CN104893388A - Resin and preparation method thereof - Google Patents
Resin and preparation method thereof Download PDFInfo
- Publication number
- CN104893388A CN104893388A CN201510301588.9A CN201510301588A CN104893388A CN 104893388 A CN104893388 A CN 104893388A CN 201510301588 A CN201510301588 A CN 201510301588A CN 104893388 A CN104893388 A CN 104893388A
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- Prior art keywords
- resin
- butanone
- add
- photo
- vinylformic acid
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Abstract
The invention discloses resin prepared from the following components in percentage by mass: 55-65% of butanone, 20-30% of polychloroacrylate, 4-6% of a 369 photoinitiator, 6-10% of BR113 and 1-3 parts of 184 photocuring monomers. The preparation method of the resin comprises the following steps of firstly, adding butanone into a reaction kettle; then, sequentially adding BR113 and polychloroacrylate, and then, stirring until the raw materials are completely dissolved; next, sequentially adding the 369 photoinitiator and the 184 photocuring monomers and stirring until the raw materials are completely dissolved, and then, stopping stirring; and filtering by using a 350-mesh filter screen to obtain a finished product. The resin has the advantages of good quality, low cost and the like.
Description
Technical field
The present invention specifically relates to a kind of resin and preparation method thereof, is applied to the manufacture field of light guiding plate mould.
Background technology
In the manufacture process of light guiding plate, need first to prepare mould, and in the preparation process of mould, need the surface-coated one deck resin at acrylic board, and then use mantle machine that PET polyester film is stamped in acrylic board, but existing resin quality is poor, easily cause the quality of the mould produced also poor, and the production technique more complicated of existing resin, cost is higher.
Summary of the invention
For solving the defect of prior art, the invention discloses resin that a kind of quality is good, cost is low and preparation method thereof.
The invention discloses a kind of resin, according to mass percent, composed of the following components: butanone 55%-65%, polychlorostyrene fat vinylformic acid 20%-30%, 369 light trigger 4%-6%, BR113 6%-10%, 184 photo-curing monomer 1%-3%.
As preferably, resin of the present invention, according to mass percent, composed of the following components: butanone 60%, polychlorostyrene fat vinylformic acid 25%, 369 light trigger 5%, BR113 8%, 184 photo-curing monomer 2%.
Further, the preparation method of resin of the present invention is as follows:
25 DEG C, under the condition of 101kPa, according to above-mentioned mass percent, in reactor, first add butanone, and then add BR113, polychlorostyrene fat vinylformic acid successively, stir, until dissolve completely, and then add 369 light triggers, 184 photo-curing monomers successively, stir, until raw material stops after dissolving completely stirring, finally use 350 mesh filter screens to filter, namely obtain finished product.
Owing to adopting technique scheme, resin of the present invention and preparation method thereof has following advantageous benefits: the resin quality produced is good, stability is also relatively good, effectively avoid the defect of the die quality difference causing the later stage to produce because of resin quality difference, and preparation method of the present invention is fairly simple, in addition 25 DEG C, can carry out under the condition of 101kPa, therefore production cost is lower, is suitable for extensive popularization.
Embodiment
The invention discloses a kind of resin, according to mass percent, composed of the following components: butanone 55%-65%, polychlorostyrene fat vinylformic acid 20%-30%, 369 light trigger 4%-6%, BR113 6%-10%, 184 photo-curing monomer 1%-3%.
As preferably, resin of the present invention, according to mass percent, composed of the following components: butanone 60%, polychlorostyrene fat vinylformic acid 25%, 369 light trigger 5%, BR113 8%, 184 photo-curing monomer 2%.
Further, the preparation method of resin of the present invention is as follows:
25 DEG C, under the condition of 101kPa, according to above-mentioned mass percent, in reactor, first add butanone, and then add BR113, polychlorostyrene fat vinylformic acid successively, stir, until dissolve completely, and then add 369 light triggers, 184 photo-curing monomers successively, stir, until raw material stops after dissolving completely stirring, finally use 350 mesh filter screens to filter, namely obtain finished product.
Embodiment 1
To prepare 1000 grams of resins
25 DEG C, under the condition of 101kPa, 600 grams of butanone are first added in reactor, and then add 80 grams of BR113,250 grams of polychlorostyrene fat vinylformic acid successively, stir, until dissolve completely, and then add 50 gram of 369 light trigger, 20 gram of 184 photo-curing monomer successively, stir, until raw material stops after dissolving completely stirring, finally use 350 mesh filter screens to filter, namely obtain finished product.
Embodiment 2
To prepare 1000 grams of resins
25 DEG C, under the condition of 101kPa, 650 grams of butanone are first added in reactor, and then add 70 grams of BR113,200 grams of polychlorostyrene fat vinylformic acid successively, stir, until dissolve completely, and then add 50 gram of 369 light trigger, 30 gram of 184 photo-curing monomer successively, stir, until raw material stops after dissolving completely stirring, finally use 350 mesh filter screens to filter, namely obtain finished product.
Above embodiment only in order to the present invention is described and and unrestricted technical scheme described in the invention; Therefore, although this specification sheets with reference to each above-mentioned embodiment to present invention has been detailed description, those of ordinary skill in the art should be appreciated that and still can modify to the present invention or equivalent to replace; And all do not depart from technical scheme and the improvement thereof of the spirit and scope of the present invention, it all should be encompassed in right of the present invention.
Claims (3)
1. a resin, is characterized in that: according to mass percent, composed of the following components: butanone 55%-65%, polychlorostyrene fat vinylformic acid 20%-30%, 369 light trigger 4%-6%, BR113 6%-10%, 184 photo-curing monomer 1%-3%.
2. a kind of resin according to claim 1, is characterized in that: according to mass percent, composed of the following components: butanone 60%, polychlorostyrene fat vinylformic acid 25%, 369 light trigger 5%, BR113 8%, 184 photo-curing monomer 2%.
3. a kind of resin according to claim 1, it is characterized in that: preparation method is as follows: 25 DEG C, under the condition of 101kPa, according to above-mentioned mass percent, in reactor, first add butanone, and then add BR113, polychlorostyrene fat vinylformic acid successively, stir, until dissolve completely, and then add 369 light triggers, 184 photo-curing monomers successively, stir, until raw material stops after dissolving completely stirring, finally use 350 mesh filter screens to filter, namely obtain finished product.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201510301588.9A CN104893388A (en) | 2015-06-05 | 2015-06-05 | Resin and preparation method thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN201510301588.9A CN104893388A (en) | 2015-06-05 | 2015-06-05 | Resin and preparation method thereof |
Publications (1)
Publication Number | Publication Date |
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CN104893388A true CN104893388A (en) | 2015-09-09 |
Family
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN201510301588.9A Pending CN104893388A (en) | 2015-06-05 | 2015-06-05 | Resin and preparation method thereof |
Country Status (1)
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CN (1) | CN104893388A (en) |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2001200022A (en) * | 2000-01-14 | 2001-07-24 | Jsr Corp | Photocurable resin composition and optical member |
CN1935917A (en) * | 2005-09-23 | 2007-03-28 | 比亚迪股份有限公司 | Bottom coating composition, and its preparing method and multilayer coat |
CN101205424A (en) * | 2007-12-11 | 2008-06-25 | 中国乐凯胶片集团公司 | Hard paint film |
CN101358048A (en) * | 2008-09-19 | 2009-02-04 | 华南理工大学 | Ultraviolet cured paint for electric product surface coating |
-
2015
- 2015-06-05 CN CN201510301588.9A patent/CN104893388A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2001200022A (en) * | 2000-01-14 | 2001-07-24 | Jsr Corp | Photocurable resin composition and optical member |
CN1935917A (en) * | 2005-09-23 | 2007-03-28 | 比亚迪股份有限公司 | Bottom coating composition, and its preparing method and multilayer coat |
CN101205424A (en) * | 2007-12-11 | 2008-06-25 | 中国乐凯胶片集团公司 | Hard paint film |
CN101358048A (en) * | 2008-09-19 | 2009-02-04 | 华南理工大学 | Ultraviolet cured paint for electric product surface coating |
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Application publication date: 20150909 |