CN104874566A - Ultrasonic wave and acid-alkaline composite ampoule cleaning method - Google Patents
Ultrasonic wave and acid-alkaline composite ampoule cleaning method Download PDFInfo
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- CN104874566A CN104874566A CN201510261493.9A CN201510261493A CN104874566A CN 104874566 A CN104874566 A CN 104874566A CN 201510261493 A CN201510261493 A CN 201510261493A CN 104874566 A CN104874566 A CN 104874566A
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- Prior art keywords
- groove
- acid
- ultrasonic wave
- alkaline
- precleaning
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B3/00—Cleaning by methods involving the use or presence of liquid or steam
- B08B3/04—Cleaning involving contact with liquid
- B08B3/10—Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration
- B08B3/12—Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration by sonic or ultrasonic vibrations
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
- B08B9/20—Cleaning containers, e.g. tanks by using apparatus into or on to which containers, e.g. bottles, jars, cans are brought
- B08B9/22—Cleaning containers, e.g. tanks by using apparatus into or on to which containers, e.g. bottles, jars, cans are brought the apparatus cleaning by soaking alone
Abstract
The invention discloses an ultrasonic wave and acid-alkaline composite ampoule cleaning method. The method comprises the steps that 1, distilled water is added into a precleaning groove, a transition groove and a clean water groove, alkaline washing liquid is added in an alkaline groove, and acid washing liquid is added in an acid groove; 2, ultrasonic wave generators in the precleaning groove, the acid groove and the alkaline groove are started to generate ultrasonic waves; 3, an ampoule is soaked in the precleaning groove, the acid groove, the transition groove, the alkaline groove and the clean water groove in sequence; in the step 2, the frequency of the ultrasonic waves in the cleaning groove is 25-30 KHz, the frequency of the ultrasonic waves in the acid groove is 35-38 KHz, and the frequency of the ultrasonic waves in the alkaline groove is 35-38 KHz; in the step 3, the socking time of the ampoule in the precleaning groove, the acid groove and the alkaline groove is respectively larger than 5 min. The ultrasonic wave and acid-alkaline composite ampoule cleaning method has the advantages of being better in cleaning effect, saving more cost, more convenient and easier to operate and the like.
Description
Technical field
The present invention relates to a kind of ultrasonic cleaning system, what be specifically related to is a kind of method of ultrasonic wave and soda acid composite clean ampulla.
Background technology
Ultrasonic wave is a kind of frequency higher than the sound wave of 20000 hertz, its good directionality, and penetration capacity is strong, is easy to obtain the acoustic energy comparatively concentrated, and in water transmission distance, can be used for finding range, tests the speed, cleans, welds, rubble, sterilizing etc.Ultrasonic effect is widely used in reality, in medical science, military affairs, industry, agriculturally has a lot of application, mainly contains the aspects such as ultrasonic examination, ultrasonic process, Ultrasonic Cleaning.
Ultrasonic effect: when ultrasonic wave is propagated in media as well, due to the interaction of ultrasonic wave and medium, that make medium generation physics with change that is chemistry, thus produce a series of mechanics, calorifics, electromagnetic and chemical ultrasonic effect, comprise following 4 kinds of effects:
1. mechanical effect.Hyperacoustic mechanism can facilitate the dispersion of the emulsification of liquid, the liquefaction of gel and solid.When forming standing wave in supersonic flow body medium, the molecule suspended in a fluid condenses upon node place because of the effect by mechanical force, forms periodic accumulation in space.When ultrasonic wave is propagated in piezoelectric and magnetostriction materials, induct electric polarization and the magnetization (see dielectric physics and magnetostriction) of inducting that cause due to hyperacoustic mechanism.
2. cavitation.Ul-trasonic irradiation can produce a large amount of minute bubbles when liquid.A reason is that in liquid, local occurs tension and forms negative pressure, and the reduction of pressure makes the dissolved gas supersaturation being originally dissolved in liquid, and from liquid effusion, becomes minute bubbles.Another reason is that powerful tension " tears " a cavity liquid, is called cavitation.Being liquid vapors or the another kind of gas being dissolved in liquid in cavity, may be even vacuum.The minute bubbles formed because of cavitation constantly can move with the vibration of surrounding medium, grow up or vanish suddenly.When vanishing, surrounding liquid pours bubble suddenly and produces high temperature, high pressure, produces shock wave simultaneously.Rub and can form electric charge in accompanying with cavitation, and produce luminescence phenomenon in the electric discharge of bubble internal cause.The technology of carrying out ultrasonic process is in a liquid mostly relevant with cavitation.
3. fuel factor.Because ultrasonic frequency is high, energy is large, can be produced significant fuel factor by during Absorption of Medium.
4. chemical effect.Hyperacoustic effect can impel generation or accelerate some chemical reaction.Such as pure distilled water produces hydrogen peroxide after ultrasonic process; The water being dissolved with nitrogen produces nitrous acid after ultrasonic process; The aqueous solution of dyestuff is understood variable color or fades after ultrasonic process.Total and the cavitation of the generation of these phenomenons accompanies.Ultrasonic wave also can accelerate hydrolysis, the decomposition and aggregation process of many chemical substances.Ultrasonic wave also has a significant effect to photochemistry and electrochemical process.The aqueous solution of each seed amino acid and other organic substances is after ultrasonic process, and characteristic absorption spectrum band disappears and generally absorbs in uniform, and this shows that cavitation makes molecular structure there occurs change.
As the ultrasonic frequency of cleaning method generally between 25KHz ~ 130KHz, conventional operating frequency is 28KHz, 33KHz, 40KHz, 80KHz, 100KHz, 120KHz etc.Frequency higher cleaning density is larger in theory, and cleaning degree is higher, but relative force is less, is used for precision cleaning.Otherwise frequency is then lower.
That is, when selecting ultrasonic cleaning apparatus frequency, because frequency higher cleaning density is larger, cleaning degree is higher, and relative force is also less.Therefore, select operating frequency be the ultrasonic cleaning apparatus of below 40KHz time, its be generally used for general industry part or dirt more when, as the oil removing of hardware machinery part except cured wait work.And the operating frequency of more than 40KHz is used for greatly the precision cleaning of precision component, the precision cleaning of the parts such as glass devices as sub-in optical/optoelectronic and semi-conducting material/device.
Summary of the invention
The method of the ultrasonic wave that the object of the present invention is to provide a kind of cleaning performance better, more cost-saving and soda acid composite clean ampulla.
For solving above-mentioned shortcoming, technical scheme of the present invention is as follows:
A method for ultrasonic wave and soda acid composite clean ampulla, comprises the following steps:
(1) in precleaning spout, lead-over groove and Rinsing Area, add distilled water, in alkali groove, add alkaline washing liquid, in acid tank, add acidic cleaning liquid;
(2) open the supersonic generator in precleaning spout, acid tank and alkali groove, send ultrasonic wave;
(3) medicine bottle is soaked in turn in precleaning spout, acid tank, lead-over groove, alkali groove, Rinsing Area;
Wherein, in described step (2), in rinse bath, hyperacoustic frequency is 25 ~ 30KHz, and in described acid tank, hyperacoustic frequency is 35 ~ 38KHz, and in described alkali groove, hyperacoustic frequency is 35 ~ 38KHz; The time of soaking in precleaning spout, acid tank and alkali groove in described step (3) is all greater than 5min.
Further, described acidic cleaning liquid to be concentration be 5% ~ 8% hydrochloric acid solution; Described alkaline washing liquid to be concentration be 1% ~ 3% sodium hydroxide solution.
Further, the temperature of described alkaline washing liquid is 40 DEG C.
As one preferably set-up mode, described medicine bottle is positioned over medicine bottle and moves in placement net, controls medicine bottle move the shift position of placing net by controller.
For the ease of the replacing of liquid in cell body, the liquid in described precleaning spout, acid tank, lead-over groove, alkali groove and Rinsing Area is all flow into from top, flows out from bottom.
The present invention compared with prior art, has the following advantages and beneficial effect:
1, the present invention adopts acid & alkali liquid to clean and Ultrasonic Cleaning mating reaction, effectively improves cleaning performance, and effectively improves cleaning efficiency;
2, the present invention is without the need to peripheral hardware nozzle for cleaning provides power-assisted, directly by needing the glass medicine bottle of cleaning to be directly placed in cell body, thus can not cause damage to bottle, and the energy required when simultaneously effectively having saved nozzle ejection liquid, saves and clean cost;
3, the setting of rinse bath, acid tank, lead-over groove, alkali groove and Rinsing Area in the present invention, it is dirty that it not only can effectively remove on medicine bottle, and this setting can not cause the mutual pollution in cleaning process in cell body between liquid, increases service life.
Accompanying drawing explanation
Fig. 1 is structured flowchart of the present invention.
Wherein, the title that in accompanying drawing, Reference numeral is corresponding is as follows:
1-precleaning spout, 2-acid tank, 3-lead-over groove, 4-alkali groove, 5-Rinsing Area, 6-supersonic generator.
Detailed description of the invention
Below in conjunction with embodiment and accompanying drawing thereof, the present invention is described in further detail, but embodiments of the present invention are not limited thereto.
Embodiment 1
A method for ultrasonic wave and soda acid composite clean ampulla, comprises the following steps:
(1) in precleaning spout, lead-over groove and Rinsing Area, add distilled water, in alkali groove, add sodium hydroxide solution, in acid tank, add hydrochloric acid solution;
(2) open the supersonic generator in precleaning spout, acid tank and alkali groove, send ultrasonic wave;
(3) medicine bottle is soaked in turn in precleaning spout, acid tank, lead-over groove, alkali groove, Rinsing Area; Wherein, the time of soaking in precleaning spout, acid tank and alkali groove is all greater than 5min, and the time of soaking in the present embodiment is 6-8min; Lead-over groove and Rinsing Area are respectively used to remove and remain in hydrochloric acid solution on medicine bottle and sodium hydroxide solution.
As shown in Figure 1, it comprises precleaning spout 1, acid tank 2, lead-over groove 3, alkali groove 4, Rinsing Area 5 to the device structure relied on when the present invention realizes.Supersonic generator 6 is provided with in described precleaning spout 1, acid tank 2 and alkali groove 4; Wherein, in described precleaning spout 1, the frequency of supersonic generator 6 is 25 ~ 30KHz, and in described acid tank 2, the frequency of supersonic generator 6 is 35 ~ 38KHz, and in described alkali groove 4, the frequency of supersonic generator 6 is 35 ~ 38KHz.
In order to reach effect best, the acidic cleaning liquid in described acid tank 2 to be concentration be 5% ~ 8% hydrochloric acid solution; Alkaline washing liquid in described alkali groove 4 to be concentration be 1% ~ 3% sodium hydroxide solution, in described alkali groove 4, the temperature of alkaline washing liquid is 40 DEG C.
For the ease of operation, the present invention also comprises medicine bottle and moves placement net, and described medicine bottle moves the controller placed and be also provided with and control its movement on the net.The water inlet of described precleaning spout 1, acid tank 2, lead-over groove 3, alkali groove 4 and Rinsing Area 5 is all positioned at top, and this delivery port is then positioned at bottom.
Embodiment 2
The present embodiment is the contrast experiment one of embodiment 1, and the difference of the present embodiment and embodiment 1 is only: the present embodiment only adopts the acid-alkali washing effect in embodiment 1, does not open supersonic generator.
Embodiment 3
The present embodiment is the contrast experiment two of embodiment 1, the difference of the present embodiment and embodiment 1 is only: the sodium hydroxide solution in embodiment 1 and hydrochloric acid solution are all replaced to distilled water by the present embodiment, enables and cleans with the ultrasonic wave of embodiment 1 same frequency.
Specific experiment result is as follows:
In same time, the cleanliness factor of the medicine bottle in embodiment 1 reaches 99.9%, and the cleanliness factor of embodiment 2 and embodiment 3 is respectively 72% and 65%.
Above-described embodiment is only the preferred embodiments of the present invention, not limiting the scope of the invention, as long as adopt design principle of the present invention, and the change carried out non-creativeness work on this basis and make, all should belong within protection scope of the present invention.
Claims (5)
1. a method for ultrasonic wave and soda acid composite clean ampulla, is characterized in that: comprise the following steps:
(1) in precleaning spout, lead-over groove and Rinsing Area, add distilled water, in alkali groove, add alkaline washing liquid, in acid tank, add acidic cleaning liquid;
(2) open the supersonic generator in precleaning spout, acid tank and alkali groove, send ultrasonic wave;
(3) medicine bottle is soaked in turn in precleaning spout, acid tank, lead-over groove, alkali groove, Rinsing Area;
Wherein, in described step (2), in rinse bath, hyperacoustic frequency is 25 ~ 30KHz, and in described acid tank, hyperacoustic frequency is 35 ~ 38KHz, and in described alkali groove, hyperacoustic frequency is 35 ~ 38KHz; The time of soaking in precleaning spout, acid tank and alkali groove in described step (3) is all greater than 5min.
2. the method for a kind of ultrasonic wave according to claim 1 and soda acid composite clean ampulla, is characterized in that: described acidic cleaning liquid to be concentration be 5% ~ 8% hydrochloric acid solution; Described alkaline washing liquid to be concentration be 1% ~ 3% sodium hydroxide solution.
3. the method for a kind of ultrasonic wave according to claim 2 and soda acid composite clean ampulla, is characterized in that: the temperature of described alkaline washing liquid is 40 DEG C.
4. the method for a kind of ultrasonic wave according to claim 1 and soda acid composite clean ampulla, is characterized in that: described medicine bottle is positioned over medicine bottle and moves in placement net, controls medicine bottle move the shift position of placing net by controller.
5. the method for a kind of ultrasonic wave according to claim 4 and soda acid composite clean ampulla, is characterized in that: the liquid in described precleaning spout, acid tank, lead-over groove, alkali groove and Rinsing Area is all flow into from top, flows out from bottom.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510261493.9A CN104874566A (en) | 2015-05-21 | 2015-05-21 | Ultrasonic wave and acid-alkaline composite ampoule cleaning method |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510261493.9A CN104874566A (en) | 2015-05-21 | 2015-05-21 | Ultrasonic wave and acid-alkaline composite ampoule cleaning method |
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| CN104874566A true CN104874566A (en) | 2015-09-02 |
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| CN201510261493.9A Pending CN104874566A (en) | 2015-05-21 | 2015-05-21 | Ultrasonic wave and acid-alkaline composite ampoule cleaning method |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105195483A (en) * | 2015-10-13 | 2015-12-30 | 广州达意隆包装机械股份有限公司 | Recovered bottle cleaning method and system |
| CN106269670A (en) * | 2016-09-30 | 2017-01-04 | 四川行来科技有限公司 | Glass cleaning process based on ultrasound wave |
| CN107755340A (en) * | 2017-10-20 | 2018-03-06 | 贰陆光学（苏州）有限公司 | A kind of cleaning method of optical mirror slip |
| CN108262302A (en) * | 2016-12-30 | 2018-07-10 | 中核建中核燃料元件有限公司 | One kind feeds intake container ultrasonic wave automatic cleaning process |
| CN115365236A (en) * | 2022-08-05 | 2022-11-22 | 福建永荣科技有限公司 | Equipment for cleaning metal film tube in ammoximation cleaning process |
-
2015
- 2015-05-21 CN CN201510261493.9A patent/CN104874566A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105195483A (en) * | 2015-10-13 | 2015-12-30 | 广州达意隆包装机械股份有限公司 | Recovered bottle cleaning method and system |
| CN106269670A (en) * | 2016-09-30 | 2017-01-04 | 四川行来科技有限公司 | Glass cleaning process based on ultrasound wave |
| CN108262302A (en) * | 2016-12-30 | 2018-07-10 | 中核建中核燃料元件有限公司 | One kind feeds intake container ultrasonic wave automatic cleaning process |
| CN107755340A (en) * | 2017-10-20 | 2018-03-06 | 贰陆光学（苏州）有限公司 | A kind of cleaning method of optical mirror slip |
| CN115365236A (en) * | 2022-08-05 | 2022-11-22 | 福建永荣科技有限公司 | Equipment for cleaning metal film tube in ammoximation cleaning process |
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Application publication date: 20150902 |