CN104925324A - Preparation method of mezlocillin sodium for injection, convenient for removing rejects - Google Patents
Preparation method of mezlocillin sodium for injection, convenient for removing rejects Download PDFInfo
- Publication number
- CN104925324A CN104925324A CN201510200609.8A CN201510200609A CN104925324A CN 104925324 A CN104925324 A CN 104925324A CN 201510200609 A CN201510200609 A CN 201510200609A CN 104925324 A CN104925324 A CN 104925324A
- Authority
- CN
- China
- Prior art keywords
- controller
- mezlocillin
- preparation
- channel switch
- convenient
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000002360 preparation method Methods 0.000 title claims abstract description 26
- KCVTVKMPZQSSNU-UHFFFAOYSA-N 2-pyridin-4-ylethanethioyl chloride Chemical compound ClC(=S)CC1=CC=NC=C1 KCVTVKMPZQSSNU-UHFFFAOYSA-N 0.000 title claims abstract description 25
- 229960001994 mezlocillin sodium Drugs 0.000 title claims abstract description 25
- 238000002347 injection Methods 0.000 title abstract description 7
- 239000007924 injection Substances 0.000 title abstract description 7
- 239000003153 chemical reaction reagent Substances 0.000 claims abstract description 39
- 239000000843 powder Substances 0.000 claims abstract description 14
- 238000012856 packing Methods 0.000 claims abstract description 12
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 10
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims abstract description 10
- 229910052782 aluminium Inorganic materials 0.000 claims abstract description 10
- 238000005303 weighing Methods 0.000 claims abstract description 8
- 238000004140 cleaning Methods 0.000 claims abstract description 7
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract description 5
- 229960000198 mezlocillin Drugs 0.000 claims description 19
- YPBATNHYBCGSSN-VWPFQQQWSA-N mezlocillin Chemical compound N([C@@H](C(=O)N[C@H]1[C@H]2SC([C@@H](N2C1=O)C(O)=O)(C)C)C=1C=CC=CC=1)C(=O)N1CCN(S(C)(=O)=O)C1=O YPBATNHYBCGSSN-VWPFQQQWSA-N 0.000 claims description 19
- 238000012544 monitoring process Methods 0.000 claims description 17
- 238000000034 method Methods 0.000 claims description 14
- 239000004411 aluminium Substances 0.000 claims description 9
- 238000001035 drying Methods 0.000 claims description 6
- 230000001954 sterilising effect Effects 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 4
- 238000012376 hot air sterilization Methods 0.000 claims description 4
- 238000004458 analytical method Methods 0.000 claims description 3
- 238000004806 packaging method and process Methods 0.000 claims description 3
- 229910001220 stainless steel Inorganic materials 0.000 claims description 3
- 239000010935 stainless steel Substances 0.000 claims description 3
- 238000005406 washing Methods 0.000 claims description 3
- 238000007689 inspection Methods 0.000 abstract 1
- 239000003814 drug Substances 0.000 description 9
- 230000000694 effects Effects 0.000 description 7
- 238000005516 engineering process Methods 0.000 description 7
- 229940079593 drug Drugs 0.000 description 6
- 238000009472 formulation Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000004659 sterilization and disinfection Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 241000304886 Bacilli Species 0.000 description 1
- 241000588914 Enterobacter Species 0.000 description 1
- 201000009906 Meningitis Diseases 0.000 description 1
- 206010031252 Osteomyelitis Diseases 0.000 description 1
- 241000588769 Proteus <enterobacteria> Species 0.000 description 1
- 206010040047 Sepsis Diseases 0.000 description 1
- 206010062255 Soft tissue infection Diseases 0.000 description 1
- 125000000738 acetamido group Chemical class [H]C([H])([H])C(=O)N([H])[*] 0.000 description 1
- -1 aseptic Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000003115 biocidal effect Effects 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000006735 deficit Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 210000002249 digestive system Anatomy 0.000 description 1
- 239000002158 endotoxin Substances 0.000 description 1
- 210000004392 genitalia Anatomy 0.000 description 1
- 230000017525 heat dissipation Effects 0.000 description 1
- 230000036571 hydration Effects 0.000 description 1
- 238000006703 hydration reaction Methods 0.000 description 1
- 208000015181 infectious disease Diseases 0.000 description 1
- 238000010255 intramuscular injection Methods 0.000 description 1
- 239000007927 intramuscular injection Substances 0.000 description 1
- 238000010253 intravenous injection Methods 0.000 description 1
- 210000000867 larynx Anatomy 0.000 description 1
- 239000013618 particulate matter Substances 0.000 description 1
- 206010034674 peritonitis Diseases 0.000 description 1
- 210000002345 respiratory system Anatomy 0.000 description 1
- 206010040872 skin infection Diseases 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 230000002485 urinary effect Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B57/00—Automatic control, checking, warning, or safety devices
- B65B57/02—Automatic control, checking, warning, or safety devices responsive to absence, presence, abnormal feed, or misplacement of binding or wrapping material, containers, or packages
- B65B57/04—Automatic control, checking, warning, or safety devices responsive to absence, presence, abnormal feed, or misplacement of binding or wrapping material, containers, or packages and operating to control, or to stop, the feed of such material, containers, or packages
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Medical Preparation Storing Or Oral Administration Devices (AREA)
Abstract
The invention relates to a preparation method of mezlocillin sodium for injection, which is convenient for removing rejects. The preparation method comprises the following steps: firstly cleaning reagent bottles for holding mezlocillin sodium powder, then loading the mezlocillin sodium powder in the cleaned reagent bottles according to specified fixed quantity, filling the reagent bottles loaded with the mezlocillin sodium powder with nitrogen, covering the reagent bottles filled with the nitrogen with pretreated rubber plugs, and then, performing cover tightening treatment with aluminum covers, so that the mezlocillin sodium is sealed; sequentially pasting internal labels, packing the reagent bottles with the tightened covers, and performing light inspection; then, pasting external labels on packing boxes, inspecting the labeled packing boxes, and packing the inspected boxes. According to the preparation method disclosed by the invention, a weighing machine, a full-loaded channel switch and an unloaded channel switch are arranged at the output end of a conveyor belt, so that the problem that the reagent bottles are unloaded is solved; an automatic taking camera, an unlabeled channel switch and a qualified product channel switch are arranged on a full-loaded passage, so that the problem that the reagent bottles are unlabeled is solved.
Description
Technical field
The present invention relates to medical drugs preparation method field, particularly, relate to a kind of preparation method being convenient to the mezlocillin for inj of rejecting off gauge.
Background technology
Mezlocillin sodium is the semi-synthetic broad-spectrum antibiotic obtained from ring acylureido-penicilin class, its active component is mezlocillin, exist with a water-soluble hydration sodium salt, chemical name is: (2S, 5R, 6R)-3,3-dimethyl-66 [(R)-2 [3-(methylsulfonyl)-2-oxo-1-imidazolidine formamido group] this acetylamino of-2-]-7-oxo-4-thia-1-azabicyclo [3.2.0]-heptane-2-formic acid sodium salt.
Mezlocillin sodium is mainly used in respiratory system in the gram negative bacillis such as EHEC, Enterobacter, proteus caused by sensitive strain, urinary system, digestive system, gynaecology and genitals official rank clinically and infects, as the indication such as blood poisoning, purulent meningitis, peritonitis, osteomyelitis, skin and soft tissue infection and eye, ear, the infection of larynx section.Its usage is intramuscular injection, intravenous injection or drip-feed.Mezlocillin sodium is as injecting drug use, and for directly injecting the formulation entered in body, its safety is most important.The medication effect of mezlocillin for inj and the index of safety evaluatio mainly comprise: the clarity of visible foreign matters, pH value, specific rotation, stability, particulate matter, solution and color, related substances, aseptic, bacterial endotoxin, mezlocillin poly-mer etc.
The effect and the safety that how to improve injecting drug use always are that pharmaceutical producing enterprise wishes the problem solved, the effect of injecting drug use solves from two aspects with safety is main, one is effect and the safety that Formulation guarantees medication, and two is effect and the safety that the process for producing of medicine guarantees medicine.Mezlocillin for inj is a most existing injection agent, and its prescription is single, guarantees that the effect of its medicine and safe main path are exactly by controlling its preparation technology.
The nonconformity of the mezlocillin for inj finished product that the preparation technology of existing injection mezlocillin sodium easily causes.
Summary of the invention
Technical matters to be solved by this invention is to provide a kind of preparation method being convenient to the mezlocillin for inj of rejecting off gauge, the inferior-quality problem of the mezlocillin for inj finished product easily caused with the preparation technology overcoming existing injection mezlocillin sodium.
The present invention's adopted technical scheme that solves the problem is: the preparation method being convenient to the mezlocillin for inj of rejecting off gauge, comprise the following steps: first cleaning is used for the reagent bottle of splendid attire mezlocillin sodium powder, then mezlocillin sodium powder is quantitatively loaded the above-mentioned reagent bottle cleaned by specification, again the reagent bottle that mezlocillin sodium powder is housed is filled with nitrogen, then pretreated plug is covered, Zha Gai process is carried out again with aluminium lid, product is sealed, successively interior label is pasted to the reagent bottle after Zha Gai, packaging, lamp is examined, then label outer on packing box, test again, packing, in above-mentioned preparation process, adopt control system to control, described control system comprises monitoring and control centre, monitoring and control centre is connected with controller, controller is connected with setting weight sensor on the belt, belt conveyor start stop switch, controller is connected with the weighing machine being arranged on belt conveyor mouth, fully loaded channel switch, unloaded channel switch, controller is connected with the automatic camera camera be arranged on fully loaded passage, unlabelled channel switch, certified products channel switch, described monitoring and control centre is connected with network service by network interface, and described controller is connected with counting machine, and monitoring and control centre is connected with data center.The nonconformity of the mezlocillin for inj finished product that the preparation technology of existing injection mezlocillin sodium easily causes is due to the speed of pipelining, manual operation does not catch up with the speed of belt conveyor sometimes, reagent bottle usually can be caused to occur unloaded, the appearance of the off-grades such as reagent bottle unlabelled, monitoring and control centre of the present invention specifically refers to Control Room, for the whole production procedure of same monitoring management, controller specifically refers to PLC, zero load refers in reagent bottle have splendid attire powder reagent, be fully loaded with the powder reagent referring in reagent bottle and be loaded with specification and arrange, weight sensor can be real-time the weight sensing the product on belt conveyor, when product have little time flow into next process cause blocking up on a moving belt time, driving band is overweight, weight sensor by the weight transmitting that senses to controller, judged whether overweight by controller, and judge whether that sending instruction stops belt conveyor, when product flow into the mouth of driving band, weighed not obtaining reagent bottle by weighing machine, the numerical value of weighing is passed to controller, according to numerical value, controller judges that whether this reagent bottle is unloaded, if unloaded controller sends instruction and opens unloaded channel switch, make product introduction arrive unloaded passage, otherwise open fully loaded channel switch, avoid unloaded off gauge to flow into next process, the reagent bottle flowing into fully loaded passage is taken pictures through automatic licence plate camera, license plate information is passed to controller, judge whether reagent bottle labels by controller, if unlabelled, controller sends instruction and opens unlabelled channel switch, make product introduction to unlabelled passage, otherwise opening certified products channel switch makes product introduction to certified products passage, the present invention, by arranging weighing machine, fully loaded channel switch, unloaded channel switch at the mouth of belt conveyor, avoids the problem of reagent bottle zero load, by being provided with automatic camera camera, unlabelled channel switch, certified products channel switch on fully loaded passage, avoid the problem of reagent bottle unlabelled, so, the inferior-quality problem of the mezlocillin for inj finished product that the preparation technology that instant invention overcomes existing injection mezlocillin sodium easily causes.
Further, controller is connected to temperature sensor, and the temperature signal sensed is passed to controller by temperature sensor, and controller analysis temperature signal judges whether the heating arrangement that unlatching is connected with controller or heat abstractor.Report and submit to controller by temperature sensor acquisition environment temperature, controller carries out the calculating of temperature data and compares, when temperature is lower than setting value time, start electro-heat equipment, and can the power of regulation heating device, thus keep whole controller not affected by too low temperature, and when ambient temperature is higher than certain setting value, start heat abstractor, and environmentally the height of temperature carrys out the power of adjusting heat dissipation device, electronic component is made to be unlikely to be burned, thus make each electronic devices and components keep more rational operating temperature, add the service life of equipment.
Further, controller is connected with camera, the picture via controller of camera shooting passes to the computing machine be connected with monitoring and control centre.So, the production procedure observing product that just can be real-time.
Further, the cleaning process of reagent bottle is followed successively by supersound washing, Shui Chong, air oven dry, oven for drying, sterilizing.Guarantee the thoroughly clean of reagent bottle and gnotobasis, avoid reagent bottle to have influence on the quality of mezlocillin sodium.
Further, sterilizing adopts hot air sterilization.The sterilization effect of hot air sterilization is good and can not cause the humidity in reagent bottle.
Further, aluminium lid need pass through and process, and pretreated concrete steps are: poured into by aluminium lid in clean porose stainless steel framework, add in electrically heated drying cabinet, be incubated PTO Power Take Off after a hour.
To sum up, the invention has the beneficial effects as follows:
1, the present invention is by arranging weighing machine, fully loaded channel switch, unloaded channel switch at the mouth of belt conveyor, avoids the problem of reagent bottle zero load; By being provided with automatic camera camera, unlabelled channel switch, certified products channel switch on fully loaded passage, avoid the problem of reagent bottle unlabelled.
2, the present invention strictly carries out handle control to each operation in the preparation technology of mezlocillin sodium, from wash bottle, packing, Zha Gai to external packing, all sterilization treatment is carried out to working environment, the problem that its result of use avoiding the performance impairment of the mezlocillin sodium caused in preparation process to cause reduces from use equipment.
Accompanying drawing explanation
Fig. 1 is functional block diagram of the present invention.
Detailed description of the invention
Below in conjunction with embodiment and accompanying drawing, to the detailed description further of invention do, but embodiments of the present invention are not limited thereto.
Embodiment:
As shown in Figure 1, be convenient to the preparation method of the mezlocillin for inj of rejecting off gauge, comprise the following steps: first cleaning is used for the reagent bottle of splendid attire mezlocillin sodium powder, the cleaning process of reagent bottle is followed successively by supersound washing, water rushes, air is dried, oven for drying, hot air sterilization, then mezlocillin sodium powder is quantitatively loaded the above-mentioned reagent bottle cleaned by specification, again the reagent bottle that mezlocillin sodium powder is housed is filled with nitrogen, then pretreated plug is covered, Zha Gai process is carried out again with aluminium lid, aluminium lid need pass through and process, pretreated concrete steps are: poured into by aluminium lid in clean porose stainless steel framework, add in electrically heated drying cabinet, being incubated PTO Power Take Off after a hour makes product seal, successively interior label is pasted to the reagent bottle after Zha Gai, packaging, lamp is examined, then label outer on packing box, test again, packing, in above-mentioned preparation process, adopt control system to control, described control system comprises monitoring and control centre, monitoring and control centre is connected with controller, controller is connected with setting weight sensor on the belt, belt conveyor start stop switch, controller is connected with the weighing machine being arranged on belt conveyor mouth, fully loaded channel switch, unloaded channel switch, controller is connected with the automatic camera camera be arranged on fully loaded passage, unlabelled channel switch, certified products channel switch, described monitoring and control centre is connected with network service by network interface, and described controller is connected with counting machine, and monitoring and control centre is connected with data center, described controller is connected to temperature sensor, the temperature signal sensed is passed to controller by temperature sensor, controller analysis temperature signal judges whether the heating arrangement that unlatching is connected with controller or heat abstractor, described controller is connected with camera, and the picture via controller of camera shooting passes to the computing machine be connected with monitoring and control centre.
As mentioned above, the present invention can be realized preferably.
Claims (6)
1. be convenient to the preparation method of the mezlocillin for inj of rejecting off gauge, it is characterized in that, comprise the following steps: cleaning is used for the reagent bottle of splendid attire mezlocillin sodium powder, then mezlocillin sodium powder is quantitatively loaded the above-mentioned reagent bottle cleaned by specification, again the reagent bottle that mezlocillin sodium powder is housed is filled with nitrogen, then pretreated plug is covered, Zha Gai process is carried out again with aluminium lid, product is sealed, successively interior label is pasted to the reagent bottle after Zha Gai, packaging, lamp is examined, then label outer on packing box, test again, packing, in above-mentioned preparation process, adopt control system to control, described control system comprises monitoring and control centre, monitoring and control centre is connected with controller, controller is connected with setting weight sensor on the belt, belt conveyor start stop switch, controller is connected with the weighing machine being arranged on belt conveyor mouth, fully loaded channel switch, unloaded channel switch, controller is connected with the automatic camera camera be arranged on fully loaded passage, unlabelled channel switch, certified products channel switch, described monitoring and control centre is connected with network service by network interface, and described controller is connected with counting machine, and monitoring and control centre is connected with data center.
2. the preparation method being convenient to the mezlocillin for inj of rejecting off gauge according to claim 1, it is characterized in that, described controller is connected to temperature sensor, the temperature signal sensed is passed to controller by temperature sensor, and controller analysis temperature signal judges whether the heating arrangement that unlatching is connected with controller or heat abstractor.
3. the preparation method being convenient to the mezlocillin for inj of rejecting off gauge according to claim 1 and 2, is characterized in that, described controller is connected with camera, and the picture via controller of camera shooting passes to the computing machine be connected with monitoring and control centre.
4. the preparation method being convenient to the mezlocillin for inj of rejecting off gauge according to claim 1, it is characterized in that, the cleaning process of described reagent bottle is followed successively by supersound washing, Shui Chong, air oven dry, oven for drying, sterilizing.
5. the preparation method being convenient to the mezlocillin for inj of rejecting off gauge according to claim 4, is characterized in that, described sterilizing adopts hot air sterilization.
6. the preparation method being convenient to the mezlocillin for inj of rejecting off gauge according to claim 1 or 4, it is characterized in that, described aluminium lid need pass through and process, pretreated concrete steps are: poured into by aluminium lid in clean porose stainless steel framework, add in electrically heated drying cabinet, be incubated PTO Power Take Off after a hour.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510200609.8A CN104925324A (en) | 2015-04-27 | 2015-04-27 | Preparation method of mezlocillin sodium for injection, convenient for removing rejects |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510200609.8A CN104925324A (en) | 2015-04-27 | 2015-04-27 | Preparation method of mezlocillin sodium for injection, convenient for removing rejects |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104925324A true CN104925324A (en) | 2015-09-23 |
Family
ID=54112816
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510200609.8A Pending CN104925324A (en) | 2015-04-27 | 2015-04-27 | Preparation method of mezlocillin sodium for injection, convenient for removing rejects |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104925324A (en) |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2001043413A (en) * | 1999-07-29 | 2001-02-16 | Iwata Label:Kk | Package insert detection method for medicines and detectable package inserts |
| US20010032441A1 (en) * | 1999-12-17 | 2001-10-25 | Ogden John Colin | Method and apparatus for product packaging |
| CN101342955A (en) * | 2008-08-15 | 2009-01-14 | 张新民 | Full-automatic intelligentized blood bar code safety recognition sorting and checking package method and system |
| CN201689317U (en) * | 2010-05-14 | 2010-12-29 | 山东大学 | Label detecting system |
| CN202624725U (en) * | 2012-06-04 | 2012-12-26 | 宜昌人福药业有限责任公司 | Online auto-detection rejection device for empty bottles or empty boxes |
| CN102895181A (en) * | 2012-10-22 | 2013-01-30 | 四川制药制剂有限公司 | Method for preparing mezlocillin sodium for injection |
-
2015
- 2015-04-27 CN CN201510200609.8A patent/CN104925324A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2001043413A (en) * | 1999-07-29 | 2001-02-16 | Iwata Label:Kk | Package insert detection method for medicines and detectable package inserts |
| US20010032441A1 (en) * | 1999-12-17 | 2001-10-25 | Ogden John Colin | Method and apparatus for product packaging |
| CN101342955A (en) * | 2008-08-15 | 2009-01-14 | 张新民 | Full-automatic intelligentized blood bar code safety recognition sorting and checking package method and system |
| CN201689317U (en) * | 2010-05-14 | 2010-12-29 | 山东大学 | Label detecting system |
| CN202624725U (en) * | 2012-06-04 | 2012-12-26 | 宜昌人福药业有限责任公司 | Online auto-detection rejection device for empty bottles or empty boxes |
| CN102895181A (en) * | 2012-10-22 | 2013-01-30 | 四川制药制剂有限公司 | Method for preparing mezlocillin sodium for injection |
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|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20150923 |