CN104893388A - Resin and preparation method thereof - Google Patents

Resin and preparation method thereof Download PDF

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Publication number
CN104893388A
CN104893388A CN201510301588.9A CN201510301588A CN104893388A CN 104893388 A CN104893388 A CN 104893388A CN 201510301588 A CN201510301588 A CN 201510301588A CN 104893388 A CN104893388 A CN 104893388A
Authority
CN
China
Prior art keywords
resin
butanone
add
photo
vinylformic acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201510301588.9A
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Chinese (zh)
Inventor
杨苏武
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Anhui Kai Shengzhongpu New Light Sources Co Ltd
Original Assignee
Anhui Kai Shengzhongpu New Light Sources Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Anhui Kai Shengzhongpu New Light Sources Co Ltd filed Critical Anhui Kai Shengzhongpu New Light Sources Co Ltd
Priority to CN201510301588.9A priority Critical patent/CN104893388A/en
Publication of CN104893388A publication Critical patent/CN104893388A/en
Pending legal-status Critical Current

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Abstract

The invention discloses resin prepared from the following components in percentage by mass: 55-65% of butanone, 20-30% of polychloroacrylate, 4-6% of a 369 photoinitiator, 6-10% of BR113 and 1-3 parts of 184 photocuring monomers. The preparation method of the resin comprises the following steps of firstly, adding butanone into a reaction kettle; then, sequentially adding BR113 and polychloroacrylate, and then, stirring until the raw materials are completely dissolved; next, sequentially adding the 369 photoinitiator and the 184 photocuring monomers and stirring until the raw materials are completely dissolved, and then, stopping stirring; and filtering by using a 350-mesh filter screen to obtain a finished product. The resin has the advantages of good quality, low cost and the like.

Description

A kind of resin and preparation method thereof
Technical field
The present invention specifically relates to a kind of resin and preparation method thereof, is applied to the manufacture field of light guiding plate mould.
Background technology
In the manufacture process of light guiding plate, need first to prepare mould, and in the preparation process of mould, need the surface-coated one deck resin at acrylic board, and then use mantle machine that PET polyester film is stamped in acrylic board, but existing resin quality is poor, easily cause the quality of the mould produced also poor, and the production technique more complicated of existing resin, cost is higher.
Summary of the invention
For solving the defect of prior art, the invention discloses resin that a kind of quality is good, cost is low and preparation method thereof.
The invention discloses a kind of resin, according to mass percent, composed of the following components: butanone 55%-65%, polychlorostyrene fat vinylformic acid 20%-30%, 369 light trigger 4%-6%, BR113 6%-10%, 184 photo-curing monomer 1%-3%.
As preferably, resin of the present invention, according to mass percent, composed of the following components: butanone 60%, polychlorostyrene fat vinylformic acid 25%, 369 light trigger 5%, BR113 8%, 184 photo-curing monomer 2%.
Further, the preparation method of resin of the present invention is as follows:
25 DEG C, under the condition of 101kPa, according to above-mentioned mass percent, in reactor, first add butanone, and then add BR113, polychlorostyrene fat vinylformic acid successively, stir, until dissolve completely, and then add 369 light triggers, 184 photo-curing monomers successively, stir, until raw material stops after dissolving completely stirring, finally use 350 mesh filter screens to filter, namely obtain finished product.
Owing to adopting technique scheme, resin of the present invention and preparation method thereof has following advantageous benefits: the resin quality produced is good, stability is also relatively good, effectively avoid the defect of the die quality difference causing the later stage to produce because of resin quality difference, and preparation method of the present invention is fairly simple, in addition 25 DEG C, can carry out under the condition of 101kPa, therefore production cost is lower, is suitable for extensive popularization.
Embodiment
The invention discloses a kind of resin, according to mass percent, composed of the following components: butanone 55%-65%, polychlorostyrene fat vinylformic acid 20%-30%, 369 light trigger 4%-6%, BR113 6%-10%, 184 photo-curing monomer 1%-3%.
As preferably, resin of the present invention, according to mass percent, composed of the following components: butanone 60%, polychlorostyrene fat vinylformic acid 25%, 369 light trigger 5%, BR113 8%, 184 photo-curing monomer 2%.
Further, the preparation method of resin of the present invention is as follows:
25 DEG C, under the condition of 101kPa, according to above-mentioned mass percent, in reactor, first add butanone, and then add BR113, polychlorostyrene fat vinylformic acid successively, stir, until dissolve completely, and then add 369 light triggers, 184 photo-curing monomers successively, stir, until raw material stops after dissolving completely stirring, finally use 350 mesh filter screens to filter, namely obtain finished product.
Embodiment 1
To prepare 1000 grams of resins
25 DEG C, under the condition of 101kPa, 600 grams of butanone are first added in reactor, and then add 80 grams of BR113,250 grams of polychlorostyrene fat vinylformic acid successively, stir, until dissolve completely, and then add 50 gram of 369 light trigger, 20 gram of 184 photo-curing monomer successively, stir, until raw material stops after dissolving completely stirring, finally use 350 mesh filter screens to filter, namely obtain finished product.
Embodiment 2
To prepare 1000 grams of resins
25 DEG C, under the condition of 101kPa, 650 grams of butanone are first added in reactor, and then add 70 grams of BR113,200 grams of polychlorostyrene fat vinylformic acid successively, stir, until dissolve completely, and then add 50 gram of 369 light trigger, 30 gram of 184 photo-curing monomer successively, stir, until raw material stops after dissolving completely stirring, finally use 350 mesh filter screens to filter, namely obtain finished product.
Above embodiment only in order to the present invention is described and and unrestricted technical scheme described in the invention; Therefore, although this specification sheets with reference to each above-mentioned embodiment to present invention has been detailed description, those of ordinary skill in the art should be appreciated that and still can modify to the present invention or equivalent to replace; And all do not depart from technical scheme and the improvement thereof of the spirit and scope of the present invention, it all should be encompassed in right of the present invention.

Claims (3)

1. a resin, is characterized in that: according to mass percent, composed of the following components: butanone 55%-65%, polychlorostyrene fat vinylformic acid 20%-30%, 369 light trigger 4%-6%, BR113 6%-10%, 184 photo-curing monomer 1%-3%.
2. a kind of resin according to claim 1, is characterized in that: according to mass percent, composed of the following components: butanone 60%, polychlorostyrene fat vinylformic acid 25%, 369 light trigger 5%, BR113 8%, 184 photo-curing monomer 2%.
3. a kind of resin according to claim 1, it is characterized in that: preparation method is as follows: 25 DEG C, under the condition of 101kPa, according to above-mentioned mass percent, in reactor, first add butanone, and then add BR113, polychlorostyrene fat vinylformic acid successively, stir, until dissolve completely, and then add 369 light triggers, 184 photo-curing monomers successively, stir, until raw material stops after dissolving completely stirring, finally use 350 mesh filter screens to filter, namely obtain finished product.
CN201510301588.9A 2015-06-05 2015-06-05 Resin and preparation method thereof Pending CN104893388A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510301588.9A CN104893388A (en) 2015-06-05 2015-06-05 Resin and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510301588.9A CN104893388A (en) 2015-06-05 2015-06-05 Resin and preparation method thereof

Publications (1)

Publication Number Publication Date
CN104893388A true CN104893388A (en) 2015-09-09

Family

ID=54026371

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510301588.9A Pending CN104893388A (en) 2015-06-05 2015-06-05 Resin and preparation method thereof

Country Status (1)

Country Link
CN (1) CN104893388A (en)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2001200022A (en) * 2000-01-14 2001-07-24 Jsr Corp Photocurable resin composition and optical member
CN1935917A (en) * 2005-09-23 2007-03-28 比亚迪股份有限公司 Bottom coating composition, and its preparing method and multilayer coat
CN101205424A (en) * 2007-12-11 2008-06-25 中国乐凯胶片集团公司 Hard paint film
CN101358048A (en) * 2008-09-19 2009-02-04 华南理工大学 Ultraviolet cured paint for electric product surface coating

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2001200022A (en) * 2000-01-14 2001-07-24 Jsr Corp Photocurable resin composition and optical member
CN1935917A (en) * 2005-09-23 2007-03-28 比亚迪股份有限公司 Bottom coating composition, and its preparing method and multilayer coat
CN101205424A (en) * 2007-12-11 2008-06-25 中国乐凯胶片集团公司 Hard paint film
CN101358048A (en) * 2008-09-19 2009-02-04 华南理工大学 Ultraviolet cured paint for electric product surface coating

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Application publication date: 20150909