液体收集器4的内腔配合; In the liquid collector mechanism, the faucet 2 is fixed on the top of the liquid collector end cap 3 through internal and external pipe threads, the collector end cap 3 and the liquid collector 4 are in clearance fit, and the collector end cap 3 is fixed on the liquid collector through screw connection. On the device 4, the liquid collector 4 is connected to the rotating shaft through the lip seal ring 5, the inner ring of the lip seal ring 5 cooperates with the rotating shaft, and the outer ring cooperates with the inner cavity of the liquid collector 4;
所述液体传质结构中,上转轴螺旋多孔板14通过螺钉联接固定在上转轴13底端,锥筒多孔板15固定上转轴螺旋多孔板14下端面,锥筒多孔板15表面均匀焊接涡流挡板16,转轴空心口与喷淋管17入口连接,喷淋管17通过内外螺纹配合固定在转轴上,下转轴19上端通过螺钉联接固定下转轴螺旋多孔板18,螺旋导流槽20通过螺钉联接固定在壳体21内部底部,壳体21底端设有出液口22。 In the liquid mass transfer structure, the upper rotating shaft spiral porous plate 14 is fixed on the bottom of the upper rotating shaft 13 through screw connection, the cone porous plate 15 is fixed on the lower end surface of the upper rotating shaft spiral porous plate 14, and the surface of the cone porous plate 15 is evenly welded to the eddy current baffle The plate 16, the hollow opening of the rotating shaft is connected with the inlet of the spray pipe 17, the spray pipe 17 is fixed on the rotating shaft through internal and external threads, the upper end of the lower rotating shaft 19 is fixed by screw connection, and the lower rotating shaft spiral perforated plate 18 is fixed, and the spiral guide groove 20 is connected by screws It is fixed on the inner bottom of the housing 21 , and the bottom of the housing 21 is provided with a liquid outlet 22 .
其中转轴为带法兰盘的阶梯轴,法兰盘上均布用于螺纹联接的通孔,转轴底部内孔设计为与喷淋管17相配合的内螺纹;锥筒多孔板15的锥度为4o,锥筒多孔板15为厚度2mm的不锈钢板,锥筒多孔板15表面均匀分布直径为2mm的微孔;所述涡流挡板16为3~6块,形状为直角梯形;所述上转轴螺旋多孔板14、下转轴螺旋多孔板18为厚度3mm的不锈钢板,在不锈钢板上均匀分布有直径为2mm的微孔,上转轴螺旋多孔板14、下转轴螺旋多孔板18的内侧和外侧都焊接有螺旋形不锈钢筋条;螺旋导流槽20由从内到外高度依次升高的隔板组成,隔板的分布采用阿基米德螺旋线呈均匀分布。 Wherein the rotating shaft is a stepped shaft with a flange, and the flange is evenly distributed with through holes for threaded connection, and the inner hole at the bottom of the rotating shaft is designed as an internal thread matched with the spray pipe 17; the taper of the cone perforated plate 15 is 4 o , the cone-tube perforated plate 15 is a stainless steel plate with a thickness of 2 mm, and micropores with a diameter of 2 mm are evenly distributed on the surface of the cone-tube perforated plate 15; the vortex baffles 16 are 3 to 6 pieces, and the shape is a right-angled trapezoid; The rotating shaft spiral perforated plate 14 and the lower rotating shaft spiral perforated plate 18 are stainless steel plates with a thickness of 3 mm, and micropores with a diameter of 2 mm are evenly distributed on the stainless steel plates. All are welded with spiral stainless steel ribs; the spiral diversion groove 20 is composed of baffles whose heights rise sequentially from the inside to the outside, and the distribution of the baffles adopts the Archimedes spiral to form a uniform distribution.
所述该撞击流超重力液液萃取器上部分的电机1停止转动,只调节下部分的电机1,该撞击流超重力液液萃取器转化为动静盘式折流超重力反应器。 The motor 1 on the upper part of the impinging flow supergravity liquid-liquid extractor stops rotating, and only the motor 1 on the lower part is adjusted, and the impinging flow supergravity liquid-liquid extractor is transformed into a dynamic and static disc baffle supergravity reactor.
以上结合附图对本发明的具体实施方式作了详细说明,但是本发明并不限于上述实施方式,在本领域普通技术人员所具备的知识范围内,还可以在不脱离本发明宗旨的前提下做出各种变化。 The specific embodiments of the present invention have been described in detail above in conjunction with the accompanying drawings, but the present invention is not limited to the above embodiments. Various changes.
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| CN114433001A (en) * | 2020-10-31 | 2022-05-06 | 中国石油化工股份有限公司 | Series high-speed spinning flow gas-liquid mass transfer system |
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| CN103372328A (en) * | 2012-04-17 | 2013-10-30 | 青岛科技大学 | Rotating packed bed for dual-phase extraction |
| CN204671936U (en) * | 2015-04-21 | 2015-09-30 | 昆明理工大学 | A kind of percussion flow hypergravity liquid-liquid extraction device |
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2015
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| US20100270238A1 (en) * | 2009-04-23 | 2010-10-28 | Industrial Technology Research Institute | Method for transferring inorganic oxide nanoparticles from aqueous phase to organic phase |
| CN102441323A (en) * | 2011-11-03 | 2012-05-09 | 袁长胜 | Swirl double hypergravity machine |
| CN102583250A (en) * | 2012-03-19 | 2012-07-18 | 瓮福(集团)有限责任公司 | Device for extracting iodine from wet process phosphate acid liquor |
| CN103372328A (en) * | 2012-04-17 | 2013-10-30 | 青岛科技大学 | Rotating packed bed for dual-phase extraction |
| CN204671936U (en) * | 2015-04-21 | 2015-09-30 | 昆明理工大学 | A kind of percussion flow hypergravity liquid-liquid extraction device |
Cited By (7)
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| CN106075950A (en) * | 2016-06-24 | 2016-11-09 | 昆明理工大学 | A kind of Dual Drive cross_flow rotating packed bed |
| CN106075950B (en) * | 2016-06-24 | 2018-03-06 | 昆明理工大学 | A kind of dual drive cross_flow rotating packed bed |
| CN107158745A (en) * | 2016-10-18 | 2017-09-15 | 四川大学 | A kind of micro-extraction component and super gravity field micro-extraction device and extracting process |
| CN107158745B (en) * | 2016-10-18 | 2019-11-12 | 四川大学 | A kind of micro-extraction assembly and supergravity field micro-extraction device and extraction method |
| CN106865674A (en) * | 2017-03-01 | 2017-06-20 | 煤炭科学技术研究院有限公司 | A kind of method of the phenol wastewater extracting and dephenolizing of multistage mixed intensified separation |
| CN114433001A (en) * | 2020-10-31 | 2022-05-06 | 中国石油化工股份有限公司 | Series high-speed spinning flow gas-liquid mass transfer system |
| CN114433001B (en) * | 2020-10-31 | 2023-10-10 | 中国石油化工股份有限公司 | Tandem type high-speed spin flow gas-liquid mass transfer system |
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